CN106982865A - A kind of insecticide of the extract solution containing tea seed cake and preparation method thereof - Google Patents
A kind of insecticide of the extract solution containing tea seed cake and preparation method thereof Download PDFInfo
- Publication number
- CN106982865A CN106982865A CN201710363043.XA CN201710363043A CN106982865A CN 106982865 A CN106982865 A CN 106982865A CN 201710363043 A CN201710363043 A CN 201710363043A CN 106982865 A CN106982865 A CN 106982865A
- Authority
- CN
- China
- Prior art keywords
- parts
- insecticide
- tea seed
- seed cake
- extract solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/06—Unsaturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/10—Aromatic or araliphatic carboxylic acids, or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/04—Sulfonic acids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/46—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom rings with more than six members
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/22—Lamiaceae or Labiatae [Mint family], e.g. thyme, rosemary, skullcap, selfheal, lavender, perilla, pennyroyal, peppermint or spearmint
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention relates to insecticide of a kind of extract solution containing tea seed cake and preparation method thereof, the insecticide includes by weight：50 70 parts of tea seed cake extract solutions, 5 12 parts of Tween 80s, 58 parts of alkyl benzene sulphonate sodium salts, 15 parts of castor oil, 10 20 parts of ethanol and 12 parts of Laurocaprams, raw material sources are abundant, low toxicity, noresidue, preparation method is simple, it is the insecticide low toxicity of the obtained extract solution containing tea seed cake, nuisanceless, it is environmentally safe, insect after being administered through insecticide spraying is not likely to produce resistance, reusable improvement insect；It is degradable, it can pluck edible behind 13 days of the insecticide of the crops sprinkling extract solution containing tea seed cake.
Description
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of insecticide of extract solution containing tea seed cake and its preparation side.
Background technology
The disease of crops has a strong impact on the yield and quality of crop, and the pesticide variety of preventing and treating diseases and pests of agronomic crop is numerous at present
It is many, but play the role of single, it is larger to have plenty of toxicity, has plenty of DeGrain.And now in widely used agricultural chemicals, such as
The missible oil race such as rotenone, antibiotic, chrysanthemum lipid agricultural chemicals, the arene material such as benzene and dimethylbenzene multi-purpose greatly makees solvent and carrier,
This kind of material is not only polluted to environment, and easily people and animals are caused harm, and serious public hazards are brought to ecological environment.
The content of the invention
In order to solve the above problems, the present invention devises a kind of efficient, micro- poison, broad-spectrum pesticide, i.e. one kind and carried containing tea seed cake
Insecticide of liquid and preparation method thereof is taken, the raw material sources are abundant, cheap, safe efficient, low toxicity, low-residual, no dirt
Dye；Preparation method technique is simple, can industrialized mass production；The insecticide control effect of the obtained extract solution containing tea seed cake
Good, nuisanceless, low toxicity, insect is not likely to produce resistance.
It is made according to the insecticide of the extract solution containing tea seed cake of the present invention, including following raw material：50-70 parts of tea seed cakes are carried
Take liquid, 5-12 part Tween-80,5-8 parts of alkyl benzene sulphonate sodium salts, 1-5 parts of castor oil, 10-20 parts of ethanol and 1-2 parts of bay nitrogen tall and erect
Ketone.
Tween-80, scientific name polyoxyethylene sorbitan monooleate, abbreviation Tween-80 is non-ionic surface
Activating agent, there is emulsification.
The insecticide of the obtained extract solution containing tea seed cake adds the tea seed cake extract solution of natural environmental-protective, good disinsection effect and has
Obvious prevention effect, environmentally safe, desinsection ensuing crop surface noresidue.
According to the insecticide of the extract solution containing tea seed cake of the present invention, the insecticide includes by weight：50-70 parts of tea seed cakes
Extract solution, 5-12 part Tween-80,5-8 parts of alkyl benzene sulphonate sodium salts, 1-5 parts of castor oil, 10-20 parts of ethanol, 1-2 parts of bay nitrogen
Tall and erect ketone and 1-5 part sodium sorbate.
