CN107162482A - A kind of energy-conserving plate material and preparation method thereof - Google Patents
A kind of energy-conserving plate material and preparation method thereof Download PDFInfo
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- CN107162482A CN107162482A CN201710471842.9A CN201710471842A CN107162482A CN 107162482 A CN107162482 A CN 107162482A CN 201710471842 A CN201710471842 A CN 201710471842A CN 107162482 A CN107162482 A CN 107162482A
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Classifications
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B26/00—Compositions of mortars, concrete or artificial stone, containing only organic binders, e.g. polymer or resin concrete
- C04B26/006—Waste materials as binder
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00017—Aspects relating to the protection of the environment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00612—Uses not provided for elsewhere in C04B2111/00 as one or more layers of a layered structure
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Organic Chemistry (AREA)
- Press-Shaping Or Shaping Using Conveyers (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)
Abstract
The invention discloses a kind of energy-conserving plate material, include the raw material of following parts by weight：20~30 parts of damaged tire sizing material, 17~28 parts of modified attapulgite clay, 8~25 parts of flyash, 7~13 parts of fire retardant, 10~30 parts of kaolin, 3~7 parts of wood sawdust, 3~5 parts of waterproofing agent of organosilicon；The energy-conserving plate material has reached useless, the environmentally friendly purpose of energy-conservation, profit by the use of damaged tire sizing material, flyash as raw material.
Description
Technical field
The invention belongs to building material technical field, and in particular to a kind of energy-conserving plate material and preparation method thereof.
Background technology
With the gradually enhancing and the continuous improvement of scientific and technological level of China's economic strength, government is in terms of building field
Energy pay attention to day by day and approval are saved using advanced power-saving technology, energy-saving material.Building energy conservation is benefited the nation and the people, exploitation energy-conservation
Construction material fully saves land, profit is useless, environmental protection, may advantageously facilitate economic growth.China is a developing country, per capita resources
It is relatively poor.
At present be commonly used for the public places such as square, park, road road base will using cement concrete, stone material,
The fluid-tight material laying such as Ceramic Tiles is formed, and about 4,500,000 mu are taken up an area in national brick and tile enterprise, and Mei electricity enterprises will arrange every year
Put more than 200,000,000 tons of flyash and gangue, do not only take up a large amount of arable lands, and pollution environment, thus greatly develop energy-conservation, save land,
Profit is given up, is incubated, heat-insulated board, accelerates sheet material innovation, it is a very urgent major issue to promote Building Energy-saving Work.
The content of the invention
The invention provides a kind of energy-conserving plate material and preparation method thereof, the energy-conserving plate material utilizes damaged tire sizing material, fine coal
Ash has reached useless, the environmentally friendly purpose of energy-conservation, profit as raw material.
In order to solve the problem of prior art is present, adopt the following technical scheme that：
A kind of energy-conserving plate material, includes the raw material of following parts by weight：
20~30 parts of damaged tire sizing material；
17~28 parts of modified attapulgite clay；
8~25 parts of flyash；
7~13 parts of fire retardant；
10~30 parts of kaolin；
3~7 parts of wood sawdust；
3~5 parts of waterproofing agent of organosilicon.
Further, the energy-conserving plate material, includes the raw material of following parts by weight：
27 parts of damaged tire sizing material；
23 parts of modified attapulgite clay；
21 parts of flyash；
11 parts of fire retardant；
19 parts of kaolin；
5 parts of wood sawdust；
4 parts of waterproofing agent of organosilicon.
Further, the preparation method of the modified attapulgite clay comprises the following steps：
（1）Concave-convex clay rod is ground, mixes, stir with deionized water, standing, filtering, the dry bumps that must be purified
Rod stone clay；
（2）Purified Concave-convex clay rod is put into reactor, inert gas is passed through, 200 DEG C are warming up to, vapor is added
Fully contacted with attapulgite, be continuously heating to 330 DEG C, kept for 2~3 hours, stop adding vapor, room temperature to be cooled to is
The modified attapulgite clay can be obtained.
