CN107321277A - A kind of synthetic latex resource recovering system - Google Patents
A kind of synthetic latex resource recovering system Download PDFInfo
- Publication number
- CN107321277A CN107321277A CN201710663395.7A CN201710663395A CN107321277A CN 107321277 A CN107321277 A CN 107321277A CN 201710663395 A CN201710663395 A CN 201710663395A CN 107321277 A CN107321277 A CN 107321277A
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- container
- chuck
- water
- tank
- recovering system
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F22—STEAM GENERATION
- F22B—METHODS OF STEAM GENERATION; STEAM BOILERS
- F22B33/00—Steam-generation plants, e.g. comprising steam boilers of different types in mutual association
- F22B33/18—Combinations of steam boilers with other apparatus
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Mechanical Engineering (AREA)
- General Engineering & Computer Science (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Abstract
The present invention relates to a kind of synthetic latex resource recovering system, including：Steam generator, stainless steel, synthesising container, container of growing up, degassing container, the first tank, the entrance of outlet and degassing container chuck with synthesising container chuck is connected；Second tank, outlet and steam generator with vessel jacket of growing up are connected；3rd tank, outlet, the JI for container of growing up with degassing container chuck are connected.The synthetic latex resource recovering system of the present invention, store the water of different temperatures respectively by three tanks, and the water of three kinds of different temperatures is applied in synthesising container, growth container, the heating of degassing container or cooling or for generating steam, water and heat energy can be made full use of, the effect of energy-saving and emission-reduction is played.
Description
Technical field
The present invention relates to a kind of synthetic latex resource recovering system, belong to synthetic latex equipment technical field.
Background technology
The reaction vessel and degassing container of synthetic latex commonly use jacketed reaction container, and jacketed reaction container is normal conjunction
What is led on into container outer wall in many outside sandwich, interlayer is thermal source or cooling agent, as water, oil or gas etc, leads to heat
During source, by heat transfer effect, it can then be cooled with heating response container during coolant to reaction vessel.Existing synthesis
In latex, there is soft water in usual raw material, flow through interlayer using steam heats to reaction vessel and degassing container, steam liquefaction
After form water, generally just be used for live use or cool, water resource therein and heat energy are just slatterned, and are one to resource
Plant and waste.
The content of the invention
The technical problem to be solved in the present invention is：For solve synthetic latex production when the wasting of resources technical problem there is provided
One kind being capable of recycle-water and heat energy synthetic latex resource recovering system.
The technical solution adopted for the present invention to solve the technical problems is：
The present invention provides a kind of synthetic latex resource recovering system, including：
Steam generator, for producing steam；
Stainless steel, for mixed material；
There is chuck, JI, which connects reception steam with steam generator and heats synthesis, to be held on synthesising container, outer wall
Material in device, for carrying out preliminary polymerization；
There is chuck on growth container, outer wall, for further being polymerize；
There is chuck, for being deaerated for latex on degassing container, outer wall；
First tank, the entrance of outlet and degassing container chuck with synthesising container chuck is connected, and is steamed for storing
High-temperature water after vapour-liquid, and high-temperature water is transported in degassing container chuck to degassing when degassing container is de-gassed operation
Material in container is heated and is incubated；
Second tank, outlet and steam generator with vessel jacket of growing up are connected, for storing growth container clip
The middle warm water of outflow is covered, and warm water in this is used in steam generator generation steam；
3rd tank, outlet, the JI and/or stainless steel of container of growing up with degassing container chuck connect
It is logical, the water at low temperature for storing the outflow of degassing container chuck, and the water at low temperature is used for cooling growth container.
Preferably, synthetic latex resource recovering system of the invention, the outlet of the second tank also connects with stainless steel
It is logical.
Preferably, synthetic latex resource recovering system of the invention, growth container on JI also with cooling water pipe
Connection, for receiving normal temperature cooling water.
Preferably, between synthetic latex resource recovering system of the invention, the tank of synthesising container JO first
Pipeline also pass through the connection of the pipeline between valve and the first tank and degassing container JI.
