CN107099671B - One kind recovering rare earth settler from waste material mixed liquor - Google Patents
One kind recovering rare earth settler from waste material mixed liquor Download PDFInfo
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- CN107099671B CN107099671B CN201710340885.3A CN201710340885A CN107099671B CN 107099671 B CN107099671 B CN 107099671B CN 201710340885 A CN201710340885 A CN 201710340885A CN 107099671 B CN107099671 B CN 107099671B
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/006—Wet processes
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B59/00—Obtaining rare earth metals
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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Abstract
The present invention relates to a kind of settlers, more particularly to one kind recovering rare earth settler from waste material mixed liquor.The technical problem to be solved in the present invention is to provide one kind from waste material mixed liquor recovering rare earth settler.In order to solve the above-mentioned technical problems, the present invention provides such a from waste material mixed liquor recovering rare earth settler includes pretipitatin jar, agitating device, receives waste liquid device, rotary shaft I, motor I, upper and lower telescopic rod I etc.；The right side that agitating device is arranged in waste liquid device is received, rotary shaft I is provided with below pretipitatin jar, rotary shaft I is connected with pretipitatin jar, the lower section of rotary shaft I is provided with motor I, motor I is connected with rotary shaft I.One kind recovering rare earth settler from waste material mixed liquor provided by the present invention, adopts a split structure, and not only facilitates the disengaging of feed liquid, and can be stirred using various ways to feed liquid.
Description
Technical field
The present invention relates to a kind of settlers, more particularly to one kind recovering rare earth settler from waste material mixed liquor.
Background technique
Rare earth has the laudatory title of " industrial vitamin ".Nowadays extremely important strategic resource is had become.Rare earth element oxidation
Object refer to period of element atom ordinal number be 57 to 71 15 kinds of lanthanide oxides, and with lanthanide series chemical property
The oxide of similar scandium and yttrium totally 17 kinds of elements.Rare earth element is in petroleum, chemical industry, metallurgy, weaving, ceramics, glass, permanent magnetism material
Material etc. fields be all widely used, with advances in technology with the continuous breakthrough of application technology, the valence of rare earth oxide
Value will be increasing.Rare earth metal or fluoride, silicide are added in steel, can play that refining, desulfurization, to neutralize low melting point nocuousness miscellaneous
The effect of matter, and the processing performance of steel can be improved；Rare earth ferrosilicon alloy, re-si-mg alloy produce rare earth ball as nodulizer
Black cast iron is widely used in automobile, drags since this spheroidal graphite cast-iron is especially suitable for producing the complicated G. Iron Castings for having particular/special requirement
The machinery manufacturing industry such as machine drawing, diesel engine；Rare earth metal is added in the non-ferrous alloys such as magnesium, aluminium, copper, zinc, nickel, can improve alloy
Physical and chemical performance, and improve Alloy At Room Temperature and high-temperature mechanical property.Rare earth element is not rich in the ore mining in China and deposit
Richness, it is large-scale be widely applied make rare earth resources using in short supply, how to make up this vacancy, optional measure is open source nothing but
Throttling, and the recycling of rare earth waste is exactly a kind of effectively means.Precipitating refers to be carried out in a container with two kinds of solution
Reaction generates deposit, final product deposit thus.
The existing recovering rare earth settler from waste material mixed liquor, generallys use traditional structure, poor recovery effect,
Recovery efficiency is low, while structure is complicated, is easy to appear failure, and maintenance maintenance is difficult, is unfavorable for the production and development of enterprise.
Summary of the invention
(1) technical problems to be solved
The present invention generallys use traditional knot to overcome the existing recovering rare earth settler from waste material mixed liquor
Structure, poor recovery effect, the low disadvantage of recovery efficiency, the technical problem to be solved in the present invention is to provide one kind from waste material mixed liquor
Recovering rare earth settler.
(2) technical solution
In order to solve the above-mentioned technical problems, the present invention provides such a from waste material mixed liquor, and recovering rare earth precipitates
Device, include pretipitatin jar, agitating device, receive waste liquid device, rotary shaft I, motor I, upper and lower telescopic rod I, upper and lower air cylinders I, into
Feed liquid pipe and valve I；It is provided with agitating device above pretipitatin jar and receives waste liquid device, receives the setting of waste liquid device and is filled in stirring
The right side set is provided with rotary shaft I below pretipitatin jar, and rotary shaft I is connected with pretipitatin jar, sets in the lower section of rotary shaft I
It is equipped with motor I, motor I is connected with rotary shaft I, and the lower section of motor I is provided with telescopic rod I up and down, upper and lower telescopic rod I and electricity
Machine I is connected, and the lower section of upper and lower telescopic rod I is provided with upper and lower air cylinders I, and upper and lower air cylinders I are connected with upper and lower telescopic rod I,
Charging liquid pipe is provided on the left of pretipitatin jar, charging liquid pipe is connected with the left side wall top of pretipitatin jar, sets in charging liquid pipe
It is equipped with valve I.
Preferably, agitating device include upper and lower air cylinders II, upper and lower telescopic rod II, motor II, rotary shaft II, agitator disk,
Stirring rod I and stirring rod II；The lower section of upper and lower air cylinders II is provided with telescopic rod II up and down, upper and lower telescopic rod II and upper and lower air cylinders
II is connected, and the lower section of upper and lower telescopic rod II is provided with motor II, motor II is connected with upper and lower telescopic rod II, in motor II
Lower section be provided with rotary shaft II, rotary shaft II is connected with motor II, the lower section of rotary shaft II is provided with agitator disk, stir
Disk is connected with rotary shaft II, several stirring rods I and stirring rod II, stirring rod are provided in the outer circle circumferential direction of agitator disk
I upper end is set as being articulated and connected with agitator disk, and the lower end of stirring rod I and the upper end of stirring rod II are set as being articulated and connected；It stirs
Mix the top that disk, stirring rod I and stirring rod II are arranged at pretipitatin jar, agitator disk, stirring rod I and stirring rod II are and pretipitatin jar
It is corresponding.
