CN107115229A - The active facial mask liquid of laminarin with anti-oxidation efficacy and preparation method - Google Patents
The active facial mask liquid of laminarin with anti-oxidation efficacy and preparation method Download PDFInfo
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- CN107115229A CN107115229A CN201710545672.4A CN201710545672A CN107115229A CN 107115229 A CN107115229 A CN 107115229A CN 201710545672 A CN201710545672 A CN 201710545672A CN 107115229 A CN107115229 A CN 107115229A
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- laminarin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8129—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal or ketal radical; Compositions of hydrolysed polymers or esters of unsaturated alcohols with saturated carboxylic acids; Compositions of derivatives of such polymers, e.g. polyvinylmethylether
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/522—Antioxidants; Radical scavengers
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Abstract
Laminarin facial mask liquid and preparation method with anti-oxidation efficacy, its component by weight percentage is：Polyvinyl alcohol 5% ~ 10%, sodium carboxymethylcellulose 0.5% ~ 2%, pearl powder 1% ~ 5%, glycerine 5% ~ 10%, absolute ethyl alcohol 7% ~ 10%, Peppermint essential oil 0.5% ~ 2%, laminarin 5% ~ 10%, deionized water 60% ~ 75%.Method and step is：（1）Sea-tangle is crushed, water-bath degreasing, filter, obtain extract；（2）Sodium carbonate liquor is added to be extracted into the extract, removing protein, then alcohol analysis is precipitated, and freeze-drying obtains laminarin；（3）Weigh polyvinyl alcohol in above-mentioned formula, plus absolute ethyl alcohol wetting, stirred in water bath dissolving；（4）Weigh the pearl powder in above-mentioned formula, sodium carboxymethylcellulose, glycerine, essential oil water-bath fully to mix, until dissolving；By above two solution mixing system into oil phase；（5）Weigh step（2）The laminarin of middle gained, is dissolved in distilled water, heating, when oil phase temperature is reduced to 50 DEG C, is added in oil phase, stirs, that is, obtain facial mask liquid.
Description
Technical field
The invention belongs to daily cosmetics field, specifically related to a kind of active facial mask of the laminarin with anti-oxidation efficacy
The preparation method of liquid.
Background technology
Sea-tangleLaminariajaponicIt is a kind of abundant tangleweed of china natural resources, is eaten and medicinal with high
Value, there is longer edible history in China.In sea-tangle containing abundant vitamin, mineral matter, protein, aliphatic acid,
The various nutritional ingredients such as laminarin and physiologically active ingredient.Wherein laminarin is the critical function material in sea-tangle, no
Only there is antitumor, hypoglycemic, reducing blood lipid, the medical health care functions such as immunity are improved, and in antiviral, antibacterial, elimination certainly
Served by base, anti-oxidant, antifatigue aspect important.
With expanding economy, the living standard of people is improved constantly, and women is also increasingly noted to skin care, facial mask
It is one of their important selection.Facial mask with various functions also arises at the historic moment, for example moisturizing, whitening, anti-oxidant etc..People
Body is because of the continuous contact with the external world, including breathing（Oxidation reaction）, the factor such as outside contamination constantly produces in body
Free radical.Scientific investigations showed that, cancer, aging or Other diseases are relevant mostly with the generation of excessive free radicals, study antioxygen
Change can effectively overcome the harm that it is brought, and be also one of most important feature demand in market.
Cosmetics brand both domestic and external is also never halted for the research and development of oxidation resistant product, the research and development to anti-oxidant face mask
It is vital, can be divided into for ingredient origin natural component source and that chemical composition is originated.From famous
SK II arrive some domestic minority's brands, have the oxidation resistant product of oneself, price is uneven, anti-oxidation efficacy also has necessarily
Difference.Generally, the good product price too expensive of anti-oxidation efficacy, compares the product anti-oxidation efficacy of par too
It is low, in addition, the relatively good facial mask excitant of some anti-oxidation efficacies is not suitable for the crowd of university's number, therefore, this hair than larger
Bright to be intended to prepare facial mask liquid by raw material of laminarin, the facial mask liquid composition is gentle, without any harmful chemicals
Matter, it is cheap and with significant anti-oxidation efficacy.
The content of the invention
It is an object of the invention to provide a kind of laminarin facial mask liquid and preparation method with anti-oxidation efficacy.
