CN106963670A - A kind of marine alga moisture saver mask liquid and preparation method thereof - Google Patents
A kind of marine alga moisture saver mask liquid and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4953—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
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Abstract
The invention discloses a kind of preserving moisture and protecting skin composition containing haematococcus pluvialis extract, count by weight, it includes, 0.1 10 parts of haematococcus pluvialis extract, 0.1 5 parts of tetrahydrochysene methylpyrimidine carboxylic acid, 0.01 0.5 parts of EDETATE SODIUM, 1 180 parts of the first NMF, 0.1 36 parts of the second NMF.Present invention also offers a kind of marine alga moisture saver mask liquid and preparation method thereof.Compared with prior art, facial mask liquid of the present invention is rich in compositions such as astaxanthin, beta glucan and hyaluronic acids, with very strong moisture-keeping efficacy, water lock can be continued, desalinate microgroove, and without glutinous soapy feeling, also contain Ai Keduoyin simultaneously, can releive moisturizing, resist injury of the environmental stimuli to skin.
Description
Technical field
The present invention relates to daily cosmetics technical field, and in particular to a kind of moisturizing face containing haematococcus pluvialis extract
The facial mask that film liquid and its moisture saver mask liquid are made.
Background technology
Skin spreads all over whole body, is the important component of human body.Skin can either be prevented outer as the important barrier of human body
The intrusion of the factors such as the physical chemistry on boundary, also can prevent internal water and nutriment to be lost in through epidermis.Skin surface can be certainly
So formed thin film protection skin, make skin keep lubrication, it is flexible.But as seasonal variations, age increase and personal
The problem of skin quality, the easy water shortage of skin and cause various problems.The key position of skin barrier function is cuticula, it is general and
Speech, the water content of keratoderma is 20%-35%, and now skin lubrication is fine and smooth, glossy, is not likely to produce wrinkle and pigment is heavy
.If the water content of keratoderma is less than 10%, the problems such as dry, the obscure coarse and colour of skin, color spot just occurs in skin.
Therefore the key of nursing skin is the water content of skin to be kept, and reduces the loss of moisture of skin, maintains skin water and oil balance, from
And improve the various problems of skin.
Concern with people to skin care, people have more to improving skin quality by now from initial protection skin is moist
High requirement, allows skin to seem more water profit health, the clear beautiful demand for increasingly becoming people.Improving the basis of skin quality is
Skin moisturizing is given, therefore, a large amount of replenishing water and preserving moisture class skin-protection products arise at the historic moment.At present, the moisturizing in preserving moisture and protecting skin class product into
Dividing mainly has Sodium Hyaluronate, glycine betaine, chitosan, polyalcohol and plant extraction liquid etc., but effect is unsatisfactory, some guarantors
Wet product simply give skin surface carry out moisturizing, using in the rear short time again can recover drying；The moisturizing effect of some moisturizers
Though fruit is good, infiltration rate is slow, is sticked with rear dermal sensation greasy airtight；The moistening effect of some moisturizers is good, infiltration rate
Also it is fast, but with rear skin is astringent and not smooth enough exquisiteness etc..In recent years, with the reach of science, many of nature, which has, protects
Wet, oxidation resistant effective ingredients in plant is found, and is widely used in cosmetics, skin care field.Continually develop new work(
Effect property cosmetics, reach more efficient moistening effect, it has also become the current important subject in this area.
The reason for skin water shortage, which sums up, two, and one is that skin water oil is unbalance, and such as Oily water shortage causes skin
Skin is dried, and Dry then oil starvation fat can not water lock cause dry skin, therefore moisturizing and regulation water and oil balance are moisturizing classes
The current topmost function of cosmetics, while skin water shortage also has Another reason to be external environment, such as prolonged air-conditioning ring
Skin water shortage caused by the skin water shortage that border, the irradiation of prolonged solar UV and rugged environment are caused, this reason
Although the injury to skin can also be alleviated by the method for moisturizing, timely moisturizing and continuous moisturizing are needed, and very
Because odjective cause can not accomplish timely moisturizing when many, very big injury will be caused to skin, thus protect skin not by
The moisturizing product of environmental stimuli more preferably can more fully accomplish preserving moisture and protecting skin.Current moisturizing moisturizing product lacks to this point
Concern.