Preferably, receiving waste liquid device includes upper and lower air cylinders III, upper and lower telescopic rod III, L shape connecting plate, valve II, waste suction
Liquid pump, waste suction liquid hose and exhausted bath box；The right side of motor II is arranged in upper and lower air cylinders III, is provided in the lower section of upper and lower air cylinders III
Upper and lower telescopic rod III, upper and lower telescopic rod III are connected with upper and lower air cylinders III, and the lower section of upper and lower telescopic rod III is provided with the connection of L shape
Plate, L shape connecting plate are connected with upper and lower telescopic rod III, and the right side of agitator disk is arranged in L shape connecting plate, under L shape connecting plate
Side is provided with waste suction liquid hose, and waste suction liquid hose is connected with L shape connecting plate, and the top of pretipitatin jar is arranged in waste suction liquid hose,
Waste suction liquid hose is set as being flexibly connected with pretipitatin jar, and the lower-left nozzle of waste suction liquid hose is corresponding with pretipitatin jar, in waste suction liquid
Valve II and waste suction liquid pump are provided on hose, the right side of L shape connecting plate is arranged in valve II, and waste suction liquid pump is arranged in valve II
Right side, exhausted bath box is provided on the right side of waste suction liquid hose, exhausted bath box is connected with waste suction liquid hose.
Preferably, further include have left and right cylinder, left and right telescopic rod, upper and lower air cylinders IV, upper and lower telescopic rod IV, dustpan, drawstring,
Pulley blocks, upper and lower telescopic rod V and upper and lower air cylinders V；The upper left side of pretipitatin jar is arranged in left and right cylinder, on the right side of left and right cylinder
It is provided with left and right telescopic rod, left and right telescopic rod is connected with left and right cylinder, is provided with upper and lower air cylinders on the right side of the telescopic rod of left and right
IV, upper and lower air cylinders IV are connected with left and right telescopic rod, and the lower section of upper and lower air cylinders IV is provided with telescopic rod IV up and down, flexible up and down
Bar IV is connected with upper and lower air cylinders IV, the lower section of upper and lower telescopic rod IV is provided with dustpan, under dustpan and upper and lower telescopic rod IV
End is set as being articulated and connected, and drawstring is provided on the right side of dustpan, the lower end of dustpan is connected with the lower end of drawstring, dustpan and drawing
The top of pretipitatin jar is arranged in rope, and dustpan and drawstring are set as being flexibly connected with pretipitatin jar, and cunning is provided on the right side of dustpan
Wheel group, pulley blocks are connected with dustpan, and drawstring is provided on pulley blocks, and drawstring is set as being flexibly connected with pulley blocks, are drawing
It is provided with telescopic rod V, drawstring up and down above rope to be connected with upper and lower telescopic rod V, is arranged in the top of upper and lower telescopic rod V
There are upper and lower air cylinders V, upper and lower air cylinders V are connected with upper and lower telescopic rod V, and the right side of upper and lower air cylinders IV is arranged in upper and lower air cylinders V,
Upper and lower air cylinders V are connected with upper and lower air cylinders IV, and the left side of agitating device is arranged in upper and lower air cylinders V and upper and lower air cylinders IV.
It preferably, further include having rewinding cylinder, pallet and universal wheel；The left side of pretipitatin jar is arranged in rewinding cylinder, and rewinding cylinder is set
It sets in the lower section of dustpan, pallet is provided with below rewinding cylinder, rewinding cylinder is set as being flexibly connected with pallet, under pallet
Side is provided with several universal wheels, and universal wheel is connected with pallet.
Preferably, the revolving speed of motor I and motor II is disposed as 800-1400r/min, and the cylinder diameter of upper and lower air cylinders I is set as
The stroke of 400-600mm, upper and lower air cylinders I are set as 8-14m.
Working principle: because the present invention include pretipitatin jar, agitating device, receive waste liquid device, rotary shaft I, motor I, on
Lower telescopic rod I, upper and lower air cylinders I, charging liquid pipe and valve I；So staff can by other conveying feed liquid equipment with into
Feed liquid pipe is attached, and then opens valve I again, a certain amount of rare earth waste mixed liquor is added in pretipitatin jar, then work
Valve I is turned off as personnel, and disconnects other conveying feed liquid equipment and feeds the connection of liquid pipe, then staff opens respectively again
Dynamic motor I and upper and lower air cylinders I, motor I drive pretipitatin jar and rare earth waste mixed liquor to be rotated together by rotary shaft I,
To be stirred to rare earth waste mixed liquor, while upper and lower air cylinders I drive the progress such as pretipitatin jar or more by upper and lower telescopic rod I
It shakes, carrying out stirring, the personnel of working at the same time up and down to rare earth waste mixed liquor can be used agitating device to dilute in pretipitatin jar
Native waste material mixed liquor is stirred, and the precipitating for subsequent rare earth particle provides convenience.When mixed to the rare earth waste in pretipitatin jar
After closing the liquid stirring regular hour, staff stands the regular hour to the rare earth waste mixed liquor in pretipitatin jar again, rare earth
Particle is precipitated out out of rare earth waste mixed liquor, and is deposited in the bottom of pretipitatin jar, and then staff passes through receipts waste liquid again
Waste liquid after precipitating is put away out of pretipitatin jar and is separately processed by device.
Because agitating device includes upper and lower air cylinders II, upper and lower telescopic rod II, motor II, rotary shaft II, agitator disk, stirring
Bar I and stirring rod II；So staff can star upper and lower air cylinders II and act, upper and lower air cylinders II pass through upper and lower telescopic rod
II drive motor II and agitator disk and stirring rod I and stirring rod II move up and down, and by agitator disk, stirring rod I and stir
It mixes bar II to move in pretipitatin jar downwardly together, then staff restarts motor II, and motor II is driven by rotary shaft II
Agitator disk, stirring rod I and stirring rod II are rotated together, stirring rod I and stirring rod II under the drive of agitator disk, due to from
The effect of mental and physical efforts is able to carry out horizontal rotation, is that rare earth particle is thorough to preferably be stirred to rare earth waste mixed liquor
Precipitation and separation provides convenience out of rare earth waste mixed liquor.
