CN107021626A - A kind of blue glaze of golden spot - Google Patents
A kind of blue glaze of golden spot Download PDFInfo
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- CN107021626A CN107021626A CN201710375268.7A CN201710375268A CN107021626A CN 107021626 A CN107021626 A CN 107021626A CN 201710375268 A CN201710375268 A CN 201710375268A CN 107021626 A CN107021626 A CN 107021626A
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- glaze
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- spot
- powder
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2204/00—Glasses, glazes or enamels with special properties
- C03C2204/04—Opaque glass, glaze or enamel
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2209/00—Compositions specially applicable for the manufacture of vitreous glazes
- C03C2209/02—Compositions specially applicable for the manufacture of vitreous glazes to produce non-uniformly coloured glazes
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Glass Compositions (AREA)
Abstract
A kind of blue glaze of golden spot, it is prepared from by the raw material of following parts by weight：62 68 parts of melilite, 10 16 parts of quartz, 12 18 parts of calcite, 1.5 2.5 parts of tin oxide, 0.5 1.5 parts of spot fossil, 0.5 1.5 parts of bovine bone powder, 1.5 2.5 parts of talcum, blue 0.5 1.5 parts of powder.The present invention is compared with prior art, pass through scientific and reasonable raw material proportioning and control burning process, having prepared glaze has the blue glaze of golden spot, blank of the blue glaze without golden spot has been filled up, has been that blue glaze pottery adds a new varieties, and the gorgeous jade-like stone of the blue glaze of golden spot prepared using the present invention is moistened, glaze is pin-free, lack the situation of glaze, firing temperature is easy to control, high yield rate, up to more than 90%.
Description
Technical field
The present invention relates to a kind of glaze, and in particular to a kind of blue glaze of golden spot.
Background technology
Pottery is one of five big kiln porcelain of China's Song Dynasty, the treasure in Chinese tradition technology in producing porcelain, with unique transmutation
Art and be renown far and wide in generation, be the exclusive national treasure porcelain in Henan Province Xuchang Yuzhou City god Hou towns." blue glaze " its glaze colours in pottery is blue
Such as deep-sea, glaze is uniform, in colour-stable, but the blue glaze glaze colours that the existing glaze formula and firing process for firing blue glaze burns out
Single, glaze is without golden spot.
The content of the invention
The purpose of the present invention is that provides a kind of golden spot blue glaze to solve the deficiencies in the prior art.
The purpose of the present invention is realized with following technical proposals：
A kind of blue glaze of golden spot, it is prepared from by the raw material of following parts by weight：62-68 parts of melilite, 10-16 parts of quartz, side
Solve 12-18 parts of stone, 1.5-2.5 parts of tin oxide, 0.5-1.5 parts of spot fossil, 0.5-1.5 parts of bovine bone powder, 1.5-2.5 parts of talcum, orchid
0.5-1.5 parts of powder.
The blue glaze of above-mentioned golden spot, wherein, it is prepared from by the raw material of following parts by weight：65 parts of melilite, quartz 13
Part, 15 parts of calcite, 2 parts of tin oxide, 1 part of spot fossil, 1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.
The blue powder is by cobalt oxide with local soil type of Datong District into the mass ratio of the cobalt oxide and Datong District's soil is 1:(9-11).
The blue powder is calcined 4-6h at 1150-1250 DEG C after cobalt oxide and Datong District's soil mixing and formed.
The preparation method of the blue glaze of above-mentioned golden spot, wherein, comprise the following steps：
（1）Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
（2）Glazing；
（3）Burn till, firing temperature is 1240-1280 DEG C.
The preparation method of the blue glaze of above-mentioned golden spot, wherein, step（3）Middle firing process is comprised the following steps that：After glazing
Base substrate be put into kiln, temperature is ramped up 1240-1280 DEG C in 2-3h；It is warming up to after 1240-1280 DEG C and starts cooling,
First 750-800 DEG C is cooled to 6-8 DEG C per minute；Then room temperature is naturally cooled to.
The preparation method of the blue glaze of above-mentioned golden spot, wherein, the firing atmosphere burnt till is oxygen atmosphere.
The present invention is using melilite as primary solvent, and melilite compares for example white feldspar of other feldspars, red feldspar, silicon, iron content
It is higher, the glossiness of pottery jade glaze can be improved, and also iron content is high, it is easier to and the formation of golden spot, calcite plays hydrotropy,
Quartz can improve the mobility of glaze, and tin oxide is assistant toner, and spot fossil is a kind of poor iron ore containing iron oxide, be cosolvent and
Colouring agent, cyan can be showed and go out cash spot, the main calcic of bovine bone powder and phosphorus by being fired under high temperature and certain atmosphere, can be carried
The opacity of high glaze, talcum is natural hydrous magnesium silicate mineral, is the cosolvent of glaze, by increasing capacitance it is possible to increase the opaque of chun glaze；It is blue
Powder is burnt till under the native high temperature of cobalt oxide and Datong District, is also a kind of colouring agent.Melilite, calcite, quartzy spot in the present invention
Fossil originates from Yuzhou.
