CN107162576A - A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant - Google Patents
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant Download PDFInfo
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- CN107162576A CN107162576A CN201710349008.2A CN201710349008A CN107162576A CN 107162576 A CN107162576 A CN 107162576A CN 201710349008 A CN201710349008 A CN 201710349008A CN 107162576 A CN107162576 A CN 107162576A
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Abstract
The invention provides a kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, it is related to binding material field, is prepared from by the raw material of following parts by weight：30 50 parts of quartz, 20 30 parts of feldspar, 5 15 parts of kaolin, 5 15 parts of borax, 1 10 parts of dextrin, 10 20 parts of polyacrylamide, 0.5 1.5 parts of phosphoric acid, 15 parts of zirconium oxide, 15 parts of aluminum oxide, 15 parts of silica flour, 70 100 parts of water, its preparation method includes：Weigh material, by quartz, feldspar and the melting cooling of borax co-grinding, pulverize and sieve, wet ball grinding simultaneously adds kaolin, dextrin and polyacrylamide and water, it is eventually adding phosphoric acid, zirconium oxide, aluminum oxide and silica flour, heating stirring, cooling, finished product is can obtain, the present invention is with gluing effect is good, intensity is high, stability good, resistant to elevated temperatures advantage.
Description
Technical field
The present invention relates to binding material field, and in particular to a kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant.
Background technology
A kind of new decoration of porcelain material and skill and technique that the seventies grow up.Also known as high temperature rapid firing stains.Pigment
Flux component is not leaded or few leaded, and implements glaze is imposed on by overglaze color method, and by high temperature rapid firing, glaze softening melting makes
Pigment is penetrated into glaze, glaze face closure after cooling.Fine and smooth sparkling and crystal-clear, moist mesh all of a sudden, anticorrosive, wear-resistant, the effect with underglaze colour,
Applique is essential step therein wherein in glaze, and concrete operations are to utilize binding agent applique after a glazing biscuiting, reglaze into
The secondary glaze firing of row, secondary temperature of glaze firing is high, and between about 1300-1400 DEG C, high temperature can harden binding agent, viscosity reduction, enters
And cause ceramic product erraic stitch pattern, overlapping, displacement etc., cause economic loss.
On overseas market, the research of ceramic mould high-temperature agglomerant is very active, and external Ye You enterprises start production, but match somebody with somebody
Side is but seldom delivered, such as the joint heatproof of the CA-110 binding agents of Man Erpaier companies production reaches 1400 DEG C, domestic at present
Although the research of this respect is just at the early-stage, fruitful.
The content of the invention
(1) technical problem solved
In view of the shortcomings of the prior art, the invention provides a kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, tool
Have that intensity is high, stability is good, resistant to elevated temperatures advantage.
(2) technical scheme
To realize object above, the present invention is achieved by the following technical programs：
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：Quartzy 30-
50 parts, 20-30 parts of feldspar, 5-15 parts of kaolin, 5-15 parts of borax, 1-10 parts of dextrin, 10-20 parts of polyacrylamide, phosphoric acid
0.5-1.5 parts, 1-5 parts of zirconium oxide, 1-5 parts of aluminum oxide, 1-5 parts of silica flour, 70-100 parts of water.
Preferably, the ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：
Quartzy 35-45 parts, 24-28 parts of feldspar, 7-12 parts of kaolin, 7-12 parts of borax, 3-7 parts of dextrin, 12-16 parts of polyacrylamide,
0.7-1.2 parts of phosphoric acid, 2-4 parts of zirconium oxide, 2-4 parts of aluminum oxide, 2-4 parts of silica flour, 80-90 parts of water.
Wherein, the preparation method of above-mentioned ceramic in-glaze decoration paster stamp high-temperature agglomerant comprises the following steps：
(1) required material is weighed in proportion；
(2) will be heated to 1600-1750 DEG C of high-temperature fusion after quartz, feldspar and borax co-grinding, then with 50-70 DEG C/
Min speed is cooled to 30-50 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, paste
Pasty state slurries are obtained after essence, polyacrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour are added into above-mentioned pasty state slurries, 50-70 DEG C is heated to, 5- is stirred
10h, is cooled to after room temperature, you can obtain the ceramic in-glaze decoration paster stamp binding agent.
Preferably, the phosphoric acid concentration is 40-50%.
Preferably, granularity is 0.5-1mm after quartz, feldspar and borax co-grinding in the step (2).
Preferably, mixing speed is 50-80r/min in the step (3).
(3) beneficial effect
The invention provides a kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, with advantages below：
(1) in the present invention, phosphoric acid is added, consolidating for binding agent can be reduced equivalent to glue chain is introduced in binding agent glue line
Change temperature and hardening time, reduction elevated cure step improves efficiency, quartz and feldspar are ceramic material, plays main glue
Knot is acted on, and borax can play the melting temperature of fluxing action, reduction quartz and feldspar, and it is steady that polyacrylamide can improve adhesive
It is qualitative, deposition is not susceptible to, kaolin and dextrin are auxiliary sizing, lift the sticky degree of binding agent, play secondary cementation,
Zirconium oxide, aluminum oxide and silica flour can lift the resistance to elevated temperatures of adhesive.