Because receiving waste liquid device includes upper and lower air cylinders III, upper and lower telescopic rod III, L shape connecting plate, valve II, waste suction liquid
Pump, waste suction liquid hose and exhausted bath box；So work as rare earth particle out of rare earth waste mixed liquor after precipitation and separation, staff
Starting upper and lower air cylinders III are acted, and upper and lower air cylinders III drive L shape connecting plate and waste suction liquid hose one by upper and lower telescopic rod III
It rises and moves up and down, and waste suction liquid hose is driven in pretipitatin jar downwards, then staff opens valve II, restarts
Waste liquid after precipitating is transported in exhausted bath box by waste suction liquid hose and is collected by waste suction liquid pump, waste suction liquid pump.
Because further including having left and right cylinder, left and right telescopic rod, upper and lower air cylinders IV, upper and lower telescopic rod IV, dustpan, drawstring, cunning
Wheel group, upper and lower telescopic rod V and upper and lower air cylinders V；So staff can star left and right cylinder and act, left and right cylinder is logical
Crossing left and right telescopic rod drives upper and lower air cylinders IV and dustpan to carry out side-to-side movement together, and dustpan is moved right the upper of pretipitatin jar
Side, then upper and lower air cylinders IV are respectively started in staff again and upper and lower air cylinders V act, upper and lower air cylinders IV and upper and lower air cylinders
V drive respectively up and down telescopic rod IV and upper and lower telescopic rod V moved downwards, and by upper and lower telescopic rod IV drive dustpan to
Under move in pretipitatin jar, when dustpan be moved downwardly to the bottom connection of pretipitatin jar touch when, staff stop upper and lower air cylinders
IV and upper and lower air cylinders V movement, then staff restarts left and right cylinder and acts, and left and right cylinder is flexible by left and right
Bar drives dustpan to be moved to the right, and dustpan pushes to the right the rare earth particle of pretipitatin jar bottom, and the personnel of working at the same time are respectively started
Upper and lower air cylinders IV and upper and lower air cylinders V are acted simultaneously, and upper and lower air cylinders V are pulled up and winnowed with a dustpan by upper and lower telescopic rod V and drawstring
Dustpan, and dustpan is pulled as horizontality, at the same upper and lower air cylinders IV drive up and down telescopic rod IV move downward, and make dustpan always
It is in contact with pretipitatin jar, therefore rare earth particle can be packed into it by dustpan, so that carry out rare earth particle collects work.
Because further including having rewinding cylinder, pallet and universal wheel, the lower section of dustpan is arranged in rewinding cylinder, so staff can
The rare earth particle in dustpan to be poured into rewinding cylinder, staff can be acted by starting left and right cylinder, and will
The dustpan for installing rare earth particle moves to the surface of rewinding cylinder, and then staff restarts upper and lower air cylinders V and acts,
Upper and lower air cylinders V drive upper and lower telescopic rod V to be moved downwards, and upper and lower telescopic rod V unclamps the drawstring hauled, and dustpan is by weight
Power effect downwardly turns over, and rare earth particle is poured into rewinding cylinder, and then staff passes through universal wheel rewinding cylinder is mobile again
To the place of needs.
Because the revolving speed of motor I and motor II is disposed as 800-1400r/min, operation is more accurate accurate, and
Staff is facilitated to adjust its revolving speed, the cylinder diameter of upper and lower air cylinders I is set as 400-600mm, and the stroke of upper and lower air cylinders I is set as 8-
14m has wide range of applications so it is safe and reliable to run smoothly.
(3) beneficial effect
One kind recovering rare earth settler from waste material mixed liquor provided by the present invention, adopts a split structure, no
But facilitate the disengaging of feed liquid, and feed liquid can be stirred using various ways, is conducive to the precipitation and separation of rare earth particle,
It is good to the recovering effect of rare earth particle high-efficient, it economizes on resources, convenient for carrying out recycling purification to rare earth particle and carrying out secondary benefit
With, structure is simple, it runs smoothly reliable, maintenance easy to maintain.
Detailed description of the invention
Fig. 1 is main view schematic diagram of the invention.
Fig. 2 is the main view schematic diagram of left and right cylinder of the invention.
Fig. 3 is the main view schematic diagram of rewinding cylinder of the invention.
The label in accompanying drawing is: 1- pretipitatin jar, 2- agitating device, 3- receive waste liquid device, 4- rotary shaft I, 5- motor I, 6-
Upper and lower telescopic rod I, 7- upper and lower air cylinders I, 8- feed liquid pipe, 9- valve I, 21- upper and lower air cylinders II, 22- or more telescopic rod II, 23-
Motor II, 24- rotary shaft II, 25- agitator disk, 26- stirring rod I, 27- stirring rod II, 31- upper and lower air cylinders III, 32- or more are flexible
Bar III, 33-L shape connecting plate, 34- valve II, 35- waste suction liquid pump, 36- waste suction liquid hose, 37- exhausted bath box, 41- left and right cylinder,
42- or so telescopic rod, 43- upper and lower air cylinders IV, 44- or more telescopic rod IV, 45- dustpan, 46- drawstring, 47- pulley blocks, 48- or more
Telescopic rod V, 49- upper and lower air cylinders V, 51- rewinding cylinder, 52- pallet, 53- universal wheel.
Specific embodiment
The present invention is further illustrated with reference to the accompanying drawings and examples.
Embodiment 1
One kind recovering rare earth settler from waste material mixed liquor, as shown in Figure 1-3, include pretipitatin jar 1, stirring dress
It sets 2, receive waste liquid device 3, rotary shaft I 4, motor I 5, upper and lower telescopic rod I 6, upper and lower air cylinders I 7, charging liquid pipe 8 and valve I 9；?
The top of pretipitatin jar 1 is provided with agitating device 2 and receives waste liquid device 3, receives the right side that agitating device 2 is arranged in waste liquid device 3,
The lower section of pretipitatin jar 1 is provided with rotary shaft I 4, and rotary shaft I 4 is connected with pretipitatin jar 1, and the lower section of rotary shaft I 4 is provided with electricity
Machine I 5, motor I 5 are connected with rotary shaft I 4, and the lower section of motor I 5 is provided with telescopic rod I 6 up and down, upper and lower telescopic rod I 6 and electricity
Machine I 5 is connected, and the lower section of upper and lower telescopic rod I 6 is provided with upper and lower air cylinders I 7, upper and lower air cylinders I 7 are connected with upper and lower telescopic rod I 6
It connects, the left side of pretipitatin jar 1 is provided with charging liquid pipe 8, charging liquid pipe 8 is connected with the left side wall top of pretipitatin jar 1, is feeding
Valve I 9 is provided in liquid pipe 8.
