CN107012011A - It is a kind of can be with washing powder of disinfecting mite-removing and preparation method thereof - Google Patents
It is a kind of can be with washing powder of disinfecting mite-removing and preparation method thereof Download PDFInfo
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- CN107012011A CN107012011A CN201710291117.3A CN201710291117A CN107012011A CN 107012011 A CN107012011 A CN 107012011A CN 201710291117 A CN201710291117 A CN 201710291117A CN 107012011 A CN107012011 A CN 107012011A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/83—Mixtures of non-ionic with anionic compounds
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/46—Stemonaceae [Stemona family], e.g. croomia
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/16—Anti-static materials
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
- C11D3/1266—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in liquid compositions
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2082—Polycarboxylic acids-salts thereof
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/36—Organic compounds containing phosphorus
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
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- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
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- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
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Abstract
It can be related to washing powder technical field with washing powder of disinfecting mite-removing and preparation method thereof, include the raw material of following part meter the invention discloses a kind of：70 ~ 80 parts of 80 ~ 90 parts of attapulgite, 55 ~ 75 parts of herbal component, 40 ~ 50 parts of bamboo vinegar, 25 ~ 35 parts of glycerine, 15 ~ 30 parts of organic acid, 10 ~ 20 parts of aromatic, 5 ~ 15 parts of auxiliary agent and water.The present invention reaches high absorption, the strong scattered, effect of well suspended, disclosure satisfy that its applications well in washing powder, the spot on clothing is removed well, with efficient sterilizing except mite, eliminate the unusual smell ability to attapulgite modified processing.
Description
Technical field
The present invention relates to washing powder technical field, and in particular to it is a kind of can be with the washing powder of disinfecting mite-removing and its preparation side
Method.
Background technology
In recent years, injury of the atom to the mankind causes the extensive concern of people.Atom refers to that some are difficult by naked eyes
Observed harmful microorganism and tiny insect.Their harmfulness is done harm in being people often carelessly by it.It is tiny
Insect mainly includes the grade such as acarid, moth even more small insect, and the harmfulness of wherein acarid is larger.Therefore except mite class production
Product obtain the approval and receiving of consumers in general in recent years., can't and most of liquid detergent can only play stain-removing effect
Reach the effect of except mite.
Washing powder in existing market adds fluorescer and some chemical substances excitatory mostly（Such as tripolyphosphate
Sodium）, to human injury than larger, our skin had both been injured, the generation of canceration is easily caused again, has been that present washing Industry is badly in need of solution
A significant problem certainly.
The content of the invention
It is an object of the invention to provide it is a kind of can be with washing powder of disinfecting mite-removing and preparation method thereof, to attapulgite modified
Processing, reaches high absorption, the strong scattered, effect of well suspended, disclosure satisfy that its applications well in washing powder, well
The spot on clothing is removed, with efficient sterilizing except mite, eliminate the unusual smell ability.
The invention provides following technical scheme：It is a kind of the original of following part meter to be included with the washing powder of disinfecting mite-removing
Material：It is 80 ~ 90 parts of attapulgite, 55 ~ 75 parts of herbal component, 40 ~ 50 parts of bamboo vinegar, 25 ~ 35 parts of glycerine, 15 ~ 30 parts of organic acid, clear
70 ~ 80 parts of 10 ~ 20 parts of pastil, 5 ~ 15 parts of auxiliary agent and water；
The herbal component includes the raw material that following part is counted：15 ~ 20 parts of the tuber of stemona, 15 ~ 20 parts of kuh-seng, Notogineng Extract 5 ~ 15
1 ~ 3 part of part, 5 ~ 15 parts of Chinese prickly ash, 5 ~ 10 parts of golden cypress, 2 ~ 8 parts of the fruit of summer cypress, 2 ~ 6 parts of hongkong kumquat leaf, 2 ~ 4 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：2 ~ 4 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy
2 ~ 4 parts of ethene ether sodium sulfate, 1 ~ 3 part of AEO, 1 ~ 3 part of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium
0.2 ~ 1.2 part.