Further, the consideration of the insecticide holding time based on the extract solution containing tea seed cake described in extension, according to the present invention
The extract solution containing tea seed cake insecticide, in addition to 0.3-1 portions of Kathon CG preservatives.
Further, it is the insecticide of the extract solution containing tea seed cake described in thickening, preferable use state is reached, according to this hair
The insecticide of the bright extract solution containing tea seed cake, in addition to 0.1-0.3 parts of xanthans.
Further, for the penetrating odor of the insecticide that relaxes the described extract solution containing tea seed cake, according to the present invention's
The insecticide of the extract solution containing tea seed cake, in addition to 0.1-0.5 parts of orange flavors.
Further, in order to obtain the tea seed cake extract solution that insecticidal effect is best, the desinsection of the extract solution containing tea seed cake is made
The insecticidal effect of agent is more preferable, it is ensured that ensure best insecticidal effect, reduction pair in the case that the usage amount of the insecticide is minimum
Crops and the pollution of environment, according to the insecticide of the extract solution containing tea seed cake of the present invention, wherein, the tea seed cake extract solution is carried
Raw material is taken for oil tea is withered and tobacco stem；Extracting method is：By oil tea is withered, tobacco stem added water after crushing and boil and be incubated, cross 40-80
Mesh sieve, takes filtrate, obtains the tea seed cake extract solution；The oil tea is withered, the weight ratio of tobacco stem and water is 9-10：2-3：8-10.
Further, fully effectively extracted for the active ingredient that enables the tea seed cake, while simplify extraction process again,
According to the insecticide of the extract solution containing tea seed cake of the present invention, the particle diameter after the oil tea is withered, tobacco stem is crushed is 40-100 mesh.
Further, in order that active ingredient in the tea seed cake by high efficiency extraction and can ensure active ingredient activity,
According to the insecticide of the extract solution containing tea seed cake of the present invention, the holding temperature is 80-90 DEG C, and soaking time is 4-6 hours.
The method for producing insecticide of the above-mentioned extract solution containing tea seed cake, comprises the following steps：
(1) raw material will be weighed according to parts by weight to be well mixed, and will obtain raw material compound；
(2) the raw material compound is subjected to homogenization, obtains the insecticide of the extract solution containing tea seed cake.
Further, to be sufficiently mixed each raw material, preparation in accordance with the present invention, the mixing temperature in step (1)
For 60-80 DEG C, the time is 50-80 minutes.Further preferably, step (1) is carried out in a kettle..
Further, to obtain the insecticide that uniform component, stable system, insecticidal effect are stable, according to the present invention
Preparation method, the homogenization temperature in step (2) is 30-50 DEG C, and rotating speed is 100-200r/min, and the time is 5-10 points
Clock.Further preferably, step (2) is carried out in homogenizer.
The application method of the insecticide of the extract solution of the present invention containing tea seed cake is, by the insecticide and water according to 1:
400-600 volume ratio is diluted and stirred, by the insecticide spraying after dilution in crop surface, 50-
The insecticide of the 80ml extract solution containing tea seed cake can effectively administer one mu of crops.The insecticidal mechanism of the insecticide is with " smell and kill "
Based on, have " tagging " effect concurrently.Aphid, aleyrodid class, thrips class, a red-spotted lizard class, withered latent class, Caloptiliatheivora, flea beetle class, red spider can be made
The insects such as class, thrips class, Liriomyza smell smell, or touch, i.e., because nervous centralis is stabbed and it is dead, so using process
Without " three wastes ", do not influence people's healthy, not pollution of ecological environment
Beneficial effects of the present invention are：
The present invention provides a kind of insecticide of the extract solution containing tea seed cake and preparation method thereof, and the insecticide is wrapped by weight
Include：50-70 parts of tea seed cake extract solutions, 5-12 parts of Tween-80s, 5-8 parts of alkyl benzene sulphonate sodium salts, 1-5 parts of castor oil, 10-20 parts of second
Alcohol and 1-2 parts of Laurocaprams, raw material sources are abundant, low toxicity, noresidue, preparation method is simple, and what is obtained described carries containing tea seed cake
The insecticide low toxicity, nuisanceless of liquid is taken, environmentally safe, the insect after being administered through insecticide spraying is not likely to produce resistance, can
Reuse and administer insect；It is degradable, it can pluck food behind 1-3 days of the insecticide of the crops sprinkling extract solution containing tea seed cake
With.