Further, the deionized water and the weight of attapulgite clay ratio are 1：20.
A kind of method for preparing the energy-conserving plate material, comprises the following steps：
（1）Damaged tire sizing material is warming up to 50~60 DEG C, Double-shaft shearing disintegrating machine is put into, is crushed, 100 mesh sieves are crossed, plus
Enter deionized water, be well mixed, stir, stand, filter, dry, be then placed in plasma handling system and carry out at plasma
Reason, obtains modified damaged tire sizing material；
（2）Kaolin was crushed into 100 mesh sieves, was well mixed with wood sawdust, add water shaping, then dries, and is put into calcining furnace, plus
Temperature is calcined 3~5 hours to 300~500 DEG C, then is heated up to 800~1000 DEG C, is calcined 5~8 hours, is taken out cooling, is ground again
Grinds, cross 200 mesh sieves, and modified kaolin is made；
（3）Modified damaged tire sizing material, modified attapulgite clay, flyash, modified kaolin are put into mixer, low speed is stirred
Mix and fire retardant and waterproofing agent of organosilicon, high-speed stirred 30~50 minutes are added after 10~20 minutes, temperature control is 100~115
DEG C, compound is made；
（4）Compound is put into twin-screw extrusion forming machine, the temperature of double screw extruder is 150~178 DEG C, the temperature of cooling water
Spend for 15~25 DEG C, extrusion molding obtains the energy-conserving plate material.
Further, the step（1）The mass ratio of middle deionized water and damaged tire sizing material is 1:10.
Further, the step（3）Middle stirring at low speed Velocity Time is 18 minutes, and the high-speed stirred time is 43 minutes.
Further, the step（3）The temperature of middle cooling water is 17 DEG C.
Compared with prior art, it has the advantages that the present invention：
（1）Junked tire sizing material and flyash are with the addition of in energy-conserving plate material of the present invention, cost of material is reduced, developed
The new application of junked tire sizing material and flyash, solve the problem of processing of junked tire sizing material is difficult, it is to avoid flyash is dirty
The phenomenon of environment is contaminated, Environmental costs are reduced；
（2）Middle addition modified attapulgite clay of the present invention, reduces the cost of sheet material, improves the property of the sheet material
Can, its service life is added, also makes the sheet material that there is the function of the toxic and harmful gas such as formaldehyde adsorption；
（3）Preparation method of the present invention is by the way of extrusion forming so that the energy-conserving plate material prepared, and intensity is big, makes
Use long lifespan；
（4）Preparation method of the present invention is low for equipment requirements, is adapted to promote.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
The present embodiment is related to a kind of energy-conserving plate material, includes the raw material of following parts by weight：
20 parts of damaged tire sizing material；
17 parts of modified attapulgite clay；
8 parts of flyash；
7 parts of fire retardant；
10 parts of kaolin；
3 parts of wood sawdust；
3 parts of waterproofing agent of organosilicon.
Wherein, the preparation method of the modified attapulgite clay comprises the following steps：
（1）Concave-convex clay rod is ground, mixes, stir with deionized water, standing, filtering, the dry bumps that must be purified
Rod stone clay；
（2）Purified Concave-convex clay rod is put into reactor, inert gas is passed through, 200 DEG C are warming up to, vapor is added
Fully contacted with attapulgite, be continuously heating to 330 DEG C, kept for 2 hours, stop adding vapor, room temperature to be cooled to
Obtain the modified attapulgite clay.
The deionized water and the weight of attapulgite clay ratio are 1：20.
