CN107308071A - It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof - Google Patents

It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof Download PDF

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Publication number
CN107308071A
CN107308071A CN201710366922.8A CN201710366922A CN107308071A CN 107308071 A CN107308071 A CN 107308071A CN 201710366922 A CN201710366922 A CN 201710366922A CN 107308071 A CN107308071 A CN 107308071A
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facial mask
parts
matrimony vine
polyglutamic acid
liquid
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乔长晟
刘建军
张卫
李雪
黄丹
严婷婷
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Tianjin Qi Yuan Tang Biological Engineering Co Ltd
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Tianjin Qi Yuan Tang Biological Engineering Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/88Polyamides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/98Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
    • A61K8/987Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/02Preparations for care of the skin for chemically bleaching or whitening the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/80Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine

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  • Health & Medical Sciences (AREA)
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  • Mycology (AREA)
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  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Cosmetics (AREA)

Abstract

The invention belongs to cosmetic skin field, and in particular to a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof.The matrimony vine facial mask of the present invention includes the facial mask stoste of spunlace non-woven cloth Face film towel and infiltration on spunlace non-woven cloth;Facial mask stoste includes the component of following parts by weight:25 40 parts of pure water;20 35 parts of fermentation Chinese wolfberry fruit liquid;25 parts of polyglutamic acid;0.1 0.5 parts of vitamin C;15 20 parts of asparagus juice;10 15 parts of pearl powder;0.3 0.8 parts of propane diols;25 parts of pulullan polysaccharide.The matrimony vine facial mask of the present invention prepares fermentation Chinese wolfberry fruit liquid using saccharomycetes to make fermentation, prepared by compounding natural moisture preserving whitening composition polyglutamic acid.This composition of the polyglutamic acid that the present invention is used not only there is extremely strong moisture retention can also effectively control the dissolution of Chinese-wolfberry nutritive composition, with slow release effect, make the using effect of matrimony vine facial mask more preferable.