Embodiment
To make the object, technical solutions and advantages of the present invention clearer, technical scheme will be carried out below
Detailed description.Obviously, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Base
Embodiment in the present invention, those of ordinary skill in the art are resulting on the premise of creative work is not made to be owned
Other embodiment, belongs to the scope that the present invention is protected.
Following examples are with 1 part for 1kg.
Embodiment 1
A kind of insecticide of extract solution containing tea seed cake, the insecticide includes by weight：50 parts of tea seed cake extract solutions, 12 parts tell
Temperature -80,5 parts of alkyl benzene sulphonate sodium salts, 5 parts of castor oil, 10 parts of ethanol and 2 parts of Laurocaprams.
The extracting method of the tea seed cake extract solution is to take that oil tea is withered, tobacco stem is crushed to add water after 40 mesh and boiled and 90
DEG C, 4 hours are incubated, 80 mesh screens is crossed, takes filtrate, obtain the tea seed cake extract solution；The oil tea is withered, the weight of tobacco stem and water
Amount is than being 9：3：8.
The method for producing insecticide of the described extract solution containing tea seed cake, comprises the following steps：
(1) raw material weighed according to parts by weight is well mixed in a kettle., mixing temperature is 80 DEG C, the time is 50 points
Clock, obtains raw material compound；
(2) the raw material compound is subjected to homogenization in homogenizer, obtains the desinsection of the extract solution containing tea seed cake
Agent, treatment temperature is 50 DEG C, and rotating speed is 100r/min, and the time is 10 minutes.
Embodiment 2
A kind of insecticide of extract solution containing tea seed cake, the insecticide includes by weight：70 parts of tea seed cake extract solutions, 5 parts tell
Temperature -80,8 parts of alkyl benzene sulphonate sodium salts, 1 part of castor oil, 20 parts of ethanol and 1 part of Laurocapram and 1 part of sodium sorbate.
The extracting method of the tea seed cake extract solution is to take that oil tea is withered, tobacco stem is crushed to add water after 100 mesh and boiled and 80
DEG C, 6 hours are incubated, 40 mesh screens is crossed, takes filtrate, obtain the tea seed cake extract solution；The oil tea is withered, the weight of tobacco stem and water
Amount is than being 10：2：10.
The method for producing insecticide of the described extract solution containing tea seed cake, comprises the following steps：
(1) raw material weighed according to parts by weight is well mixed in a kettle., mixing temperature is 60 DEG C, the time is 80 points
Clock, obtains raw material compound；
(2) the raw material compound is subjected to homogenization in homogenizer, obtains the desinsection of the extract solution containing tea seed cake
Agent, treatment temperature is 30 DEG C, and rotating speed is 200r/min, and the time is 5 minutes.
Embodiment 3
A kind of insecticide of extract solution containing tea seed cake, the insecticide includes by weight：60 parts of tea seed cake extract solutions, 8 parts tell
Temperature -80,6 parts of alkyl benzene sulphonate sodium salts, 2 parts of castor oil, 12 parts of ethanol and 1 part of Laurocapram, 2 parts of sodium sorbates and 0.3 part
Kathon CG preservative.
The extracting method of the tea seed cake extract solution is to take that oil tea is withered, tobacco stem is crushed to add water after 80 mesh and boiled and 85
DEG C, 5 hours are incubated, 60 mesh screens is crossed, takes filtrate, the insecticide of the extract solution containing tea seed cake is obtained；The oil tea is withered, tobacco
The weight ratio of stem and water is 10：2：9.