The present invention is laminarin facial mask liquid and preparation method with anti-oxidation efficacy, laminarin facial mask liquid, by weight
Percentages are measured, its component is：Polyvinyl alcohol 5% ~ 10%, sodium carboxymethylcellulose 0.5% ~ 2%, pearl powder 1% ~ 5%, glycerine 5% ~
10%, absolute ethyl alcohol 7% ~ 10%, Peppermint essential oil 0.5% ~ 2%, laminarin 5% ~ 10%, deionized water 60% ~ 75%.
The preparation method of laminarin facial mask liquid with anti-oxidation efficacy, its step is：
（1）Sea-tangle is ground into Kelp Powder, temperature is placed in carry out water-bath degreasing in 80 DEG C of thermostatted waters, filtering obtains extract；
（2）Add sodium carbonate liquor to be extracted into the extract, merge extract solution, then centrifuged, concentrated, use
Sevag methods, n-butanol: chloroform=1: 5, then removing protein is analysed with absolute ethyl alcohol alcohol, is precipitated, and freeze-drying obtains laminarin；
（3）Polyvinyl alcohol in above-mentioned formula, plus a small amount of absolute ethyl alcohol wetting are weighed, appropriate hot water is added after standing 5 min, in 75
It is sufficiently stirred in DEG C water-bath, until dissolving；
（4）Weigh the pearl powder in above-mentioned formula, sodium carboxymethylcellulose, glycerine, essential oil fully to mix in 75 DEG C of water-baths, directly
To dissolving；Above two solution is uniformly mixed while hot, oil phase is made；
（5）Weigh step（2）The laminarin of middle gained, is dissolved in appropriate distilled water, is heated to 50 DEG C, treats the reduction of oil phase temperature
During to 50 DEG C, it is added under conditions of stirring in oil phase, is stirred well to uniformly, that is, obtains facial mask liquid.
The characteristics of this product, is：All raw materials are all pure natural, and without any heavy metal, human body is not hindered
Evil.In addition, its preparation technology is simple, cost is relatively low, and antioxidant effect substantially, is applicable not only to ordinary people and used, be also suitable
In industrial production, with good Social benefit and economic benefit.
Brief description of the drawings
Fig. 1 is the measurement result that laminarin facial mask liquid embodiment 2 and Vc remove DPPH free radicals, and Fig. 2 is laminarin
Facial mask liquid embodiment 2 and Vc remove the measurement result of hydroxyl radical free radical.
Embodiment
The present invention is laminarin facial mask liquid and preparation method with anti-oxidation efficacy, laminarin facial mask liquid, by weight
Percentages are measured, its component is：Polyvinyl alcohol 5% ~ 10%, sodium carboxymethylcellulose 0.5% ~ 2%, pearl powder 1% ~ 5%, glycerine 5% ~
10%, absolute ethyl alcohol 7% ~ 10%, Peppermint essential oil 0.5% ~ 2%, laminarin 5% ~ 10%, deionized water 60% ~ 75%.
The preparation method of laminarin facial mask liquid with anti-oxidation efficacy, its step is：
（1）Sea-tangle is ground into Kelp Powder, temperature is placed in carry out water-bath degreasing in 80 DEG C of thermostatted waters, filtering obtains extract；
（2）Add sodium carbonate liquor to be extracted into the extract, merge extract solution, then centrifuged, concentrated, use
Sevag methods, n-butanol: chloroform=1: 5, then removing protein is analysed with absolute ethyl alcohol alcohol, is precipitated, and freeze-drying obtains laminarin；
（3）Polyvinyl alcohol in above-mentioned formula, plus a small amount of absolute ethyl alcohol wetting are weighed, appropriate hot water is added after standing 5 min, in 75
It is sufficiently stirred in DEG C water-bath, until dissolving；
（4）Weigh the pearl powder in above-mentioned formula, sodium carboxymethylcellulose, glycerine, essential oil fully to mix in 75 DEG C of water-baths, directly
To dissolving；Above two solution is uniformly mixed while hot, oil phase is made；
（5）Weigh step（2）The laminarin of middle gained, is dissolved in appropriate distilled water, is heated to 50 DEG C, treats the reduction of oil phase temperature
During to 50 DEG C, it is added under conditions of stirring in oil phase, is stirred well to uniformly, that is, obtains facial mask liquid.
This product facial mask liquid can invade bubble with commercially available non-woven fabrics compression facial mask, and face can be spread on after facial mask liquid by fully absorbing
Portion, facial mask is removed after 15 minutes or so, and the skin care of next step is cleaned or directly carried out by personal habits.