Description

It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof
Technical field
The invention belongs to cosmetic skin field, and in particular to a kind of matrimony vine facial mask for adding polyglutamic acid and its preparation Method.
Background technology
With the improvement of living standards, people also increasingly pursue beautiful pursuit inherent and natural.Therefore to skin Health care consciousness is also being improved.Concept to cosmetics also progressively changes.In the past using beauty as main purpose, turning now to Beauty is laid equal stress on nursing, especially in the conceptive of facial mask, is more the nursing skin of promotion science, and in the market majorityization The complex manufacturing technology of cosmetic and mostly contain artificial synthesized chemicals, easily stimulate to skin, especially some skins it is quick Touching group and the crowd of particular time, cause allergy, people is produced query to the composition of cosmetics.
Matrimony vine, the also known as fruit of Chinese wolfberry, are Solanaceae deciduous plant (Lycium chintnse) or lycium barbarum (Lycium Barbarum ripening fruits), is famous nourishing Chinese medicine, is included in by health ministry《It is both food and the article of medicine List》.Modern pharmacological research result shows that matrimony vine is except having reducing blood lipid known to people, decompression, hypoglycemic, enhancing body to exempt from Epidemic disease function etc. is acted on, moreover it is possible to make erythrocyte sod activity rise.Its polysaccharide Wheat Protein, to safeguarding the normal of human body cell Develop, improve DNA repair ability and promote senile cell to be reversed to young direction and all play beneficial effect.The chemistry of matrimony vine Composition mainly contains LBP-X (LBP), glycine betaine, carotenoid and carotenoid ester, vitamin C, several amino acids and Various trace elements.Because of place of production difference, component content slightly has difference to matrimony vine.By the fermentation process of saccharomycete, Chinese holly can be lifted The absorbability of the nutriment of Qi, converts some compositions to skin sensitivity, reduces allergic reaction.
The application for preparing facial mask using matrimony vine is existing a lot, such as refer in patent CN201610219829.X a kind of black Matrimony vine facial mask, it uses lycium ruthenicum to take its extract solution after grinding, then constitutes the raw materials such as itself and cucumber, its process be not related to by Fermentation Chinese wolfberry fruit prepares facial mask technique.A kind of preparation method of matrimony vine facial mask is relate in patent CN201610830191.3, by Chinese holly Qi zymotic fluid, collagen, vitamin C, asparagus juice pearl powder and propane diols simply compounding are formed.The advantage of the above method is to adopt With pure natural raw material as facial mask stoste, fermentation Chinese wolfberry fruit liquid is added, is not destroyed based on active ingredient at utmost, retain matrimony vine hair Active ingredient in zymotic fluid, obtained facial mask has moisturizing, whitening, effect of anti-aging, but it makes to different crowd It is need to be improved with effect.
Therefore, the using effect for how further improving matrimony vine facial mask is the current technical issues that need to address.
The content of the invention
The purpose of the present invention be in view of the shortcomings of the prior art there is provided a kind of matrimony vine facial mask for adding polyglutamic acid and its Preparation method.The matrimony vine facial mask of the present invention prepares fermentation Chinese wolfberry fruit liquid using saccharomycetes to make fermentation, and compounding natural moisture preserving whitening composition gathers It is prepared by glutamic acid.This composition of the polyglutamic acid that the present invention is used not only there is extremely strong moisture retention can also effectively control matrimony vine The dissolution of nutritional ingredient, with slow release effect, makes the using effect of matrimony vine facial mask more preferable.
To achieve the above object, the present invention is adopted the following technical scheme that:
A kind of matrimony vine facial mask for adding polyglutamic acid, the matrimony vine facial mask includes spunlace non-woven cloth Face film towel and infiltration exists Facial mask stoste on spunlace non-woven cloth;The facial mask stoste includes the component of following parts by weight:
The molecular weight of the polyglutamic acid is 91-101 ten thousand.
It is used as preferred technical scheme:
It is preferred that, the saccharomycete used during the fermentation Chinese wolfberry fruit liquid fermentation is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:The saccharomycete of 1 mixing.
It is preferred that, the particle diameter of the pearl powder is 100-200nm.
It is preferred that, the pulullan polysaccharide is 20-40 ten thousand for molecular weight.Increase pulullan polysaccharide composition, the composition and Polyglutamic acid is compounded, and can be beneficial to the film-formation result of facial mask, moisturizing and slow release effect are more preferable.
The present invention also provides the preparation method for the matrimony vine facial mask for adding polyglutamic acid, comprises the following steps:
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, become thick liquid;It is poly- Glutamic acid solution viscosity is larger, can be very good suspension pearl powder.Help to be well mixed.
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit Liquid is stirred and evenly mixed, and obtains facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked in facial mask stoste, then vacuum seal Dress, is made matrimony vine facial mask.
It is preferred that, the preparation method of the fermentation Chinese wolfberry fruit liquid is:By dry wolfberry and water in mass ratio 1:8-15 mixing is abundant Mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5-1%, dipotassium hydrogen phosphate 0.03-0.1%, manganese sulfate 0.5-1%, sterilize after fully mixing, inoculation yeast bacterium;It is subsequently placed in 180rpm on shaking table, 30 DEG C, 48h is cultivated, fermentation Chinese wolfberry fruit stoste is obtained;By the fermenation raw liquid filtration sterilization, retain supernatant and be adjusted to the pH value of supernatant Neutrality, obtains fermentation Chinese wolfberry fruit liquid.
It is preferred that, when being stirred in step (1), the speed of stirring is 80-100r/min.
It is preferred that, when being stirred in step (2), it need to stir at ambient temperature, the speed of stirring is 80-100r/min.
It is preferred that, the time of immersion is 30-40min in step (3).
Inventive principle:
Due to, containing the ultrahydrophilic group (- COOH) of more than 1000, can fully keep water in polyglutamic acid molecule Point, can be in skin table for improving voidage in matrimony vine facial mask between nutritional ingredient, being absorbed beneficial to the effective nutritional ingredient of matrimony vine Face forms thin film protection skin and absorbed, and is the optimal transport platform of nutrient, moisture and Touch skin familiarity in matrimony vine facial mask, Effectively increase dissolving, storage, conveying and the absorption in matrimony vine facial mask active ingredient.In addition, polyglutamic acid has hydrophilic radical, Carboxyl, ionizable negatively charged, the adsorbable nutritional ingredient of negative electrical charge, polyglutamic acid can be released slowly due to its powerful group attribute Chinese-wolfberry nutritive composition is put, during face mask film, moisture and the uniform dissolution of nutrition can be made so that skin slow-absorbing.
Beneficial effect:
Polyglutamic acid has extremely strong moisture retention, can form layer protecting film on skin to prevent the steaming of skin moisture Hair, it can penetrate into skin deep layer, self moisture-keeping system of recovery skin.With advancing age with the aggravation of physical fatigue, The function of profit certainly of skin can gradually weaken, or even disappear, and the facial mask that with the addition of polyglutamic acid can repair the profit work(certainly of skin Energy.Therefore polyglutamic acid has good beauty protecting effect for the skin of the mankind.
The present invention is substituted original using moisturizing whitening composition of the pure natural polymer substance polyglutamic acid as facial mask stoste Component collagen albumen, add fermentation Chinese wolfberry fruit liquid, using saccharomycetes to make fermentation, some skins of farthest degrading be not easy absorb and The material of easy sensitization, retains the active ingredient in fermentation Chinese wolfberry fruit liquid, and the facial mask of preparation has moisturizing, whitening, the work(of anti-aging Effect, has certain effect to different crowd.This composition of polyglutamic acid not only there is extremely strong moisture retention can also effectively control The dissolution of Chinese-wolfberry nutritive composition, with slow release effect.Therefore, polyglutamic acid of the invention this be not merely that instead of collagen egg In vain, this moisturizing ingredient of hyaluronic acid, glycerine etc., moreover it is possible to acted synergistically with fermentation Chinese wolfberry fruit liquid, imitate the use of matrimony vine facial mask Fruit is more preferably.
Polyglutamic acid be it is a kind of water-soluble, it is biodegradable, be a kind of to the high-end of the nutritious effect of skin without toxicity Product, is completely suitable for all skins, and provide the lasting moistening effect better than hyaluronic acid and collagen, it is only necessary to Very low concentration, it is possible to reach good effect, therefore cost is very low.Available for skin care item, shampoo, hair-cream, shaving cream In lipstick.Therefore, matrimony vine preparation method of the invention is easy, and feasibility is high, it is easy to promote production, and cost is not high.
Embodiment
The invention will be further elucidated with reference to specific embodiments.It should be understood that these embodiments are merely to illustrate this hair Bright rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, art technology Personnel can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims and limited Fixed scope.
Embodiment 1
The present invention the matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows:
25 parts of pure water;
20 parts of fermentation Chinese wolfberry fruit liquid;
2 parts of polyglutamic acid;Molecular weight is 950,000
0.1 part of vitamin C;
15 parts of asparagus juice;
10 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.3 part of propane diols;
2 parts of pulullan polysaccharide;Molecular weight is 200,000;
The preparation method of the matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 80r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 80r/min, obtains facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 30min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.By the fermenation raw liquid filtration sterilization, reserve rich in Chinese-wolfberry nutritive into The supernatant divided, adjusts pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixes Close, obtain fermentation Chinese wolfberry fruit liquid.
Embodiment 2
The present invention the matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows:
30 parts of pure water;
22 parts of fermentation Chinese wolfberry fruit liquid;
5 parts of polyglutamic acid;Molecular weight is 910,000
0.2 part of vitamin C;
16 parts of asparagus juice;
12 parts of pearl powder;The particle diameter of pearl powder is 200 nanometers;
0.4 part of propane diols;
4 parts of pulullan polysaccharide;Molecular weight is 250,000;
The preparation method of the matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 90r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 90r/min, obtains facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 35min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:10 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, sulfuric acid Manganese 0.5%, sterilizes after fully mixing, inoculation yeast bacterium.180rpm on shaking table is placed in, 30 DEG C, 48h is cultivated, obtains fermentation Chinese wolfberry fruit Stoste.By the fermenation raw liquid filtration sterilization, the supernatant rich in Chinese-wolfberry nutritive composition is reserved, pH value is adjusted to neutrality.Saccharomycete is CGMCCNO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains fermentation Chinese wolfberry fruit liquid.
Embodiment 3
The present invention the matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows:Matrimony vine facial mask system The addition of standby middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
30 parts of pure water;
25 parts of fermentation Chinese wolfberry fruit liquid;
5 parts of polyglutamic acid;Molecular weight is 1,000,000
0.4 part of vitamin C;
17 parts of asparagus juice;
15 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.8 part of propane diols;
5 parts of pulullan polysaccharide;Molecular weight is 300,000;
The preparation method of the matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 100r/min, makes it As thick liquid;
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 100r/min, obtains facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 40min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
Wherein fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:By dry wolfberry and water in mass ratio 1:15 mixing fully mashing, as Basal liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, sulfuric acid Manganese 0.5%, sterilizes after fully mixing, inoculation yeast bacterium.180rpm on shaking table is placed in, 30 DEG C, 48h is cultivated, obtains fermentation Chinese wolfberry fruit Stoste.By the fermenation raw liquid filtration sterilization, the supernatant rich in Chinese-wolfberry nutritive composition is reserved, pH value is adjusted to neutrality.Saccharomycete is CGMCCNO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixing, obtains fermentation Chinese wolfberry fruit liquid.
The matrimony vine facial mask that embodiment 3 is prepared is given different age group crowd and used, each people of age bracket 100, obtains Result such as table 1.
Table 1 is the preparation effect of matrimony vine facial mask prepared by embodiment 3
Found by table 1, the moisturizing of such matrimony vine facial mask, whitening, effect of anti-aging, to having very for different crowd Good effect.
Embodiment 4
The present invention the matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows:
40 parts of pure water;
35 parts of fermentation Chinese wolfberry fruit liquid;
3 parts of polyglutamic acid;Molecular weight is 1,000,000
0.5 part of vitamin C;
20 parts of asparagus juice;
15 parts of pearl powder;The particle diameter of pearl powder is 100 nanometers;
0.8 part of propane diols;
3 parts of pulullan polysaccharide;Molecular weight is 200,000;
The preparation method of the matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 85r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 85r/min, obtains facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 33min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.By the fermenation raw liquid filtration sterilization, reserve rich in Chinese-wolfberry nutritive into The supernatant divided, adjusts pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixes Close, obtain fermentation Chinese wolfberry fruit liquid.
Embodiment 5
The present invention the matrimony vine facial mask for adding polyglutamic acid, by weight, including composition it is as follows:
30 parts of pure water;
30 parts of fermentation Chinese wolfberry fruit liquid;
4 parts of polyglutamic acid;Molecular weight is 1,010,000
0.4 part of vitamin C;
18 parts of asparagus juice;
13 parts of pearl powder;The particle diameter of pearl powder is 100nm;
0.6 part of propane diols;
5 parts of pulullan polysaccharide;Molecular weight is 300,000;
The preparation method of the matrimony vine facial mask for adding polyglutamic acid of the present invention, comprises the following steps:It is prepared by matrimony vine facial mask The addition of middle each component is identical with the parts by weight of each component in above-mentioned matrimony vine facial mask;
(1) polyglutamic acid and pearl powder are dissolved in pure water, and stirred, stir speed (S.S.) is 95r/min, make its into For thick liquid;
(2) asparagus juice is added in aforesaid liquid, adds vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit Mixing is stirred at room temperature in liquid, and stir speed (S.S.) is 95r/min, obtains facial mask stoste;
(3) after facial mask stoste is sterilized, then spunlace non-woven cloth Face film towel soaked into 38min, Ran Houzhen in facial mask stoste Sky encapsulation, is made matrimony vine facial mask.
The preparation method of wherein matrimony vine facial mask is as follows:Fermentation Chinese wolfberry fruit liquid and preparation method thereof is as follows:Dry wolfberry and water are pressed into quality Than 1:8 mixing fully mashing, based on liquid, following percentage by weight material is added into basal liquid:Anhydrous magnesium sulfate 0.5%, dipotassium hydrogen phosphate 0.03%, manganese sulfate 0.5% sterilizes after fully mixing, inoculation yeast bacterium.It is placed on shaking table 180rpm, cultivates 48h, obtains fermentation Chinese wolfberry fruit stoste by 30 DEG C.By the fermenation raw liquid filtration sterilization, reserve rich in Chinese-wolfberry nutritive into The supernatant divided, adjusts pH value to neutrality, saccharomycete is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:1 mixes Close, obtain fermentation Chinese wolfberry fruit liquid.

