CN107137240A - A kind of colorful cleawhite pack of painting type and preparation method thereof - Google Patents
A kind of colorful cleawhite pack of painting type and preparation method thereof Download PDFInfo
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- CN107137240A CN107137240A CN201710539174.9A CN201710539174A CN107137240A CN 107137240 A CN107137240 A CN 107137240A CN 201710539174 A CN201710539174 A CN 201710539174A CN 107137240 A CN107137240 A CN 107137240A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
- A61K8/602—Glycosides, e.g. rutin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Public Health (AREA)
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- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Emergency Medicine (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
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Abstract
The invention discloses colorful cleawhite pack of a kind of painting type and preparation method thereof.The present invention the colorful cleawhite pack of painting type according to weight than each group be divided into：Toning base-material：400 500 parts, interleaving agent：200 300 parts, continuous phase：300 400 parts.The colorful cleawhite pack color of painting type of the present invention appears, pleasing, gives the enjoyment of U.S.；The facial mask uses the raw material of environmental protection, will not have a negative impact to human body and environment；The mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, and whitening effect is notable；The mature preparation process of the facial mask, adapts to industrialized production.
Description
Technical field
The invention belongs to field of fine chemical, and in particular to a kind of colorful cleawhite pack of painting type and preparation method thereof.
Background technology
Nowadays, with the raising of people's quality of the life and to beautiful pursuit, more and more people's selections are maintained using facial mask
Skin.Cleawhite pack is a kind of carrier of face beautifying health keeping product, and sufficient moisture and nutriment can be provided to skin, there is whitening
Many effects such as brighten, be loved by people.Cleawhite pack on the market is largely sticking type facial mask now.Sticking type facial mask
It is to use non-woven fabrics etc. as matrix, infiltrates Essence etc. and spread on skin.The subject matter that this mode is present is due to individual
Body difference, facial mask can not completely fit with skin.Daubing-type facial mask solves this problem.In use, cream pack is uniform
It is applied on skin, treats that Essence absorbs and finish, can tear in flakes.The painting type cleawhite pack beautiful jade of all kinds of brands on the market
Meet the eye on every side.In order to win the market, manufacturers, which try one's best, makes miscellaneous product.They are formulated health environment-friendly, and packaging is beautiful
See generous.By contrast, the visual effect of the content that consumer more takes notice of in itself, which but has no characteristic, to be sayed.Now, on the market
Daubing-type facial mask be transparent or monochromatic lotion.Product colour is single, it is impossible to meet consumer to beautiful pursuit.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide a kind of colorful cleawhite pack of painting type and its preparation
Method.The colorful cleawhite pack color of the painting type appears, pleasing, gives the enjoyment of U.S.；And use environmental protection
Raw material, will not have a negative impact to human body and environment；Patch skin is good when using, and adhesion is moderate, and film forming is fast, pliability
Good, whitening effect is notable；Mature preparation process, adapts to industrialized production.
To achieve the above object, the present invention is adopted the following technical scheme that：
A kind of colorful cleawhite pack of painting type, is made up of the raw material of following parts by weight：400-500 parts of base-material of toning, interleaving agent
200-300 parts and 300-400 parts of continuous phase.
Described interleaving agent is made up of the raw material of following parts by weight：850-950 parts of deionized water, 50-150 parts of insulating powder,
1-3 parts of preservative.
Described insulating powder is lithium magnesium silicate, aluminium-magnesium silicate, S482 one or more of compositions；Described preservative
For Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one or more of compositions in propylben.
The preparation process of described interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 400-500 revs/min of rotating speed is controlled；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring is extremely dissolved for 30-40 minutes；
3）Surplus insulating powder is put into reactor, is stirred 30-40 minutes under same rotational speed.
The continuous phase is made up of the raw material of following parts by weight：600-750 parts of deionized water, 200-400 parts of water-base resin,
10-20 parts of whitening agent, 10-30 parts of NMF, 3-15 parts of thickener, 3-5 parts of preservative, 0-5 parts of pH adjusting agent, complexing agent 0.2-
1 part.