The method for producing insecticide of the described extract solution containing tea seed cake, comprises the following steps：
(1) raw material weighed according to parts by weight is well mixed in a kettle., mixing temperature is 70 DEG C, the time is 60 points
Clock, obtains raw material compound；
(2) the raw material compound is subjected to homogenization in homogenizer, obtains the tea seed cake extract solution, treatment temperature
For 40 DEG C, rotating speed is 160r/min, and the time is 7 minutes.
Embodiment 4
As different from Example 3, a kind of insecticide of extract solution containing tea seed cake, the insecticide includes by weight：60
Part tea seed cake extract solution, 10 parts of Tween-80s, 6 parts of alkyl benzene sulphonate sodium salts, 3 parts of castor oil, 15 parts of ethanol and 1 part of Laurocapram,
1 part of sodium sorbate, 1 portion of Kathon CG preservative and 0.1 part of xanthans.
The extracting method of the tea seed cake extract solution is to take that oil tea is withered, tobacco stem is crushed to add water after 80 mesh and boiled and 80
DEG C, 5 hours are incubated, 50 mesh screens is crossed, takes filtrate, obtain the tea seed cake extract solution；The oil tea is withered, the weight of tobacco stem and water
Amount is than being 10：2：9.
The method for producing insecticide of the described extract solution containing tea seed cake, comprises the following steps：
(1) raw material weighed according to parts by weight is well mixed in a kettle., mixing temperature is 78 DEG C, the time is 54 points
Clock, obtains raw material compound；
(2) the raw material compound is subjected to homogenization in homogenizer, obtains the desinsection of the extract solution containing tea seed cake
Agent, treatment temperature is 40 DEG C, and rotating speed is 180r/min, and the time is 8 minutes.
Embodiment 5
As different from Example 4, a kind of insecticide of extract solution containing tea seed cake, the insecticide includes by weight：60
Part tea seed cake extract solution, 6 parts of Tween-80s, 5 parts of alkyl benzene sulphonate sodium salts, 3 parts of castor oil, 15 parts of ethanol and 1 part of Laurocapram, 1
Part sodium sorbate, 0.5 portion of Kathon CG preservative, 0.3 part of xanthans and 0.1 part of orange flavor.
Other technological parameters are same as Example 4.
Embodiment 6
As different from Example 4, a kind of insecticide of extract solution containing tea seed cake, the insecticide includes by weight：60
Part tea seed cake extract solution, 6 parts of Tween-80s, 5 parts of alkyl benzene sulphonate sodium salts, 3 parts of castor oil, 17 parts of ethanol and 1 part of Laurocapram, 1
Part sodium sorbate, 0.5 portion of Kathon CG preservative, 0.2 part of xanthans and 0.5 part of orange flavor.
Other technological parameters are same as Example 4.
Experimental example
To administer green vegetables worm and diamondback moth with pressing down too using the insecticide of the extract solution containing tea seed cake described in the embodiment of the present invention 3
The farmland that guarantor, high chlorine do not apply any insecticide products carries out Experimental comparison：
Table 1 is 1d, 3d, 7d preventing and treating cabbage caterpillar test of pesticide effectiveness data statistic after medicine.Table 1 shows, is obtained using embodiment 3
The extract solution containing tea seed cake insecticide after 1d, 3d and 7d after, the disappointed rate of blue or green worm is being incrementally increased, and shows the effective of its desinsection
Acting duration is long；And compared in same phase, the desinsection death rate height after all relatively suppression hooligan and Gao chlorine are applied especially exists
After 1d, this shows more traditional suppression hooligan and Gao chlorine, the insecticide for the extract solution containing tea seed cake that the embodiment of the present invention 3 is obtained
Insecticide efficiency is greatly improved.
Table 1
Table 2 is 1d, 3d, 7d preventing and treating diamondback moth test of pesticide effectiveness data statistic after medicine.With table 1, the embodiment of the present invention 3 is obtained
The extract solution containing tea seed cake the insecticide insecticide efficiency of having withdrawn deposit out splendid to diamondback moth and persistence.