Preferably, synthetic latex resource recovering system of the invention, the outlet of the first tank also with steam generator
Connection.
Preferably, synthetic latex resource recovering system of the invention, synthetic latex resource recovering system provides for styrene-butadiene latex
Source recovery system or carboxylic styrene butadiene latex resource recovering system.
The beneficial effects of the invention are as follows：
The synthetic latex resource recovering system of the present invention, the water of different temperatures is stored by three tanks respectively, and
And the water of three kinds of different temperatures is applied in synthesising container, growth container, the heating of degassing container or cooling or is used for
Steam is generated, water and heat energy can be made full use of, the effect of energy-saving and emission-reduction is played.
Brief description of the drawings
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the structural representation of the synthetic latex resource recovering system of the embodiment of the present invention；
Reference in figure is：
1- steam generators；2- stainless steels；3- synthesising containers；4- growth containers；5- degassing containers；The water storages of 61- first
Container；The tanks of 62- second；The tanks of 63- the 3rd.
Embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These accompanying drawings are simplified schematic diagram, only with
Illustration illustrates the basic structure of the present invention, therefore it only shows the composition relevant with the present invention.
Embodiment
The present embodiment provides a kind of synthetic latex resource recovering system, as shown in figure 1, including：
Steam generator 1 (steam boiler), for producing steam；
Stainless steel 2, for mixed material；
There is chuck, JI connects reception steam with steam generator 1 and heats synthesis on synthesising container 3, outer wall
Material in container, for carrying out preliminary polymerization；
There is chuck on growth container 4, outer wall, for further being polymerize；
There is chuck, for being deaerated for latex on degassing container 5, outer wall；
First tank 61, the entrance of outlet and the chuck of degassing container 5 with the chuck of synthesising container 3 is connected, for depositing
The high-temperature water after steam liquefied is stored up, and is transported to high-temperature water in the chuck of degassing container 5 when degassing container 5 is de-gassed operation
Material in degassing container 5 is heated and is incubated；
Second tank 62, outlet and steam generator 1 (also can be with stainless steel 2) with the chuck of container 4 of growing up are even
It is logical, the middle warm water for storing the chuck outflow of growth container 4, and water is provided when steam generator 1 produces steam, or will be low
Warm water be used for as polymerize when raw material -- soft water (is passed through stainless steel 2)；
3rd tank 63, outlet, the JI for container 4 of growing up with the chuck of degassing container 5 are connected, for storing
The water at low temperature of the chuck of degassing container 5 outflow, and the material by the water at low temperature for cooling down growth container 4.
The synthetic latex resource recovering system of the present embodiment, for producing styrene-butadiene latex or carboxylic styrene butadiene latex, mixing
Container 2, synthesising container 3, growth container 4, degassing container 5 are sequentially communicated, and part material mixing, synthesis are completed in stainless steel 2
Container 3 carries out preliminary polymerization, now needs heating, and steam generator 1 produces steam and is passed into progress in the chuck of synthesising container 3
Heating, initiation reaction, steam forms high-temperature water (about 80-90 DEG C) in the chuck heat release of synthesising container 3, is stored into the first water storage appearance
In device 61, (show as gas butadiene reaction therein to complete, container inner pressure declines after monomer is completely polymerized into small molecule
It is considered as completion reaction to an atmospheric pressure), carried out in material press-in growth container 4 in synthesising container 3；Container 4 of growing up is interior to be relied on
The polymerisation of heat release is spontaneous to be polymerize, due to exothermic heat of reaction in growth container 4, in order to prevent that temperature is too high, it is necessary to introduce
Cooling water, therefore, the water at low temperature (about 30-50 DEG C) of the 3rd tank 63 introduce when heat is absorbed in the growth chuck of container 4 into
Temperature required by long container holding technique, water at low temperature warm water (about 50-60 DEG C) in being formed after the growth chuck of container 4,
It is stored in the 3rd tank 63；Material reaction forms latex after terminating in growth container 4, and material is pressed into degassing container
In 5, nitrogen blowing degassing is carried out to latex in degassing container 5, nitrogen blowing can cause latex temperature drop, in order under compensation temperature
High-temperature water in drop, the first tank 61 is introduced in the chuck of degassing container 5, is added for the latex for degassing container 5
Heat, it is generally the case that high-temperature water can be more, therefore the first tank 61 can also be connected with steam generator 1, by high temperature water gas
Steam is melted into, water at low temperature storage is become into the 3rd tank 63 by the high-temperature water of the chuck of degassing container 5.Second water storage
Middle warm water in container 62, which is passed into steam generator 1, to be used to produce steam, or is passed into and is passed through in stainless steel 2.