Embodiment 2
One kind recovering rare earth settler from waste material mixed liquor, as shown in Figure 1-3, include pretipitatin jar 1, stirring dress
It sets 2, receive waste liquid device 3, rotary shaft I 4, motor I 5, upper and lower telescopic rod I 6, upper and lower air cylinders I 7, charging liquid pipe 8 and valve I 9；?
The top of pretipitatin jar 1 is provided with agitating device 2 and receives waste liquid device 3, receives the right side that agitating device 2 is arranged in waste liquid device 3,
The lower section of pretipitatin jar 1 is provided with rotary shaft I 4, and rotary shaft I 4 is connected with pretipitatin jar 1, and the lower section of rotary shaft I 4 is provided with electricity
Machine I 5, motor I 5 are connected with rotary shaft I 4, and the lower section of motor I 5 is provided with telescopic rod I 6 up and down, upper and lower telescopic rod I 6 and electricity
Machine I 5 is connected, and the lower section of upper and lower telescopic rod I 6 is provided with upper and lower air cylinders I 7, upper and lower air cylinders I 7 are connected with upper and lower telescopic rod I 6
It connects, the left side of pretipitatin jar 1 is provided with charging liquid pipe 8, charging liquid pipe 8 is connected with the left side wall top of pretipitatin jar 1, is feeding
Valve I 9 is provided in liquid pipe 8.
Agitating device 2 includes upper and lower air cylinders II 21, upper and lower telescopic rod II 22, motor II 23, rotary shaft II 24, agitator disk
25, stirring rod I 26 and stirring rod II 27；The lower section of upper and lower air cylinders II 21 is provided with telescopic rod II 22 up and down, upper and lower telescopic rod
II 22 are connected with upper and lower air cylinders II 21, and the lower section of upper and lower telescopic rod II 22 is provided with motor II 23, motor II 23 and up and down
Telescopic rod II 22 is connected, and the lower section of motor II 23 is provided with rotary shaft II 24, and rotary shaft II 24 is connected with motor II 23,
The lower section of rotary shaft II 24 is provided with agitator disk 25, agitator disk 25 is connected with rotary shaft II 24, in the outer circle of agitator disk 25
Several stirring rods I 26 and stirring rod II 27 are provided in circumferential direction, upper end and the agitator disk 25 of stirring rod I 26 are set as hinged
Connection, the lower end of stirring rod I 26 and the upper end of stirring rod II 27 are set as being articulated and connected；Agitator disk 25, stirring rod I 26 and stirring
Bar II 27 is arranged at the top of pretipitatin jar 1, and agitator disk 25, stirring rod I 26 and stirring rod II 27 are corresponding with pretipitatin jar 1.
Embodiment 3
One kind recovering rare earth settler from waste material mixed liquor, as shown in Figure 1-3, include pretipitatin jar 1, stirring dress
It sets 2, receive waste liquid device 3, rotary shaft I 4, motor I 5, upper and lower telescopic rod I 6, upper and lower air cylinders I 7, charging liquid pipe 8 and valve I 9；?
The top of pretipitatin jar 1 is provided with agitating device 2 and receives waste liquid device 3, receives the right side that agitating device 2 is arranged in waste liquid device 3,
The lower section of pretipitatin jar 1 is provided with rotary shaft I 4, and rotary shaft I 4 is connected with pretipitatin jar 1, and the lower section of rotary shaft I 4 is provided with electricity
Machine I 5, motor I 5 are connected with rotary shaft I 4, and the lower section of motor I 5 is provided with telescopic rod I 6 up and down, upper and lower telescopic rod I 6 and electricity
Machine I 5 is connected, and the lower section of upper and lower telescopic rod I 6 is provided with upper and lower air cylinders I 7, upper and lower air cylinders I 7 are connected with upper and lower telescopic rod I 6
It connects, the left side of pretipitatin jar 1 is provided with charging liquid pipe 8, charging liquid pipe 8 is connected with the left side wall top of pretipitatin jar 1, is feeding
Valve I 9 is provided in liquid pipe 8.
Agitating device 2 includes upper and lower air cylinders II 21, upper and lower telescopic rod II 22, motor II 23, rotary shaft II 24, agitator disk
25, stirring rod I 26 and stirring rod II 27；The lower section of upper and lower air cylinders II 21 is provided with telescopic rod II 22 up and down, upper and lower telescopic rod
II 22 are connected with upper and lower air cylinders II 21, and the lower section of upper and lower telescopic rod II 22 is provided with motor II 23, motor II 23 and up and down
Telescopic rod II 22 is connected, and the lower section of motor II 23 is provided with rotary shaft II 24, and rotary shaft II 24 is connected with motor II 23,
The lower section of rotary shaft II 24 is provided with agitator disk 25, agitator disk 25 is connected with rotary shaft II 24, in the outer circle of agitator disk 25
Several stirring rods I 26 and stirring rod II 27 are provided in circumferential direction, upper end and the agitator disk 25 of stirring rod I 26 are set as hinged
Connection, the lower end of stirring rod I 26 and the upper end of stirring rod II 27 are set as being articulated and connected；Agitator disk 25, stirring rod I 26 and stirring
Bar II 27 is arranged at the top of pretipitatin jar 1, and agitator disk 25, stirring rod I 26 and stirring rod II 27 are corresponding with pretipitatin jar 1.
