CN107314970A - The test device and method of the carbon fiber fibrillation expanding of controllable temperature - Google Patents

The test device and method of the carbon fiber fibrillation expanding of controllable temperature Download PDF

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Publication number
CN107314970A
CN107314970A CN201710645777.7A CN201710645777A CN107314970A CN 107314970 A CN107314970 A CN 107314970A CN 201710645777 A CN201710645777 A CN 201710645777A CN 107314970 A CN107314970 A CN 107314970A
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carbon fiber
expanding
exhibition yarn
test
fibrillation
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徐牛牛
卢临杭
杭传伟
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Jiangsu Hengshen Co Ltd
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Jiangsu Hengshen Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N19/00Investigating materials by mechanical methods
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00Investigating or analyzing materials by the use of thermal means

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  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
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  • Inorganic Fibers (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

The present invention provides a kind of test device and method of the carbon fiber fibrillation expanding of controllable temperature, the device includes totally-enclosed casing, madial wall is provided with device case behind totally-enclosed casing, the thread supply shaft for laying spindle is sequentially placed in device case from left to right, spacing hole, first driven rod, first width laser analyzer, second driven rod, first exhibition yarn roller, some Electromagnetic Heatings open up yarn roller, second exhibition yarn roller, 3rd driven rod, second width laser analyzer, 4th driven rod and wire drawing shaft, wire drawing shaft is driven by electrodeless variable-speed motor, by putting belt on thread supply shaft, one end of belt is fixed on device case, the other end of belt is provided with hook and is hung with definite value counterweight.The test device and method of the carbon fiber fibrillation expanding of this kind of controllable temperature, can test fibrillation expanding and breadth uniformity of the fiber under controllable temperature.

Description

The test device and method of the carbon fiber fibrillation expanding of controllable temperature
Technical field
The present invention relates to the test device and method of a kind of carbon fiber fibrillation expanding of controllable temperature.
Background technology
Carbon fibre composite has light weight, and the excellent performance characteristics of intensity, modulus are widely used in Aero-Space, wind The fields such as energy blade, deepwater oilfield, infrastructure, auto industry and Leisure Sports articles for use.In the preparation of carbon fibre composite During, it is necessary to which carbon fiber has good process industrial art performance, the fibrillation expanding and expanding uniformity of carbon fiber are fibers The important indicator of process industrial art performance.In carbon fiber prepreg preparation and carbon fiber winding technique, the fibrillation all to carbon fiber Expanding and exhibition yarn uniformity propose requirement.The fibrillation expanding of fiber is poor, the prepreg surface of preparation can produce gap and Bar shadow, influences prepreg quality;Fiber expanding is uneven, when preparing product using winding process, occurs between fibre bundle Overlap joint or crack phenomenon, influence winding product performance.Therefore the fibrillation expanding and breadth uniformity of fiber are to prepare high-quality The important guarantee of prepreg and winding product.It is how convenient, fast, efficient, it is inexpensive evaluate carbon fiber fibrillation expanding be Put an important topic in face of carbon fiber R & D Enterprises.
Test device and the survey of a kind of carbon fiber fibrillation expanding (convergence) are disclosed in patent CN204346883U Method for testing.The device can be the technique fitness-for-service assessment of carbon fiber with the fibrillation expanding (convergence) of quantitative test carbon fiber There is provided reference data.But the device can only test carbon fiber fibrillation expanding under normal temperature condition, it is impossible to test evaluation carbon The performance of fiber fiber detaching expanding under the high temperature conditions, it is impossible to meet carbon fiber in prepreg production process to fibrillation expanding The Research Requirements of energy.In carbon fiber industry, the evaluation to the high temperature exhibition yarn of carbon fiber is limited to presoak equipment accordingly, not had Condition carries out fiber high temperature exhibition yarn test, even if or have preimpregnation equipment, due to needing substantial amounts of material, human resources, evaluate Cost is very high, and the evaluation experimental time is long, and fiber high temperature exhibition yarn performance is not often evaluated timely.Finally, it will lack high The carbon fiber product of temperature exhibition yarn test evaluation invests market, and problem is exposed into client, influence product quality and corporate reputation.