(2) raw material composition is mainly inorganic salts and oxide, and aboundresources, easy construction does not pollute the environment.
(3) adhesive of the present invention has that gluing effect is good, intensity is high, stability good, resistant to elevated temperatures advantage.
Embodiment
To make the purpose, technical scheme and advantage of the embodiment of the present invention clearer, below in conjunction with the embodiment of the present invention,
Technical scheme in the embodiment of the present invention is clearly and completely described, it is clear that described embodiment is the present invention one
Divide embodiment, rather than whole embodiments.Based on the embodiment in the present invention, those of ordinary skill in the art are not making
The every other embodiment obtained under the premise of creative work, belongs to the scope of protection of the invention.
Embodiment 1：
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：Quartz 35
0.7 part of phosphoric acid, the oxygen of part, 24 parts of feldspar, 7 parts of kaolin, 7 parts of borax, 3 parts of dextrin, 12 parts of polyacrylamide, concentration for 45%
Change 2 parts of zirconium, 2 parts of aluminum oxide, 2 parts of silica flour, 80 parts of water.
Wherein, the preparation method of above-mentioned ceramic in-glaze decoration paster stamp high-temperature agglomerant comprises the following steps：
(1) required material is weighed in proportion；
(2) it is 0.8mm by quartz, feldspar and borax co-grinding to granularity, 1650 DEG C of high-temperature fusions is heated to, with 65
DEG C/min speed is cooled to 35 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, paste
Pasty state slurries are obtained after essence, polyacrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour that concentration is 45% are added into above-mentioned pasty state slurries, 65 are heated to
DEG C, 8h is stirred with 80r/min speed, is cooled to after room temperature, you can obtain ceramic in-glaze decoration paster stamp binding agent.
Embodiment 2：
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：Quartz 45
Part, 28 parts of feldspar, 12 parts of kaolin, 12 parts of borax, 7 parts of dextrin, 16 parts of polyacrylamide, concentration for 40% .2 parts of phosphatase 11,
4 parts of zirconium oxide, 4 parts of aluminum oxide, 4 parts of silica flour, 90 parts of water.
Wherein, the preparation method of above-mentioned ceramic in-glaze decoration paster stamp high-temperature agglomerant comprises the following steps：
(1) required material is weighed in proportion；
(2) it is 0.5mm by quartz, feldspar and borax co-grinding to granularity, 1600 DEG C of high-temperature fusions is heated to, with 50
DEG C/min speed is cooled to 30 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, paste
Pasty state slurries are obtained after essence, polyacrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour that concentration is 40% are added into above-mentioned pasty state slurries, 50 are heated to
DEG C, 5h is stirred with 50r/min speed, is cooled to after room temperature, you can obtain ceramic in-glaze decoration paster stamp binding agent.
Embodiment 3：
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：Quartz 30
0.5 part of phosphoric acid, the oxygen of part, 20 parts of feldspar, 5 parts of kaolin, 5 parts of borax, 1 part of dextrin, 10 parts of polyacrylamide, concentration for 50%
Change 1 part of zirconium, 1 part of aluminum oxide, 1 part of silica flour, 70 parts of water.
Wherein, the preparation method of above-mentioned ceramic in-glaze decoration paster stamp high-temperature agglomerant comprises the following steps：
(1) required material is weighed in proportion；
(2) it is 1mm by quartz, feldspar and borax co-grinding to granularity, 1750 DEG C of high-temperature fusions is heated to, with 70
DEG C/min speed is cooled to 50 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, paste
Pasty state slurries are obtained after essence, polyacrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour that concentration is 50% are added into above-mentioned pasty state slurries, 70 are heated to
DEG C, 10h is stirred with 80r/min speed, is cooled to after room temperature, you can obtain ceramic in-glaze decoration paster stamp binding agent.
Embodiment 4：
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：Quartz 50
Part, the phosphatase 11 .5 that 30 parts of feldspar, 15 parts of kaolin, 15 parts of borax, 10 parts of dextrin, 20 parts of polyacrylamide, concentration are 45%
Part, 5 parts of zirconium oxide, 5 parts of aluminum oxide, 5 parts of silica flour, 100 parts of water.
Wherein, the preparation method of above-mentioned ceramic in-glaze decoration paster stamp high-temperature agglomerant comprises the following steps：
(1) required material is weighed in proportion；
(2) it is 1mm by quartz, feldspar and borax co-grinding to granularity, 1700 DEG C of high-temperature fusions is heated to, with 60
DEG C/min speed is cooled to 45 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, paste
Pasty state slurries are obtained after essence, polyacrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour that concentration is 45% are added into above-mentioned pasty state slurries, 55 are heated to
DEG C, 8h is stirred with 75r/min speed, is cooled to after room temperature, you can obtain ceramic in-glaze decoration paster stamp binding agent.
