CN107311162A - A kind of continuous production graphene device - Google Patents
A kind of continuous production graphene device Download PDFInfo
- Publication number
- CN107311162A CN107311162A CN201710522934.5A CN201710522934A CN107311162A CN 107311162 A CN107311162 A CN 107311162A CN 201710522934 A CN201710522934 A CN 201710522934A CN 107311162 A CN107311162 A CN 107311162A
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- Prior art keywords
- bistrique
- box
- stationary
- condenser
- continuous production
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/18—Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
- B02C23/36—Adding fluid, other than for crushing or disintegrating by fluid energy the crushing or disintegrating zone being submerged in liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C7/00—Crushing or disintegrating by disc mills
- B02C7/02—Crushing or disintegrating by disc mills with coaxial discs
- B02C7/08—Crushing or disintegrating by disc mills with coaxial discs with vertical axis
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C7/00—Crushing or disintegrating by disc mills
- B02C7/11—Details
- B02C7/12—Shape or construction of discs
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C19/00—Other disintegrating devices or methods
- B02C19/18—Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
- B02C2019/183—Crushing by discharge of high electrical energy
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B2204/00—Structure or properties of graphene
- C01B2204/02—Single layer graphene
Abstract
The invention discloses a kind of continuous production graphene device, including frame, once mounting has motor to the machine frame inside from the bottom to top, separator box, charging box and condenser box, insulating lid is provided with the top of the separator box, centrifugal pan is provided with inside the separator box, the centrifugal pan is provided with rotary bistrique, stationary bistrique is provided with the top of the rotary bistrique, the stationary bistrique is fixedly mounted on insulating lid, and junction is provided with No. two sealing rings, the stationary bistrique lower end is in taper hole shape, the rotary bistrique upper end is in axis of cone shape, and the taper of the axis of cone and the taper of taper hole are equal, the axis of cone of the rotary bistrique upper end is additionally provided with the even liquid bath of rotary bistrique, gland is provided with the top of the stationary bistrique, fluid injection pore is offered inside the stationary bistrique, connection ascending pipe at the top of the fluid injection pore, the ascending pipe runs through gland.Apparatus of the present invention overall structure is simple and convenient to operate, and less energy consumption, yield are high, lightweight, non-environmental-pollution, can realize graphene separation, the continuous production of purification.
Description
Technical field
The present invention relates to technical field of novel materials, more particularly to a kind of continuous production graphene device.
Background technology
The production of graphene, traditional handicraft has mechanical stripping method, expanded graphite graft process;Mechanical stripping method workload is big,
Efficiency is low, and production graphene cost is high, and graphene can not be widely applied.Expanded graphite graft process produces graphene, production technology
Numerous rope, in expanded graphite production process, intercalator is done using strong corrosive material, is produced in enormous quantities, and local environment is polluted
It is larger, it is impossible to popularization and application.Therefore, a kind of it is proposed that continuous production graphene device.
The content of the invention
It is a primary object of the present invention to provide a kind of continuous production graphene device, effectively it can solve in background technology
The problem of.
To achieve the above object, the technical scheme taken of the present invention is:
A kind of continuous production graphene device, including frame, once mounting has motor, separation to the machine frame inside from the bottom to top
Be provided with the top of case, charging box and condenser box, the separator box inside insulating lid, the separator box and be provided with centrifugal pan, it is described from
Cartridge is provided with the top of rotary bistrique, the rotary bistrique and is provided with stationary bistrique, and the stationary bistrique is fixedly mounted on insulating lid, and connection
Place is provided with No. two sealing rings, and the stationary bistrique lower end is in taper hole shape, and the rotary bistrique upper end is in axis of cone shape, and the cone of the axis of cone
Degree is equal with the taper of taper hole, and the axis of cone of the rotary bistrique upper end, which is additionally provided with the top of the even liquid bath of rotary bistrique, the stationary bistrique, to be provided with
Connection ascending pipe at the top of fluid injection pore, the fluid injection pore is offered inside gland, the stationary bistrique, the ascending pipe is through pressure
Lid, the gland is fixed on insulating lid by two groups of screw mandrels, and the part that the ascending pipe is located at gland bottom is equipped with spring,
Connection return duct on the inside of the ascending pipe, one end of the return duct connects the bottom of side, the one of the remote fluid injection pore
End connection suction line, the side of described suction line one end connection separator box bottom, the insulating lid provided with charging pore, it is described enter
Expects pipe hole is connected with charging box by pipeline, and internal described in condenser box to be provided with condenser pipe, described condenser pipe one end is run through and prolonged
Extend inside separator box, the condenser pipe other end connects condensator outlet, the centrifugation tray bottom is connected with motor output shaft,
And junction, provided with a sealing ring, the motor output shaft outside is provided with slip ring.