Preferably, the raw material of following part meter is included：85 parts of attapulgite, 65 parts of herbal component, 45 parts of bamboo vinegar, glycerine 30
Part, 22 parts of organic acid, 15 parts of aromatic, 10 parts of auxiliary agent and 75 parts of water；
The herbal component includes the raw material that following part is counted：17 parts of the tuber of stemona, 17 parts of kuh-seng, 10 parts of Notogineng Extract, Chinese prickly ash 10
2 parts of part, 8 parts of golden cypress, 5 parts of the fruit of summer cypress, 4 parts of hongkong kumquat leaf, 3 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：3 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy second
0.7 part of 3 parts of alkene ether sodium sulfate, 2 parts of AEO, 2 parts of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium.
Preferably, the bamboo vinegar is the extract of natural mao bamboon.
Preferably, the organic acid is citric acid, oxalic acid, 1-hydroxy ethylidene-1,1-diphosphonic acid, diethylene triamine pentacetic acid (DTPA), ethylenediamine
One or more in tetraacethyl, tartaric acid and malic acid.
Preferably, the aromatic is the one or more in water-soluble menthol, peppermint essence and fruity essence.
Preferably, the preparation method of the Notogineng Extract is：Pseudo-ginseng is rinsed well with clear water, be put into boiling water and boil 5 ~
Taken out after 8min and carry out slicing treatment, the piece thickness of section is 4 ~ 6mm, and the pseudo-ginseng after section is put into the marmite for filling wheat bran
In, heating keeping temperature is natural cooling after 90 ~ 100 DEG C, the 30 ~ 50min that stir-fries, and taking-up crushed 90 ~ 100 mesh sieves, and placed into 2
In 70 ~ 80% ethanol solutions of ~ 4 times of parts by weight, it is Notogineng Extract to obtain extract solution after 5 ~ 7h of immersion refluxing extraction.
Present invention offer is a kind of to be comprised the following steps with the preparation method of the washing powder of disinfecting mite-removing：
（1）, attapulgite pretreatment：Take attapulgite to crush and cross 100 ~ 120 mesh sieves, obtain attapulgite powder, add 25 ~
In the distilled water of 30 times of parts by weight, slurry is obtained after stirring 2~2.5h at normal temperatures with 300~500 r/min, will with centrifuge
The pulp centrifuged removing detrital mineral of gained, attapulgite essence soil is obtained by filtering, drying steps；
（2）, attapulgite modified processing：By step（1）The obtained smart soil of attapulgite is added in aqueous slkali, and heating water bath is extremely
88 ~ 90 DEG C, 0.5 ~ 1h, filtering are stirred with 600 ~ 700r/min, filter residue is washed with deionized to neutrality, dried, crushes, mistake
100 ~ 150 mesh sieves, obtain attapulgite modified；
（3）, high-temperature calcination：By step（2）In attapulgite feeding calcining furnace after obtained modification, at 500 ~ 650 DEG C
1 ~ 2h of lower calcining, takes out attapulgite modified after being calcined, standby；
（4）, prepare Chinese herbal medicine fluid：The tuber of stemona, kuh-seng, Notogineng Extract, Chinese prickly ash, golden cypress, the fruit of summer cypress, mountain tangerine are weighed according to proportioning
Leaf, Kadsura Root-bark and fortune paulownia flower, crush and cross 30 ~ 60 mesh sieves, obtain mixing powder, ultrasonic assistant ethanol is carried out to mixing powder
Extract, 50 ~ 65% ethanol of 5~10 times of parts by weight are added into mixing powder, under ultrasonic assistant effect, 60~80 DEG C of bars
30~50min of refluxing extraction under part, is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 10~20h, in 55~85 DEG C of bars
Be concentrated under reduced pressure recovery ethanol under part, obtains concentrate for the Chinese herbal medicine fluid, standby；
（5）, prepare finished product：By step（3）Attapulgite modified and step after obtained calcining（4）Obtained Chinese herbal medicine fluid is mixed
Close, sequentially add surplus stock according to proportioning, heat and stir, obtain mixed material, be then spray-dried, obtained
Finished product be the disinfecting mite-removing washing powder.