Embodiment 5：
A kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, is prepared from by the raw material of following parts by weight：Quartz 47
Part, 22 parts of feldspar, 10 parts of kaolin, 10 parts of borax, 5 parts of dextrin, 15 parts of polyacrylamide, concentration for 40% .2 parts of phosphatase 11,
3 parts of zirconium oxide, 3 parts of aluminum oxide, 4 parts of silica flour, 90 parts of water.
Wherein, the preparation method of above-mentioned ceramic in-glaze decoration paster stamp high-temperature agglomerant comprises the following steps：
(1) required material is weighed in proportion；
(2) it is 0.7mm by quartz, feldspar and borax co-grinding to granularity, 1600 DEG C of high-temperature fusions is heated to, with 60
DEG C/min speed is cooled to 30 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, paste
Pasty state slurries are obtained after essence, polyacrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour that concentration is 40% are added into above-mentioned pasty state slurries, 10 are heated to
DEG C, 10h is stirred with 80r/min speed, is cooled to after room temperature, you can obtain ceramic in-glaze decoration paster stamp binding agent.
Quality testing：
Table 1 is 1-5 quality measurements of the embodiment of the present invention：
Table 1：Testing result
To sum up, the embodiment of the present invention has the advantages that：Water absorption rate is low, and intensity is high, and setting time is short, sticking temperature
It is low, and being capable of high temperature resistant.
It should be noted that herein, such as first and second or the like relational terms are used merely to a reality
Body or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or deposited between operating
In any this actual relation or order.Moreover, term " comprising ", "comprising" or its any other variant are intended to
Nonexcludability is included, so that process, method, article or equipment including a series of key elements not only will including those
Element, but also other key elements including being not expressly set out, or also include being this process, method, article or equipment
Intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that
Also there is other identical element in process, method, article or equipment including the key element.
The above embodiments are merely illustrative of the technical solutions of the present invention, rather than its limitations；Although with reference to the foregoing embodiments
The present invention is described in detail, it will be understood by those within the art that：It still can be to foregoing each implementation
Technical scheme described in example is modified, or carries out equivalent substitution to which part technical characteristic；And these modification or
Replace, the essence of appropriate technical solution is departed from the spirit and scope of various embodiments of the present invention technical scheme.
Claims (6)
1. a kind of ceramic in-glaze decoration paster stamp high-temperature agglomerant, it is characterised in that prepared by the raw material of following parts by weight and
Into：Quartzy 30-50 parts, 20-30 parts of feldspar, 5-15 parts of kaolin, 5-15 parts of borax, 1-10 parts of dextrin, polyacrylamide 10-20
Part, 0.5-1.5 parts of phosphoric acid, 1-5 parts of zirconium oxide, 1-5 parts of aluminum oxide, 1-5 parts of silica flour, 70-100 parts of water.
2. ceramics in-glaze decoration paster stamp high-temperature agglomerant as claimed in claim 1, it is characterised in that by following parts by weight
Raw material be prepared from：Quartzy 35-45 parts, 24-28 parts of feldspar, 7-12 parts of kaolin, 7-12 parts of borax, 3-7 parts of dextrin, poly- third
12-16 parts of acrylamide, 0.7-1.2 parts of phosphoric acid, 2-4 parts of zirconium oxide, 2-4 parts of aluminum oxide, 2-4 parts of silica flour, 80-90 parts of water.
3. ceramics in-glaze decoration paster stamp high-temperature agglomerant as claimed in claim 1 or 2, it is characterised in that its preparation side
Method comprises the following steps：
(1) required material is weighed in proportion；
(2) 1600-1750 DEG C of high-temperature fusion will be heated to after quartz, feldspar and borax co-grinding, then with 50-70 DEG C/min's
Speed is cooled to 30-50 DEG C, after pulverizing and sieving, wet ball grinding, during wet ball grinding, is slowly added to kaolin, dextrin, poly- third
Pasty state slurries are obtained after acrylamide and water, wet ball grinding；
(3) phosphoric acid, zirconium oxide, aluminum oxide and silica flour are added into above-mentioned pasty state slurries, 50-70 DEG C is heated to, 5-10h is stirred,
It is cooled to after room temperature, you can obtain the ceramic in-glaze decoration paster stamp binding agent.
4. ceramics in-glaze decoration paster stamp high-temperature agglomerant as claimed in claim 1, it is characterised in that the phosphoric acid concentration
For 40-50%.
5. ceramics in-glaze decoration paster stamp high-temperature agglomerant as claimed in claim 3, it is characterised in that the step (2)
Granularity is 0.5-1mm after middle quartz, feldspar and borax co-grinding.
6. ceramics in-glaze decoration paster stamp high-temperature agglomerant as claimed in claim 3, it is characterised in that the step (3)
Middle mixing speed is 50-80r/min.
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