Further, the preferred ingredient of the laminarin facial mask liquid with anti-oxidation function of the invention is as shown in table 1：
The present invention is described in further detail with reference to embodiments.
Embodiment 1：
The laminarin facial mask with anti-oxidation efficacy of the present invention, is mainly made up by weight ratio of following components：
Polyvinyl alcohol 3g, sodium carboxymethylcellulose 0.5g, pearl powder 1g, glycerine 3g, absolute ethyl alcohol 5g, Peppermint essential oil 0.5g, sea
Band polysaccharide 3g, deionized water 40g.
The preparation method of the above-mentioned laminarin facial mask liquid with anti-oxidation efficacy, comprises the following steps：
（1）Sea-tangle crushing-Kelp Powder water bath with thermostatic control degreasing（80℃）- filtering-extract-plus sodium carbonate liquor extraction-conjunction
And Sevag methods are used in extract solution-centrifugation-concentration-（N-butanol：Chloroform=1：5）Removing protein-absolute ethyl alcohol alcohol analysis-precipitation-
Freeze-drying-laminarin；
（2）Polyvinyl alcohol in above-mentioned formula is weighed, a small amount of absolute ethyl alcohol wetting is added, appropriate hot water is added after standing 5 min, in
It is sufficiently stirred in 75 DEG C of water-baths, until dissolving；
（3）The pearl powder in above-mentioned formula, sodium carboxymethylcellulose, glycerine, Peppermint essential oil is weighed fully to mix in 75 DEG C of water-baths
It is even, until dissolving；Above two solution is uniformly mixed while hot, oil phase is made；
（4）Weigh step（1）Obtained in laminarin, be dissolved in appropriate distilled water, be heated to 50 DEG C, treat oil phase temperature drop
It is low to 50 DEG C when, add in oil phase under conditions of the stirring, be stirred well to uniform, that is, obtain facial mask liquid.
Take the facial mask liquid of above-mentioned preparation to determine its pH value, judge whether irritant.In addition, passing through the heat-resisting resistance to of facial mask liquid
Cold and centrefuge experiment judges the stability of facial mask liquid prepared, as a result proves the pH value of the facial mask liquid prepared 5.5 or so,
The excitant of facial mask liquid is assessed by 12 healthy student enrollment, prepared facial mask liquid is gently nonirritant, leads to
The heat-resisting and centrefuge experiment that resists cold is crossed, can learn that the facial mask liquid prepared according to the above method has good stability.
Table 3 is the physicochemical property of laminarin facial mask liquid：
Embodiment 2：
The laminarin facial mask with anti-oxidation efficacy of the present invention, is mainly made up by weight ratio of following components：
Polyvinyl alcohol 4g, sodium carboxymethylcellulose 1g, pearl powder 2g, glycerine 5g, absolute ethyl alcohol 6g, Peppermint essential oil 1g, sea-tangle is more
Sugared 4g, deionized water 50g.
The preparation method of the above-mentioned laminarin facial mask liquid with anti-oxidation efficacy, comprises the following steps：
（1）Sea-tangle crushing-Kelp Powder water bath with thermostatic control degreasing（80℃）- filtering-extract-plus sodium carbonate liquor extraction-conjunction
And Sevag methods are used in extract solution-centrifugation-concentration-（N-butanol：Chloroform=1：5）Removing protein-absolute ethyl alcohol alcohol analysis-precipitation-
Freeze-drying-laminarin；
（2）Polyvinyl alcohol in above-mentioned formula is weighed, a small amount of absolute ethyl alcohol wetting is added, appropriate hot water is added after standing 5 min, in
It is sufficiently stirred in 75 DEG C of water-baths, until dissolving；
（3）The pearl powder in above-mentioned formula, sodium carboxymethylcellulose, glycerine, Peppermint essential oil is weighed fully to mix in 75 DEG C of water-baths
It is even, until dissolving；Above two solution is uniformly mixed while hot, oil phase is made；
（4）Weigh step（1）Obtained in laminarin, be dissolved in appropriate distilled water, be heated to 50 DEG C, treat oil phase temperature drop
It is low to 50 DEG C when, add in oil phase under conditions of the stirring, be stirred well to uniform, that is, obtain facial mask liquid.