Waste liquid device 3 is received to include upper and lower air cylinders III 31, upper and lower telescopic rod III 32, L shape connecting plate 33, valve II 34, inhale
Waste drains pump 35, waste suction liquid hose 36 and exhausted bath box 37；The right side of motor II 23 is arranged in upper and lower air cylinders III 31, in upper and lower air cylinders III
31 lower section is provided with telescopic rod III 32 up and down, and upper and lower telescopic rod III 32 is connected with upper and lower air cylinders III 31, in upper and lower telescopic rod
III 32 lower section is provided with L shape connecting plate 33, and L shape connecting plate 33 is connected with upper and lower telescopic rod III 32, and L shape connecting plate 33 is arranged
On the right side of agitator disk 25, the lower section of L shape connecting plate 33 is provided with waste suction liquid hose 36, waste suction liquid hose 36 is connect with L shape
Plate 33 is connected, and the top of pretipitatin jar 1 is arranged in waste suction liquid hose 36, and waste suction liquid hose 36 and pretipitatin jar 1 are set as activity even
It connects, the lower-left nozzle of waste suction liquid hose 36 is corresponding with pretipitatin jar 1, is provided with valve II 34 and waste suction on waste suction liquid hose 36
The right side of L shape connecting plate 33 is arranged in liquid pump 35, valve II 34, and the right side of valve II 34 is arranged in waste suction liquid pump 35, in waste suction
The right side of liquid hose 36 is provided with exhausted bath box 37, and exhausted bath box 37 is connected with waste suction liquid hose 36.
Embodiment 4
One kind recovering rare earth settler from waste material mixed liquor, as shown in Figure 1-3, include pretipitatin jar 1, stirring dress
It sets 2, receive waste liquid device 3, rotary shaft I 4, motor I 5, upper and lower telescopic rod I 6, upper and lower air cylinders I 7, charging liquid pipe 8 and valve I 9；?
The top of pretipitatin jar 1 is provided with agitating device 2 and receives waste liquid device 3, receives the right side that agitating device 2 is arranged in waste liquid device 3,
The lower section of pretipitatin jar 1 is provided with rotary shaft I 4, and rotary shaft I 4 is connected with pretipitatin jar 1, and the lower section of rotary shaft I 4 is provided with electricity
Machine I 5, motor I 5 are connected with rotary shaft I 4, and the lower section of motor I 5 is provided with telescopic rod I 6 up and down, upper and lower telescopic rod I 6 and electricity
Machine I 5 is connected, and the lower section of upper and lower telescopic rod I 6 is provided with upper and lower air cylinders I 7, upper and lower air cylinders I 7 are connected with upper and lower telescopic rod I 6
It connects, the left side of pretipitatin jar 1 is provided with charging liquid pipe 8, charging liquid pipe 8 is connected with the left side wall top of pretipitatin jar 1, is feeding
Valve I 9 is provided in liquid pipe 8.
Agitating device 2 includes upper and lower air cylinders II 21, upper and lower telescopic rod II 22, motor II 23, rotary shaft II 24, agitator disk
25, stirring rod I 26 and stirring rod II 27；The lower section of upper and lower air cylinders II 21 is provided with telescopic rod II 22 up and down, upper and lower telescopic rod
II 22 are connected with upper and lower air cylinders II 21, and the lower section of upper and lower telescopic rod II 22 is provided with motor II 23, motor II 23 and up and down
Telescopic rod II 22 is connected, and the lower section of motor II 23 is provided with rotary shaft II 24, and rotary shaft II 24 is connected with motor II 23,
The lower section of rotary shaft II 24 is provided with agitator disk 25, agitator disk 25 is connected with rotary shaft II 24, in the outer circle of agitator disk 25
Several stirring rods I 26 and stirring rod II 27 are provided in circumferential direction, upper end and the agitator disk 25 of stirring rod I 26 are set as hinged
Connection, the lower end of stirring rod I 26 and the upper end of stirring rod II 27 are set as being articulated and connected；Agitator disk 25, stirring rod I 26 and stirring
Bar II 27 is arranged at the top of pretipitatin jar 1, and agitator disk 25, stirring rod I 26 and stirring rod II 27 are corresponding with pretipitatin jar 1.
Waste liquid device 3 is received to include upper and lower air cylinders III 31, upper and lower telescopic rod III 32, L shape connecting plate 33, valve II 34, inhale
Waste drains pump 35, waste suction liquid hose 36 and exhausted bath box 37；The right side of motor II 23 is arranged in upper and lower air cylinders III 31, in upper and lower air cylinders III
31 lower section is provided with telescopic rod III 32 up and down, and upper and lower telescopic rod III 32 is connected with upper and lower air cylinders III 31, in upper and lower telescopic rod
III 32 lower section is provided with L shape connecting plate 33, and L shape connecting plate 33 is connected with upper and lower telescopic rod III 32, and L shape connecting plate 33 is arranged
On the right side of agitator disk 25, the lower section of L shape connecting plate 33 is provided with waste suction liquid hose 36, waste suction liquid hose 36 is connect with L shape
Plate 33 is connected, and the top of pretipitatin jar 1 is arranged in waste suction liquid hose 36, and waste suction liquid hose 36 and pretipitatin jar 1 are set as activity even
It connects, the lower-left nozzle of waste suction liquid hose 36 is corresponding with pretipitatin jar 1, is provided with valve II 34 and waste suction on waste suction liquid hose 36
The right side of L shape connecting plate 33 is arranged in liquid pump 35, valve II 34, and the right side of valve II 34 is arranged in waste suction liquid pump 35, in waste suction
The right side of liquid hose 36 is provided with exhausted bath box 37, and exhausted bath box 37 is connected with waste suction liquid hose 36.