In continuous phase, described water-base resin is one or both of Carfil 9221 or Carfil 9220；
Described whitening agent is one or more of compositions in vitamin C, ursin, Glycolic acid, azalaic acid, Trenaxmine；Institute
NMF is stated for 1,2-PD, glycerine, ethylene glycol, sorbierite, one or more of compositions in butanediol；Described
Thickener is guar gum, carbomer, sodium carboxymethylcellulose, hydroxyethyl cellulose, the one or more in hydroxypropyl cellulose
Composition；Described pH adjusting agent is diethanol amine, triethanolamine, CP-950, one or more of combinations in AMP-95
Thing；Described complexing agent is one kind in disodium ethylene diamine tetraacetate, the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is
One or more of compositions in Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, propylben.
The preparation process of the continuous phase is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, it is beautiful
White agent, complexing agent and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener is slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces continuous phase.
Described toning base-material is made up of the raw material of following parts by weight：980-1000 parts of base-material, 0-20 parts of dyestuff；It is described
Base-material be made up of the raw material of following parts by weight：350-550 parts of deionized water, 300-500 parts of water-base resin, interleaving agent 50-
150 parts, 10-20 parts of whitening agent, 10-30 parts of NMF；20-80 parts of thickener, 0-50 parts of pH adjusting agent, 3-5 parts of preservative, network
0.2-1 parts of mixture；The dyestuff is assorted food-grade or cosmetics-stage transparency dye.
In base-material, described water-base resin is one or both of Carfil 9221 or Carfil 9220；Institute
The whitening agent stated is one or more of compositions in vitamin C, ursin, Glycolic acid, azalaic acid, Trenaxmine；It is described
NMF is 1,2-PD, glycerine, ethylene glycol, sorbierite, one or more of compositions in butanediol；Described increasing
Thick dose is one or more of compositions in Aculyn 33, Vesmody A901, Vesmody A406；Described pH
Conditioning agent is diethanol amine, triethanolamine, CP-950, one or more of compositions in AMP-95；Described complexing agent is
One kind in disodium ethylene diamine tetraacetate, the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, Buddhist nun
Moor one or more of compositions in tortoise beetle ester, propylben.
The preparation process of described base-material is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, it is beautiful
White agent, complexing agent and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, stirs 20-30 minutes, produces toning base-material.
A kind of method for preparing the colorful cleawhite pack of painting type as described above, including step as described below：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into interleaving agent, and granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, is stirred 20-30 minutes with 100-150 revs/min of speed, produces painting type many
Color cleawhite pack.
The beneficial effects of the present invention are：
1）Mask sheet skin is good, and adhesion is moderate, and film forming is fast, and pliability is good, and whitening effect is notable；Due to skin temperature compared with
Height, after colorful cleawhite pack is coated on skin, interleaving agent fails rapidly, promotes the elite thing in toning base-material and continuous phase
Release, while water-base resin formation diaphragm structure, in favor of maintenance terminate after depart from skin；
2）The colorful cleawhite pack color of painting type appears, pleasing, gives the enjoyment of U.S.；And it is former using environmental protection
Material is made, and will not have a negative impact to human body and environment；
3）The mature preparation process of facial mask, adapts to industrialized production.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described.
Obviously, described embodiment is only the part of the present invention, and based on the embodiment in the present invention, those skilled in the art exist
The every other embodiment obtained under the premise of creative work is not made, the scope of protection of the invention is belonged to.