Preferably, the step（5）It is middle to heat and the condition that stirs is：It is 60 ~ 70 DEG C to control heating-up temperature, heating
Time is 20 ~ 30min, and mixing speed is 500 ~ 800r/min.
Beneficial effects of the present invention：To attapulgite modified processing, high absorption, the strong scattered, effect of well suspended are reached
Really, its applications well in washing powder is disclosure satisfy that, the spot on clothing is removed well, with efficient sterilizing except mite, is removed
Peculiar smell ability, it is specific as follows：
（1）, the present invention washing powder, each material composition is harmless to human body and environment, environmental protection, wherein, with attapulgite
The sodium tripolyphosphate in washing powder is substituted, environmental pollution is reduced, in addition, attapulgite resource is abundant, raw material is cheap, it is possible to decrease into
This；Specifically, attapulgite is modified and high-temperature calcination processing, increases its interfloor distance, suction-operated enhancing, processing
Attapulgite granule strength afterwards is high, specific surface area is big, suspension is good, with disinfecting mite-removing worm and stronger anti-recontamination energy
Power, can effectively adsorb spot and bacterium；
（2）, the octadecyldimethyl ethoxy quaternary ammonium nitrate that adds in the present invention, on the one hand can strengthen washing powder
Washing effect, on the other hand also has antistatic property；
（3）, sodium sulfate of polyethenoxy ether of fatty alcohol, AEO and the linear alkyl benzene sulfonic acid added in the present invention
Sodium has potent dirt-removing power, and safe and harmless reaches cleaning decontamination；
（4）, the bamboo vinegar that adds in the present invention, be the extract of natural mao bamboon, main component is acetic acid, and acetic acid is a kind of common
Organic monoacid, meets alkali and occurs neutralization reaction, acetic acid property is gentle, will not damaging laundry cotton fiber, as in nertralizer and residual
Alkali and impurity, make the clothing after washing more clean bright-coloured；
（5）, the herbal component that adds cooperates in the present invention, with good sterilization and except mite suppression mite effect, and safety
Gently, have no toxic side effect, have no adverse reaction.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.
Embodiment 1
It is a kind of the raw material of following part meter to be included with the washing powder of disinfecting mite-removing：
80 parts of attapulgite；
55 parts of herbal component；
40 parts of bamboo vinegar；
25 parts of glycerine；
15 parts of organic acid；
10 parts of aromatic；
5 parts of auxiliary agent；
70 parts of water；
The herbal component includes the raw material that following part is counted：15 parts of the tuber of stemona, 15 parts of kuh-seng, 5 parts of Notogineng Extract, 5 parts of Chinese prickly ash,
1 part of 5 parts of golden cypress, 2 parts of the fruit of summer cypress, 2 parts of hongkong kumquat leaf, 2 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：2 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy second
0.2 part of 2 parts of alkene ether sodium sulfate, 1 part of AEO, 1 part of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium.
Wherein, the bamboo vinegar is the extract of natural mao bamboon.
Wherein, the organic acid is citric acid.
Wherein, the aromatic is water-soluble menthol.
Wherein, the preparation method of the Notogineng Extract is：Pseudo-ginseng is rinsed well with clear water, is put into boiling water and boils 5min
After take out and carry out slicing treatment, the piece thickness of section is 4mm, and the pseudo-ginseng after section is put into the marmite for filling wheat bran, plus
Hot keeping temperature is natural cooling after 90 DEG C, the 30min that stir-fries, and taking-up crushed 90 mesh sieves, and placed into 70% second of 2 times of parts by weight
In alcoholic solution, it is Notogineng Extract to obtain extract solution after immersion refluxing extraction 5h.