Above mentioned problem is the problem of should pay attention to and solve during testing carbon fiber fibrillation expanding.
The content of the invention
In view of the foregoing, it is an object of the invention to provide a kind of test of the carbon fiber fibrillation expanding of controllable temperature dress Put and method, carbon fiber can be evaluated in different fibrillation expanding and stent uniformity at each temperature, is carbon fiber prepreg Production and evaluate and provide definite reference data, reduce research and development and the production cost of carbon fiber and prepreg, solve existing Present in technology can not test evaluation carbon fiber fiber detaching expanding under the high temperature conditions phenomenon, it is impossible to meet carbon fiber and exist The problem of prepreg production process is to the Research Requirements of fibrillation expanding performance.
The present invention technical solution be:
A kind of test device of the carbon fiber fibrillation expanding of controllable temperature, including totally-enclosed casing, totally-enclosed casing Bottom is provided with some horizontal adjustment knobs, and totally-enclosed casing front is provided with sliding door, and sliding door is provided with door handle, and sliding door is used The sliding door that colourless transparent plastic plate is made, the bottom surface of totally-enclosed casing, two sides, is respectively adopted stainless steel plate system below Into madial wall is provided with device case behind totally-enclosed casing, and device case is made of stainless steel, in device case from left to right It is sequentially placed for the thread supply shaft for laying spindle, spacing hole, the first driven rod, the first width laser analyzer, the second transmission Bar, the first exhibition yarn roller, some Electromagnetic Heatings exhibition yarn roller, the second exhibition yarn roller, the 3rd driven rod, the second width laser analyzer, the Four driven rods and wire drawing shaft, wire drawing shaft are driven by electrodeless variable-speed motor, and by belt is put on thread supply shaft, one end of belt is fixed on On device case, the other end of belt is provided with linking up with and being hung with definite value counterweight, and the side of totally-enclosed casing is provided with display screen Control panel and power switch, the shift knob for adjusting wire drawing shaft rotating speed, the temperature control button of control Electromagnetic Heating exhibition yarn roll temperature.
Further, the length of totally-enclosed casing is respectively 1000mm, 500mm, 400mm, and totally-enclosed casing is located at In constant temperature and humidity room.
Further, the length of device case is respectively 850mm, 50mm, 300mm.
Further, exhibition yarn roller is made of plating straight-chromiun stainless steel, and exhibition yarn roller is wine barrel-shaped, and the minimum diameter of exhibition yarn roller is 15mm, length are that 40mm, radian are π/6.
Further, Electromagnetic Heating exhibition yarn roller is made of metal, and a diameter of 20mm of Electromagnetic Heating exhibition yarn roller, length are 40mm。
A kind of method of testing of the carbon fiber fibrillation expanding of the controllable temperature of above-mentioned test device, comprises the following steps,
First maintain test room temperature and humidity constant before step 1, test, room temperature is 20 DEG C ± 2 DEG C, and relative humidity is 45% ± 3%, then make by horizontal adjustment knob the level of totally-enclosed casing;
Step 2, turn on the power switch, adjust temperature control button, select a temperature, state is maintained 30 minutes;
Step 3, some same models of ingot of selection test fibrillation expanding with a batch of carbon fiber;
Step 4, opening sliding door, take carbon fiber ingot to be put on thread supply shaft, are sequentially sequentially passed through after fiber is involved spacing Hole, the first driven rod, the first width laser analyzer, the second driven rod, the first exhibition yarn roller, some Electromagnetic Heatings exhibition yarn roller, the Two exhibition yarn rollers, the 3rd driven rod, the second width laser analyzer, the 4th driven rod, finally from wound thereon in the sky of wire drawing shaft Receive on silk ingot, close sliding door;
Step 5, regulation shift knob make the tow speed of service of display screen display be 15rpm, are then read every 10s First width laser analyzer, the numerical value of the second width laser analyzer on display screen, read 10 times altogether, wherein the first width What laser determination instrument was measured is width before exhibition yarn, and what the second width laser analyzer was measured is width after exhibition yarn, finally tries to achieve exhibition Yarn rate It is fiber width average value before exhibition yarn,It is fiber width average value after exhibition yarn, using EXCEL tables Lattice handle 10 batch datas, obtain data discrete coefficient Cv values;
Step 6, remaining carbon fiber operated according to above-mentioned steps 4-5 successively, by the test number of all carbon fibers Average, finally give the test data of fibrillation expanding of the model batch carbon fiber under the specified temp.
The beneficial effects of the invention are as follows:The test device and method of the carbon fiber fibrillation expanding of this kind of controllable temperature, energy Enough test fibrillation expanding and breadth uniformity of the fiber under controllable temperature.By adjusting exhibition yarn roll temperature, carbon fiber is tested Fiber breadth at different temperatures, evaluates the exhibition yarn of carbon fiber at different temperatures;Further by being surveyed to breadth The investigation of the discrete case of examination value, can determine whether that fiber opens up the uniformity of yarn, is provided for the production and evaluation of carbon fiber prepreg Definite reference data, judges whether carbon fiber possesses the process conditions that prepreg is made, and reduces grinding for carbon fiber and prepreg Hair and production cost.
Brief description of the drawings
Fig. 1 is the side view structural representation of the test device of the carbon fiber fibrillation expanding of controllable temperature of the embodiment of the present invention Figure;
Fig. 2 is the plan structure signal of the test device of the carbon fiber fibrillation expanding of controllable temperature of the embodiment of the present invention Figure;
Wherein:The totally-enclosed casings of 1-, 2- horizontal adjustment knobs, 3- door handles, 4- belts, 5- definite value counterweights, 6- spindles, 7- Spacing hole, the driven rods of 8- first, 9- the first width laser analyzers, the exhibition yarn rollers of 10- first, 11- Electromagnetic Heatings exhibition yarn roller, 12- Receive silk ingot, 13- device casees, 14- thread supply shafts, 15- wire drawing shafts, 16- control panels, 17- power switches, 18- shift knobs, 19- Temperature control button, the driven rods of 20- second, the exhibition yarn rollers of 21- second, the driven rods of 22- the 3rd, the driven rods of 23- the 4th, the width of 24- second Laser determination instrument.
Embodiment
The preferred embodiment that the invention will now be described in detail with reference to the accompanying drawings.
Embodiment
A kind of test device of the carbon fiber fibrillation expanding of controllable temperature, including totally-enclosed casing 1, totally-enclosed casing 1 Bottom be provided with some horizontal adjustment knobs 2, the totally-enclosed front of casing 1 is provided with sliding door, and sliding door is provided with door handle 3, push-and-pull The sliding door that door is made of colourless transparent plastic plate, the bottom surface of totally-enclosed casing 1, two sides, be respectively adopted below it is stainless Steel plate is made, and madial wall is provided with device case 13 behind totally-enclosed casing 1, and device case 13 is made of stainless steel, device It is sequentially placed from left to right in case 13 for the thread supply shaft 14 for laying spindle 6, spacing hole 7, the first driven rod 8, the first width Laser determination instrument 9, the second driven rod 20, first exhibition yarn roller 10, some Electromagnetic Heatings exhibition yarn roller 11, second open up yarn roller the 21, the 3rd Driven rod 22, the second width laser analyzer 24, the 4th driven rod 23 and wire drawing shaft 15, wire drawing shaft 15 is by electrodeless variable-speed motor By belt 4 is put on driving, thread supply shaft 14, one end of belt 4 is fixed on device case 13, and the other end of belt 4 is provided with hook simultaneously Definite value counterweight 5 is hung with, the side of totally-enclosed casing 1 is received provided with the control panel 16 with display screen and power switch 17, regulation The shift knob 18 of the silk rotating speed of axle 15, the temperature control button 19 of the temperature of control Electromagnetic Heating exhibition yarn roller 11.20 DEG C -150 of temperature control scope DEG C, precision ± 0.5 DEG C, the tow speed of service, fiber width, Electromagnetic Heating open up the numerical value such as the temperature of yarn roller 11 all can be in display screen Display.
The test device of the carbon fiber fibrillation expanding of this kind of controllable temperature, can test fiber opening under controllable temperature Fine expanding and breadth uniformity.By adjusting exhibition yarn roll temperature, the fiber breadth of test carbon fiber at different temperatures is evaluated The exhibition yarn of carbon fiber at different temperatures;Further by the investigation of the discrete case to breadth test value, it can determine whether Fiber opens up the uniformity of yarn, and the production and evaluation for carbon fiber prepreg provide definite reference data, judge that carbon fiber is It is no to possess the process conditions that prepreg is made, reduce research and development and the production cost of carbon fiber and prepreg.
In embodiment, the length of totally-enclosed casing 1 is respectively 1000mm, 500mm, 400mm, and totally-enclosed casing 1 is set In in constant temperature and humidity room.The length of device case 13 is respectively 850mm, 50mm, 300mm.Yarn roller is opened up using plating straight-chromiun stainless steel It is made, exhibition yarn roller is wine barrel-shaped, the minimum diameter of exhibition yarn roller is that 15mm, length are that 40mm, radian are π/6.Electromagnetic Heating opens up yarn Roller 11 is made of metal, and a diameter of 20mm of Electromagnetic Heating exhibition yarn roller 11, length are 40mm.
Receive later after utility model certificate, relevant invoice and certificate can be mailed to you.
Embodiment method testing step includes:Each technical parameter before setting test, test is opened up at various temperatures The width of carbon fiber before and after yarn, draws the fibrillation expanding of carbon fiber, evaluates the carbon fiber expanding of carbon fiber at various temperatures Sex differernce and stent uniformity.
Embodiment 1
1. first maintaining test room temperature and humidity constant before test, room temperature is 20 DEG C ± 2 DEG C, and relative humidity is 45% ± 3%, then by horizontal adjustment knob 2, make the totally-enclosed level of casing 1.
2. turning on the power switch 17, temperature control button 19 is adjusted, the temperature of display Electromagnetic Heating exhibition yarn roller 11 is 50 DEG C, state dimension Hold 30 minutes.
3. choose same model tests fibrillation expanding with a batch of ingot of HF10-3K-E carbon fibers 3.
4. opening sliding door, carbon fiber ingot is taken to be put on thread supply shaft 14, after fiber is involved according to the order in Fig. 1 successively By spacing hole 7, the first driven rod 8, the first width laser analyzer 9, the second driven rod 20, first exhibition yarn roller 10, Ruo Gan electricity Magnetic heating exhibition yarn roller 11, second opens up yarn roller 21, the 3rd driven rod 22, the second width laser analyzer 24, the 4th driven rod 23, most Received afterwards from wound thereon in the empty of wire drawing shaft 15 on silk ingot 12, close sliding door.
5. regulation shift knob 18 makes the receipts silk speed of display screen display be 15rpm, then display screen is read every 10s Upper first width laser analyzer 9, the numerical value of the second width laser analyzer 24, read 10 times altogether, read the first width and swash Light measurement instrument 9, the number average value of the second width laser analyzer 24 are respectively 3.5mm, 4.3mm, then open up yarn rate and be10 batch datas are handled using Microsoft Excel, obtaining data discrete coefficient Cv values is 2.5%.
6. remaining two ingot carbon fiber is operated according to above-mentioned steps 4-5 successively, the test result of the second ingot carbon fiber It is 2.1% for 29.1%, Cv values;The test result of 3rd ingot carbon fiber is that 27.9%, Cv values are 1.9%.Average and obtain Exhibition yarn rate of the model batch carbon fiber at 50 DEG C is 28.53%.
Embodiment 2
1. first maintaining test room temperature and humidity constant before test, room temperature is 20 DEG C ± 2 DEG C, and relative humidity is 45% ± 3%, then by horizontal adjustment knob 2, make the level of casing.
2. turning on the power switch 17, temperature control button 19 is adjusted, the temperature of display Electromagnetic Heating exhibition yarn roller 11 is 60 DEG C, state dimension Hold 30 minutes.
3. choose same model tests fibrillation expanding with a batch of ingot of HF10-12K-A carbon fibers 3.
4. opening sliding door, carbon fiber ingot is taken to be put on thread supply shaft 14, after fiber is involved according to the order in Fig. 1 successively By spacing hole 7, the first driven rod 8, the first width laser analyzer 9, the second driven rod 20, first exhibition yarn roller 10, Ruo Gan electricity Magnetic heating exhibition yarn roller 11, second opens up yarn roller 21, the 3rd driven rod 22, the second width laser analyzer 24, the 4th driven rod 23, most Received afterwards from wound thereon in the empty of wire drawing shaft 15 on silk ingot 12, close sliding door.
5. regulation shift knob 18 makes the receipts silk speed of display screen display be 15rpm, then display screen is read every 10s Upper first width laser analyzer 9, the numerical value of the second width laser analyzer 24, read 10 times altogether, read the first width and swash Light measurement instrument 9, the number average value of the second width laser analyzer 24 are respectively 6.1mm, 9.5mm, then open up yarn rateCv values are 1.6%;
6. remaining two ingot carbon fiber is operated according to above-mentioned steps 4-5 successively, the test result of the second ingot carbon fiber It is 2.2% for 53.2%, Cv values;The test result of 3rd ingot carbon fiber is that 56.1%, Cv values are 3.5%.Average and obtain Exhibition yarn rate of the model batch carbon fiber at 80 DEG C is 55%.
Embodiment 3
1. first maintaining test room temperature and humidity constant before test, room temperature is 20 DEG C ± 2 DEG C, and relative humidity is 45% ± 3%, then by horizontal adjustment knob 2, make the level of totally-enclosed casing 1.
2. turning on the power switch 17, temperature control button 19 is adjusted, the temperature of display Electromagnetic Heating exhibition yarn roller 11 is 80 DEG C, state dimension Hold 30 minutes.
3. choose same model tests fibrillation expanding with a batch of ingot of HF30S-12K-H carbon fibers 3;
4. opening sliding door, carbon fiber ingot is taken to be put on thread supply shaft 14, after fiber is involved according to the order in Fig. 1 successively By spacing hole 7, the first driven rod 8, the first width laser analyzer 9, the second driven rod 20, first exhibition yarn roller 10, Ruo Gan electricity Magnetic heating exhibition yarn roller 11, second opens up yarn roller 21, the 3rd driven rod 22, the second width laser analyzer 24, the 4th driven rod 23, most Received afterwards from wound thereon in the empty of wire drawing shaft 15 on silk ingot 12, close sliding door.
5. regulation shift knob 18 makes the receipts silk speed of display screen display be 15rpm, then display screen is read every 10s Upper first width laser analyzer 9, the numerical value of the second width laser analyzer 24, read 10 times altogether, read the first width and swash Light measurement instrument 9, the number average value of the second width laser analyzer 24 are respectively 6.0mm, 10.2mm, then open up yarn rateCv values are 3.1%.
6. by remaining two ingot carbon fiber successively according to above-mentioned 4-5 the step of operated, the test knot of the second ingot carbon fiber Fruit is that 68.3%, Cv values are 2.9%;The test result of 3rd ingot carbon fiber is that 71.5%, Cv values are 2.7%.Average It is 69.9% to exhibition yarn rate of the model batch carbon fiber at 120 DEG C.

Claims (6)

1. a kind of test device of the carbon fiber fibrillation expanding of controllable temperature, it is characterised in that:Including totally-enclosed casing, full envelope The bottom of closed box body is provided with some horizontal adjustment knobs, and totally-enclosed casing front is provided with sliding door, and sliding door is provided with door handle, pushed away The sliding door that sliding door is made of colourless transparent plastic plate, the bottom surface of totally-enclosed casing, two sides, be respectively adopted below it is stainless Steel plate is made, and madial wall is provided with device case behind totally-enclosed casing, and device case is made of stainless steel, in device case from It is sequentially placed from left to right for the thread supply shaft for laying spindle, spacing hole, the first driven rod, the first width laser analyzer, Two driven rods, the first exhibition yarn roller, some Electromagnetic Heatings exhibition yarn roller, the second exhibition yarn roller, the 3rd driven rod, the second width laser are determined Instrument, the 4th driven rod and wire drawing shaft, wire drawing shaft are driven by electrodeless variable-speed motor, by putting belt, one end of belt on thread supply shaft It is fixed on device case, the other end of belt is provided with linking up with and being hung with definite value counterweight, and the side of totally-enclosed casing is provided with band and shown The control panel and power switch of display screen, the shift knob for adjusting wire drawing shaft rotating speed, the temperature of control Electromagnetic Heating exhibition yarn roll temperature Control button.
2. the test device of the carbon fiber fibrillation expanding of controllable temperature as claimed in claim 1, it is characterised in that:It is totally-enclosed The length of casing is respectively 1000mm, 500mm, 400mm, and totally-enclosed casing is in constant temperature and humidity room.
3. the test device of the carbon fiber fibrillation expanding of controllable temperature as claimed in claim 1, it is characterised in that:Device case Length be respectively 850mm, 50mm, 300mm.
4. the test device of the carbon fiber fibrillation expanding of controllable temperature as claimed in claim 1, it is characterised in that:Open up yarn roller Be made of plating straight-chromiun stainless steel, exhibition yarn roller is wine barrel-shaped, the minimum diameter of exhibition yarn roller be 15mm, length be 40mm, radian be π/ 6。
5. the test device of the carbon fiber fibrillation expanding of the controllable temperature as described in claim any one of 1-4, its feature exists In:Electromagnetic Heating exhibition yarn roller is made of metal, and a diameter of 20mm of Electromagnetic Heating exhibition yarn roller, length are 40mm.
6. a kind of usage right requires the test of any one of the 1-5 carbon fiber fibrillation expanding of the controllable temperature of the test device Method, it is characterised in that:Comprise the following steps,
First maintain test room temperature and humidity constant before step 1, test, room temperature is 20 DEG C ± 2 DEG C, and relative humidity is 45% ± 3%, then make by horizontal adjustment knob the level of totally-enclosed casing;
Step 2, turn on the power switch, adjust temperature control button, select a temperature, state is maintained 30 minutes;
Step 3, some same models of ingot of selection test fibrillation expanding with a batch of carbon fiber;
Step 4, sliding door is opened, take carbon fiber ingot to be put on thread supply shaft, spacing hole, the are sequentially sequentially passed through after fiber is involved One driven rod, the first width laser analyzer, the second driven rod, the first exhibition yarn roller, some Electromagnetic Heatings exhibition yarn roller, the second exhibition yarn Roller, the 3rd driven rod, the second width laser analyzer, the 4th driven rod, finally receive silk ingot from wound thereon in the empty of wire drawing shaft On, close sliding door;
Step 5, regulation shift knob make the tow speed of service of display screen display be 15rpm, then read and show every 10s The upper first width laser analyzer of screen, the numerical value of the second width laser analyzer, read 10 times altogether, wherein the first width laser What analyzer was measured is width before exhibition yarn, and what the second width laser analyzer was measured is width after exhibition yarn, finally tries to achieve exhibition yarn rateIt is fiber width average value before exhibition yarn,It is fiber width average value after exhibition yarn, using Microsoft Excel 10 batch datas are handled, data discrete coefficient Cv values are obtained;
Step 6, remaining carbon fiber operated according to above-mentioned steps 4-5 successively, the test number of all carbon fibers is made even Average, finally gives the test data of fibrillation expanding of the model batch carbon fiber under the specified temp.
CN201710645777.7A 2017-07-31 2017-07-31 The test device and method of the carbon fiber fibrillation expanding of controllable temperature Pending CN107314970A (en)

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Publication number Priority date Publication date Assignee Title
CN108680498A (en) * 2018-08-10 2018-10-19 江苏恒神股份有限公司 A kind of carbon fiber friction coefficient testing device and method
WO2022147884A1 (en) * 2021-01-11 2022-07-14 北京航空航天大学 Real-time adjustment apparatus for broadening and thickening of impregnated fiber bundle
CN116443666A (en) * 2023-06-15 2023-07-18 江苏高倍智能装备有限公司 Special-shaped workpiece yarn winding machine
CN117104985A (en) * 2023-10-23 2023-11-24 德州联合拓普复合材料科技有限公司 Carbon fiber yarn spreading fiber creel in carbon fiber prepreg preparation
CN117104985B (en) * 2023-10-23 2024-01-09 德州联合拓普复合材料科技有限公司 Carbon fiber yarn spreading fiber creel in carbon fiber prepreg preparation

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Application publication date: 20171103