Embodiment 1
A kind of colorful cleawhite pack of painting type is made up of the raw material of following parts by weight：400 parts of base-material of toning, 250 parts of interleaving agent, even
Continuous 350 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：441 parts of deionized water, 9,221 350 parts of Carfil, silicic acid
100 parts of the magnesium lithium aqueous solution, 25 parts of 1,2-PD, 15 parts of vitamin C, 33 35 parts of Aculyn, 30 parts of triethanolamine, benzene oxygen
3.2 parts of ethanol, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
Grey and the compound method of white basic material are identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and are configured to
Grey base-material, 99.8 parts of base-materials add 0.2 part of white dye and are configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,2-PD, is tieed up
Raw element C, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）Carfil 9221 and the lithium magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of lithium magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The lithium magnesium silicate powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus lithium magnesium silicate powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：660 parts of deionized water, 9,221 280 parts of Carfil, third
25 parts of triol, 20 parts of vitamin C, 21 5 parts of carbomer Carbopol Ultrez, 1 part of hydroxyethyl cellulose 250HBR, benzene
3 parts of oxyethanol, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds glycerine, vitamin
C, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful cleawhite pack of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into the lithium magnesium silicate aqueous solution, and granulation terminates
Continue to stir 10 minutes afterwards；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful whitening of painting type
Facial mask 1.
Embodiment 2
A kind of colorful cleawhite pack of painting type is made up of the raw material of following parts by weight：500 parts of base-material of toning, 200 parts of interleaving agent, even
Continuous 400 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：466 parts of deionized water, 9,221 320 parts of Carfil, silicic acid
The magnalium aqueous solution（Interleaving agent）100 parts, 25 parts of 1,2-PD, 20 parts of Glycolic acid, 35 parts of Vesmody A901, three ethanol
30 parts of amine, 3 parts of propylben, 1 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, grey, blueness, white food-grade transparency dye.
Toning base-material preparation process be：
1）199.6 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.4 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of grey, blueness and white basic material is identical with yellow base-material, and 99.8 parts of base-materials add 0.2 part of gray dyes and matched somebody with somebody
Grey base-material is made, 99.8 parts of base-materials add 0.2 part of blue dyes and prepare au bleu base-material, and 99.8 parts of base-materials add 0.2 part in vain
Color dyestuff is configured to white basic material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,2-PD, it is sweet
Alkyd, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）Carfil 9221 and the aluminium-magnesium silicate aqueous solution are sequentially added, is stirred 30 minutes；
3）Aculyn 33 is added, is stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of aluminium-magnesium silicate, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The magnesium silicate aluminium powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus magnesium silicate aluminium powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：660 parts of deionized water, 9,221 280 parts of Carfil, third
25 parts of triol, 20 parts of Glycolic acid, 21 5 parts of Carbopol Ultrez, 1 part of 250HBR, 3 parts of propylben, AMP-95 5
Part, 1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds glycerine, glycol
Acid, disodium ethylene diamine tetraacetate, propylben is stirred 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful cleawhite pack of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into the aluminium-magnesium silicate aqueous solution, and granulation terminates
Continue to stir 10 minutes afterwards；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful whitening of painting type
Facial mask 2.
Embodiment 3
A kind of colorful cleawhite pack of painting type is made up of the raw material of following parts by weight：450 parts of base-material of toning, 300 parts of interleaving agent, even
Continuous 300 parts of phase.
The toning base-material is made up of the raw material of following parts by weight：998 parts of base-material, 2 parts of dyestuff.
Base-material is specifically made up of the raw material of following parts by weight：450 parts of deionized water, 9,220 350 parts of Carfil, S-
482 solution（Interleaving agent）100 parts, 20 parts of 1,2-PD, 5 parts of glycerine, 15 parts of ursin, 30 parts of Vesmody A901,
26 parts of triethanolamine, 3.2 parts of methyl hydroxybenzoate, 0.8 part of disodium ethylene diamine tetraacetate.
The dyestuff is yellow, red, blue food-grade transparency dye.
Toning base-material preparation process be：
1）100 parts of base-materials are added in reactor, stirred with 200 revs/min of speed；
2）0.2 part of weld is added, stirs 20 minutes, produces yellow base-material；
The compound method of red and blue base-material is identical with yellow base-material, and 199.6 parts of base-materials add 0.4 part of orchil and are configured to
Red base-material, 149.7 parts of base-materials add 0.3 part of gray dyes and prepare grey base-material；
The preparation process of the base-material is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,2-PD, third
Triol, ursin, disodium ethylene diamine tetraacetate, Phenoxyethanol is stirred 30 minutes；
2）Carfil 9221 and S-482 solution are sequentially added, is stirred 30 minutes；
3）Vesmody A901 are added, are stirred 15 minutes；
4）Triethanolamine is added, makes system pH=7, stirs 30 minutes, produces base-material.