A kind of method for preparing the energy-conserving plate material, comprises the following steps：
（1）Damaged tire sizing material is warming up to 50 DEG C, Double-shaft shearing disintegrating machine is put into, is crushed, 100 mesh sieves are crossed, addition is gone
Ionized water, is well mixed, and stirs, and stands, and filters, and dries, is then placed in plasma handling system and carries out plasma treatment, obtain
Modified damaged tire sizing material；
（2）Kaolin was crushed into 100 mesh sieves, was well mixed with wood sawdust, add water shaping, then dries, and is put into calcining furnace, plus
Temperature is calcined 3 hours to 300 DEG C, then is heated up to 800 DEG C, is calcined 5 hours, takes out cooling, regrinds into powder, crosses 200 mesh sieves,
Modified kaolin is made；
（3）Modified damaged tire sizing material, modified attapulgite clay, flyash, modified kaolin are put into mixer, low speed is stirred
Mix and fire retardant and waterproofing agent of organosilicon are added after 10 minutes, compound is made at 100 DEG C in high-speed stirred 30 minutes, temperature control；
（4）Compound is put into twin-screw extrusion forming machine, the temperature of double screw extruder is 150 DEG C, and the temperature of cooling water is
15 DEG C, extrusion molding obtains the energy-conserving plate material.
Wherein, the step（1）The mass ratio of middle deionized water and damaged tire sizing material is 1:10.
Embodiment 2
The present embodiment is related to a kind of energy-conserving plate material, includes the raw material of following parts by weight：
30 parts of damaged tire sizing material；
28 parts of modified attapulgite clay；
25 parts of flyash；
13 parts of fire retardant；
30 parts of kaolin；
7 parts of wood sawdust；
5 parts of waterproofing agent of organosilicon.
Wherein, the preparation method of the modified attapulgite clay comprises the following steps：
（1）Concave-convex clay rod is ground, mixes, stir with deionized water, standing, filtering, the dry bumps that must be purified
Rod stone clay；
（2）Purified Concave-convex clay rod is put into reactor, inert gas is passed through, 200 DEG C are warming up to, vapor is added
Fully contacted with attapulgite, be continuously heating to 330 DEG C, kept for 3 hours, stop adding vapor, room temperature to be cooled to
Obtain the modified attapulgite clay.
The deionized water and the weight of attapulgite clay ratio are 1：20.
A kind of method for preparing the energy-conserving plate material, comprises the following steps：
（1）Damaged tire sizing material is warming up to 60 DEG C, Double-shaft shearing disintegrating machine is put into, is crushed, 100 mesh sieves are crossed, addition is gone
Ionized water, is well mixed, and stirs, and stands, and filters, and dries, is then placed in plasma handling system and carries out plasma treatment, obtain
Modified damaged tire sizing material；
（2）Kaolin was crushed into 100 mesh sieves, was well mixed with wood sawdust, add water shaping, then dries, and is put into calcining furnace, plus
Temperature is calcined 5 hours to 500 DEG C, then is heated up to 1000 DEG C, is calcined 8 hours, takes out cooling, regrinds into powder, crosses 200 mesh sieves,
Modified kaolin is made；
（3）Modified damaged tire sizing material, modified attapulgite clay, flyash, modified kaolin are put into mixer, low speed is stirred
Mix and fire retardant and waterproofing agent of organosilicon are added after 20 minutes, compound is made at 115 DEG C in high-speed stirred 50 minutes, temperature control；
（4）Compound is put into twin-screw extrusion forming machine, the temperature of double screw extruder is 178 DEG C, and the temperature of cooling water is
25 DEG C, extrusion molding obtains the energy-conserving plate material.
The step（1）The mass ratio of middle deionized water and damaged tire sizing material is 1:10.
Embodiment 3
The present embodiment is related to a kind of energy-conserving plate material, includes the raw material of following parts by weight：
27 parts of damaged tire sizing material；
23 parts of modified attapulgite clay；
21 parts of flyash；
11 parts of fire retardant；
19 parts of kaolin；
5 parts of wood sawdust；
Wherein, the preparation method of the modified attapulgite clay comprises the following steps：
（1）Concave-convex clay rod is ground, mixes, stir with deionized water, standing, filtering, the dry bumps that must be purified
Rod stone clay；
（2）Purified Concave-convex clay rod is put into reactor, inert gas is passed through, 200 DEG C are warming up to, vapor is added
Fully contacted with attapulgite, be continuously heating to 330 DEG C, kept for 2.5 hours, stop adding vapor, room temperature to be cooled to is
The modified attapulgite clay can be obtained.
