CN107228778A - A kind of sampling rectifier unit of TBP tributyl phosphates - Google Patents
A kind of sampling rectifier unit of TBP tributyl phosphates Download PDFInfo
- Publication number
- CN107228778A CN107228778A CN201710626681.6A CN201710626681A CN107228778A CN 107228778 A CN107228778 A CN 107228778A CN 201710626681 A CN201710626681 A CN 201710626681A CN 107228778 A CN107228778 A CN 107228778A
- Authority
- CN
- China
- Prior art keywords
- connecting tube
- rectifier unit
- tributyl phosphates
- spherical top
- tbp tributyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- -1 TBP tributyl phosphates Chemical class 0.000 title claims abstract description 29
- 238000005070 sampling Methods 0.000 title claims abstract description 22
- 239000007788 liquid Substances 0.000 claims abstract description 34
- 239000012530 fluid Substances 0.000 claims abstract description 10
- 238000003780 insertion Methods 0.000 claims abstract description 4
- 230000037431 insertion Effects 0.000 claims abstract description 4
- 238000002347 injection Methods 0.000 claims description 8
- 239000007924 injection Substances 0.000 claims description 8
- 239000011521 glass Substances 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 3
- 230000008016 vaporization Effects 0.000 abstract description 5
- 238000009834 vaporization Methods 0.000 abstract description 5
- 239000000243 solution Substances 0.000 description 6
- STCOOQWBFONSKY-UHFFFAOYSA-N tributyl phosphate Chemical compound CCCCOP(=O)(OCCCC)OCCCC STCOOQWBFONSKY-UHFFFAOYSA-N 0.000 description 4
- 239000001506 calcium phosphate Substances 0.000 description 3
- 229910000389 calcium phosphate Inorganic materials 0.000 description 3
- 235000011010 calcium phosphates Nutrition 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 239000004459 forage Substances 0.000 description 3
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 229920002301 cellulose acetate Polymers 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000013530 defoamer Substances 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229920001596 poly (chlorostyrenes) Polymers 0.000 description 1
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical compound CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/10—Devices for withdrawing samples in the liquid or fluent state
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/09—Esters of phosphoric acids
- C07F9/11—Esters of phosphoric acids with hydroxyalkyl compounds without further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Hydrology & Water Resources (AREA)
- Physics & Mathematics (AREA)
- Analytical Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
A kind of sampling rectifier unit of TBP tributyl phosphates, is related to a kind of rectifier unit, in liquid kettle（7）Top center be provided with the connecting tube that upwardly extends（6）, in connecting tube（6）Upper end be provided with necking down（5）, connecting tube（6）Upper end extend into spherical top（3）It is interior, in spherical top（3）Edge and connecting tube（6）Outer wall between provided with arc connection（2）, in arc connection（2）Bottom be provided with one end insertion cavity A（4）Drain pipe（10）, drain pipe（10）The other end connection fluid reservoir（12）；The present invention at the top of liquid kettle by setting connecting tube, at the top of connecting tube, spherical top is set, the TBP tributyl phosphates of vaporization are collected using spherical top, and the arcuate bottom in arc connection flows into drain pipe, fluid reservoir is finally flowed into, the purpose that the TBP tributyl phosphates after sampling rectifying are collected using spherical top is realized.
Description
【Technical field】
The present invention relates to a kind of rectifier unit, more particularly, to a kind of sampling rectifier unit of TBP tributyl phosphates.
【Background technology】
The agent of TBP calcium phosphate+ forages is used as solvent, also frequently as NC Nitroncellulose, cellulose acetate, chlorinated rubber and polychlorostyrene
The plasticizer of ethene, the extractant of rare metal etc., heat exchange medium.Due to its low surface tension, the physical property of water is insoluble in,
The film of established foam can be effectively set to be in an unsure state and rapid froth breaking as industrial defoamer.Preparing
During TBP calcium phosphate+ forage agent, the step for processing step therein has rectifying, traditional rectifier unit is generally rectifying
Kettle, but be due to that rectifying still is larger, when rectifying is sampled in the TBP calcium phosphate+ forages agent to needing rectifying, rectifying still just shows
Obtain more huge and impracticable.
【The content of the invention】
In order to overcome the shortcomings of in background technology, the present invention a kind of sampling rectifier unit of TBP tributyl phosphates is disclosed, by
The top of liquid kettle sets connecting tube, sets spherical top at the top of connecting tube, the TBP tricresyl phosphates of vaporization are collected using spherical top
Butyl ester, and the arcuate bottom inflow drain pipe in arc connection, finally flow into fluid reservoir, realize to collect using spherical top and adopt
The purpose of TBP tributyl phosphates after sample rectifying.
In order to realize the goal of the invention, the present invention is adopted the following technical scheme that：
A kind of sampling rectifier unit of TBP tributyl phosphates, including spherical top, liquid kettle and fluid reservoir, set in the inside of spherical top
There is cavity A, cavity B is provided with the inside of liquid kettle, the connecting tube upwardly extended is provided with the top center of liquid kettle, in connection
The upper end of pipe is provided with necking down, and the upper end of connecting tube is extend into spherical top, between the edge of spherical top and the outer wall of connecting tube
Provided with arc connection, the bottom connected in arc is provided with one end insertion cavity A drain pipe, the other end connection liquid storage of drain pipe
Tank.