Interleaving agent is specifically made up of the raw material of following parts by weight：917 parts of deionized water, 80 parts of S-482 powder, Phenoxyethanol 3
Part.
The preparation process of interleaving agent is：
1）The deionized water of formula ratio is put into reactor, 500 revs/min of rotating speed is controlled；
2）The S-482 powder of 1/2 formula ratio and the Phenoxyethanol of formula ratio are put into reactor, stirring is extremely dissolved for 30 minutes；
3）Surplus S-482 powder is put into reactor, is stirred 30 minutes under same rotational speed, obtains S-482 solution.
Continuous phase is specifically made up of the raw material of following parts by weight：658 parts of deionized water, 9,221 280 parts of Carfil, 1,
25 parts of 2- propane diols, 5 parts of glycerine, 17 parts of ursin, 21 5 parts of Carbopol Ultrez, 1 part of 250HBR, Metagin
3 parts of ester, 5 parts of AMP-95,1 part of disodium ethylene diamine tetraacetate.
The preparation process of continuous phase is：
1）The deionized water of formula ratio is added in reactor, 800 revs/min of rotating speed is controlled, sequentially adds 1,2-PD, third
Triol, ursin, disodium ethylene diamine tetraacetate and methyl hydroxybenzoate, are stirred 30 minutes；
2）The water-base resins of Carfil 9221 are added, are stirred 15 minutes；
3）Carbopol Ultrez 21 and 250HBR are slowly added to, are stirred 40 minutes；
4）Adding AMP-95 makes system pH=7 or so, stirs 30 minutes, produces white continuous phase.
A kind of preparation method of the colorful cleawhite pack of painting type, comprises the following steps：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into the S482 aqueous solution, and granulation terminates follow-up
Continuous stirring 10 minutes；
3）Continuous phase is slowly added to reactor, stirred 30 minutes with 150 revs/min of speed.Produce the colorful whitening of painting type
Facial mask 3.
Use feeling and white-skinned face function evaluation, specific test side are carried out to the embodiment 1-3 colorful cleawhite pack of painting type
Method is as follows：
Each test group chooses 20 female volunteers, and age 20-40 Sui, skin health, health is good, altogether 60 people.
Application method：Volunteer is cleaned after face, and tested facial mask is homogeneously applied to left face as test section, and right face is without surveying
Try, as a comparison area.Facial mask is thrown off after 15 minutes.Experiment facial mask is used every other day, continues after 2 months, volunteer is used
Impression investigation, evaluation is divided into 5 grades：More than 90% subject is satisfied with, and comments 5 points；80%-90% subject is satisfied with, and comments 4 points；70%-
80% subject is satisfied with, and comments 3 points；60-70% subject is satisfied with, and comments 2 points；Less than 60% subject satisfaction, 1 point is commented.Evaluation result is arranged
For table 1.
The use feeling evaluation of the colorful cleawhite pack of embodiment 1-3 of table 1.
Contrast table 1 can be seen that the made colorful cleawhite pack whitening effects of embodiment 1-3 significantly, good permeability, to skin irritatin
Property it is small, complete skin care after easily torn off from face.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, therefore it is all not
Depart from technical solution of the present invention content, according to the present invention technical spirit to it is made for any of the above embodiments it is any it is simple modification,
Equivalent variations and modification, in the range of still falling within technical solution of the present invention.
