CN107163271A - The preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant - Google Patents

The preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant Download PDF

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Publication number
CN107163271A
CN107163271A CN201710366065.1A CN201710366065A CN107163271A CN 107163271 A CN107163271 A CN 107163271A CN 201710366065 A CN201710366065 A CN 201710366065A CN 107163271 A CN107163271 A CN 107163271A
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Prior art keywords
prevention film
electrostatic prevention
resistant
wear
parts
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CN201710366065.1A
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Chinese (zh)
Inventor
何松龙
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Chengdu Huijia Gluing Products Co Ltd
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Chengdu Huijia Gluing Products Co Ltd
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Priority to CN201710366065.1A priority Critical patent/CN107163271A/en
Publication of CN107163271A publication Critical patent/CN107163271A/en
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
    • C08J7/04—Coating
    • C08J7/0427—Coating with only one layer of a composition containing a polymer binder
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L79/00—Compositions of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen or carbon only, not provided for in groups C08L61/00 - C08L77/00
    • C08L79/02—Polyamines
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D163/00—Coating compositions based on epoxy resins; Coating compositions based on derivatives of epoxy resins
    • C09D163/04—Epoxynovolacs
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/24—Electrically-conducting paints
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2379/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen with or without oxygen, or carbon only, not provided for in groups C08J2361/00 - C08J2377/00
    • C08J2379/02—Polyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2463/00—Characterised by the use of epoxy resins; Derivatives of epoxy resins
    • C08J2463/04—Epoxynovolacs
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/38—Boron-containing compounds
    • C08K2003/387—Borates
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/02—Elements
    • C08K3/04—Carbon
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/04—Antistatic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00—Applications
    • C08L2203/16—Applications used for films
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/14—Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16—Fibres; Fibrils

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Manufacturing & Machinery (AREA)
  • Manufacture Of Macromolecular Shaped Articles (AREA)
  • Laminated Bodies (AREA)

Abstract

The invention discloses the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, denatured conductive polyaniline fiber, high-temperature fusion polyvinyl chloride, makrolon, silane coupler, solvent naphtha are mixed to get compound in proportion；Add mixture into inflation film manufacturing machine and extruded at 230 DEG C 250 DEG C, electrostatic prevention film is obtained after cooling；Tourmaline powder, biomass carbon dust are uniformly mixed in proportion, novolac epoxy resin is added, is applied to after stirring on above-mentioned obtained electrostatic prevention film；It is compressing at 180 210 DEG C under 2.1 2.5MPa, obtain the electrostatic prevention film.