It further include having left and right cylinder 41, left and right telescopic rod 42, upper and lower air cylinders IV 43, upper and lower telescopic rod IV 44, dustpan 45, drawing
Rope 46, pulley blocks 47, upper and lower telescopic rod V 48 and upper and lower air cylinders V 49；The upper left side of pretipitatin jar 1 is arranged in left and right cylinder 41,
The right side of left and right cylinder 41 is provided with left and right telescopic rod 42, and left and right telescopic rod 42 is connected with left and right cylinder 41, flexible in left and right
The right side of bar 42 is provided with upper and lower air cylinders IV 43, and upper and lower air cylinders IV 43 are connected with left and right telescopic rod 42, in upper and lower air cylinders IV 43
Lower section be provided with up and down telescopic rod IV 44, upper and lower telescopic rod IV 44 is connected with upper and lower air cylinders IV 43, in upper and lower telescopic rod IV
44 lower section is provided with dustpan 45, and dustpan 45 and the lower end of upper and lower telescopic rod IV 44 are set as being articulated and connected, on the right side of dustpan 45
Side is provided with drawstring 46, and the lower end of dustpan 45 is connected with the lower end of drawstring 46, and pretipitatin jar 1 is arranged in dustpan 45 and drawstring 46
Top, dustpan 45 and drawstring 46 are set as being flexibly connected with pretipitatin jar 1, and the right side of dustpan 45 is provided with pulley blocks 47, sliding
Wheel group 47 is connected with dustpan 45, and drawstring 46 is provided on pulley blocks 47, and drawstring 46 is set as being flexibly connected with pulley blocks 47,
The top of drawstring 46 is provided with telescopic rod V 48 up and down, drawstring 46 is connected with upper and lower telescopic rod V 48, in upper and lower telescopic rod
V 48 top is provided with upper and lower air cylinders V 49, and upper and lower air cylinders V 49 are connected with upper and lower telescopic rod V 48, upper and lower air cylinders V 49
The right side of upper and lower air cylinders IV 43 is set, upper and lower air cylinders V 49 are connected with upper and lower air cylinders IV 43, upper and lower air cylinders V 49 and up and down
The left side of agitating device 2 is arranged in cylinder IV 43.
It further include having rewinding cylinder 51, pallet 52 and universal wheel 53；The left side of pretipitatin jar 1, rewinding cylinder is arranged in rewinding cylinder 51
51 are arranged in the lower section of dustpan 45, the lower section of rewinding cylinder 51 are provided with pallet 52, rewinding cylinder 51 and pallet 52 are set as activity
Connection, is provided with several universal wheels 53 in the lower section of pallet 52, universal wheel 53 is connected with pallet 52.
The revolving speed of motor I 5 and motor II 23 is disposed as 800-1400r/min, and the cylinder diameter of upper and lower air cylinders I 7 is set as
The stroke of 400-600mm, upper and lower air cylinders I 7 are set as 8-14m.
Working principle: because the present invention includes pretipitatin jar 1, agitating device 2, receives waste liquid device 3, rotary shaft I 4, motor I
5, upper and lower telescopic rod I 6, upper and lower air cylinders I 7, charging liquid pipe 8 and valve I 9；So staff can pass through other conveying feed liquids
Equipment is attached with charging liquid pipe 8, then opens valve I 9 again, a certain amount of rare earth waste mixed liquor is added to pretipitatin jar
In 1, then staff turns off valve I 9, and disconnects other conveying feed liquid equipment and feed the connection of liquid pipe 8, then works
Motor I 5 and upper and lower air cylinders I 7 is respectively started in personnel again, and motor I 5 drives pretipitatin jar 1 and rare earth waste mixed by rotary shaft I 4
It closes liquid to be rotated together, to be stirred rare earth waste mixed liquor, while upper and lower air cylinders I 7 pass through upper and lower telescopic rod I 6
It drives pretipitatin jar 1 etc. to teetertotter, stirring up and down is carried out to rare earth waste mixed liquor, the personnel of working at the same time, which can be used, to be stirred
It mixes device 2 to be stirred the rare earth waste mixed liquor in pretipitatin jar 1, the precipitating for subsequent rare earth particle provides convenience.When
After stirring the regular hour to the rare earth waste mixed liquor in pretipitatin jar 1, staff is mixed to the rare earth waste in pretipitatin jar 1 again
It closing liquid and stands the regular hour, rare earth particle is precipitated out out of rare earth waste mixed liquor, and is deposited in the bottom of pretipitatin jar 1,
Then staff passes through again receives waste liquid device 3 and puts the waste liquid after precipitating away out of pretipitatin jar 1 and separately process.
Because agitating device 2 includes upper and lower air cylinders II 21, upper and lower telescopic rod II 22, motor II 23, rotary shaft II 24, stirs
Mix disk 25, stirring rod I 26 and stirring rod II 27；So staff can star upper and lower air cylinders II 21 and act, upper and lower gas
Cylinder II 21 drives motor II 23 and agitator disk 25 and stirring rod I 26 and stirring rod II 27 to carry out by upper and lower telescopic rod II 22
It moves up and down, and agitator disk 25, stirring rod I 26 and stirring rod II 27 is moved to downwardly together in pretipitatin jar 1, then work people
Member restarts motor II 23, and motor II 23 drives agitator disk 25, stirring rod I 26 and stirring rod II 27 together by rotary shaft II 24
It is rotated, stirring rod I 26 and stirring rod II 27 due to the effect of centrifugal force, are able to carry out water under the drive of agitator disk 25
Flat rotation is that rare earth particle thoroughly divides out of rare earth waste mixed liquor to preferably be stirred to rare earth waste mixed liquor
Convenience is provided from precipitating.
Because receiving waste liquid device 3 includes upper and lower air cylinders III 31, upper and lower telescopic rod III 32, L shape connecting plate 33, valve II
34, waste suction liquid pump 35, waste suction liquid hose 36 and exhausted bath box 37；So working as rare earth particle precipitation and separation out of rare earth waste mixed liquor
After, staff starts upper and lower air cylinders III 31 and acts, and upper and lower air cylinders III 31 drive L shape by upper and lower telescopic rod III 32
Connecting plate 33 and waste suction liquid hose 36 move up and down together, and waste suction liquid hose 36 is driven into pretipitatin jar 1 downwards, so
Staff opens valve II 34 afterwards, restarts waste suction liquid pump 35, waste suction liquid pump 35 is finished precipitating by waste suction liquid hose 36
Waste liquid afterwards is transported in exhausted bath box 37 and collects.