Claims (9)
1. a kind of colorful cleawhite pack of painting type, it is characterised in that：It is made up of the raw material of following parts by weight：Mix colours base-material 400-
500 parts, 300-400 parts of 200-300 parts of interleaving agent and continuous phase；Described interleaving agent is made up of the raw material of following parts by weight：Go
850-950 parts of ionized water, 50-150 parts of insulating powder, 1-3 parts of preservative；The continuous phase is made up of the raw material of following parts by weight：
600-750 parts of deionized water, 200-400 parts of water-base resin, 10-20 parts of whitening agent, 10-30 parts of NMF, 3-15 parts of thickener,
3-5 parts of preservative, 0-5 parts of pH adjusting agent, 0.2-1 parts of complexing agent.
2. the colorful cleawhite pack of painting type according to claim 1, it is characterised in that：Described insulating powder is magnesium silicate
One or more of compositions in lithium, aluminium-magnesium silicate, S482；Described preservative is Kathon CG, Phenoxyethanol, Metagin
One or more of compositions in ester, propylben.
3. the colorful cleawhite pack of painting type according to claim 1 or 2, it is characterised in that：The preparation of described interleaving agent
Process is：
1）The deionized water of formula ratio is put into reactor, 400-500 revs/min of rotating speed is controlled；
2）The insulating powder of 1/2 formula ratio and the preservative of formula ratio are put into reactor, stirring is extremely dissolved for 30-40 minutes；
3）Surplus insulating powder is put into reactor, is stirred 30-40 minutes under same rotational speed, interleaving agent is made.
4. the colorful cleawhite pack of painting type according to claim 1 or 2, it is characterised in that：Described water-base resin is
One or both of Carfil 9221 or Carfil 9220；Described whitening agent is vitamin C, ursin, glycol
One or more of compositions in acid, azalaic acid, Trenaxmine；The NMF is 1,2-PD, glycerine, second two
One or more of compositions in alcohol, sorbierite, butanediol；Described thickener is guar gum, carbomer, carboxymethyl cellulose
One or more of compositions in plain sodium, hydroxyethyl cellulose, hydroxypropyl cellulose；Described pH adjusting agent is diethanol
One or more of compositions in amine, triethanolamine, CP-950, AMP-95；Described complexing agent is ethylenediamine tetra-acetic acid two
One kind in sodium, the sodium of diethylene triamine pentacetic acid (DTPA) five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, nipalgin
One or more of compositions in propyl ester.
5. the colorful cleawhite pack of painting type according to claim 1 or 2, it is characterised in that：The preparation step of the continuous phase
Suddenly it is：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, it is beautiful
White agent, complexing agent and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener is slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces continuous phase.
6. the colorful cleawhite pack of painting type according to claim 1 or 2, it is characterised in that：The toning base-material is by following
The raw material composition of parts by weight：980-1000 parts of base-material, 0-20 parts of dyestuff；Described base-material by following parts by weight raw material group
Into：350-550 parts of deionized water, 300-500 parts of water-base resin, 50-150 parts of interleaving agent, 10-20 parts of whitening agent, NMF 10-
30 parts, 20-80 parts of thickener, 0-50 parts of pH adjusting agent, 3-5 parts of preservative, 0.2-1 parts of complexing agent；The dyestuff is eaten to be assorted
Grade or cosmetics-stage transparency dye.
7. the colorful cleawhite pack of painting type according to claim 6, it is characterised in that：In base-material, described water-base resin
For one or both of Carfil 9221 or Carfil 9220；Described whitening agent is vitamin C, ursin, sweet
One or more of compositions in alkyd, azalaic acid, Trenaxmine；The NMF is 1,2-PD, glycerine, second two
One or more of compositions in alcohol, sorbierite, butanediol；Described thickener is Aculyn 33, Vesmody
One or more of compositions in A901, Vesmody A406；Described pH adjusting agent be diethanol amine, triethanolamine,
One or more of compositions in CP-950, AMP-95；Described complexing agent is disodium ethylene diamine tetraacetate, diethylenetriamine
One kind in the sodium of pentaacetic acid five；Described preservative is Kathon CG, Phenoxyethanol, methyl hydroxybenzoate, one kind in propylben
Or several compositions.