The deionized water and the weight of attapulgite clay ratio are 1：20.
A kind of method for preparing the energy-conserving plate material, comprises the following steps：
（1）Damaged tire sizing material is warming up to 55 DEG C, Double-shaft shearing disintegrating machine is put into, is crushed, 100 mesh sieves are crossed, addition is gone
Ionized water, is well mixed, and stirs, and stands, and filters, and dries, is then placed in plasma handling system and carries out plasma treatment, obtain
Modified damaged tire sizing material；
（2）Kaolin was crushed into 100 mesh sieves, was well mixed with wood sawdust, add water shaping, then dries, and is put into calcining furnace, plus
Temperature is calcined 4 hours to 400 DEG C, then is heated up to 900 DEG C, is calcined 6 hours, takes out cooling, regrinds into powder, crosses 200 mesh sieves,
Modified kaolin is made；
（3）Modified damaged tire sizing material, modified attapulgite clay, flyash, modified kaolin are put into mixer, low speed is stirred
Mix and fire retardant and waterproofing agent of organosilicon are added after 18 minutes, compound is made at 110 DEG C in high-speed stirred 43 minutes, temperature control；
（4）Compound is put into twin-screw extrusion forming machine, the temperature of double screw extruder is 160 DEG C, and the temperature of cooling water is
17 DEG C, extrusion molding obtains the energy-conserving plate material.
Wherein, the step（1）The mass ratio of middle deionized water and damaged tire sizing material is 1:10.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (8)
1. a kind of energy-conserving plate material, it is characterised in that include the raw material of following parts by weight：
20~30 parts of damaged tire sizing material；
17~28 parts of modified attapulgite clay；
8~25 parts of flyash；
7~13 parts of fire retardant；
10~30 parts of kaolin；
3~7 parts of wood sawdust；
3~5 parts of waterproofing agent of organosilicon.
2. energy-conserving plate material according to claim 1, it is characterised in that include the raw material of following parts by weight：
27 parts of damaged tire sizing material；
23 parts of modified attapulgite clay；
21 parts of flyash；
11 parts of fire retardant；
19 parts of kaolin；
5 parts of wood sawdust；
4 parts of waterproofing agent of organosilicon.
3. energy-conserving plate material according to claim 1, it is characterised in that the preparation method of the modified attapulgite clay includes
Following steps：
（1）Concave-convex clay rod is ground, mixes, stir with deionized water, standing, filtering, the dry bumps that must be purified
Rod stone clay；
（2）Purified Concave-convex clay rod is put into reactor, inert gas is passed through, 200 DEG C are warming up to, vapor is added
Fully contacted with attapulgite, be continuously heating to 330 DEG C, kept for 2~3 hours, stop adding vapor, room temperature to be cooled to is
The modified attapulgite clay can be obtained.
4. energy-saving material according to claim 3, it is characterised in that the deionized water and the weight of attapulgite clay ratio
For 1：20.
5. a kind of method of the energy-conserving plate material prepared described in Claims 1 to 4, it is characterised in that comprise the following steps：
（1）Damaged tire sizing material is warming up to 50~60 DEG C, Double-shaft shearing disintegrating machine is put into, is crushed, 100 mesh sieves are crossed, plus
Enter deionized water, be well mixed, stir, stand, filter, dry, be then placed in plasma handling system and carry out at plasma
Reason, obtains modified damaged tire sizing material；
（2）Kaolin was crushed into 100 mesh sieves, was well mixed with wood sawdust, add water shaping, then dries, and is put into calcining furnace, plus
Temperature is calcined 3~5 hours to 300~500 DEG C, then is heated up to 800~1000 DEG C, is calcined 5~8 hours, is taken out cooling, is ground again
Grinds, cross 200 mesh sieves, and modified kaolin is made；
（3）Modified damaged tire sizing material, modified attapulgite clay, flyash, modified kaolin are put into mixer, low speed is stirred
Mix and fire retardant and waterproofing agent of organosilicon, high-speed stirred 30~50 minutes are added after 10~20 minutes, temperature control is 100~115
DEG C, compound is made；
（4）Compound is put into twin-screw extrusion forming machine, the temperature of double screw extruder is 150~178 DEG C, the temperature of cooling water
Spend for 15~25 DEG C, extrusion molding obtains the energy-conserving plate material.
6. preparation method according to claim 5, it is characterised in that the step（1）Middle deionized water and damaged tire glue
The mass ratio of material is 1:10.
7. preparation method according to claim 5, it is characterised in that the step（3）Middle stirring at low speed Velocity Time is
18 minutes, high speed time was 43 minutes.
8. preparation method according to claim 5, it is characterised in that the step（3）The temperature of middle cooling water is 17 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710471842.9A CN107162482A (en) | 2017-06-20 | 2017-06-20 | A kind of energy-conserving plate material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710471842.9A CN107162482A (en) | 2017-06-20 | 2017-06-20 | A kind of energy-conserving plate material and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107162482A true CN107162482A (en) | 2017-09-15 |
Family
ID=59819048
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| CN201710471842.9A Withdrawn CN107162482A (en) | 2017-06-20 | 2017-06-20 | A kind of energy-conserving plate material and preparation method thereof |
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Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1047272A (en) * | 1989-05-19 | 1990-11-28 | 朱连生 | The manufacture method of fly ash composite material |
| CN101381211A (en) * | 2008-10-16 | 2009-03-11 | 中国科学院长春应用化学研究所 | Method for preparing building mould using various solid wastes |
| CN103894143A (en) * | 2014-03-18 | 2014-07-02 | 苏州宇希新材料科技有限公司 | Method for activating attapulgite |
| CN104761846A (en) * | 2015-03-29 | 2015-07-08 | 安徽同丰橡塑工业有限公司 | Preparation method of rubber powder composite material |
| CN105399374A (en) * | 2015-12-09 | 2016-03-16 | 文登蓝岛建筑工程有限公司 | Waterproof thermal insulation sheet and preparation method thereof |
| CN105461345A (en) * | 2015-05-12 | 2016-04-06 | 惠州市惠阳皇磁陶瓷有限公司 | Environmentally friendly tile blank capable of purifying air, and tile made thereofrom |
-
2017
- 2017-06-20 CN CN201710471842.9A patent/CN107162482A/en not_active Withdrawn
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1047272A (en) * | 1989-05-19 | 1990-11-28 | 朱连生 | The manufacture method of fly ash composite material |
| CN101381211A (en) * | 2008-10-16 | 2009-03-11 | 中国科学院长春应用化学研究所 | Method for preparing building mould using various solid wastes |
| CN103894143A (en) * | 2014-03-18 | 2014-07-02 | 苏州宇希新材料科技有限公司 | Method for activating attapulgite |
| CN104761846A (en) * | 2015-03-29 | 2015-07-08 | 安徽同丰橡塑工业有限公司 | Preparation method of rubber powder composite material |
| CN105461345A (en) * | 2015-05-12 | 2016-04-06 | 惠州市惠阳皇磁陶瓷有限公司 | Environmentally friendly tile blank capable of purifying air, and tile made thereofrom |
| CN105399374A (en) * | 2015-12-09 | 2016-03-16 | 文登蓝岛建筑工程有限公司 | Waterproof thermal insulation sheet and preparation method thereof |
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Application publication date: 20170915 |