Because further including having left and right cylinder 41, left and right telescopic rod 42, upper and lower air cylinders IV 43, upper and lower telescopic rod IV 44, dustpan
45, drawstring 46, pulley blocks 47, upper and lower telescopic rod V 48 and upper and lower air cylinders V 49；So staff can star left and right cylinder
41 are acted, and left and right cylinder 41 drives upper and lower air cylinders IV 43 and dustpan 45 to carry out left and right fortune together by left and right telescopic rod 42
Dynamic, and dustpan 45 is moved right to the top of pretipitatin jar 1, then upper and lower air cylinders IV 43 and up and down are respectively started in staff again
Cylinder V 49 is acted, and upper and lower air cylinders IV 43 and upper and lower air cylinders V 49 drive telescopic rod IV 44 and upper and lower telescopic rod up and down respectively
V 48 are moved downwards, and by upper and lower telescopic rod IV 44 drive dustpan 45 be moved downwardly in pretipitatin jar 1, when dustpan 45 to
Under move to the bottom connection of pretipitatin jar 1 touch when, staff stop upper and lower air cylinders IV 43 and upper and lower air cylinders V 49 movement,
Then staff restarts left and right cylinder 41 and acts, and left and right cylinder 41 drives dustpan 45 to the right by left and right telescopic rod 42
It is moved, dustpan 45 pushes to the right the rare earth particle of 1 bottom of pretipitatin jar, and upper and lower air cylinders IV 43 are respectively started in the personnel of working at the same time
It is acted simultaneously with upper and lower air cylinders V 49, upper and lower air cylinders V 49 pull up dustpan by upper and lower telescopic rod V 48 and drawstring 46
45, and dustpan 45 is pulled as horizontality, at the same upper and lower air cylinders IV 43 drive up and down telescopic rod IV 44 move downward, and make to winnow with a dustpan
Dustpan 45 is in contact with pretipitatin jar 1 always, and therefore rare earth particle can be packed into it by dustpan 45, to carry out the receipts of rare earth particle
Take work.
Because further including having rewinding cylinder 51, pallet 52 and universal wheel 53, the lower section of dustpan 45 is arranged in rewinding cylinder 51, so
Rare earth particle in dustpan 45 can be poured into rewinding cylinder 51 by staff, and staff can be by starting left and right cylinder
41 are acted, and the dustpan 45 for installing rare earth particle is moved to the surface of rewinding cylinder 51, and then staff restarts
Upper and lower air cylinders V 49 are acted, and telescopic rod V 48 is moved downwards the drive of upper and lower air cylinders V 49 up and down, upper and lower telescopic rod V
48 unclamp the drawstring 46 hauled, and dustpan 45 is downwardly turned over by gravity, rare earth particle is poured into rewinding cylinder 51, then
Staff passes through the place that rewinding cylinder 51 is moved to needs by universal wheel 53 again.
Because the revolving speed of motor I 5 and motor II 23 is disposed as 800-1400r/min, operation is more accurate accurate,
And staff is facilitated to adjust its revolving speed, the cylinder diameter of upper and lower air cylinders I 7 is set as 400-600mm, the stroke setting of upper and lower air cylinders I 7
It has wide range of applications for 8-14m so it is safe and reliable to run smoothly.
The preferred embodiment of the present invention above described embodiment only expresses, the description thereof is more specific and detailed, but simultaneously
Limitations on the scope of the patent of the present invention therefore cannot be interpreted as.It should be pointed out that for those of ordinary skill in the art
For, without departing from the inventive concept of the premise, several deformations can also be made, improves and substitutes, these belong to this hair
Bright protection scope.Therefore, the scope of protection of the patent of the invention shall be subject to the appended claims.
Claims (4)
1. one kind recovering rare earth settler from waste material mixed liquor, which is characterized in that include pretipitatin jar (1), stirring dress
It sets (2), receive waste liquid device (3), rotary shaft I (4), motor I (5), upper and lower telescopic rod I (6), upper and lower air cylinders I (7), charging liquid pipe
(8) and valve I (9)；It is provided with agitating device (2) above pretipitatin jar (1) and receives waste liquid device (3), receives waste liquid device (3)
Right side in agitating device (2) is set, rotary shaft I (4), rotary shaft I (4) and pretipitatin jar are provided with below pretipitatin jar (1)
(1) it is connected, motor I (5) is provided with below rotary shaft I (4), motor I (5) is connected with rotary shaft I (4), in motor I
(5) telescopic rod I (6) up and down is provided with below, upper and lower telescopic rod I (6) is connected with motor I (5), in upper and lower telescopic rod I (6)
Lower section be provided with upper and lower air cylinders I (7), upper and lower air cylinders I (7) are connected with upper and lower telescopic rod I (6), in the left side of pretipitatin jar (1)
It is provided with charging liquid pipe (8), charging liquid pipe (8) is connected with the left side wall top of pretipitatin jar (1), sets in charging liquid pipe (8)
It is equipped with valve I (9)；Agitating device (2) includes upper and lower air cylinders II (21), upper and lower telescopic rod II (22), motor II (23), rotation
Axis II (24), agitator disk (25), stirring rod I (26) and stirring rod II (27)；It is provided with below upper and lower air cylinders II (21)
Lower telescopic rod II (22), upper and lower telescopic rod II (22) are connected with upper and lower air cylinders II (21), under upper and lower telescopic rod II (22)
Side is provided with motor II (23), and motor II (23) is connected with upper and lower telescopic rod II (22), is arranged in the lower section of motor II (23)
There is rotary shaft II (24), rotary shaft II (24) is connected with motor II (23), and stirring is provided with below rotary shaft II (24)
Disk (25), agitator disk (25) are connected with rotary shaft II (24), are provided with several in the outer circle circumferential direction of agitator disk (25)
Stirring rod I (26) and stirring rod II (27), upper end and the agitator disk (25) of stirring rod I (26) are set as being articulated and connected, stirring rod I
(26) lower end and the upper end of stirring rod II (27) are set as being articulated and connected；Agitator disk (25), stirring rod I (26) and stirring rod II
(27) be arranged at the top of pretipitatin jar (1), agitator disk (25), stirring rod I (26) and stirring rod II (27) with pretipitatin jar (1)
It is corresponding；Receiving waste liquid device (3) includes upper and lower air cylinders III (31), upper and lower telescopic rod III (32), L shape connecting plate (33), valve
II (34), waste suction liquid pump (35), waste suction liquid hose (36) and exhausted bath box (37)；Upper and lower air cylinders III (31) are arranged in motor II (23)
Right side, telescopic rod III (32) up and down, upper and lower telescopic rod III (32) and upper and lower gas are provided with below upper and lower air cylinders III (31)
Cylinder III (31) is connected, and is provided with L shape connecting plate (33) below upper and lower telescopic rod III (32), L shape connecting plate (33) with it is upper
Lower telescopic rod III (32) is connected, and L shape connecting plate (33) is arranged on the right side of agitator disk (25), under L shape connecting plate (33)
Side is provided with waste suction liquid hose (36), and waste suction liquid hose (36) is connected with L shape connecting plate (33), waste suction liquid hose (36) setting
In the top of pretipitatin jar (1), waste suction liquid hose (36) is set as being flexibly connected with pretipitatin jar (1), a left side for waste suction liquid hose (36)
Lower nozzle is corresponding with pretipitatin jar (1), and valve II (34) and waste suction liquid pump (35), valve are provided on waste suction liquid hose (36)
On the right side of L shape connecting plate (33), waste suction liquid pump (35) setting is soft in waste suction liquid on the right side of valve II (34) for II (34) setting
It is provided with exhausted bath box (37) on the right side of pipe (36), exhausted bath box (37) is connected with waste suction liquid hose (36).
