CN107057906A - A kind of grape wine and its production method rich in OPC - Google Patents
A kind of grape wine and its production method rich in OPC Download PDFInfo
- Publication number
- CN107057906A CN107057906A CN201710318811.XA CN201710318811A CN107057906A CN 107057906 A CN107057906 A CN 107057906A CN 201710318811 A CN201710318811 A CN 201710318811A CN 107057906 A CN107057906 A CN 107057906A
- Authority
- CN
- China
- Prior art keywords
- grape
- opc
- pip
- rich
- wine
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12G—WINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
- C12G1/00—Preparation of wine or sparkling wine
- C12G1/02—Preparation of must from grapes; Must treatment and fermentation
- C12G1/0203—Preparation of must from grapes; Must treatment and fermentation by microbiological or enzymatic treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Microbiology (AREA)
- Molecular Biology (AREA)
- Biochemistry (AREA)
- Bioinformatics & Cheminformatics (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Biotechnology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
98% grape seed extract, sucrose and zymosan is no less than the invention discloses a kind of grape wine rich in OPC, including grape berry, procyanidin content.The invention also discloses a kind of production method of grape wine rich in OPC, including：Fresh grape is removed the peel and gone grape pip, and obtained grape berry is smashed to pieces, obtain grape slurry；Using above-mentioned grape pip as raw material, grape seed extract is extracted from the grape pip；Grape seed extract, sucrose and zymosan are added in the grape slurry obtained after being smashed to pieces to the grape berry, and is fermented, fermentation process continues at least 5 days；The separation of grape wine and material residue is carried out after the fermentation has been completed, and the grape wine after separation is moved into storage tank carrying out the old stage.The present invention improves the content of grape wine procyanidins, enhances the health-care effect of grape wine, eliminates the fermented flavour that the bitter taste and fermentation process of grape pip are produced, substantially increases the mouthfeel of grape wine.
Description
Technical field
The present invention relates to wine production technical field, it is more particularly related to a kind of rich in OPC
Grape wine and its production method.
Background technology
Research in recent years shows that the natural plant extracts containing polyphenols show stronger oxidation resistance, to people
Body health produces wholesome effect.Wherein flavone compound OPC is increasingly subject to the concern of people, after grinding for many years
Study carefully exploitation, the superior antioxidant capacity of OPC and free radical scavenging activity are approved for people, and it is in medicine, health care, food
Have been widely used Deng having in field.
OPC is widely present in plant, the rich content particularly in the kind skin of grape pip.Each position of grape
All contain phenols chemical analysis in various degree, with going deep into for research, lot of domestic and international it was discovered by researchers that in grape pip
Polyphenols natural content or species are all more far richer than Grape Skin and grape berry, these polyphenol in seed
Class material exhibits have gone out extremely strong oxidation resistance, can be dissolved in wine liquid during wine brewing and occur the change of numerous and complicated
Change, these changes not only influence the appearance luster and taste flavor of grape wine, and influence its alimentary health-care function.
Because OPC has many physiological activities to human body, the external performance study for OPC compares
It is many, and it is widely used in food, beverage, cosmetics and field of health care products, play anti-oxidant, anti-corrosion, extension Shelf-life of Food-a Review
And the effect of beauty, anti-aging.But the fermented flavour produced in grape pip bitter taste in itself and Fermentation of Grape Wine can shadow
Ring mouthfeel.The content of OPC in the grape seed extract extracted from discarded object grape pip simultaneously need to be improved.
The content of the invention
It is an object of the invention to solve at least the above, and provide the advantage that at least will be described later.
It is a still further object of the present invention to provide a kind of grape wine rich in OPC, grape wine Central Plains flower is improved
The content of blue or green element, improves the health-care effect of grape wine, while improving the extraction process and grape wine of grape seed extract
Production process so that the fermented flavour in eliminating the bitter taste and fermentation process of the grape pip in grape wine, is substantially increased
The mouthfeel of grape wine, and realize the OPC that high content is extracted from discarded grape pip.