Table 2
The foregoing is only a specific embodiment of the invention, but protection scope of the present invention is not limited thereto, any
Those familiar with the art the invention discloses technical scope in, change or replacement can be readily occurred in, should all be contained
Cover within protection scope of the present invention.Therefore, protection scope of the present invention should be based on the protection scope of the described claims.
Claims (10)
1. the insecticide of a kind of extract solution containing tea seed cake, it is characterised in that the insecticide includes by weight：50-70 parts of tea seed cakes
Extract solution, 5-12 part Tween-80,5-8 parts of alkyl benzene sulphonate sodium salts, 1-5 parts of castor oil, 10-20 parts of ethanol and 1-2 parts of bay nitrogen
Tall and erect ketone.
2. the insecticide of the extract solution according to claim 1 containing tea seed cake, it is characterised in that the insecticide is wrapped by weight
Include：50-70 parts of tea seed cake extract solutions, 5-12 parts of Tween-80s, 5-8 parts of alkyl benzene sulphonate sodium salts, 1-5 parts of castor oil, 10-20 parts of second
Alcohol, 1-2 part Laurocapram and 1-5 parts of sodium sorbates.
3. the insecticide of the extract solution according to claim 2 containing tea seed cake, it is characterised in that also anti-including 0.3-1 parts of Kathon CGs
Rotten agent.
4. the insecticide of the extract solution according to claim 3 containing tea seed cake, it is characterised in that also including 0.1-0.3 parts of xanthan
Glue.
5. the insecticide of the extract solution according to claim 4 containing tea seed cake, it is characterised in that also including 0.1-0.5 portions of sweet oranges
Essence.
6. the insecticide of the extract solution according to claim 1 containing tea seed cake, it is characterised in that the extraction of the tea seed cake extract solution
Raw material is that oil tea is withered and tobacco stem；Extracting method is：By oil tea is withered, tobacco stem added water after crushing and boil and be incubated, filter, take filter
Liquid, obtains the tea seed cake extract solution；The oil tea is withered, the weight ratio of tobacco stem and water is 9-10：2-3：8-10.
7. the insecticide of the extract solution according to claim 6 containing tea seed cake, it is characterised in that 4-6 is incubated at 80-90 DEG C small
When.
8. the method for producing insecticide of any described extract solutions containing tea seed cake of claim 1-7, it is characterised in that the preparation
Method comprises the following steps：
(1) raw material weighed according to parts by weight is well mixed, obtains raw material compound；
(2) the raw material compound is subjected to homogenization, obtains the insecticide of the extract solution containing tea seed cake.
9. preparation method according to claim 8, it is characterised in that the mixing temperature in step (1) is 60-80 DEG C, when
Between be 50-80 minutes.