The present invention compared with prior art, by scientific and reasonable raw material proportioning and control burning process, has prepared glaze
Face has the blue glaze of golden spot, has filled up blank of the blue glaze without golden spot, is that blue glaze pottery adds a new varieties, and utilize
The gorgeous jade-like stone profit of the blue glaze of golden spot that the present invention is prepared, glaze is pin-free, lack the situation of glaze, and firing temperature is easy to control, yield rate
Height, up to more than 90%.
Brief description of the drawings
Fig. 1 is the golden spot blue glaze glaze schematic diagram of pottery that the embodiment of the present invention 2 is obtained.
Embodiment
Embodiment 1
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：62-68 parts of melilite, 10-16 parts of quartz, calcite
12-18 parts, 1.5-2.5 parts of tin oxide, 0.5-1.5 parts of lithosporic, 0.5-1.5 parts of bovine bone powder, 1.5-2.5 parts of talcum, Lan Fen
0.5-1.5 parts.
The blue powder is by cobalt oxide with local soil type of Datong District into the mass ratio of the cobalt oxide and Datong District's soil is 1:(9-11).
The blue powder is calcined 4-6h at 1150-1250 DEG C after cobalt oxide and Datong District's soil mixing and formed.
The preparation method of the above-mentioned blue glaze of golden spot, comprises the following steps：
（1）Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 150 mesh sieves, obtain glaze slip；
（2）The glazing by the way of leaching glaze on base substrate after biscuiting；
（3）Burn till, firing temperature is 1240-1280 DEG C；Specifically include following steps：Base substrate after glazing is put into kiln,
Temperature is set to be ramped up 1240-1280 DEG C in 2-3h；It is warming up to after 1240-1280 DEG C and starts cooling, first with 6-8 DEG C per minute drop
Temperature is to 750-800 DEG C；Then room temperature is naturally cooled to.The firing atmosphere entirely burnt till is oxygen atmosphere.
Embodiment 2
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：65 parts of melilite, 13 parts of quartz, 15 parts of calcite, oxygen
Change 2 parts of tin, lithosporicization 1,1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.
The preparation method of the above-mentioned blue glaze of golden spot, comprises the following steps：
（1）Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 150 mesh sieves, obtain glaze slip；
（2）The glazing by the way of leaching glaze on base substrate after biscuiting；
（3）Burn till, firing temperature is 1260 DEG C；Specifically include following steps：Base substrate after glazing is put into kiln, makes temperature
1260 DEG C are ramped up in 2.5h；It is warming up to after 1260 DEG C and starts cooling, is first cooled to 780 DEG C with 7 DEG C per minute；Then it is natural
It is cooled to room temperature.The firing atmosphere entirely burnt till is oxygen atmosphere.
The blue glaze glaze of golden spot obtained using said ratio and method is as shown in figure 1, the gorgeous jade-like stone profit of its glaze colours, Lan Rushen
Sea, glaze is pin-free, lack the situation of glaze, and firing temperature is easy to control, and yield rate reaches more than 92%.
Embodiment 3
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：65 parts of melilite, 13 parts of quartz, 15 parts of calcite, oxygen
Change 2 parts of tin, lithosporicization 1,1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.
The preparation method of the above-mentioned blue glaze of golden spot, comprises the following steps：
（1）Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 150 mesh sieves, obtain glaze slip；
（2）The glazing by the way of leaching glaze on base substrate after biscuiting；
（3）Burn till, firing temperature is 1280 DEG C；Specifically include following steps：Base substrate after glazing is put into kiln, makes temperature
1280 DEG C are ramped up in 2h；It is warming up to after 1280 DEG C and starts cooling, is first cooled to 800 DEG C with 8 DEG C per minute；Then it is naturally cold
But to room temperature.The firing atmosphere entirely burnt till is oxygen atmosphere.
The gorgeous jade-like stone profit of pottery glaze colours obtained using said ratio and method, it is blue such as deep-sea, the feelings of pin-free, the scarce glaze of glaze
Condition, firing temperature is easy to control, and yield rate is 90% or so.
Embodiment 4
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：65 parts of melilite, 13 parts of quartz, 15 parts of calcite, oxygen
Change 2 parts of tin, lithosporicization 1,1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.