The sampling rectifier unit of described TBP tributyl phosphates, support is provided with the bottom of liquid kettle.
The sampling rectifier unit of described TBP tributyl phosphates, liquid injection port is provided with the top side of liquid kettle.
The sampling rectifier unit of described TBP tributyl phosphates, is provided with lid in liquid injection port.
The material of the sampling rectifier unit of described TBP tributyl phosphates, spherical top and liquid kettle is respectively glass.
By adopting the above-described technical solution, the present invention has the advantages that：
The sampling rectifier unit of TBP tributyl phosphates of the present invention, by setting connecting tube at the top of liquid kettle, in connection
The top of pipe sets spherical top, and the TBP tributyl phosphates of vaporization, and the arc in arc connection are collected using spherical top
Underflow enters drain pipe, finally flows into fluid reservoir, realizes the mesh that the TBP tributyl phosphates after sampling rectifying are collected using spherical top
's；The present invention is simple in construction, reasonable in design, easily operated, practical.
【Brief description of the drawings】
Fig. 1 is structural representation of the invention；
In figure：1st, liquid injection port；2nd, arc is connected；3rd, spherical top；4th, cavity A；5th, necking down；6th, connecting tube；7th, liquid kettle；8th, cavity B；
9th, TBP tributyl phosphates solution；10th, drain pipe；11st, support；12nd, fluid reservoir.
【Embodiment】
The present invention can be explained in more detail by the following examples, it is open the invention is not limited in the following examples
The purpose of the present invention is intended to protect all changes and improvements in the scope of the invention；
The sampling rectifier unit of TBP tributyl phosphates with reference to described in accompanying drawing 1, including spherical top 3, liquid kettle 7 and fluid reservoir 12,
The inside of spherical top 3 is provided with cavity A4, and cavity B8 is provided with the inside of liquid kettle 7, is provided with upward in the top center of liquid kettle 7
The connecting tube 6 of extension, is provided with necking down 5, the upper end of connecting tube 6 is extend into spherical top 3, in spherical top 3 in the upper end of connecting tube 6
Edge and connecting tube 6 outer wall between provided with arc connection 2, connect 2 bottom provided with one end insertion cavity A4 in arc
Drain pipe 10, the other end connection fluid reservoir 12 of drain pipe 10, is provided with support 11, at the top one of liquid kettle 7 in the bottom of liquid kettle 7
Side is provided with liquid injection port 1, provided with lid in liquid injection port 1, and the material of spherical top 3 and liquid kettle 7 is respectively glass.
Implement the sampling rectifier unit of TBP tributyl phosphates of the present invention, it would be desirable to carry out the appropriate of sampling rectifying
TBP tributyl phosphates solution 9 is injected in liquid kettle 7 by liquid injection port 1, and alcolhol burner is placed in support 11 and is lighted, treats that temperature reaches
After arriving, the TBP tributyl phosphates solution 9 of vaporization reaches the inner edge surface of spherical top 3, and the TBP tributyl phosphates solution 9 of vaporization is half
The inner edge surface of top dome 3 is flowed into the arc connection 2 of the bottom of spherical top 3, and flowed into along drain pipe 10 in fluid reservoir 12 to the cold, real
The sampling rectifying of TBP tributyl phosphates solution 9 is showed.
Part not in the detailed description of the invention is prior art.
Claims (5)
1. a kind of sampling rectifier unit of TBP tributyl phosphates, it is characterized in that：Including spherical top（3）, liquid kettle（7）And fluid reservoir
（12）, in spherical top（3）Inside be provided with cavity A（4）, in liquid kettle（7）Inside be provided with cavity B（8）, in liquid kettle（7）Top
Portion centre is provided with the connecting tube upwardly extended（6）, in connecting tube（6）Upper end be provided with necking down（5）, connecting tube（6）It is upper
End extend into spherical top（3）It is interior, in spherical top（3）Edge and connecting tube（6）Outer wall between provided with arc connection（2）,
Arc is connected（2）Bottom be provided with one end insertion cavity A（4）Drain pipe（10）, drain pipe（10）The other end connection liquid storage
Tank（12）.
2. the sampling rectifier unit of TBP tributyl phosphates according to claim 1, it is characterized in that：In liquid kettle（7）Bottom
Provided with support（11）.
3. the sampling rectifier unit of TBP tributyl phosphates according to claim 1, it is characterized in that：In liquid kettle（7）Top
Side is provided with liquid injection port（1）.
4. the sampling rectifier unit of TBP tributyl phosphates according to claim 3, it is characterized in that：In liquid injection port（1）On set
There is lid.
5. the sampling rectifier unit of TBP tributyl phosphates according to claim 1, it is characterized in that：Spherical top（3）With liquid kettle
（7）Material be respectively glass.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710626681.6A CN107228778A (en) | 2017-07-28 | 2017-07-28 | A kind of sampling rectifier unit of TBP tributyl phosphates |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710626681.6A CN107228778A (en) | 2017-07-28 | 2017-07-28 | A kind of sampling rectifier unit of TBP tributyl phosphates |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107228778A true CN107228778A (en) | 2017-10-03 |
Family
ID=59956312
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710626681.6A Pending CN107228778A (en) | 2017-07-28 | 2017-07-28 | A kind of sampling rectifier unit of TBP tributyl phosphates |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107228778A (en) |
Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2702967A1 (en) * | 1993-03-23 | 1994-09-30 | Desmet Frederic | Process for molecular separation of one or more bodies mixed in a liquid mixture with a solvent, characterised by the use of microwaves which produce the separation by molecular agitation |
| US20060289288A1 (en) * | 2002-11-08 | 2006-12-28 | Finn John B | Distillation unit and a method of distillation |
| DE102009035858A1 (en) * | 2009-07-31 | 2011-02-03 | Strauß, Maximilian Thomas | Mobile device, which is mounted as domed housing on heatable container, for the distillation of raw water, comprises raw water supply pipeline guided to outer side of housing from bottom to top, and upwardly opened collecting groove |
| CN202700115U (en) * | 2012-08-03 | 2013-01-30 | 梅晓锋 | Novel distilling device |
| CN103740468A (en) * | 2014-02-07 | 2014-04-23 | 郭永来 | Steam distillation aromatic essential oil equipment |
| CN203736884U (en) * | 2014-02-28 | 2014-07-30 | 深圳市绿绿达环保有限公司 | Segmented heating distillation still |
| CN204147570U (en) * | 2014-09-11 | 2015-02-11 | 张若琪 | A kind of distillation equipment |
| CN104606909A (en) * | 2015-01-22 | 2015-05-13 | 李而宏 | Distillatory kettle for plant sesame oil |
| CN204798882U (en) * | 2015-07-13 | 2015-11-25 | 商巧玲 | Distillation plant with filtering capability |
| CN204932903U (en) * | 2015-08-18 | 2016-01-06 | 江苏劲嘉新型包装材料有限公司 | The solvent circulation of novel process ink and waste gas |
| CN205699523U (en) * | 2016-04-27 | 2016-11-23 | 天津市致远化学试剂有限公司 | One may filter that efficient distillation equipment |
| CN206081692U (en) * | 2016-08-27 | 2017-04-12 | 嘉兴富成化工科技有限公司 | Environment -friendly distillation plant |
| CN207123409U (en) * | 2017-07-28 | 2018-03-20 | 洛阳市三诺化工有限公司 | A kind of sampling rectifier unit of TBP tributyl phosphates |
-
2017
- 2017-07-28 CN CN201710626681.6A patent/CN107228778A/en active Pending
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2702967A1 (en) * | 1993-03-23 | 1994-09-30 | Desmet Frederic | Process for molecular separation of one or more bodies mixed in a liquid mixture with a solvent, characterised by the use of microwaves which produce the separation by molecular agitation |
| US20060289288A1 (en) * | 2002-11-08 | 2006-12-28 | Finn John B | Distillation unit and a method of distillation |
| DE102009035858A1 (en) * | 2009-07-31 | 2011-02-03 | Strauß, Maximilian Thomas | Mobile device, which is mounted as domed housing on heatable container, for the distillation of raw water, comprises raw water supply pipeline guided to outer side of housing from bottom to top, and upwardly opened collecting groove |
| CN202700115U (en) * | 2012-08-03 | 2013-01-30 | 梅晓锋 | Novel distilling device |
| CN103740468A (en) * | 2014-02-07 | 2014-04-23 | 郭永来 | Steam distillation aromatic essential oil equipment |
| CN203736884U (en) * | 2014-02-28 | 2014-07-30 | 深圳市绿绿达环保有限公司 | Segmented heating distillation still |
| CN204147570U (en) * | 2014-09-11 | 2015-02-11 | 张若琪 | A kind of distillation equipment |
| CN104606909A (en) * | 2015-01-22 | 2015-05-13 | 李而宏 | Distillatory kettle for plant sesame oil |
| CN204798882U (en) * | 2015-07-13 | 2015-11-25 | 商巧玲 | Distillation plant with filtering capability |
| CN204932903U (en) * | 2015-08-18 | 2016-01-06 | 江苏劲嘉新型包装材料有限公司 | The solvent circulation of novel process ink and waste gas |
| CN205699523U (en) * | 2016-04-27 | 2016-11-23 | 天津市致远化学试剂有限公司 | One may filter that efficient distillation equipment |
| CN206081692U (en) * | 2016-08-27 | 2017-04-12 | 嘉兴富成化工科技有限公司 | Environment -friendly distillation plant |
| CN207123409U (en) * | 2017-07-28 | 2018-03-20 | 洛阳市三诺化工有限公司 | A kind of sampling rectifier unit of TBP tributyl phosphates |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171003 |