To achieve these goals, the invention provides a kind of grape wine rich in OPC, including grape berry, original
Anthocyanidin content is no less than 98% grape seed extract, sucrose and zymosan.
Preferably, wherein, the parts by weight of each component are in grape wine：
90~100 parts of grape berry, procyanidin content is no less than 98% 1~18 part of grape seed extract, sucrose 25
~150 parts, 0.4~0.8 part of zymosan.
Present invention also offers a kind of production method of grape wine rich in OPC, comprise the following steps：
Step 1: grape pip is removed the peel and gone to fresh grape, and obtained grape berry is smashed to pieces, obtained
Grape slurry；
Step 2: using grape pip as raw material, grape seed extract is extracted from the grape pip, and ensure the grape pip
The content of extract procyanidins is no less than 98%；
Step 3: adding 1~18 part of OPC in the grape slurry obtained after being smashed to pieces to 90~100 parts of grape berries
Content is no less than 98% grape seed extract, 25~150 portions of sucrose and 0.4~0.8 part of zymosan, and uses natural ferment
Female bacterium or the saccharomycetes to make fermentation manually added, fermentation process continue at least 5 days；
Step 4: carrying out the separation of grape wine and material residue after the fermentation has been completed, and the grape wine after separation is moved into storage tank
Carry out the old stage.
Preferably, wherein, in the step 2, using grape pip as raw material, extract procyanidin content be no less than 98%
The detailed process of grape seed extract be：
S1, using pressafiner grape pip is rolled, and collect slag charge, the slag charge is carried out using water extraction
Extract, obtain extract solution, the extract solution is filtered, and collect filtrate；
S2, using macromolecular resin the filtrate is adsorbed, reuse ethanol and eluted, collected rich in former cyanine
The eluent of element；
S3, the eluent rich in OPC is centrifuged and centrifugate is collected, use PSPP
Tubular ultra-filtration membrane centrifugate is filtered successively, and collect permeate；
S4, separation concentration is carried out to the permeate, carried so as to obtain procyanidin content no less than 98% grape pip
Take thing.
Preferably, wherein, in the S3, first by tubular type ultrafiltration of the molecule interception between 10000~20000
Film is filtered to the centrifugate, obtains efflux；Reuse tubular ultra-filtration membrane of the molecule interception between 1000~2000
The efflux is filtered, permeate is obtained.
Preferably, wherein, in the S1, obtained after being rolled using pressafiner to grape pip particle diameter for 40~
The slag charge of 50 mesh.
Preferably, wherein, in the S1, the extract solution is filtered using microfiltration membranes and milipore filter successively, from
And obtain filtrate.
The present invention at least includes following beneficial effect：
1st, the grape wine of the present invention rich in OPC by using procyanidin content higher in the feed
Grape seed extract, so as to substantially increase the content of grape wine procyanidins, improves the healthcare function of grape wine, daily
The amount of drinking is the function that 50~100mL can be realized as health care.
2nd, the grape wine of the present invention rich in OPC extracts grape pip by improving from discarded grape pip
The extraction process of extract, so as to improve the content of the OPC of grape seed extract, and combines the fermentation of grape wine
Journey, produces the grape wine for having obtained in good taste, full aroma, being of high nutritive value, and raw material drawing is convenient, saved grape
The production cost of wine, can realize the industrialized production of grape wine.
Further advantage, target and the feature of the present invention embodies part by following explanation, and part will also be by this
The research and practice of invention and be understood by the person skilled in the art.
Embodiment
With reference to specific embodiment, the present invention is described in further detail, to make those skilled in the art's reference say
Bright book word can be implemented according to this.
It should be appreciated that such as " having ", "comprising" and " comprising " term used herein are not precluded from one or many
The presence or addition of individual other elements or its combination.
Embodiment 1：
A kind of grape wine rich in OPC, wherein containing 90 parts of grape berries, procyanidin content is 99% Portugal
18 parts of grape seed extract, 150 parts of sucrose, 0.8 part of zymosan.