Take the facial mask liquid according to prepared by embodiment 2 to carry out the measure of antioxidation activity, determine clear by positive control of Vc
The activity of hydroxyl-removal free radical and DPPH free radicals, concrete operation method is as follows：
（1）The measure of DPPH radical scavenging activities：
Laminarin facial mask is made into certain density solution for standby, it is another to prepare the volume integral that DPPH concentration is 0.2 m mol/L
Number is kept in dark place for 95% ethanol solution.Draw the DPPH solution (4 that 3 mL solution to be measured is added to the m mol/L of concentration 0.2
ML in), in reacting 15 min at 25 DEG C, it is considered to which the light absorption value of analyte sample fluid in itself is different, with 4 mL distilled water with it is difference dense
The mL of sample liquid 3 is spent as the background absorption value of solution to be measured.Laminarin facial mask solution is replaced as control using distilled water,
Absorbance is determined at the nm of wavelength 520.
Clearance rate calculation formula is：
Clearance rate（%）=[A-(B-C)]/A×100%
A--- blank samples（The mL DPPH of 3.0 mL distilled water+4.0）Absorbance
B--- samples（The mL DPPH of 3.0 m L sample liquids+4.0）Reacted absorbance
C--- background groups（The mL distilled water of 3.0 m L sample liquids+4.0）Absorbance
Sample liquid is changed to the Vc solution of various concentrations into, other steps ibid, determine its light absorption value, compare laminarin facial mask with
Elimination effects of the synthetized oxidation preventive agent Vc to DPPH.
（2）Hydroxyl radical free radical Scavenging activity is determined：
Compound concentration is sample liquid 1mL, 1mL 6 containing various concentrations in 0.01-0.1mg/mL sample liquid, reaction system
mol/L H 2O2、1mL 0.15mol/LFeSO4Reaction system, wherein being eventually adding the mL of 6 mmol/L salicylic acids ethanol solution 1
Start whole reaction.After 37 DEG C of 30 min of reaction, 5000 r/min centrifuge 5 min, using distilled water as reference, under 510 nm
Determine absorbance.Consider to treat that the light absorption value of sample measuring liquid in itself is different, with 1 mL 0.15mol/L FeSO4、1mL 6 mol/L
H2O2, the mL of various concentrations sample liquid 1 and distilled water as solution to be measured background absorption value.
Clearance rate calculation formula is：
Clearance rate（%）=[A-(B-C)]/A×100%
A --- blank sample（1 mL H2O2 +1 mL FeSO4+ 1mL salicylic acids ethanol+distilled water）Absorbance；
B --- sample（1 mL sample liquids+1mLH2O2 +1 mL FeSO4+ 1 mL salicylic acids ethanol+distilled water）Extinction
Degree；
C --- background group（The mL H of 1mL sample liquids+12O2 +1 mL FeSO4 + distilled water）Absorbance.
Sample liquid is changed to the Vc solution of various concentrations into, other steps ibid, determine its light absorption value, compare sea-tangle many
Sugared facial mask and elimination effects of the synthetized oxidation preventive agent Vc to hydroxy radical.
Table 3 is that Vc removes DPPH determining free radicals results：
。
Table 4 is that laminarin facial mask liquid embodiment 2 removes DPPH determining free radicals results：
。
Table 5 is the measurement result that Vc removes hydroxyl radical free radical：
。
Table 6 is the measurement result that laminarin facial mask removes hydroxyl radical free radical：
。
The facial mask liquid of above-mentioned preparation is taken to carry out the moisture of skin of face and the measure of oil value, this experiment has randomly selected six
The healthy student enrollment of name is tested, and their face is determined respectively before non-face mask film, firm face mask film and surface application
The moisture value and oil value of film skin after one hour, under test result is as shown in table 7：
Table 7.
。
Volunteer's face moisture content value is as shown in table 8：
Table 8.
。
Can obtain the facial mask liquid of the invention prepared from the experimental result of moisture content and oil content value has obvious moisture-keeping function,
The skin of face of people can be improved by adjusting water and oil balance.
Claims (5)
1. the laminarin facial mask liquid with anti-oxidation efficacy, it is characterized in that：By weight percentage, its component is：
Polyvinyl alcohol 5% ~ 10%, sodium carboxymethylcellulose 0.5% ~ 2%, pearl powder 1% ~ 5%, glycerine 5% ~ 10%, absolute ethyl alcohol 7% ~
10%, Peppermint essential oil 0.5% ~ 2%, laminarin 5% ~ 10%, deionized water 60% ~ 75%.