Further, the stationary bistrique is connected with an electrode wires, and the rotary bistrique is connected with conductor wire, the conductor wire
One end connects No. two electrode wires, the machine frame inside and is provided with carbon brush with slip ring correspondence position.
Further, the Pipe installing has a valve, and the ascending pipe is provided with No. three valves, the suction line peace
Equipped with circulating pump, the return duct is provided with No. two valves.
Further, the side of the separator box bottom is provided with drainage tube, and the side is provided with capping, described and capping
Connection is screwed, and junction is provided with leak-proof washer.
Further, it is provided with inside the charging box at the top of mixed liquor, the charging box and is provided with charge door, the condenser
Cooling fluid is housed, the part that the condenser pipe is located inside condenser box is provided with fin inside case.
Compared with prior art, the present invention has the advantages that:Apparatus of the present invention overall structure is simple, operation side
Just, and less energy consumption, yield is high, lightweight, non-environmental-pollution, graphene separation, the continuous production of purification can be realized.
Brief description of the drawings
Fig. 1 is a kind of overall structure diagram of continuous production graphene device of the present invention.
Fig. 2 is a kind of internal structure schematic diagram of continuous production graphene device of the present invention.
In figure:1st, frame;2nd, charge door;3rd, charging box;4th, mixed liquor;5th, pipeline;6th, a valve;7th, an electrode
Line;8th, stationary bistrique;9th, insulating lid;10th, pore is fed;11st, fluid injection pore;12nd, separator box;13rd, rotary bistrique;14th, centrifugal pan;
15th, drainage tube;16th, a sealing ring;17th, conductor wire;18th, slip ring;19th, motor;20th, carbon brush;21st, No. two electrode wires;22nd, two
Number valve;23rd, the even liquid bath of rotary bistrique;24th, cover;25th, condenser pipe;26th, circulating pump;27th, No. two sealing rings;28th, screw mandrel;29、
Spring;30th, gland;31st, ascending pipe;32nd, condensator outlet;33rd, fin;34th, cooling fluid;35th, condenser box;36th, No. three
Valve;37th, suction line;38th, return duct.
Embodiment
To be easy to understand the technical means, the inventive features, the objects and the advantages of the present invention, with reference to
Embodiment, is expanded on further the present invention.
As shown in Figure 1-2, from the bottom to top one inside a kind of continuous production graphene device, including frame 1, the frame 1
Secondary to be provided with motor 19, separator box 12, charging box 3 and condenser box 35, the top of separator box 12 is provided with insulating lid 9, described
The inside of separator box 12 is provided with centrifugal pan 14, and the centrifugal pan 14 is provided with rotary bistrique 13, and the top of rotary bistrique 13 is provided with fixed mill
First 8, the stationary bistrique 8 is fixedly mounted on insulating lid 9, and junction, provided with No. two sealing rings 27, the lower end of stationary bistrique 8 is in
Taper hole shape, the upper end of rotary bistrique 13 is in axis of cone shape, and the taper of the axis of cone and the taper of taper hole are equal, the rotary bistrique 13
The axis of cone of upper end is additionally provided with the even liquid bath 23 of rotary bistrique, and the top of stationary bistrique 8, which is provided with inside gland 30, the stationary bistrique 8, to be opened up
There is fluid injection pore 11, the top of the fluid injection pore 11 connection ascending pipe 31, the ascending pipe 31 runs through gland 30, the gland 30
It is fixed on by two groups of screw mandrels 28 on insulating lid 9, the part that the ascending pipe 31 is located at the bottom of gland 30 is equipped with spring 29, institute
The inner side of ascending pipe 31 connection return duct 38 is stated, one end of the return duct 38 connects the bottom of 12 sides, and described 31 away from fluid injection
One end connection suction line 37 of pore 11, the side of the one end of suction line 37 connection separator box 12 bottom, the insulating lid 9 is set
There is charging pore 10, the charging pore 10 is connected with charging box 3 by pipeline 5, and 35 inside are provided with condensation described in condenser box
Pipe 25, described one end of condenser pipe 25 is through 9 and extends to inside separator box 12, and the other end of the condenser pipe 25 connection condenser goes out
Mouth 32, the bottom of centrifugal pan 14 is connected with the output shaft of motor 19, and junction, provided with a sealing ring 16, the motor 19 is defeated
Slip ring 18 is provided with the outside of shaft.