2. one kind recovering rare earth settler from waste material mixed liquor according to claim 1, which is characterized in that also wrap
Left and right cylinder (41), left and right telescopic rod (42), upper and lower air cylinders IV (43), upper and lower telescopic rod IV (44), dustpan (45), drawstring are included
(46), pulley blocks (47), upper and lower telescopic rod V (48) and upper and lower air cylinders V (49)；Left and right cylinder (41) is arranged in pretipitatin jar (1)
Upper left side, be provided on the right side of left and right cylinder (41) left and right telescopic rod (42), left and right telescopic rod (42) and left and right cylinder
(41) it is connected, upper and lower air cylinders IV (43) is provided on the right side of left and right telescopic rod (42), upper and lower air cylinders IV (43) is stretched with left and right
Contracting bar (42) is connected, and telescopic rod IV (44) up and down, upper and lower telescopic rod IV (44) are provided with below upper and lower air cylinders IV (43)
Be connected with upper and lower air cylinders IV (43), be provided with below upper and lower telescopic rod IV (44) dustpan (45), dustpan (45) and up and down
The lower end of telescopic rod IV (44) is set as being articulated and connected, and is provided on the right side of dustpan (45) drawstring (46), under dustpan (45)
End is connected with the lower end of drawstring (46), and dustpan (45) and drawstring (46) setting are in the top of pretipitatin jar (1), dustpan (45) and drawing
Rope (46) is set as being flexibly connected with pretipitatin jar (1), is provided on the right side of dustpan (45) pulley blocks (47), pulley blocks (47)
It is connected with dustpan (45), is provided on pulley blocks (47) drawstring (46), drawstring (46) and pulley blocks (47) is set as activity
Connection is provided with telescopic rod V (48), drawstring (46) up and down above drawstring (46) and is connected with upper and lower telescopic rod V (48),
Upper and lower air cylinders V (49), upper and lower air cylinders V (49) and upper and lower telescopic rod V (48) are provided with above upper and lower telescopic rod V (48)
It is connected, upper and lower air cylinders V (49) setting is in the right side of upper and lower air cylinders IV (43), upper and lower air cylinders V (49) and upper and lower air cylinders IV
(43) it is connected, upper and lower air cylinders V (49) and upper and lower air cylinders IV (43) are arranged in the left side of agitating device (2).
3. one kind recovering rare earth settler from waste material mixed liquor according to claim 2, which is characterized in that also wrap
Rewinding cylinder (51), pallet (52) and universal wheel (53) are included；Rewinding cylinder (51) is arranged in the left side of pretipitatin jar (1), rewinding cylinder
(51) it is arranged in the lower section of dustpan (45), is provided with below rewinding cylinder (51) pallet (52), rewinding cylinder (51) and pallet
(52) it is set as being flexibly connected, several universal wheels (53), universal wheel (53) and pallet is provided with below pallet (52)
(52) it is connected.
4. one kind recovering rare earth settler from waste material mixed liquor according to claim 3, which is characterized in that motor
The revolving speed of I (5) and motor II (23) is disposed as 800-1400r/min, and the cylinder diameter of upper and lower air cylinders I (7) is set as 400-
The stroke of 600mm, upper and lower air cylinders I (7) are set as 8-14m.
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| CN201710340885.3A CN107099671B (en) | 2017-05-16 | 2017-05-16 | One kind recovering rare earth settler from waste material mixed liquor |
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| CN201710340885.3A CN107099671B (en) | 2017-05-16 | 2017-05-16 | One kind recovering rare earth settler from waste material mixed liquor |
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| CN107586974A (en) * | 2017-09-30 | 2018-01-16 | 无锡市稀土永磁厂 | The rare-earth precipitation extraction element of subsidiary rabbling mechanism |
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| JP5283783B2 (en) * | 2010-04-21 | 2013-09-04 | 春男 上原 | Rare metal recovery method and apparatus |
| CN201890910U (en) * | 2010-11-30 | 2011-07-06 | 清远市嘉禾稀有金属有限公司 | Rare earth ore coprecipitation settling device |
| JP5516534B2 (en) * | 2011-08-22 | 2014-06-11 | 住友金属鉱山株式会社 | Nickel recovery loss reduction method, nickel oxide ore hydrometallurgy method, and sulfurization treatment system |
| CN205759833U (en) * | 2016-06-21 | 2016-12-07 | 赣县鑫亿化工有限公司 | A kind of ammonium chloride crystals body Stirring formula collection device |
| CN205761202U (en) * | 2016-06-22 | 2016-12-07 | 信丰县包钢新利稀土有限责任公司 | A kind of double salt of rare earth solution rapid precipitation reaction unit |
| CN106179169A (en) * | 2016-09-09 | 2016-12-07 | 深圳市福田区青少年科技教育协会 | A kind of rare earth uniform stirring highly effective reaction still |
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