Production method of grape wine rich in OPC is：
1st, fresh grape is removed the peel and gone grape pip, and obtained grape berry is smashed to pieces, obtain grape
Slurry；
2nd, using grape pip as raw material, the grape seed extract in grape pip is extracted, and ensure in the grape seed extract
The content of OPC is 99%；
3rd, it is 99% that 18 parts of procyanidin contents are added in the grape slurry obtained after being smashed to pieces to 90 parts of grape berries
Grape seed extract, 150 portions of sucrose and 0.8 part of zymosan, and sent out using unartificial yeast bacterium or the saccharomycete manually added
Ferment, fermentation process continues 10 days；
4th, carry out the separation of grape wine and material residue after the fermentation has been completed, and by the grape wine after separation move to storage tank carry out it is old
Stage in year.
The extraction process for the grape seed extract that procyanidin content is 99% is：
(1), rolled using pressafiner is a certain degree of to grape pip progress, remove juice, and collect slag charge, used
Water extraction is extracted to the slag charge of 40 mesh, obtains extract solution, and extract solution is filtered using microfiltration membranes and milipore filter successively,
And collect filtrate；
(2), filtrate is adsorbed using macromolecular resin, reuses ethanol and is eluted, collects and is rich in OPC
Eluent；
(3), the eluent rich in OPC is centrifuged and centrifugate is collected, is existed first by molecule interception
20000 tubular ultra-filtration membrane is filtered to the centrifugate, obtains efflux；The tubular type that molecule interception is reused 2000 surpasses
Filter membrane is filtered to the efflux, obtains permeate；
(4) separation concentration, is carried out to permeate, so as to obtain the grape seed extract that procyanidin content is 99%.
Embodiment 2：
A kind of grape wine rich in OPC, wherein containing 100 parts of grape berries, 10 parts of procyanidin contents are
99.5% grape seed extract, 25 portions of sucrose, 0.4 part of zymosan.
Production method of grape wine rich in OPC is：
1st, fresh grape is removed the peel and gone grape pip, and obtained grape berry is smashed to pieces, obtain grape
Slurry；
2nd, using grape pip as raw material, grape seed extract is extracted from the grape pip, and ensure that the grape pip is extracted
The content of thing procyanidins is 99.5%；
3rd, it is 99.5% that 10 parts of procyanidin contents are added in the grape slurry obtained after being smashed to pieces to 100 parts of grape berries
Grape seed extract, 25 portions of sucrose and 0.4 part of zymosan, and use unartificial yeast bacterium or the saccharomycete manually added to send out
Ferment, fermentation process continues 8 days；
4th, carry out the separation of grape wine and material residue after the fermentation has been completed, and by the grape wine after separation move to storage tank carry out it is old
Stage in year.
The detailed process for the grape seed extract that procyanidin content is 99.5% is：
(1), grape pip is rolled using pressafiner, the slag charge of 40 mesh is obtained, using water extraction to 40 purposes
Slag charge is extracted, and obtains extract solution, is filtered successively using microfiltration membranes and milipore filter extract solution, and collect filtrate；
(2), the filtrate is adsorbed using macromolecular resin, reuses ethanol and is eluted, is collected rich in former flower
The eluent of blue or green element；
(3), the eluent rich in OPC is centrifuged and centrifugate is collected, is existed first by molecule interception
15000 tubular ultra-filtration membrane is filtered to the centrifugate, obtains efflux；The tubular type that molecule interception is reused 1500 surpasses
Filter membrane is filtered to the efflux, obtains permeate；
(4) separation concentration, is carried out to permeate, so as to obtain the grape seed extract that procyanidin content is 99.5%.
Embodiment 3：
A kind of grape wine rich in OPC, specific containing 95 parts of grape berries, 16 parts of procyanidin contents are
99.7% grape seed extract, 120 portions of sucrose, 0.7 part of zymosan.