A kind of continuous production graphene device of the invention, during work, by an electrode wires 7, No. two electrode wires 21 and motor
19 switch on power, can normal work, mixed liquor 4 is added in charging box 3 by charge door 2, number valve 6 of turn will
Mixed liquor 4 adds separator box 12 by pipeline 5, and a number valve 6 of adjustment makes mixed liquor 4 enter the flow of separator box 12 and graphene stream
Go out the flow of separator box 12 impartial, start circulating pump 26 4 point of two tunnel of mixed liquor in separator box 12, graphite stationary bistrique is injected all the way
8, spray in the crack between graphite stationary bistrique 8 and graphite rotary bistrique 13, another road enters return duct 38 and rinses stirring separation
Mixed liquor 4 in case 12, starts the motor 19 of graphite rotary bistrique 13, makes graphite rotary bistrique 13 in the tapered hole of graphite stationary bistrique 8
Rotate at a high speed, using one group of graphite rotary bistrique 13, the stationary bistrique 8 of close contact, fluid injection pore 11 is drilled with stationary bistrique 8, from
Fluid injection pore 11 pressurization injection graphite solution, rotary bistrique 13 add power drive under rotate at a high speed, by graphite rotary bistrique 13,
Apply electric field respectively in stationary bistrique 8, the graphite particle in graphite solution is continuously broken up using the electric arc in electric field, is broken
The centrifugal pan 14 that graphite particle is installed by rotary bistrique 13 rotates at a high speed the centrifugal force separate of generation, the larger graphite of particle diameter
The fluid injection pore 11 that powder solution injects stationary bistrique 8 through circulating pump 26 enters to be continued to break up in the crack of two bistriques, and electric arc is broken up
The condensed pipe 25 of the less gaseous state thing of graphite particle diameter flows into container, and the liquid that condensed pipe 25 is flowed into container after liquefying is just
Single-layer graphene mixed solution, in the continuous cyclic process of graphite solution, by rotary bistrique 13 centrifuge out it is thick
Graphene mixture can be bonded at the inwall of separator box 12, be bonded at the inwall of separator box 12 it is thick be exactly graphite and graphene mixing
Thing, graphite and multi-layer graphene mixture are rinsed through high pressure reflow mixed liquor, the graphite particle in the graphite solution not being breached
Stationary bistrique 8 is again introduced into through circulating pump 26 to continue to break up, breaking up graphite particle and multi-layer graphene with multi-layer graphene relic
During relic, multi-layer graphene relic is smaller because of resistance, in rotary bistrique 13, the electric field crack of stationary bistrique 8, the electric field being subject to
Power is maximum, breaks up speed and breaks up speed more than graphite particle, until the graphite particle in graphite solution is converted to multilayer --
Single-layer graphene solution, while in sealing container inwall formation multi-layer graphene paste, completing graphite and directly producing graphene
Flow.
Wherein, the stationary bistrique 8 is connected with an electrode wires 7, and the rotary bistrique 13 is connected with conductor wire 17, the conduction
The one end of line 17 connects No. two electrode wires 21, the inside of the frame 1 and is provided with carbon brush 20 with the correspondence position of slip ring 18, by by one
Number electrode wires 7 and No. two electrode wires 21 switch on power, and make stationary bistrique 8 and the formation electric field of rotary bistrique 13.
Wherein, the pipeline 5 is provided with a valve 6, and the ascending pipe 31 is provided with No. three valves 36, the suction line
37 are provided with circulating pump 26, and the return duct 38 is provided with No. two valves 22, adjust a valve 6, make a flow of valve 6 and
Condensator outlet 32 keeps impartial, No. two valves 22 of adjustment, the flow of No. three valves 36, makes graphite stationary bistrique 8 and the dynamic mill of graphite
Solution pressure and the pressure of spring 29 between first 13 keep impartial.
Wherein, the side of the bottom of separator box 12 is provided with drainage tube 15, and 12 side is provided with capping 24, described 12
Connection is screwed with capping 24, and junction is provided with leak-proof washer.
Wherein, the inside of charging box 3 is provided with mixed liquor 4, and the top of charging box 3 is provided with charge door 2, the condenser
The inside of case 35 is equipped with cooling fluid 34, and the part that the condenser pipe 25 is located inside condenser box 35 is provided with fin 33.
In the present invention, graphite stationary bistrique 8 and the friction contact surface of graphite rotary bistrique 13 make planar shaped, live meaning taper angle
Shape, has no effect on the application of the technology of the present invention.
In the present invention, graphite stationary bistrique 8 and the installation site of graphite rotary bistrique 13 are exchanged, and have no effect on the technology of the present invention
Using.
In the present invention, graphite stationary bistrique 8 and graphite rotary bistrique 13 installation direction in machine frame are arbitrarily selected, not
Influence the application of the technology of the present invention.
In the present invention, the graphite powder in mixed liquor 4, can select the graphite that any carbon structure is constituted, has no effect on
The application of the technology of the present invention.
In the present invention, the solution in mixed liquor 4, can select aqueous, oiliness, organic matter, inorganic matter, has no effect on this hair
The application of bright technology.
In the present invention, the concentration of mixed liquor 4 is large and small, and the pressure that circulating pump 26 is produced is high and low, has no effect on the present invention
The application of technology.
In the present invention, the electric field between graphite stationary bistrique 8 and graphite rotary bistrique 13, can select alternating current, direct current, change
Frequency electricity, electrostatic, have no effect on the application of the technology of the present invention.
In the present invention, from the intensity of electric field, graphite rotary bistrique 13 between graphite stationary bistrique 8 and graphite rotary bistrique 13
Rotating speed speed, has no effect on the application of the technology of the present invention.
In the present invention, rotary bistrique 13 used, stationary bistrique 8 can select graphite material, metal material, have no effect on this hair
The application of bright technology.
In the present invention, rotary bistrique 13 used, stationary bistrique 8 can single group work, can also it is multigroup with one heart, combine work side by side
Make, have no effect on the application of the technology of the present invention.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (5)
1. a kind of continuous production graphene device, including frame(1), it is characterised in that:The frame(1)Internal from the bottom to top one
It is secondary that motor is installed(19), separator box(12), charging box(3)And condenser box(35), the separator box(12)Top is provided with exhausted
Edge lid(9), the separator box(12)Inside is provided with centrifugal pan(14), the centrifugal pan(14)Rotary bistrique is installed(13), it is described
Rotary bistrique(13)Top is provided with stationary bistrique(8), the stationary bistrique(8)It is fixedly mounted on insulating lid(9)On, and junction is provided with two
Number sealing ring(27), the stationary bistrique(8)Lower end is in taper hole shape, the rotary bistrique(13)Upper end is in axis of cone shape, and the axis of cone
Taper and taper hole taper it is equal, the rotary bistrique(13)The axis of cone of upper end is additionally provided with the even liquid bath of rotary bistrique(23), it is described fixed
Bistrique(8)Top is provided with gland(30), the stationary bistrique(8)Inside offers fluid injection pore(11), the fluid injection pore(11)
Top connects ascending pipe(31), the ascending pipe(31)Through gland(30), the gland(30)Pass through two groups of screw mandrels(28)Gu
It is scheduled on insulating lid(9)On, the ascending pipe(31)Positioned at gland(30)The part of bottom is equipped with spring(29), the ascending pipe
(31)Inner side connects return duct(38), the return duct(38)One end connection(12)The bottom of side, it is described(31)Away from note
Liquid pipe hole(11)One end connection suction line(37), the suction line(37)One end connects separator box(12)The side of bottom, institute
State insulating lid(9)Provided with charging pore(10), the charging pore(10)And charging box(3)Pass through pipeline(5)It is connected, condenser
Described in case(35)Inside is provided with condenser pipe(25), the condenser pipe(25)One end is run through(9)And extend to separator box(12)Inside,
The condenser pipe(25)The other end connects condensator outlet(32), the centrifugal pan(14)Bottom and motor(19)Output shaft connects
Connect, and junction is provided with a sealing ring(16), the motor(19)Slip ring is provided with the outside of output shaft(18).
2. a kind of continuous production graphene device according to claim 1, it is characterised in that:The stationary bistrique(8)Connection
There are an electrode wires(7), the rotary bistrique(13)It is connected with conductor wire(17), the conductor wire(17)One end connects No. two electrodes
Line(21), the frame(1)Internal and and slip ring(18)Correspondence position is provided with carbon brush(20).
3. a kind of continuous production graphene device according to claim 1, it is characterised in that:The pipeline(5)It is provided with
A number valve(6), the ascending pipe(31)No. three valves are installed(36), the suction line(37)Circulating pump is installed(26),
The return duct(38)No. two valves are installed(22).
4. a kind of continuous production graphene device according to claim 1, it is characterised in that:The separator box(12)Bottom
Side drainage tube is installed(15), it is described(12)Side is provided with capping(24), it is described(12)And capping(24)It is solid by screw
Fixed connection, and junction is provided with leak-proof washer.
5. a kind of continuous production graphene device according to claim 1, it is characterised in that:The charging box(3)It is internal
Provided with mixed liquor(4), the charging box(3)Top is provided with charge door(2), the condenser box(35)Inside is equipped with cooling fluid
(34), the condenser pipe(25)Positioned at condenser box(35)Internal part is provided with fin(33).
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CN201710522934.5A CN107311162B (en) | 2017-06-30 | 2017-06-30 | A kind of continuous production graphene device |
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CN201710522934.5A CN107311162B (en) | 2017-06-30 | 2017-06-30 | A kind of continuous production graphene device |
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CN107311162B CN107311162B (en) | 2019-10-22 |
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Cited By (8)
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CN107892294A (en) * | 2017-12-31 | 2018-04-10 | 周思齐 | The method and apparatus that high purity graphite rod produces graphene |
CN108238598A (en) * | 2018-04-20 | 2018-07-03 | 上海地霸电子科技有限公司 | A kind of mechanical device of continuous production graphene |
CN109809395A (en) * | 2019-01-22 | 2019-05-28 | 上海地霸电子科技有限公司 | A kind of graphite directly produces the method and device of graphene composite particulate material |
CN111320163A (en) * | 2018-12-17 | 2020-06-23 | 上海地霸电子科技有限公司 | Graphene mixed solution preparation device and method and mixed solution |
CN111318242A (en) * | 2018-12-17 | 2020-06-23 | 上海地霸电子科技有限公司 | Graphene composite material preparation device and method and composite material |
CN112236026A (en) * | 2020-09-30 | 2021-01-15 | 扬州斯帕克实业有限公司 | Graphene composite wave-absorbing preparation device and coating agent prepared by using same |
CN114014309A (en) * | 2021-12-13 | 2022-02-08 | 哈尔滨盛世康虹生物技术有限公司 | Water-soluble graphene production equipment and method based on electric field melting |
WO2023115152A1 (en) * | 2021-12-23 | 2023-06-29 | 2MS Mining Pty Ltd | Apparatus and process for processing materials |
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CN107892294A (en) * | 2017-12-31 | 2018-04-10 | 周思齐 | The method and apparatus that high purity graphite rod produces graphene |
CN108238598A (en) * | 2018-04-20 | 2018-07-03 | 上海地霸电子科技有限公司 | A kind of mechanical device of continuous production graphene |
CN111320163A (en) * | 2018-12-17 | 2020-06-23 | 上海地霸电子科技有限公司 | Graphene mixed solution preparation device and method and mixed solution |
CN111318242A (en) * | 2018-12-17 | 2020-06-23 | 上海地霸电子科技有限公司 | Graphene composite material preparation device and method and composite material |
CN109809395A (en) * | 2019-01-22 | 2019-05-28 | 上海地霸电子科技有限公司 | A kind of graphite directly produces the method and device of graphene composite particulate material |
CN112236026A (en) * | 2020-09-30 | 2021-01-15 | 扬州斯帕克实业有限公司 | Graphene composite wave-absorbing preparation device and coating agent prepared by using same |
CN114014309A (en) * | 2021-12-13 | 2022-02-08 | 哈尔滨盛世康虹生物技术有限公司 | Water-soluble graphene production equipment and method based on electric field melting |
WO2023115152A1 (en) * | 2021-12-23 | 2023-06-29 | 2MS Mining Pty Ltd | Apparatus and process for processing materials |
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