Description

The preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant
Technical field
The present invention relates to a kind of electrostatic prevention film, and in particular to the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant.
Background technology
Electrostatic is a kind of common but complicated physical phenomenon, it without a trace, it is ubiquitous.With science and technology it is fast Hail exhibition, the raising of the high efficiency and automaticity of production, electronic equipment it is widely used, make electrostatic and electromagnetic environment more next More deteriorate, this just gives and product such as integrated circuit, electromagnetic control system, chemical agent etc. of electrostatic and electromagnetic radiation sensitivity are caused Threaten.Because external electromagnetic radiation causes integrated circuit, electromagnetic control system failure, misoperation, chemical products burning, blast Accident happen occasionally.Chemical products, electronic device are during production, storage, transport and use due to rubbing, hitting, connecing Touch, separation produces accumulation of static electricity and discharges, the consequence caused is destructive even catastrophic.
, it is necessary to be packed using antistatic material such as electrostatic prevention film in the production and transport of electronic component, prevent by electrostatic Damage.The simple substance anti-static polythene film of the marketization nineties in last century, because it is polar material, and double sheet resistances Value is low, it is impossible to carries out sided corona treatment, thus can not be combined into layered packaging materials with other base materials.The film of simple substance is because of its machinery Physical property is low, it is impossible to provides reliable protection to inner packing product, thus limits its extensive use.
Polyester film and metal-foil composite film are also a kind of electrostatic prevention film of complete industrialized production and application, this compound Film can also be made in polyethylene film top layer coating electrostatic layer.As using top layer aluminium, nickel, titanium, copper, chromium, the zinc in polyester film Deng metallics evaporation or spraying method, the metallic diaphragm on the top layer evaporation of polyester film or spraying is prevented so as to obtain having The polyester film material of electrostatic function, and antistatic packaging bag is made with the material；Or passed through using surfactant, carbon black Coating method is coated into anti-static coating on polyethylene film surface, so as to obtain the polyethylene membrane material with electrostatic-proof function Material, is then made into antistatic packaging bag.Plastic material will obtain certain electric conductivity, need to be by conductive material such as Conductive black is mixed with certain proportion with thermoplastic resin, and adds coupling agent, plasticizer, slipping agent, stabilizer, antioxidant etc. Multiple additives.
The content of the invention
The technical problems to be solved by the invention are that existing electrostatic prevention film does not have a kind of Wear-resistant, high-temperature resistant and can adsorbed The electrostatic prevention film of harmful substance in air, it is therefore intended that the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, solution are provided Certainly existing electrostatic prevention film poor performance, it is impossible to the problem of heat resistant and wear resistant adsorbs harmful substance.
The present invention is achieved through the following technical solutions：
The preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, comprises the following steps：
(1) denatured conductive polyaniline fiber, high-temperature fusion polyvinyl chloride, makrolon, silane coupler, solvent naphtha are pressed Ratio is mixed to get compound；
(2) add mixture into inflation film manufacturing machine and extruded at 230 DEG C -250 DEG C, electrostatic prevention film is obtained after cooling；
(3) tourmaline powder, biomass carbon dust are uniformly mixed in proportion, novolac epoxy resin is added, after stirring It is applied on above-mentioned obtained electrostatic prevention film；
(4) it is compressing at 180-210 DEG C under 2.1-2.5MPa, obtain the electrostatic prevention film.
Compound is extruded at 245 DEG C in the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, the step (2).
In the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, the step (4), under 2.4MPa, obtain described Electrostatic prevention film.
It is compressing at 205 DEG C in the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, the step (4), obtain To the electrostatic prevention film.
The preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, the parts by weight of raw material are：Denatured conductive polyaniline is fine 42 parts of dimension, 16 parts of high-temperature fusion polyvinyl chloride, 12 parts of makrolon, 7 parts of silane coupler, 7 parts of solvent naphtha, tourmaline powder 17 Part, 10 parts of biomass carbon dust, 17 parts of novolac epoxy resin.
The present invention compared with prior art, has the following advantages and advantages：
1st, the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant of the present invention, the electrostatic prevention film obtained by the present invention has The characteristics of Wear-resistant, high-temperature resistant, and better than the performance of existing electrostatic prevention film；
2nd, the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant of the present invention, the electrostatic prevention film obtained by the present invention can be inhaled The toluene in air is received, it is more environment-friendly and safer；
3rd, the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant of the present invention, preparation method of the present invention is simple and component Complement each other, and obtained electrostatic prevention film best results under the scope of this component.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment, to present invention work Further to describe in detail, exemplary embodiment and its explanation of the invention is only used for explaining the present invention, is not intended as to this The restriction of invention.
Embodiment
(1) denatured conductive polyaniline fiber, high-temperature fusion polyvinyl chloride, makrolon, silane coupler, solvent naphtha are pressed Ratio is mixed to get compound；
(2) add mixture into inflation film manufacturing machine and extruded at 230 DEG C -250 DEG C, electrostatic prevention film is obtained after cooling；
(3) tourmaline powder, biomass carbon dust are uniformly mixed in proportion, novolac epoxy resin is added, after stirring It is applied on above-mentioned obtained electrostatic prevention film；
(4) it is compressing at 180-210 DEG C under 2.1-2.5MPa, obtain the electrostatic prevention film.
Compound is extruded at 245 DEG C in the step (2)；In the step (4), under 2.4MPa, obtain described anti- Electrostatic film；It is compressing at 205 DEG C in the step (4), obtain the electrostatic prevention film.
The performance of electrostatic prevention film according to obtained by embodiment 1-6 such as table 1：
It can be obtained according to table 1, the antistatic performance of the electrostatic prevention film obtained by embodiment 1, the energy of the formaldehyde removed in air Power and wearability, heat resistance are all optimal, and embodiment 2 and embodiment 3 are identical with the component in embodiment 1, still, are implemented The scope of example 2 and the component in embodiment 3 is outside the scope of the present invention, therefore the performance of its obtained electrostatic prevention film is all worse than reality Apply example 1；The value of embodiment 4-6 component is same as Example 1, but on the basis of embodiment 1, reduces some groups Point, its effect is also poor.
In summary, component of the invention complements each other, under the formula range of the component of the present invention, and in the present invention Preparation method under, obtained electrostatic prevention film has preferable wearability, heat-resisting quantity and preferably can removed in air Formaldehyde.And the performance for removing formaldehyde of the electrostatic prevention film obtained by the present invention is better than existing electrostatic prevention film, and using effect is more It is good.
Above-described embodiment, has been carried out further to the purpose of the present invention, technical scheme and beneficial effect Describe in detail, should be understood that the embodiment that the foregoing is only the present invention, be not intended to limit the present invention Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc. all should be included Within protection scope of the present invention.