2. the laminarin facial mask liquid according to claim 1 with anti-oxidation efficacy, it is characterized in that：Its preferred ingredient
For：
Polyvinyl alcohol 5.3%, sodium carboxymethylcellulose 0.9%, pearl powder 1.8%, glycerine 5.4%, absolute ethyl alcohol 8.9%, Peppermint essential oil
0.9%, laminarin 5.3%, deionized water 71.5%.
3. the laminarin facial mask liquid according to claim 1 with anti-oxidation efficacy, it is characterized in that：Its preferred ingredient
For：
Polyvinyl alcohol 5.5%, sodium carboxymethylcellulose 1.4%, pearl powder 2.7%, glycerine 6.8%, absolute ethyl alcohol 8.2%, Peppermint essential oil
1.4%, laminarin 5.0%, deionized water 69%.
4. the laminarin facial mask liquid according to claim 1 with anti-oxidation efficacy, it is characterized in that：Its preferred ingredient
For：
Polyvinyl alcohol 5.6%, sodium carboxymethylcellulose 1.7%, pearl powder 3.4%, glycerine 6.7%, absolute ethyl alcohol 7.9%, Peppermint essential oil
1.7%, laminarin 5.6%, deionized water 67.4%.
5. the preparation method of the laminarin facial mask liquid with anti-oxidation efficacy, it is characterized in that：Its step is：
（1）Sea-tangle is ground into Kelp Powder, temperature is placed in carry out water-bath degreasing in 80 DEG C of thermostatted waters, filtering obtains extract；
（2）Add sodium carbonate liquor to be extracted into the extract, merge extract solution, then centrifuged, concentrated, use
Sevag methods, n-butanol: chloroform=1: 5, then removing protein is analysed with absolute ethyl alcohol alcohol, is precipitated, and freeze-drying obtains laminarin；
（3）Polyvinyl alcohol in above-mentioned formula, plus a small amount of absolute ethyl alcohol wetting are weighed, appropriate hot water is added after standing 5 min, in 75
It is sufficiently stirred in DEG C water-bath, until dissolving；
（4）Weigh the pearl powder in above-mentioned formula, sodium carboxymethylcellulose, glycerine, essential oil fully to mix in 75 DEG C of water-baths, directly
To dissolving；Above two solution is uniformly mixed while hot, oil phase is made；
（5）Weigh step（2）The laminarin of middle gained, is dissolved in appropriate distilled water, is heated to 50 DEG C, treats the reduction of oil phase temperature
During to 50 DEG C, it is added under conditions of stirring in oil phase, is stirred well to uniformly, that is, obtains facial mask liquid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710545672.4A CN107115229A (en) | 2017-07-06 | 2017-07-06 | The active facial mask liquid of laminarin with anti-oxidation efficacy and preparation method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710545672.4A CN107115229A (en) | 2017-07-06 | 2017-07-06 | The active facial mask liquid of laminarin with anti-oxidation efficacy and preparation method |
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| CN201710545672.4A Pending CN107115229A (en) | 2017-07-06 | 2017-07-06 | The active facial mask liquid of laminarin with anti-oxidation efficacy and preparation method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109125179A (en) * | 2018-10-15 | 2019-01-04 | 华侨大学 | A kind of anti-oxidant Hydra Zen composition and preparation method thereof |
| CN110897990A (en) * | 2019-12-26 | 2020-03-24 | 姜静 | Traditional Chinese medicine mask and preparation method thereof |
-
2017
- 2017-07-06 CN CN201710545672.4A patent/CN107115229A/en active Pending
Non-Patent Citations (2)
| Title |
|---|
| 刘利萍等: "海带多糖的超声波提取及对自由基清除作用研究", 《绍兴文理学院学报》 * |
| 李泽均: "《人生的艺术：人生必备万事通》", 31 October 2005, 江西人民出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109125179A (en) * | 2018-10-15 | 2019-01-04 | 华侨大学 | A kind of anti-oxidant Hydra Zen composition and preparation method thereof |
| CN109125179B (en) * | 2018-10-15 | 2021-04-30 | 华侨大学 | Antioxidant soothing moisturizing cream composition and preparation method thereof |
| CN110897990A (en) * | 2019-12-26 | 2020-03-24 | 姜静 | Traditional Chinese medicine mask and preparation method thereof |
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Application publication date: 20170901 |