Claims (9)

1. a kind of matrimony vine facial mask for adding polyglutamic acid, it is characterized in that:The matrimony vine facial mask includes spunlace non-woven cloth Face film towel With facial mask stoste of the infiltration on spunlace non-woven cloth;The facial mask stoste includes the component of following parts by weight:
25-40 parts of pure water;
20-35 parts of fermentation Chinese wolfberry fruit liquid;
2-5 parts of polyglutamic acid;
0.1-0.5 parts of vitamin C;
15-20 parts of asparagus juice;
10-15 parts of pearl powder;
0.3-0.8 parts of propane diols;
2-5 parts of pulullan polysaccharide;
The molecular weight of the polyglutamic acid is 91-101 ten thousand.
2. the matrimony vine facial mask according to claim 1 for adding polyglutamic acid, it is characterised in that the fermentation Chinese wolfberry fruit liquid hair The saccharomycete used during ferment is CGMCC NO.3336 and CGMCC NO.1.8551 in mass ratio 1:The saccharomycete of 1 mixing.
3. the matrimony vine facial mask according to claim 1 for adding polyglutamic acid, it is characterised in that the particle diameter of the pearl powder For 100-200nm.
4. the matrimony vine facial mask according to claim 2 for adding polyglutamic acid, it is characterised in that the pulullan polysaccharide It is 20-40 ten thousand for molecular weight.
5. the preparation method of the matrimony vine facial mask for adding polyglutamic acid as described in claim 1-4 is any, it is characterized in that, including Following steps:
(1)Polyglutamic acid and pearl powder are dissolved in pure water, and stirred, thick liquid is become;
(2)Asparagus juice is added in aforesaid liquid, vitamin C, propane diols, pulullan polysaccharide and fermentation Chinese wolfberry fruit liquid is added and stirs Mixing is mixed, facial mask stoste is obtained;
(3)Soaked after the sterilizing of facial mask stoste, then by spunlace non-woven cloth Face film towel in facial mask stoste, then Vacuum Package, system Obtain matrimony vine facial mask.
6. the preparation method of the matrimony vine facial mask according to claim 5 for adding polyglutamic acid, it is characterised in that:The Chinese holly The preparation method of Qi zymotic fluid is:By dry wolfberry and water in mass ratio 1:The abundant mashing of 8-15 mixing, based on liquid, to basis Following percentage by weight material is added in liquid:Anhydrous magnesium sulfate 0.5-1%, dipotassium hydrogen phosphate 0.03-0.1%, manganese sulfate 0.5-1%, Sterilized after fully mixing, inoculation yeast bacterium;180rpm on shaking table is subsequently placed in, 30 DEG C, 48h is cultivated, obtains fermentation Chinese wolfberry fruit stoste; By the fermenation raw liquid filtration sterilization, retain supernatant and the pH value of supernatant is adjusted to neutrality, obtain fermentation Chinese wolfberry fruit liquid.
7. the preparation method of the matrimony vine facial mask according to claim 5 for adding polyglutamic acid, it is characterised in that:Step (1)During middle stirring, the speed of stirring is 80-100r/min.
8. the preparation method of the matrimony vine facial mask according to claim 5 for adding polyglutamic acid, it is characterised in that:Step (2)During middle stirring, it need to stir at ambient temperature, the speed of stirring is 80-100r/min.
9. the preparation method of the matrimony vine facial mask according to claim 5 for adding polyglutamic acid, it is characterised in that:Step (3)The time of middle immersion is 30-40min.
CN201710366922.8A 2017-05-23 2017-05-23 It is a kind of to add matrimony vine facial mask of polyglutamic acid and preparation method thereof Pending CN107308071A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109010199A (en) * 2018-10-19 2018-12-18 天津科技大学 A kind of skin whitening, moisturizing composition and its preparation method and application
WO2024059429A1 (en) * 2022-09-14 2024-03-21 The Gillette Company Llc Lubricating member comprising polyglutamic acid

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JP2005145908A (en) * 2003-11-18 2005-06-09 Nishikawa Rubber Co Ltd Water-absorbing drying sheet for makeup or beauty and method for using the same
CN101416930A (en) * 2008-12-22 2009-04-29 山东省生物药物研究院 Face mask containing pullulan
KR101206263B1 (en) * 2011-06-22 2012-11-29 (주)진코스텍 moisture mask pack improved strength and elasticity, and method for manufacturing the mask pack
CN106265447A (en) * 2016-09-18 2017-01-04 天津北洋百川生物技术有限公司 A kind of preparation method of fermentation Chinese wolfberry fruit liquid level film

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Publication number Priority date Publication date Assignee Title
JP2005145908A (en) * 2003-11-18 2005-06-09 Nishikawa Rubber Co Ltd Water-absorbing drying sheet for makeup or beauty and method for using the same
CN101416930A (en) * 2008-12-22 2009-04-29 山东省生物药物研究院 Face mask containing pullulan
KR101206263B1 (en) * 2011-06-22 2012-11-29 (주)진코스텍 moisture mask pack improved strength and elasticity, and method for manufacturing the mask pack
CN106265447A (en) * 2016-09-18 2017-01-04 天津北洋百川生物技术有限公司 A kind of preparation method of fermentation Chinese wolfberry fruit liquid level film

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109010199A (en) * 2018-10-19 2018-12-18 天津科技大学 A kind of skin whitening, moisturizing composition and its preparation method and application
WO2024059429A1 (en) * 2022-09-14 2024-03-21 The Gillette Company Llc Lubricating member comprising polyglutamic acid

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