Claims (5)

1. the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant, it is characterised in that comprise the following steps：
(1) by denatured conductive polyaniline fiber, high-temperature fusion polyvinyl chloride, makrolon, silane coupler, solvent naphtha in proportion It is mixed to get compound；
(2) add mixture into inflation film manufacturing machine and extruded at 230 DEG C -250 DEG C, electrostatic prevention film is obtained after cooling；
(3) tourmaline powder, biomass carbon dust are uniformly mixed in proportion, adds novolac epoxy resin, smeared after stirring On above-mentioned obtained electrostatic prevention film；
(4) it is compressing at 180-210 DEG C under 2.1-2.5MPa, obtain the electrostatic prevention film.
2. the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant according to claim 1, it is characterised in that the step Suddenly compound is extruded at 245 DEG C in (2).
3. the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant according to claim 1, it is characterised in that the step Suddenly in (4), under 2.4MPa, the electrostatic prevention film is obtained.
4. the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant according to claim 1, it is characterised in that the step Suddenly it is compressing at 205 DEG C in (4), obtain the electrostatic prevention film.
5. the preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant according to claim 1, it is characterised in that raw material Parts by weight are：It is 42 parts of denatured conductive polyaniline fiber, 16 parts of high-temperature fusion polyvinyl chloride, 12 parts of makrolon, silane coupled 7 parts of agent, 7 parts of solvent naphtha, 17 parts of tourmaline powder, 10 parts of biomass carbon dust, 17 parts of novolac epoxy resin.
CN201710366065.1A 2017-05-23 2017-05-23 The preparation method of the environmentally friendly electrostatic prevention film of Wear-resistant, high-temperature resistant Withdrawn CN107163271A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108164732A (en) * 2018-01-24 2018-06-15 合肥同佑电子科技有限公司 A kind of preparation method of antistatic film material for electronic component
CN109021261A (en) * 2018-04-28 2018-12-18 苏州迪诺美特包装科技有限公司 A kind of preparation method of antistatic film

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104788697A (en) * 2015-03-31 2015-07-22 苏州市鼎立包装有限公司 Oxygen anion anti-static membrane material and preparation method thereof
CN106519413A (en) * 2016-11-15 2017-03-22 山东中塑泰富科技有限公司 Anti-static composite film
CN106519414A (en) * 2016-11-15 2017-03-22 山东中塑泰富科技有限公司 Environmentally friendly antistatic film material and preparation method thereof

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104788697A (en) * 2015-03-31 2015-07-22 苏州市鼎立包装有限公司 Oxygen anion anti-static membrane material and preparation method thereof
CN106519413A (en) * 2016-11-15 2017-03-22 山东中塑泰富科技有限公司 Anti-static composite film
CN106519414A (en) * 2016-11-15 2017-03-22 山东中塑泰富科技有限公司 Environmentally friendly antistatic film material and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108164732A (en) * 2018-01-24 2018-06-15 合肥同佑电子科技有限公司 A kind of preparation method of antistatic film material for electronic component
CN109021261A (en) * 2018-04-28 2018-12-18 苏州迪诺美特包装科技有限公司 A kind of preparation method of antistatic film

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