The present embodiment offer is a kind of to be comprised the following steps with the preparation method of the washing powder of disinfecting mite-removing：
（1）, attapulgite pretreatment：Take attapulgite to crush and cross 100 mesh sieves, obtain attapulgite powder, add 25 times of weights
Measure part distilled water in, at normal temperatures with 300 r/min stirring 2h after obtain slurry, with centrifuge by gained it is pulp centrifuged remove
Detrital mineral, attapulgite essence soil is obtained by filtering, drying steps；
（2）, attapulgite modified processing：By step（1）The obtained smart soil of attapulgite is added in aqueous slkali, and heating water bath is extremely
88 DEG C, 0.5h, filtering are stirred with 600r/min, filter residue is washed with deionized to neutrality, dried, crush, crosses 100 mesh sieves, obtain
To attapulgite modified；
（3）, high-temperature calcination：By step（2）In attapulgite feeding calcining furnace after obtained modification, forged at 500 DEG C
1 ~ 2h is burnt, takes out attapulgite modified after being calcined, it is standby；
（4）, prepare Chinese herbal medicine fluid：The tuber of stemona, kuh-seng, Notogineng Extract, Chinese prickly ash, golden cypress, the fruit of summer cypress, mountain tangerine are weighed according to proportioning
Leaf, Kadsura Root-bark and fortune paulownia flower, crush and cross 30 mesh sieves, obtain mixing powder, and carrying out ultrasonic assistant ethanol to mixing powder carries
Take, 50% ethanol of 5 times of parts by weight is added into mixing powder, under ultrasonic assistant effect, refluxing extraction under the conditions of 60 DEG C
30min, is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 10h, and be concentrated under reduced pressure recovery ethanol under the conditions of 55 DEG C, obtains
It is the Chinese herbal medicine fluid to concentrate, it is standby；
（5）, prepare finished product：By step（3）Attapulgite modified and step after obtained calcining（4）Obtained Chinese herbal medicine fluid is mixed
Close, sequentially add surplus stock according to proportioning, heat and stir, obtain mixed material, be then spray-dried, obtained
Finished product be the disinfecting mite-removing washing powder.
Wherein, the step（5）It is middle to heat and the condition that stirs is：It is 60 DEG C to control heating-up temperature, and the heat time is
20min, mixing speed is 500r/min.
Embodiment 2
It is a kind of the raw material of following part meter to be included with the washing powder of disinfecting mite-removing：
90 parts of attapulgite；
75 parts of herbal component；
50 parts of bamboo vinegar；
35 parts of glycerine；
30 parts of organic acid；
20 parts of aromatic；
15 parts of auxiliary agent；
80 parts of water；
The herbal component includes the raw material that following part is counted：20 parts of the tuber of stemona, 20 parts of kuh-seng, 15 parts of Notogineng Extract, Chinese prickly ash 15
3 parts of part, 10 parts of golden cypress, 8 parts of the fruit of summer cypress, 6 parts of hongkong kumquat leaf, 4 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：4 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy second
1.2 parts of 4 parts of alkene ether sodium sulfate, 3 parts of AEO, 3 parts of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium.
Wherein, the bamboo vinegar is the extract of natural mao bamboon.
Wherein, the organic acid is oxalic acid.
Wherein, the aromatic is peppermint essence.
Wherein, the preparation method of the Notogineng Extract is：Pseudo-ginseng is rinsed well with clear water, is put into boiling water and boils 8min
After take out and carry out slicing treatment, the piece thickness of section is 6mm, and the pseudo-ginseng after section is put into the marmite for filling wheat bran, plus
Hot keeping temperature is natural cooling after 100 DEG C, the 50min that stir-fries, and taking-up crushed 100 mesh sieves, and placed into the 80% of 4 times of parts by weight
In ethanol solution, it is Notogineng Extract to obtain extract solution after immersion refluxing extraction 7h.
Also provide and a kind of can be comprised the following steps with the preparation method of the washing powder of disinfecting mite-removing in the present embodiment：
（1）, attapulgite pretreatment：Take attapulgite to crush and cross 120 mesh sieves, obtain attapulgite powder, add 30 times of weights
In the distilled water for measuring part, at normal temperatures to obtain slurry after 500 r/min stirrings 2.5h, removed with centrifuge by gained is pulp centrifuged
Detrital mineral is removed, attapulgite essence soil is obtained by filtering, drying steps；
（2）, attapulgite modified processing：By step（1）The obtained smart soil of attapulgite is added in aqueous slkali, and heating water bath is extremely
90 DEG C, 1h, filtering are stirred with 700r/min, filter residue is washed with deionized to neutrality, dried, crush, crosses 150 mesh sieves, obtain
It is attapulgite modified；
（3）, high-temperature calcination：By step（2）In attapulgite feeding calcining furnace after obtained modification, forged at 650 DEG C
2h is burnt, takes out attapulgite modified after being calcined, it is standby；
（4）, prepare Chinese herbal medicine fluid：The tuber of stemona, kuh-seng, Notogineng Extract, Chinese prickly ash, golden cypress, the fruit of summer cypress, mountain tangerine are weighed according to proportioning
Leaf, Kadsura Root-bark and fortune paulownia flower, crush and cross 60 mesh sieves, obtain mixing powder, and carrying out ultrasonic assistant ethanol to mixing powder carries
Take, 65% ethanol of 10 times of parts by weight is added into mixing powder, under ultrasonic assistant effect, refluxing extraction under the conditions of 80 DEG C
50min, is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 20h, and be concentrated under reduced pressure recovery ethanol under the conditions of 85 DEG C, obtains
It is the Chinese herbal medicine fluid to concentrate, it is standby；
（5）, prepare finished product：By step（3）Attapulgite modified and step after obtained calcining（4）Obtained Chinese herbal medicine fluid is mixed
Close, sequentially add surplus stock according to proportioning, heat and stir, obtain mixed material, be then spray-dried, obtained
Finished product be the disinfecting mite-removing washing powder.
Preferably, the step（5）It is middle to heat and the condition that stirs is：It is 70 DEG C to control heating-up temperature, and the heat time is
30min, mixing speed is 800r/min.
Embodiment 3
It is a kind of the raw material of following part meter to be included with the washing powder of disinfecting mite-removing：
85 parts of attapulgite；
65 parts of herbal component；
45 parts of bamboo vinegar；
30 parts of glycerine；
22 parts of organic acid；
15 parts of aromatic；
10 parts of auxiliary agent；
75 parts of water；
The herbal component includes the raw material that following part is counted：17 parts of the tuber of stemona, 17 parts of kuh-seng, 10 parts of Notogineng Extract, Chinese prickly ash 10
2 parts of part, 8 parts of golden cypress, 5 parts of the fruit of summer cypress, 4 parts of hongkong kumquat leaf, 3 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：3 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy second
0.7 part of 3 parts of alkene ether sodium sulfate, 2 parts of AEO, 2 parts of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium.
Wherein, the bamboo vinegar is the extract of natural mao bamboon.
Wherein, the organic acid is 1-hydroxy ethylidene-1,1-diphosphonic acid.
Wherein, the aromatic is fruity essence.
Wherein, the preparation method of the Notogineng Extract is：Pseudo-ginseng is rinsed well with clear water, is put into boiling water and boils 6min
After take out and carry out slicing treatment, the piece thickness of section is 5mm, and the pseudo-ginseng after section is put into the marmite for filling wheat bran, plus
Hot keeping temperature is natural cooling after 95 DEG C, the 40min that stir-fries, and taking-up crushed 95 mesh sieves, and placed into 75% second of 3 times of parts by weight
In alcoholic solution, it is Notogineng Extract to obtain extract solution after immersion refluxing extraction 6h.
There is provided and a kind of can be comprised the following steps with the preparation method of the washing powder of disinfecting mite-removing in the present embodiment：
（1）, attapulgite pretreatment：Take attapulgite to crush and cross 110 mesh sieves, obtain attapulgite powder, add 27 times of weights
Measure part distilled water in, at normal temperatures with 400 r/min stirring 2h after obtain slurry, with centrifuge by gained it is pulp centrifuged remove
Detrital mineral, attapulgite essence soil is obtained by filtering, drying steps；
（2）, attapulgite modified processing：By step（1）The obtained smart soil of attapulgite is added in aqueous slkali, and heating water bath is extremely
89 DEG C, 0.5h, filtering are stirred with 650r/min, filter residue is washed with deionized to neutrality, dried, crush, crosses 125 mesh sieves, obtain
To attapulgite modified；
（3）, high-temperature calcination：By step（2）In attapulgite feeding calcining furnace after obtained modification, forged at 550 DEG C
1.5h is burnt, takes out attapulgite modified after being calcined, it is standby；
（4）, prepare Chinese herbal medicine fluid：The tuber of stemona, kuh-seng, Notogineng Extract, Chinese prickly ash, golden cypress, the fruit of summer cypress, mountain tangerine are weighed according to proportioning
Leaf, Kadsura Root-bark and fortune paulownia flower, crush and cross 45 mesh sieves, obtain mixing powder, and carrying out ultrasonic assistant ethanol to mixing powder carries
Take, 55% ethanol of 7 times of parts by weight is added into mixing powder, under ultrasonic assistant effect, refluxing extraction under the conditions of 70 DEG C
40min, is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 15h, and be concentrated under reduced pressure recovery ethanol under the conditions of 70 DEG C, obtains
It is the Chinese herbal medicine fluid to concentrate, it is standby；
（5）, prepare finished product：By step（3）Attapulgite modified and step after obtained calcining（4）Obtained Chinese herbal medicine fluid is mixed
Close, sequentially add surplus stock according to proportioning, heat and stir, obtain mixed material, be then spray-dried, obtained
Finished product be the disinfecting mite-removing washing powder.
Wherein, the step（5）It is middle to heat and the condition that stirs is：It is 65 DEG C to control heating-up temperature, and the heat time is
25min, mixing speed is 650r/min.
The present invention is described in detail with reference to the foregoing embodiments, for those skilled in the art, its according to
The technical scheme described in foregoing embodiments can so be modified, or which part technical characteristic is equally replaced
Change.Within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., should be included in the present invention
Protection domain within.
Claims (8)
1. a kind of can be with the washing powder of disinfecting mite-removing, it is characterised in that the raw material counted including following part：80 ~ 90 parts of attapulgite,
55 ~ 75 parts of herbal component, 40 ~ 50 parts of bamboo vinegar, 25 ~ 35 parts of glycerine, 15 ~ 30 parts of organic acid, 10 ~ 20 parts of aromatic, auxiliary agent 5 ~
15 parts and 70 ~ 80 parts of water；
The herbal component includes the raw material that following part is counted：15 ~ 20 parts of the tuber of stemona, 15 ~ 20 parts of kuh-seng, Notogineng Extract 5 ~ 15
1 ~ 3 part of part, 5 ~ 15 parts of Chinese prickly ash, 5 ~ 10 parts of golden cypress, 2 ~ 8 parts of the fruit of summer cypress, 2 ~ 6 parts of hongkong kumquat leaf, 2 ~ 4 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：2 ~ 4 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy
2 ~ 4 parts of ethene ether sodium sulfate, 1 ~ 3 part of AEO, 1 ~ 3 part of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium
0.2 ~ 1.2 part.
2. according to claim 1 can be with the washing powder of disinfecting mite-removing, it is characterised in that the raw material counted including following part：
85 parts of attapulgite, 65 parts of herbal component, 45 parts of bamboo vinegar, 30 parts of glycerine, 22 parts of organic acid, 15 parts of aromatic, 10 parts of auxiliary agent
With 75 parts of water；
The herbal component includes the raw material that following part is counted：17 parts of the tuber of stemona, 17 parts of kuh-seng, 10 parts of Notogineng Extract, Chinese prickly ash 10
2 parts of part, 8 parts of golden cypress, 5 parts of the fruit of summer cypress, 4 parts of hongkong kumquat leaf, 3 parts of Kadsura Root-bark and fortune paulownia flower；
The auxiliary agent includes the raw material that following part is counted：3 parts of octadecyldimethyl ethoxy quaternary ammonium nitrate, fatty alcohol polyoxy second
0.7 part of 3 parts of alkene ether sodium sulfate, 2 parts of AEO, 2 parts of sodium n-alkylbenzenesulfonate and hydroxypropyl methylcellulose sodium.
3. according to claim 1 can be with the washing powder of disinfecting mite-removing, it is characterised in that the bamboo vinegar is natural mao bamboon
Extract.