Production method of grape wine rich in OPC is：
1st, fresh grape is removed the peel and gone grape pip, and obtained grape berry is smashed to pieces, obtain grape
Slurry；
2nd, using grape pip as raw material, grape seed extract is extracted from grape pip, and ensure that grape seed extract Central Plains is spent
The content of blue or green element is 99.7%；
3rd, the Portugal that 16 parts of procyanidin contents are 99.7% is added in the grape slurry obtained after being smashed to pieces to 95 parts of grape berries
Grape seed extract, 120 portions of sucrose and 0.7 part of zymosan, and using unartificial yeast bacterium or the saccharomycetes to make fermentation manually added,
Fermentation process continues 12 days；
4th, carry out the separation of grape wine and material residue after the fermentation has been completed, and by the grape wine after separation move to storage tank carry out it is old
Stage in year.
The extraction process for the grape seed extract that procyanidin content is 99.7% is：
(1), grape pip is rolled using pressafiner, the slag charge of 50 mesh is obtained, using water extraction to 50 purposes
Slag charge is extracted, and obtains extract solution, extract solution is filtered using microfiltration membranes and milipore filter successively, and collect filtrate；
(2), filtrate is adsorbed using macromolecular resin, reuses ethanol and is eluted, collects and is rich in OPC
Eluent；
(3), the eluent rich in OPC is centrifuged and centrifugate is collected, is existed first by molecule interception
10000 tubular ultra-filtration membrane is filtered to the centrifugate, obtains efflux；The tubular type that molecule interception is reused 1000 surpasses
Filter membrane is filtered to the efflux, obtains permeate；
(4) separation concentration, is carried out to permeate, so as to obtain the grape seed extract that procyanidin content is 99.7%.
After being preserved 3 months to the grape wine that embodiment 1~3 is produced, the trial test of aesthetic quality is carried out, through produced by the invention
The mouthfeel of grape wine is full, gives off a strong fragrance, and the purity height of grape seed extract and the content of OPC are high, eliminate because of Portugal
The bitter taste of the not high grape wine caused of the purity of grape seed extract, improves the nutritive value and healthcare function of grape wine, together
When screw press not only hard grape pip has been carried out certain broken, be easy to water extraction process below, and by Portugal
The kernel of grape seed is extruded, and eliminates the grease contained in grape pip, so as to ensure that the purity of the extraction of OPC
With the content of extraction, while coordinating the macromolecules adsorption behind water extraction, the filtering of tubular ultra-filtration membrane and separation concentration, obtain
The grape seed extract of the OPC of high content.
Although embodiment of the present invention is disclosed as above, it is not restricted in specification and embodiment listed
With it can be applied to various suitable the field of the invention completely, can be easily for those skilled in the art
Other modification is realized, therefore under the universal limited without departing substantially from claim and equivalency range, the present invention is not limited
In specific details.
Claims (7)
1. a kind of grape wine rich in OPC, it is characterised in that be no less than 98% including grape berry, procyanidin content
Grape seed extract, sucrose and zymosan.
2. a kind of grape wine rich in OPC according to claim 1, it is characterised in that including following parts by weight
Component：
90~100 parts of grape berry, procyanidin content is no less than 98% 1~18 part of grape seed extract, sucrose 25~150
Part, 0.4~0.8 part of zymosan.
3. a kind of method of the grape wine rich in OPC produced according to claim 1~2 any one, its feature
It is, comprises the following steps：
Step 1: grape pip is removed the peel and gone to fresh grape, and obtained grape berry is smashed to pieces, obtain grape
Slurry；
Step 2: using grape pip as raw material, grape seed extract is extracted from the grape pip, and ensure that the grape pip is extracted
The content of thing procyanidins is no less than 98%；
Step 3: adding 1~18 part of procyanidin content in the grape slurry obtained after being smashed to pieces to 90~100 parts of grape berries
Grape seed extract, 25~150 portions of sucrose and 0.4~0.8 part of zymosan no less than 98%, and use unartificial yeast bacterium
Or the saccharomycetes to make fermentation manually added, fermentation process continues at least 5 days；
Step 4: carrying out the separation of grape wine and material residue after the fermentation has been completed, and the grape wine after separation is moved into storage tank progress
The old stage.