The preparation method of the above-mentioned blue glaze of golden spot, comprises the following steps：
（4）Take the raw material of above-mentioned parts by weight to add water and be put into ball milling in ball mill, cross 150 mesh sieves, obtain glaze slip；
（5）The glazing by the way of leaching glaze on base substrate after biscuiting；
（6）Burn till, firing temperature is 1240 DEG C；Specifically include following steps：Base substrate after glazing is put into kiln, makes temperature
1240 DEG C are ramped up in 3h；It is warming up to after 1240 DEG C and starts cooling, is first cooled to 750 DEG C with 6 DEG C per minute；Then it is naturally cold
But to room temperature.The firing atmosphere entirely burnt till is oxygen atmosphere.
The gorgeous jade-like stone profit of pottery glaze colours obtained using said ratio and method, it is blue such as deep-sea, the feelings of pin-free, the scarce glaze of glaze
Condition, firing temperature is easy to control, and yield rate is 91% or so.
Embodiment 5
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：62 parts of melilite, 16 parts of quartz, 17 parts of calcite, oxygen
Change 2 parts of tin, lithosporicization 1,1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.
The gorgeous jade-like stone profit of pottery glaze colours obtained using said ratio and method, it is blue such as deep-sea, the feelings of pin-free, the scarce glaze of glaze
Condition, firing temperature is easy to control, and yield rate is 90% or so.
Comparative example 1
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：Red 65 parts of feldspar, 13 parts of quartz, 15 parts of calcite, oxygen
Change 2 parts of tin, 1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.Preparation method be the same as Example 2.This example compared with Example 2, is not used
Spot fossil, and melilite is changed to red feldspar, the glaze that red feldspar makes easily is precipitated, and firing glaze texture is poor, and red length
Iron content in stone is relatively seldom, and iron oxide content is few in raw material, burns out glaze and occurs without golden spot, and yield rate only has
60% or so.
Comparative example 2
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：65 parts of melilite, 13 parts of quartz, 15 parts of calcite, oxygen
Change 2 parts of tin, lithosporicization 1,1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.This preparation method and the preparation method in embodiment 2
Compare, firing atmosphere is changed to reducing atmosphere, the pottery glaze colours yellowing prepared using the method in the present embodiment, glaze is without gold
Spot occurs, and yield rate only has 10% or so.
Comparative example 3
A kind of blue glaze of golden spot, is prepared from by the raw material of following parts by weight：65 parts of melilite, 13 parts of quartz, 15 parts of calcite, oxygen
Change 2 parts of tin, lithosporicization 1,1 part of bovine bone powder, 2 parts of talcum.Compared with Example 2, orchid powder, the pottery glaze of firing is not used in this example
Though there is a small amount of golden spot to occur, glaze colours is in cinerous, and pottery yield rate is 70% or so.
The blue glaze formula of an ancient unit of weight that 6-21 of the embodiment of the present invention is provided is shown in Table 1-2.
Claims (7)
1. a kind of blue glaze of golden spot, it is characterised in that：It is prepared from by the raw material of following parts by weight：62-68 parts of melilite, stone
10-16 parts of English, 12-18 parts of calcite, 1.5-2.5 parts of tin oxide, 0.5-1.5 parts of spot fossil, 0.5-1.5 parts of bovine bone powder, talcum
1.5-2.5 parts, blue 0.5-1.5 parts of powder.
2. the blue glaze of gold spot as claimed in claim 1, it is characterised in that：It is prepared from by the raw material of following parts by weight：It is yellow
65 parts of feldspar, 13 parts of quartz, 15 parts of calcite, 2 parts of tin oxide, 1 part of spot fossil, 1 part of bovine bone powder, 2 parts of talcum, blue 1 part of powder.
3. the blue glaze of golden spot as described in claim any one of 1-2, it is characterised in that the blue powder is by cobalt oxide and local soil type of Datong District
Into the mass ratio of the cobalt oxide and Datong District's soil is 1:(9-11).
4. the blue glaze of gold spot as claimed in claim 3, it is characterised in that the blue powder after cobalt oxide and Datong District's soil mixing
4-6h is calcined at 1150-1250 DEG C to form.
5. the preparation method of the blue glaze of golden spot as described in claim any one of 1-4, it is characterised in that comprise the following steps：
Above-mentioned raw materials are added water mixing, ball milling obtains glaze slip；
Glazing；
Burn till, firing temperature is 1240-1280 DEG C.
6. the preparation method of the blue glaze of gold spot as claimed in claim 3, it is characterised in that step（3）Middle firing process specific steps
It is as follows：Base substrate after glazing is put into kiln, temperature is ramped up 1240-1280 DEG C in 2-3h；It is warming up to 1240-1280
Start cooling after DEG C, be first cooled to 750-800 DEG C with 6-8 DEG C per minute；Then room temperature is naturally cooled to.
7. the preparation method of the blue glaze of gold spot as claimed in claim 3, it is characterised in that：The firing atmosphere burnt till is oxygen
Atmosphere.
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| CN201710375268.7A CN107021626A (en) | 2017-05-24 | 2017-05-24 | A kind of blue glaze of golden spot |
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| CN201710375268.7A CN107021626A (en) | 2017-05-24 | 2017-05-24 | A kind of blue glaze of golden spot |
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| CN201710375268.7A Pending CN107021626A (en) | 2017-05-24 | 2017-05-24 | A kind of blue glaze of golden spot |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107540220A (en) * | 2017-10-12 | 2018-01-05 | 禹州市锦丰源瓷业有限公司 | A kind of Lu's chun glaze of blue tail band gold spot |
| CN107619190A (en) * | 2017-10-13 | 2018-01-23 | 沈阳建筑大学 | Tin ash darkviolet point-like metallic crystal ceramic glaze and preparation method thereof |
| CN108585498A (en) * | 2018-07-30 | 2018-09-28 | 赵红刚 | A kind of orchid chun glaze and preparation method thereof |
| CN109437565A (en) * | 2018-12-19 | 2019-03-08 | 禹州市正玉钧窑有限公司 | A kind of radix curcumae glaze |
| CN110642614A (en) * | 2019-09-25 | 2020-01-03 | 张军召 | Jun porcelain formed by demolding and preparation method thereof |
| CN110642591A (en) * | 2019-09-25 | 2020-01-03 | 张军召 | Jun porcelain with rust golden flower colored glaze and preparation method thereof |
| CN112358186A (en) * | 2020-12-02 | 2021-02-12 | 禹州市神器钧窑有限公司 | Jun porcelain iron sand gold glaze and preparation method thereof |
| CN116589186A (en) * | 2023-05-12 | 2023-08-15 | 陕西科技大学 | Blue-grain Jin Banhua glaze and preparation method thereof |
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| CN103172406A (en) * | 2013-04-12 | 2013-06-26 | 徐维茂 | Gold spot temmoku glaze and preparation technology thereof |
| CN105175017A (en) * | 2015-07-24 | 2015-12-23 | 郏县神前传奇陶瓷钧瓷厂 | Complex Tang-dynasty jun glaze with white spots in blue and process for preparing jun porcelain by use of complex Tang-dynasty jun glaze |
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| CN103172406A (en) * | 2013-04-12 | 2013-06-26 | 徐维茂 | Gold spot temmoku glaze and preparation technology thereof |
| CN105175017A (en) * | 2015-07-24 | 2015-12-23 | 郏县神前传奇陶瓷钧瓷厂 | Complex Tang-dynasty jun glaze with white spots in blue and process for preparing jun porcelain by use of complex Tang-dynasty jun glaze |
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Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107540220A (en) * | 2017-10-12 | 2018-01-05 | 禹州市锦丰源瓷业有限公司 | A kind of Lu's chun glaze of blue tail band gold spot |
| CN107619190A (en) * | 2017-10-13 | 2018-01-23 | 沈阳建筑大学 | Tin ash darkviolet point-like metallic crystal ceramic glaze and preparation method thereof |
| CN108585498A (en) * | 2018-07-30 | 2018-09-28 | 赵红刚 | A kind of orchid chun glaze and preparation method thereof |
| CN109437565A (en) * | 2018-12-19 | 2019-03-08 | 禹州市正玉钧窑有限公司 | A kind of radix curcumae glaze |
| CN109437565B (en) * | 2018-12-19 | 2021-10-01 | 禹州市正玉钧窑有限公司 | Jade and gold glaze |
| CN110642614A (en) * | 2019-09-25 | 2020-01-03 | 张军召 | Jun porcelain formed by demolding and preparation method thereof |
| CN110642591A (en) * | 2019-09-25 | 2020-01-03 | 张军召 | Jun porcelain with rust golden flower colored glaze and preparation method thereof |
| CN112358186A (en) * | 2020-12-02 | 2021-02-12 | 禹州市神器钧窑有限公司 | Jun porcelain iron sand gold glaze and preparation method thereof |
| CN116589186A (en) * | 2023-05-12 | 2023-08-15 | 陕西科技大学 | Blue-grain Jin Banhua glaze and preparation method thereof |
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