10. preparation method according to claim 8, it is characterised in that the homogenization temperature in step (2) is 30-50
DEG C, rotating speed is 100-200r/min, and the time is 5-10 minutes.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710363043.XA CN106982865B (en) | 2017-05-22 | 2017-05-22 | A kind of insecticide of the extracting solution containing tea seed cake and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710363043.XA CN106982865B (en) | 2017-05-22 | 2017-05-22 | A kind of insecticide of the extracting solution containing tea seed cake and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106982865A true CN106982865A (en) | 2017-07-28 |
| CN106982865B CN106982865B (en) | 2019-05-24 |
Family
ID=59420068
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710363043.XA Active CN106982865B (en) | 2017-05-22 | 2017-05-22 | A kind of insecticide of the extracting solution containing tea seed cake and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106982865B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109315430A (en) * | 2017-08-01 | 2019-02-12 | 金伟明 | A kind of insecticide and preparation method thereof |
| CN109769863A (en) * | 2019-03-11 | 2019-05-21 | 江苏安心养老服务股份有限公司 | Tea seed cake pesticide composition and preparation method thereof |
| CN111960898A (en) * | 2020-08-21 | 2020-11-20 | 中南林业科技大学 | Water-soluble fertilizer containing tea seed cake extracting solution and application thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1390462A (en) * | 2002-07-03 | 2003-01-15 | 舒朝然 | Biologic insecticidal bactericide without environmental pollution |
| CN102511510A (en) * | 2011-12-05 | 2012-06-27 | 华南理工大学 | Tea saponin biological pesticide and preparation method as well as application thereof |
| CN104222179A (en) * | 2014-09-26 | 2014-12-24 | 广西天峨五福种业有限公司 | Botanical insecticide |
-
2017
- 2017-05-22 CN CN201710363043.XA patent/CN106982865B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1390462A (en) * | 2002-07-03 | 2003-01-15 | 舒朝然 | Biologic insecticidal bactericide without environmental pollution |
| CN102511510A (en) * | 2011-12-05 | 2012-06-27 | 华南理工大学 | Tea saponin biological pesticide and preparation method as well as application thereof |
| CN104222179A (en) * | 2014-09-26 | 2014-12-24 | 广西天峨五福种业有限公司 | Botanical insecticide |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109315430A (en) * | 2017-08-01 | 2019-02-12 | 金伟明 | A kind of insecticide and preparation method thereof |
| CN109769863A (en) * | 2019-03-11 | 2019-05-21 | 江苏安心养老服务股份有限公司 | Tea seed cake pesticide composition and preparation method thereof |
| CN111960898A (en) * | 2020-08-21 | 2020-11-20 | 中南林业科技大学 | Water-soluble fertilizer containing tea seed cake extracting solution and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106982865B (en) | 2019-05-24 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101361494B (en) | Green non-poisonous pesticides and preparation method thereof | |
| CN102754667B (en) | High-efficiency composite botanical pesticide | |
| CN103636660B (en) | A kind of for preventing and treating the Environmental-protection particle agent of Sugarcane Pests | |
| CN103548895A (en) | Botanical vegetable insecticide | |
| CN103875722A (en) | Botanical fungiticide prepared by carrying out combined extraction on Chinese herbal medicines | |
| CN106982865B (en) | A kind of insecticide of the extracting solution containing tea seed cake and preparation method thereof | |
| CN102217659A (en) | Botanical pesticide and its preparation method and use | |
| CN103814964B (en) | A kind of emulsion for killing aphid and two spotted spider mite and preparation method thereof | |
| CN103931678B (en) | A kind of biopesticide and preparation technology thereof preventing and treating Bradysia fungus gnat | |
| CN101209046B (en) | Insecticidal-miticidal composition | |
| CN107996628A (en) | Environment-friendly pesticide and preparation method thereof | |
| CN107646893A (en) | A kind of plants and flowers plant source efficient pesticides and preparation method thereof | |
| CN102578109A (en) | Alkaloid liquid | |
| CN104026163A (en) | Composite natural insecticide for preventing and controlling aphids and preparation method of composite natural insecticide | |
| CN106508978A (en) | Smoke agent for control of greenhouse botrytis cinerea and preparation method thereof | |
| CN105851097A (en) | Botanical insecticide for preventing and controlling cotton bollworm and preparing method thereof | |
| CN105994424A (en) | Preparation method of botanical insect repellent | |
| CN107873743A (en) | Plant insecticide containing selfheal and preparation method thereof | |
| CN109699645A (en) | A kind of citrus tip killing agent and its preparation, application method and application | |
| CN109662106A (en) | A kind of plant source insecticide and preparation method thereof | |
| CN107980820A (en) | Plant insecticide and its preparation method and application | |
| CN103814961B (en) | Tung oil tree paulownia cake extract and beauveria bassiana compounded pesticides and preparation method thereof | |
| CN105410052A (en) | Dichocrocis punctiferalis attractive toxicant | |
| CN103609603A (en) | Botanical insecticide and preparation method thereof | |
| CN107549220A (en) | A kind of gardens synergy compound plant source pesticide and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |