CN107200661A - The technique that a kind of organic sludge produces organic fertilizer - Google Patents

The technique that a kind of organic sludge produces organic fertilizer Download PDF

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Publication number
CN107200661A
CN107200661A CN201710271878.2A CN201710271878A CN107200661A CN 107200661 A CN107200661 A CN 107200661A CN 201710271878 A CN201710271878 A CN 201710271878A CN 107200661 A CN107200661 A CN 107200661A
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CN
China
Prior art keywords
organic
sludge
organic fertilizer
glutamic acid
mother liquor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710271878.2A
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Chinese (zh)
Inventor
颉红涛
曹飞
李虹谕
李喜春
李虎俊
吴学峰
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Inner Mongolia Wofeng Agricultural Development Co Ltd
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Inner Mongolia Wofeng Agricultural Development Co Ltd
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Priority to CN201710271878.2A priority Critical patent/CN107200661A/en
Publication of CN107200661A publication Critical patent/CN107200661A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05CNITROGENOUS FERTILISERS
    • C05C11/00Other nitrogenous fertilisers
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00Multistage treatment of water, waste water or sewage
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity
    • C05G3/80Soil conditioners
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/52Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00Treatment of water, waste water, or sewage
    • C02F1/66Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00Biological treatment of water, waste water, or sewage
    • C02F3/30Aerobic and anaerobic processes

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  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Soil Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Hydrology & Water Resources (AREA)
  • Engineering & Computer Science (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Fertilizers (AREA)

Abstract

The invention discloses the technique that a kind of organic sludge produces organic fertilizer, it includes, and prepared by process (1) powder sludge, prepared by process (2) organic fertilizer;The waste water produced in the present invention using during starch, glucose and glutamate production is used as raw material, organic sludge and sewage are obtained through microbiological treatment, organic sludge produces the organic fertilizer for obtaining high economic value added, solve the process problem of sludge, turn waste into wealth, steady quality, improves the use value of sludge.In the present invention when roller is granulated, added using glutamic acid concentrated mother liquor as liquid phase in powder sludge, provide not only nutrient, but also neutralized pH value, while also mitigating the pressure of soil conditioner production.

Description

The technique that a kind of organic sludge produces organic fertilizer
Technical field:
The present invention relates to the technique that a kind of organic sludge produces organic fertilizer, belong to the processing of biofermentation industry fermentation wastes Field.
Background technology:
Some waste water are inevitably produced in the production process of starch, glucose and monosodium glutamate, are rich in the waste water The organic matters such as polysaccharide, amino acid, protein;Waste water after microbiological treatment, obtains sewage and rich in organic matter in environmentally friendly process Sludge, sewage recycles or qualified discharge after recycled water advanced treatment;The sludge of generation is delivered in glutamic acid concentrated mother liquor, Directly mixed with glutamic acid concentrated mother liquor, carry out slurry-spraying pelletizing.First, the sludge rich in organic matter concentrates female with glutamic acid The processing mode of liquid mixing slurry-spraying pelletizing causes very big pressure to simple glutamic acid concentrated mother liquor slurry-spraying pelletizing, adds Workload;Secondly as sludge and the mixed solution concentration of glutamic acid concentrated mother liquor are high, sediment is more, easily blocks whitewashing Pipette tips, to production bring certain difficulty, add production cost;Furthermore, the sludge rich in organic matter is concentrated with glutamic acid The product that mother liquor mixing slurry-spraying pelletizing is obtained, its content of organic matter and total nutrient can not meet organic fertilizer rower (NY525- simultaneously 2012), economic value added is low, can only be used as soil conditioner.
The content of the invention:
It is an object of the invention to provide a kind of by the use of organic wastewater as raw material, high economic value added organic fertilizer is produced Technique.
The purpose of the present invention is implemented by following technical scheme, and a kind of organic sludge produces the technique of organic fertilizer, its process (1) Prepared by powder sludge, prepared by process (2) organic fertilizer;Wherein
It is prepared by process (1) the powder sludge:The organic sludge is dried and pulverization process successively, obtains moisture content ≤ 5%, the mesh powder sludge of fineness >=40;
It is prepared by process (2) organic fertilizer:By the powder sludge and Baume degrees is 26-28, temperature is 70-95 DEG C paddy Propylhomoserin concentrated mother liquor is by weight (4-6):1 mixing back roll granulation, control glutamic acid concentrated mother liquor temperature, be easy to fertilizer into Ball;Powder sludge is sufficiently mixed with glutamic acid concentrated mother liquor, by rolling, mutual extruding granulating between granule;Then pass through successively Cross after drying and sieving, obtain moisture content≤30%, the organic fertilizer of granularity (1-4.75mm) >=90%, the organic fertilizer is packaged into Storehouse;The unqualified material of granularity returns in prepared by the process (1) powder sludge and re-starts pulverization process.
Further, the glutamic acid concentrated mother liquor is concentrated by glutamic acid mother liquor and is made, and glutamic acid mother liquor is corn fermentation Afterwards, remaining aminoacids solution after glutamic acid is extracted, mainly containing N, P, K, organic matter and amino acid, making organic fertilizer can be used as Liquid phase feed;After glutamic acid mother liquor is concentrated, the content of its nutrient and organic matter is improved, and viscosity is improved, it is easy to Organic fertilizer granulating.
In the glutamic acid mother liquor evaporating concentration process, when its Baume degrees reaches 26-28, glutamic acid concentrated mother liquor is obtained.
Further, the organic sludge is made as follows:Alkaline conditioner is added into organic wastewater, institute is adjusted State organic wastewater pH to 6-8;The processing of aerobic and anaerobe is then sequentially passed through, activated sludge process AO works can be specifically used Precipitated after the organic matters such as polysaccharide, amino acid, protein in skill, consumption waste water;Treat that the organic wastewater settling ratio reaches 60- When 80%, separation of solid and liquid obtains N, P and K in sediment and supernatant, organic wastewater through flocculation sediment, into sediment, makees For the nutrient of organic fertilizer, the sediment obtains sewage and organic sludge after compression, and the supernatant and the sewage are carried out Sewerage disposing, obtains recirculated water, the recirculated water is produced available for enterprise, therefore non-wastewater discharge.It is heavy that separation of solid and liquid is obtained Starch is the organic sludge.
Further, the organic wastewater be starch, glucose and glutamate production during produce waste water any one, Or two of which or three kinds of mixed liquor.
Further, the alkaline conditioner is KOH or lime.
Advantages of the present invention:
1st, the waste water produced in the present invention using during starch, glucose and glutamate production has been concentrated to give as raw material Machine sludge and sewage, organic sludge, which is produced, obtains the organic fertilizer of high economic value added, solves the process problem of sludge, change give up into Treasured, steady quality improves the use value of sludge.
2nd, in the present invention when roller is granulated, added in powder sludge, not only carried using glutamic acid concentrated mother liquor as liquid phase Nutrient has been supplied, but also has neutralized pH value, while also mitigating the pressure of soil conditioner production.
Brief description of the drawings:
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing There is the accompanying drawing used required in technology description to be briefly described, it should be apparent that, drawings in the following description are only this Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with Other accompanying drawings are obtained according to these accompanying drawings.
Fig. 1 produces the process chart of organic fertilizer for a kind of organic sludge of the invention.
Embodiment:
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made Embodiment, belongs to the scope of protection of the invention.
Embodiment 1:
A kind of organic sludge produces the technique of organic fertilizer, and it includes the preparation of process (1) organic sludge, the dirt of process (2) powder It is prepared by clay standby, process (3) organic fertilizer;Wherein
It is prepared by process (1) organic sludge:Added in the organic wastewater produced to the production process of starch, glucose and monosodium glutamate KOH is used as alkaline conditioner, regulation organic wastewater pH to 6-8;The processing of aerobic and anaerobe is then sequentially passed through, specifically may be used Using activated sludge process AO techniques, precipitated after the organic matter such as polysaccharide, amino acid, protein in consumption waste water;Treat organic wastewater When settling ratio reaches 60-80%, separation of solid and liquid obtains N, P and K in sediment and supernatant, organic wastewater through flocculation sediment, Into sediment, as the nutrient of organic fertilizer, sediment obtains sewage and organic sludge after compression, and supernatant and sewage are carried out Sewerage disposing, obtains recirculated water, recirculated water is produced available for enterprise, therefore non-wastewater discharge;
It is prepared by process (2) powder sludge:Organic sludge is dried and pulverization process successively, obtains moisture content≤5%, thin Spend >=40 mesh powder sludge;
It is prepared by process (3) organic fertilizer:
Glutamic acid mother liquor is concentrated by evaporation, and when its Baume degrees reaches 26-28, obtains glutamic acid concentrated mother liquor;
It is 4 by weight by powder sludge and Baume degrees is 26-28, temperature is 70 DEG C glutamic acid concentrated mother liquor:1 is abundant Mixing;Then add and roller granulation is carried out in roller pelletizer, by rolling, mutual extruding granulating between granule;Then successively After drying and screening, moisture content≤30% is obtained, the organic fertilizer of granularity (1-4.75mm) >=90%, organic fertilizer is packaged into Storehouse;The unqualified material of granularity returns in prepared by process (2) powder sludge and re-starts pulverization process.
After glutamic acid mother liquor is corn fermentation, remaining aminoacids solution after glutamic acid is extracted, mainly containing N, P, K, organic Matter and amino acid, can be used as the liquid phase feed for making organic fertilizer;After glutamic acid mother liquor is concentrated, the content of its nutrient and organic matter It is improved, and viscosity is improved, it is easy to organic fertilizer granulating.
Embodiment 2:
A kind of organic sludge produces the technique of organic fertilizer, and it includes the preparation of process (1) organic sludge, the dirt of process (2) powder It is prepared by clay standby, process (3) organic fertilizer;Wherein
It is prepared by process (1) organic sludge:Added in the organic wastewater produced to the production process of starch, glucose and monosodium glutamate KOH is used as alkaline conditioner, regulation organic wastewater pH to 6-8;The processing of aerobic and anaerobe is then sequentially passed through, specifically may be used Using activated sludge process AO techniques, precipitated after the organic matter such as polysaccharide, amino acid, protein in consumption waste water;Treat organic wastewater When settling ratio reaches 60-80%, separation of solid and liquid obtains N, P and K in sediment and supernatant, organic wastewater through flocculation sediment, Into sediment, as the nutrient of organic fertilizer, sediment obtains sewage and organic sludge after compression, and supernatant and sewage are carried out Sewerage disposing, obtains recirculated water, recirculated water is produced available for enterprise, therefore non-wastewater discharge;
It is prepared by process (2) powder sludge:Organic sludge is dried and pulverization process successively, obtains moisture content≤5%, thin Spend >=40 mesh powder sludge;
It is prepared by process (3) organic fertilizer:
Glutamic acid mother liquor is concentrated by evaporation, and when its Baume degrees reaches 26-28, obtains glutamic acid concentrated mother liquor;
It is 5 by weight by powder sludge and Baume degrees is 26-28, temperature is 80 DEG C glutamic acid concentrated mother liquor:1 is abundant Mixing;Then add and roller granulation is carried out in roller pelletizer, by rolling, mutual extruding granulating between granule;Then successively After drying and screening, moisture content≤30% is obtained, the organic fertilizer of granularity (1-4.75mm) >=90%, organic fertilizer is packaged into Storehouse;The unqualified material of granularity returns in prepared by process (2) powder sludge and re-starts pulverization process.
After glutamic acid mother liquor is corn fermentation, remaining aminoacids solution after glutamic acid is extracted, mainly containing N, P, K, organic Matter and amino acid, can be used as the liquid phase feed for making organic fertilizer;After glutamic acid mother liquor is concentrated, the content of its nutrient and organic matter It is improved, and viscosity is improved, it is easy to organic fertilizer granulating.
Embodiment 3:
A kind of organic sludge produces the technique of organic fertilizer, and it includes the preparation of process (1) organic sludge, the dirt of process (2) powder It is prepared by clay standby, process (3) organic fertilizer;Wherein
It is prepared by process (1) organic sludge:Added in the organic wastewater produced to the production process of starch, glucose and monosodium glutamate Lime is used as alkaline conditioner, regulation organic wastewater pH to 6-8;The processing of aerobic and anaerobe is then sequentially passed through, specifically Precipitated after the organic matters such as polysaccharide, amino acid, protein in activated sludge process AO techniques, consumption waste water can be used;Treat organic waste When water settling ratio reaches 60-80%, N, P and K that separation of solid and liquid is obtained in sediment and supernatant, organic wastewater are heavy through flocculation Form sediment, into sediment, as the nutrient of organic fertilizer, sediment obtains sewage and organic sludge after compression;Supernatant and sewage Sewerage disposing is carried out, recirculated water is obtained, recirculated water is produced available for enterprise, therefore non-wastewater discharge;
It is prepared by process (2) powder sludge:Organic sludge is dried and pulverization process successively, obtains moisture content≤5%, thin Spend >=40 mesh powder sludge;
It is prepared by process (3) organic fertilizer:
Glutamic acid mother liquor is concentrated by evaporation, and when its Baume degrees reaches 26-28, obtains glutamic acid concentrated mother liquor;
It is 6 by weight by powder sludge and Baume degrees is 26-28, temperature is 95 DEG C glutamic acid concentrated mother liquor:1 is abundant Mixing;Then add and roller granulation is carried out in roller pelletizer, by rolling, mutual extruding granulating between granule;Then successively After drying and screening, moisture content≤30% is obtained, the organic fertilizer of granularity (1-4.75mm) >=90%, organic fertilizer is packaged into Storehouse;The unqualified material of granularity returns in prepared by process (2) powder sludge and re-starts pulverization process.
After glutamic acid mother liquor is corn fermentation, remaining aminoacids solution after glutamic acid is extracted, mainly containing N, P, K, organic Matter and amino acid, can be used as the liquid phase feed for making organic fertilizer;After glutamic acid mother liquor is concentrated, the content of its nutrient and organic matter It is improved, and viscosity is improved, it is easy to organic fertilizer granulating.
Table 1 is organic matter, total nutrient, moisture, the pH value of each stage material in embodiment 1/2/3, and organic fertilizer Each index content range as defined in rower NY525-2012, as known from Table 1, the organic fertilizer produced using the inventive method, its is each Item index meets rower requirement.
Organic fertilizer index and parameter as defined in 1 embodiment of table 1/2/3 each stage material and NY525-2012
These are only presently preferred embodiments of the present invention, be not intended to limit the invention, it is all the present invention spirit and Within principle, any modification, equivalent substitution and improvements made etc. should be included in the scope of the protection.

Claims (5)

1. the technique that a kind of organic sludge produces organic fertilizer, it is characterised in that it includes the preparation of process (1) powder sludge, process (2) prepared by organic fertilizer;Wherein
It is prepared by process (1) the powder sludge:Organic sludge is dried and pulverization process successively, obtain moisture content≤5%, The mesh powder sludge of fineness >=40;
It is prepared by process (2) organic fertilizer:By the powder sludge and Baume degrees is 26-28, temperature is 70-95 DEG C glutamic acid Concentrated mother liquor is by weight (4-6):1 mixing back roll granulation, then sequentially pass through dry and screening after, obtain moisture content≤ 30%, the organic fertilizer of granularity (1-4.75mm) >=90%;The unqualified material of granularity returns to the preparation of the process (1) powder sludge In re-start pulverization process.
2. a kind of technique that organic sludge produces organic fertilizer according to claim 1, it is characterised in that the glutamic acid concentration Mother liquor is concentrated by evaporation by glutamic acid mother liquor and is made;In the glutamic acid mother liquor evaporating concentration process, its Baume degrees reaches 26-28 When, obtain the glutamic acid concentrated mother liquor.
3. the technique that a kind of organic sludge produces organic fertilizer according to claim 1, it is characterised in that the organic sludge is pressed Following method is made:Alkaline conditioner is added into the organic wastewater, organic wastewater pH to the 6-8 is adjusted;Then successively By the processing of aerobic and anaerobe, when the organic wastewater settling ratio reaches 60-80%, separation of solid and liquid obtains sediment And supernatant, the sediment obtains the organic sludge after compression.
4. the technique that a kind of organic sludge produces organic fertilizer according to claim 3, it is characterised in that the organic wastewater is Any one of waste water, or two of which or three kinds of mixed liquor are produced during starch, glucose and glutamate production.
5. a kind of technique that organic sludge produces organic fertilizer according to claim 3, it is characterised in that the alkaline conditioner For KOH or lime.
CN201710271878.2A 2017-04-24 2017-04-24 The technique that a kind of organic sludge produces organic fertilizer Pending CN107200661A (en)

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CN107200661A true CN107200661A (en) 2017-09-26

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Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101195550A (en) * 2007-12-11 2008-06-11 马长庆 Technique for producing fertilizer with gourmet powder waste liquor
CN102093110A (en) * 2010-12-23 2011-06-15 欧美投资集团(内蒙古)生物科技有限公司 Method for producing biological fermentation compound fertilizer by fermenting organic waste water with glutamic acid
CN103044117A (en) * 2012-12-23 2013-04-17 菱花集团有限公司 Organic fertilizer based on solid waste comprehensive utilization of monosodium glutamate industry

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101195550A (en) * 2007-12-11 2008-06-11 马长庆 Technique for producing fertilizer with gourmet powder waste liquor
CN102093110A (en) * 2010-12-23 2011-06-15 欧美投资集团(内蒙古)生物科技有限公司 Method for producing biological fermentation compound fertilizer by fermenting organic waste water with glutamic acid
CN103044117A (en) * 2012-12-23 2013-04-17 菱花集团有限公司 Organic fertilizer based on solid waste comprehensive utilization of monosodium glutamate industry

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Application publication date: 20170926

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