8. the colorful cleawhite pack of painting type according to claim 6, it is characterised in that：The preparation process of described base-material
For：
1）The deionized water of formula ratio is added in reactor, 700-800 revs/min of rotating speed is controlled, sequentially adds NMF, it is beautiful
White agent, complexing agent and preservative, are stirred 30-40 minutes；
2）Water-base resin is added, is stirred 15-20 minutes；
3）Thickener and interleaving agent are slowly added to, is stirred 30-40 minutes；
4）PH adjusting agent is added, makes system pH=7, stirs 20-30 minutes, produces base-material；
The preparation process of described toning base-material is：
1）The base-material of formula ratio is added in reactor, stirred with 200-300 revs/min of speed；
2）The dyestuff of formula ratio is separately added into, stirs 20-30 minutes, produces toning base-material.
9. a kind of method of the colorful cleawhite pack of the painting type prepared as described in claim 1-2, it is characterised in that：Including as follows
The step：
1）The interleaving agent of formula ratio is added in reactor and stirred, control mixing speed is at 100-150 revs/min；
2）By the toning base-material of formula ratio by comminutor, gained particle is directly added into interleaving agent, and granulation continues to stir after terminating
Mix 10-15 minutes；
3）Continuous phase is slowly added to reactor, stirred 20-30 minutes with 100-150 revs/min of speed.Produce painting type many
Color cleawhite pack.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710539174.9A CN107137240A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful cleawhite pack of painting type and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710539174.9A CN107137240A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful cleawhite pack of painting type and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107137240A true CN107137240A (en) | 2017-09-08 |
Family
ID=59785927
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710539174.9A Pending CN107137240A (en) | 2017-07-04 | 2017-07-04 | A kind of colorful cleawhite pack of painting type and preparation method thereof |
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| Country | Link |
|---|---|
| CN (1) | CN107137240A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
| CN102772345A (en) * | 2012-06-29 | 2012-11-14 | 安徽省王巢食品有限公司 | All-natural bee pollen facial mask paste and production method thereof |
| CN103181861A (en) * | 2011-12-30 | 2013-07-03 | 广东雅威生物科技有限公司 | Bubble facial mask and preparation process thereof |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
| CN105168054A (en) * | 2015-09-17 | 2015-12-23 | 长沙九超生物科技有限公司 | Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask |
-
2017
- 2017-07-04 CN CN201710539174.9A patent/CN107137240A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1608330A1 (en) * | 2003-04-01 | 2005-12-28 | MGP Ingredients Inc | Skin-tightening preparations containing gliadin |
| CN103181861A (en) * | 2011-12-30 | 2013-07-03 | 广东雅威生物科技有限公司 | Bubble facial mask and preparation process thereof |
| CN102772345A (en) * | 2012-06-29 | 2012-11-14 | 安徽省王巢食品有限公司 | All-natural bee pollen facial mask paste and production method thereof |
| CN104688621A (en) * | 2015-03-02 | 2015-06-10 | 上海卡卡化妆品有限公司 | Self-foaming cosmetic composition and preparation method thereof |
| CN105168054A (en) * | 2015-09-17 | 2015-12-23 | 长沙九超生物科技有限公司 | Mask capable of supplementing water, whitening and removing wrinkles and preparation method of mask |
Non-Patent Citations (2)
| Title |
|---|
| 化工百科全书编委会: "《化工百科全书 第7卷 核能技术-计算机技术》", 30 September 1994, 化学工业出版社 * |
| 董艳: "《化学与健康消费》", 31 August 2008, 中国石油大学出版社 * |
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Address after: 350100 first and second floors of No.1 Workshop, No.1 East Road, phase I, Minhou economic and Technological Development Zone, Jingxi Town, Minhou County, Fuzhou City, Fujian Province Applicant after: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. Address before: Near East Taihe square in Jinan District of Fuzhou city in Fujian province 350011 SOHO office building No. 3 room 308-313 Applicant before: FUJIAN HUAXIALAN NEW MATERIAL TECHNOLOGY CO., LTD. |
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Application publication date: 20170908 |