4. a kind of production method of grape wine rich in OPC according to claim 3, it is characterised in that the step
In rapid two, using grape pip as raw material, the detailed process for extracting grape seed extract of the procyanidin content no less than 98% is：
S1, using pressafiner grape pip is rolled, and collect slag charge, the slag charge is carried using water extraction
Take, obtain extract solution, the extract solution is filtered, and collect filtrate；
S2, using macromolecular resin the filtrate is adsorbed, reuse ethanol and eluted, collected rich in OPC
Eluent；
S3, the eluent rich in OPC is centrifuged and centrifugate is collected, use the pipe of PSPP
Formula milipore filter is filtered successively to centrifugate, and collects permeate；
S4, to the permeate carry out separation concentration so that obtain procyanidin content be no less than 98% grape seed extract.
5. a kind of production method of grape wine rich in OPC according to claim 4, it is characterised in that the S3
In, the centrifugate is filtered first by tubular ultra-filtration membrane of the molecule interception between 10000~20000, must be flowed
Go out liquid；Reuse tubular ultra-filtration membrane of the molecule interception between 1000~2000 to filter the efflux, obtain
Cross liquid.
6. a kind of production method of grape wine rich in OPC according to claim 4, it is characterised in that the S1
In, the slag charge that particle diameter is 40~50 mesh is obtained after being rolled using pressafiner to grape pip.
7. a kind of production method of grape wine rich in OPC according to claim 4, it is characterised in that the S1
In, the extract solution is filtered using microfiltration membranes and milipore filter successively, so as to obtain filtrate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710318811.XA CN107057906A (en) | 2017-05-08 | 2017-05-08 | A kind of grape wine and its production method rich in OPC |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710318811.XA CN107057906A (en) | 2017-05-08 | 2017-05-08 | A kind of grape wine and its production method rich in OPC |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107057906A true CN107057906A (en) | 2017-08-18 |
Family
ID=59596083
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710318811.XA Pending CN107057906A (en) | 2017-05-08 | 2017-05-08 | A kind of grape wine and its production method rich in OPC |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107057906A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107400590A (en) * | 2017-09-28 | 2017-11-28 | 久为利华（天津）文化发展有限公司 | Wine-making technique rich in anthocyanidin |
| CN107552536A (en) * | 2017-09-05 | 2018-01-09 | 贵州慧静生物科技有限公司 | Grape wine waste residue integrated extraction technique |
| CN110272791A (en) * | 2019-08-02 | 2019-09-24 | 马祖生物科技(福建)有限责任公司 | A kind of processing method of brandy |
| CN113831995A (en) * | 2021-08-06 | 2021-12-24 | 劲牌有限公司 | Composition with enhanced stability of content of active ingredients of compound wine and application thereof |
| CN114736760A (en) * | 2022-03-18 | 2022-07-12 | 浙江工商大学 | Preparation method of instant red wine |
| CN115404138A (en) * | 2022-10-31 | 2022-11-29 | 西夫拉姆酒业集团有限公司 | Method for brewing grape wine rich in procyanidine |
| CN116042336A (en) * | 2023-03-14 | 2023-05-02 | 西夫拉姆酒业集团有限公司 | Method for brewing grape wine rich in procyanidine |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101125844A (en) * | 2007-09-28 | 2008-02-20 | 天津市尖峰天然产物研究开发有限公司 | Method for extracting procyanidins B2 |
| CN101633873A (en) * | 2009-08-25 | 2010-01-27 | 天津市尖峰天然产物研究开发有限公司 | Grape wine added with procyanidin B2 and preparation method |
-
2017