The synthetic latex resource recovering system of above-described embodiment, different temperatures is stored by three tanks respectively
Water, and the water of three kinds of different temperatures is applied in synthesising container 3, growth container 4, the heating of degassing container 5 or cooling
Or for generating steam, water and heat energy can be made full use of, play the effect of energy-saving and emission-reduction.
As an improvement, the JI on growth container 4 is also connected with cooling water pipe, for receiving normal temperature cooling
Water, to prevent the water of the 3rd tank 63 from not reaching cooling effect not enough.
As a further improvement, pipeline between the first tank of JO 61 of synthesising container 3 also by valve with
The connection of pipeline between first tank 61 and the JI of degassing container 5, the JO of synthesising container 3 when valve is opened
The high-temperature water of outflow is flowed into the chuck of degassing container 5 without between the first tank 61.
What deserves to be explained is, steam generator 1 and stainless steel 2 and synthesising container 3 and growth container 4 are with taking off in accompanying drawing 1
Annexation between gas container 5 is not showed, and this is respectively managed in the common connected mode of synthetic latex equipment, recovery system
Flow control valve is installed, for controlling flow, to ensure the temperature control of synthesis technique on road.
Heat release when the synthetic latex resource recovering system of the present embodiment is available for any synthesis, and polymerization process is divided into two
The synthetic latex equipment divided.
Using the above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to its technical scope is determined according to right.
Claims (6)
1. a kind of synthetic latex resource recovering system, it is characterised in that including：
Steam generator (1), for producing steam；
Stainless steel (2), for mixed material；
There is chuck, JI connects reception steam with steam generator (1) and heats synthesis on synthesising container (3), outer wall
Material in container, for carrying out preliminary polymerization；
There is chuck, for further being polymerize on growth container (4), outer wall；
There is chuck, for being deaerated for latex on degassing container (5), outer wall；
First tank (61), the entrance of outlet and degassing container (5) chuck with synthesising container (3) chuck is connected, and is used for
The high-temperature water after steam liquefied is stored, and high-temperature water is transported to degassing container (5) when degassing container (5) is de-gassed operation
The material in degassing container (5) is heated and is incubated in chuck；
Second tank (62), outlet and steam generator (1) with container (4) chuck of growing up are connected, for storing growth
The middle warm water of container (4) chuck outflow, and warm water in this is used in steam generator (1) generation steam；
3rd tank (63), outlet, the JI of growth container (4) with degassing container (5) chuck are connected, for depositing
The water at low temperature of degassing container (5) chuck outflow is stored up, and the water at low temperature is used for cooling growth container (4).
2. synthetic latex resource recovering system according to claim 1, it is characterised in that the second tank (62) go out
Mouth is also connected with stainless steel (2).
3. synthetic latex resource recovering system according to claim 1, it is characterised in that the chuck on growth container (4)
Entrance is also connected with cooling water pipe, for receiving normal temperature cooling water.
4. synthetic latex resource recovering system according to claim 1, it is characterised in that synthesising container (3) JO
Pipeline between first tank (61) also by valve and the first tank (61) and degassing container (5) JI it
Between pipeline connection.
5. the synthetic latex resource recovering system according to claim any one of 1-4, it is characterised in that the first tank
(61) outlet is also connected with steam generator (1).
6. the synthetic latex resource recovering system according to claim any one of 1-5, it is characterised in that synthetic latex resource
Recovery system is styrene-butadiene latex resource recovering system or carboxylic styrene butadiene latex resource recovering system.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710663395.7A CN107321277B (en) | 2017-08-05 | 2017-08-05 | A kind of synthetic latex resource recovering system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710663395.7A CN107321277B (en) | 2017-08-05 | 2017-08-05 | A kind of synthetic latex resource recovering system |
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| Publication Number | Publication Date |
|---|---|
| CN107321277A true CN107321277A (en) | 2017-11-07 |
| CN107321277B CN107321277B (en) | 2019-01-22 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710663395.7A Active CN107321277B (en) | 2017-08-05 | 2017-08-05 | A kind of synthetic latex resource recovering system |
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| CN (1) | CN107321277B (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108187596A (en) * | 2018-03-14 | 2018-06-22 | 德莱创节能科技（苏州）有限公司 | A kind of synthetic latex production system for recycling heat energy from waste gas |
| CN108380149A (en) * | 2018-03-14 | 2018-08-10 | 德莱创节能科技（苏州）有限公司 | A kind of method of synthetic latex production system recycling heat energy from waste gas |
| CN108467459A (en) * | 2018-04-16 | 2018-08-31 | 德莱创节能科技（苏州）有限公司 | A kind of styrene-butadiene latex production system of energy-saving and emission-reduction |
| CN111569808A (en) * | 2020-05-22 | 2020-08-25 | 中石化上海工程有限公司 | Energy integrated utilization bulk drug reaction purification system and process method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010004666A1 (en) * | 1999-09-14 | 2001-06-21 | Kaneka Corporation | Method of stripping for latex of vinyl chloride paste resin, stripping apparatus, and vinyl chloride paste resin latex having low concentration of residual monomer |
| CN202538754U (en) * | 2012-03-16 | 2012-11-21 | 骏马化纤股份有限公司 | Constant temperature device for preparing glue solution |
| CN105892521A (en) * | 2016-04-19 | 2016-08-24 | 山东豪迈机械制造有限公司 | Efficient temperature control system and temperature control method thereof |
| CN205575993U (en) * | 2016-04-28 | 2016-09-14 | 浙江天晨胶业股份有限公司 | Synthetic latex production system of closed recovery styrene |
-
2017
- 2017-08-05 CN CN201710663395.7A patent/CN107321277B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20010004666A1 (en) * | 1999-09-14 | 2001-06-21 | Kaneka Corporation | Method of stripping for latex of vinyl chloride paste resin, stripping apparatus, and vinyl chloride paste resin latex having low concentration of residual monomer |
| CN202538754U (en) * | 2012-03-16 | 2012-11-21 | 骏马化纤股份有限公司 | Constant temperature device for preparing glue solution |
| CN105892521A (en) * | 2016-04-19 | 2016-08-24 | 山东豪迈机械制造有限公司 | Efficient temperature control system and temperature control method thereof |
| CN205575993U (en) * | 2016-04-28 | 2016-09-14 | 浙江天晨胶业股份有限公司 | Synthetic latex production system of closed recovery styrene |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108187596A (en) * | 2018-03-14 | 2018-06-22 | 德莱创节能科技（苏州）有限公司 | A kind of synthetic latex production system for recycling heat energy from waste gas |
| CN108380149A (en) * | 2018-03-14 | 2018-08-10 | 德莱创节能科技（苏州）有限公司 | A kind of method of synthetic latex production system recycling heat energy from waste gas |
| CN108467459A (en) * | 2018-04-16 | 2018-08-31 | 德莱创节能科技（苏州）有限公司 | A kind of styrene-butadiene latex production system of energy-saving and emission-reduction |
| CN108467459B (en) * | 2018-04-16 | 2021-04-20 | 德莱创节能科技（苏州）有限公司 | Energy-saving and emission-reducing styrene-butadiene latex production system |
| CN111569808A (en) * | 2020-05-22 | 2020-08-25 | 中石化上海工程有限公司 | Energy integrated utilization bulk drug reaction purification system and process method thereof |
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| Publication number | Publication date |
|---|---|
| CN107321277B (en) | 2019-01-22 |
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