4. according to claim 1 can be with the washing powder of disinfecting mite-removing, it is characterised in that the organic acid be citric acid,
One kind or many in oxalic acid, 1-hydroxy ethylidene-1,1-diphosphonic acid, diethylene triamine pentacetic acid (DTPA), ethylenediamine tetra-acetic acid, tartaric acid and malic acid
Kind.
5. according to claim 1 can be with the washing powder of disinfecting mite-removing, it is characterised in that the aromatic is thin, water soluble
One or more in lotus brain, peppermint essence and fruity essence.
6. according to claim 1 can be with the washing powder of disinfecting mite-removing, it is characterised in that the preparation of the Notogineng Extract
Method is：Pseudo-ginseng is rinsed well with clear water, is put into boiling water to boil and slicing treatment is taken out and carried out after 5 ~ 8min, the piece of section is thick
For 4 ~ 6mm, the pseudo-ginseng after section is put into the marmite for filling wheat bran, heating keeping temperature is 90 ~ 100 DEG C, stir-fry 30 ~
90 ~ 100 mesh sieves were crushed in natural cooling after 50min, taking-up, in 70 ~ 80% ethanol solutions for placing into 2 ~ 4 times of parts by weight, immersion
It is Notogineng Extract that extract solution is obtained after 5 ~ 7h of refluxing extraction.
7. a kind of can be existed with the preparation method of the washing powder of disinfecting mite-removing, its feature according to any one of claim 1 ~ 6
In comprising the following steps：
（1）, attapulgite pretreatment：Take attapulgite to crush and cross 100 ~ 120 mesh sieves, obtain attapulgite powder, add 25 ~
In the distilled water of 30 times of parts by weight, slurry is obtained after stirring 2~2.5h at normal temperatures with 300~500 r/min, will with centrifuge
The pulp centrifuged removing detrital mineral of gained, attapulgite essence soil is obtained by filtering, drying steps；
（2）, attapulgite modified processing：By step（1）The obtained smart soil of attapulgite is added in aqueous slkali, and heating water bath is extremely
88 ~ 90 DEG C, 0.5 ~ 1h, filtering are stirred with 600 ~ 700r/min, filter residue is washed with deionized to neutrality, dried, crushes, mistake
100 ~ 150 mesh sieves, obtain attapulgite modified；
（3）, high-temperature calcination：By step（2）In attapulgite feeding calcining furnace after obtained modification, at 500 ~ 650 DEG C
1 ~ 2h of lower calcining, takes out attapulgite modified after being calcined, standby；
（4）, prepare Chinese herbal medicine fluid：The tuber of stemona, kuh-seng, Notogineng Extract, Chinese prickly ash, golden cypress, the fruit of summer cypress, mountain tangerine are weighed according to proportioning
Leaf, Kadsura Root-bark and fortune paulownia flower, crush and cross 30 ~ 60 mesh sieves, obtain mixing powder, ultrasonic assistant ethanol is carried out to mixing powder
Extract, 50 ~ 65% ethanol of 5~10 times of parts by weight are added into mixing powder, under ultrasonic assistant effect, 60~80 DEG C of bars
30~50min of refluxing extraction under part, is extracted 3 times, and the filtrate of extraction is merged, and refrigeration is placed after 10~20h, in 55~85 DEG C of bars
Be concentrated under reduced pressure recovery ethanol under part, obtains concentrate for the Chinese herbal medicine fluid, standby；
（5）, prepare finished product：By step（3）Attapulgite modified and step after obtained calcining（4）Obtained Chinese herbal medicine fluid is mixed
Close, sequentially add surplus stock according to proportioning, heat and stir, obtain mixed material, be then spray-dried, obtained
Finished product be the disinfecting mite-removing washing powder.
8. according to claim 7 can be with the preparation method of the washing powder of disinfecting mite-removing, it is characterised in that the step
（5）It is middle to heat and the condition that stirs is：It is 60 ~ 70 DEG C to control heating-up temperature, and the heat time is 20 ~ 30min, mixing speed
For 500 ~ 800r/min.
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Application publication date: 20170804 |