- 2017-05-08 CN CN201710318811.XA patent/CN107057906A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101125844A (en) * | 2007-09-28 | 2008-02-20 | 天津市尖峰天然产物研究开发有限公司 | Method for extracting procyanidins B2 |
| CN101633873A (en) * | 2009-08-25 | 2010-01-27 | 天津市尖峰天然产物研究开发有限公司 | Grape wine added with procyanidin B2 and preparation method |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107552536A (en) * | 2017-09-05 | 2018-01-09 | 贵州慧静生物科技有限公司 | Grape wine waste residue integrated extraction technique |
| CN107400590A (en) * | 2017-09-28 | 2017-11-28 | 久为利华（天津）文化发展有限公司 | Wine-making technique rich in anthocyanidin |
| CN110272791A (en) * | 2019-08-02 | 2019-09-24 | 马祖生物科技(福建)有限责任公司 | A kind of processing method of brandy |
| CN113831995A (en) * | 2021-08-06 | 2021-12-24 | 劲牌有限公司 | Composition with enhanced stability of content of active ingredients of compound wine and application thereof |
| CN113831995B (en) * | 2021-08-06 | 2023-07-25 | 劲牌有限公司 | Composition capable of enhancing content stability of active ingredients of compound wine and application thereof |
| CN114736760A (en) * | 2022-03-18 | 2022-07-12 | 浙江工商大学 | Preparation method of instant red wine |
| CN115404138A (en) * | 2022-10-31 | 2022-11-29 | 西夫拉姆酒业集团有限公司 | Method for brewing grape wine rich in procyanidine |
| CN116042336A (en) * | 2023-03-14 | 2023-05-02 | 西夫拉姆酒业集团有限公司 | Method for brewing grape wine rich in procyanidine |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107057906A (en) | A kind of grape wine and its production method rich in OPC | |
| CN101285023B (en) | Red raspberry health wine and brewing process thereof | |
| CN101156704B (en) | Rosa roxburghii pollen honey Rosa roxburghii juice beverage | |
| CN104232422A (en) | Brewing method of blueberry fruit wine | |
| KR100701587B1 (en) | Manufacturing method of sparassis crispa an extract and sparassis crispa alcoholic drinks using of sparassis crispa an extract | |
| CN100350849C (en) | Green tea beverage, and its prepn. method | |
| CN101313766A (en) | Black-fruit matrimony vine fruit juice concentrate and preparation method | |
| CN107557224B (en) | Hovenia acerba and Chinese wolfberry health wine and brewing method thereof | |
| CN101245302A (en) | Method for preparing alcoholic beverage using incubated wild ginseng root | |
| CN104845858A (en) | Production technology of alcohol-free wolfberry fruit wine | |
| CN112852573A (en) | Lycium ruthenicum wine, preparation method thereof and compound wine | |
| CN107183462B (en) | Mulberry enzyme beverage and preparation method thereof | |
| JP7211637B2 (en) | Method for producing grape wine vinegar and grape wine vinegar using the same | |
| CN105907529B (en) | Roxburgh rose and black tea wine and preparation method thereof | |
| CN105950350A (en) | Mulberry wine making method | |
| CN110004011B (en) | Solid-liquid fermentation combined mulberry wine formula and preparation method | |
| CN101560451B (en) | Method for producing peach dry wine | |
| CN106947654A (en) | A kind of blue Red Hill raisin wine of ganoderma lucidum snow and preparation method thereof | |
| CN103773660A (en) | Manufacturing method of ginkgo health-care wine | |
| CN107475034B (en) | Preparation method of storage-resistant composite fruit wine | |
| CN108048290A (en) | A kind of cyanine wine and preparation method thereof | |
| JP2000135071A (en) | Food or pharmaceutical composition containing wine strained lee extract | |
| CN101560449B (en) | Method for producing peach sweet wine | |
| CN105695207A (en) | Hibiscus sabdariffa-grape composite fruit wine and production method thereof | |
| CN111647492A (en) | Radix puerariae and bamboo leaf green wine and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170818 |
|
| RJ01 | Rejection of invention patent application after publication |