The content of the invention
It is an object of the invention to provide a kind of preserving moisture and protecting skin composition containing haematococcus pluvialis extract.
The second object of the present invention is to provide a kind of marine alga moisture saver mask liquid containing haematococcus pluvialis extract.
The third object of the present invention is to provide a kind of system of the marine alga moisture saver mask liquid containing haematococcus pluvialis extract
Preparation Method.
To achieve the above object, present invention firstly provides a kind of preserving moisture and protecting skin composition, it includes haematococcus pluvialis extraction
0.1-10 parts of thing, 0.1-5 parts of tetrahydrochysene methylpyrimidine carboxylic acid, 0.01-0.5 parts of EDETATE SODIUM, 1-180 parts of the first NMF, second
0.1-36 parts of NMF.
Preferably, first NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan,
One in 1,3 butylene glycol, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite, PEG/PPG-14/7 dimethyl ethers
Plant or a variety of.
Preferably, second NMF be carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic acid, thoroughly
One kind in the sour sodium of bright matter, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and trehalose
Or it is a variety of.
Preferably, the preserving moisture and protecting skin composition also include anti wrinkling agent, emollient, thickener, emulsifying agent, preservative and/
Or daily essence.
Preferably, the anti wrinkling agent is the one or more in tocopherol acetate, adenosine, niacinamide and collagen；
Preferably, the emollient is pentaerythrite four (thylhexoic acid) ester, White Mineral Oil, dimethyl silicone polymer, ring five
One or more in dimethyl silicone polymer and Miglyol 812N.
Preferably, the thickener is carbomer, xanthans, hydroxyethyl cellulose, PAA/acryloyldimethyl ox
One or more in sodium sulfonate copolymers, C10-30 alkylol acrylamide acid esters cross-linked polymers and the hard ester alcohol of spermaceti.
Preferably, the emulsifying agent is hydrolecithin, lysolecithin, PEG-100 stearates, C12-20 alkyl Portugal
One or more in glucosides and ethylene glycol palmitate.
Preferably, the preservative is parahydroxyacet-ophenone, 1,2- hexylene glycols, methyl hydroxybenzoate, ethyl hydroxy benzoate, oxybenzene third
Ester, imidazolidinyl urea, double imidazolidinyl urea, Phenoxyethanol, methylisothiazolinone, methylchloroisothiazandnone, benzisothia
Oxazoline ketone, iodine propilolic alcohol butyl mephenesin Carbamate, DMDMH, the bromo- 2- nitropropanes -1,3- glycol of 2-, potassium sorbate, benzene
One or more in sodium formate, Chlorphenesin and Sensiva SC50.
Further, the invention provides a kind of marine alga moisture saver mask liquid containing haematococcus pluvialis, by weight percentage
Meter, the facial mask liquid is made up of following components, haematococcus pluvialis extract 0.01-1%, tetrahydrochysene methylpyrimidine carboxylic acid 0.01-
0.5%th, EDETATE SODIUM 0.001-0.05%, the first NMF 0.1-18%, the second NMF 0.01-3.6%, anti wrinkling agent
0.01-1%, emollient 0.1-2%, thickener 0.05-0.5%, emulsifying agent 0.1-4%, preservative 0.3-1%, daily essence
0.01-0.2%, NaOH 0.01-0.1% and deionized water:Its surplus.
Preferably, first NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan,
One in 1,3 butylene glycol, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite, PEG/PPG-14/7 dimethyl ethers
Plant or a variety of.
Preferably, second NMF be carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic acid, thoroughly
One kind in the sour sodium of bright matter, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and trehalose
Or it is a variety of.
Preferably, by weight percentage, the facial mask liquid is made up of following components, haematococcus pluvialis extract 0.05-
0.15%th, tetrahydrochysene methylpyrimidine carboxylic acid 0.01-0.5%, EDETATE SODIUM 0.01-0.05%, the first NMF 3-16%, second protect
Humectant 0.2-2%, anti wrinkling agent 0.1-1%, emollient 0.1-1%, thickener 0.1-0.3%, emulsifying agent 0.2-1%, preservative
0.6-1%, daily essence 0.01-0.1%, NaOH 0.01-0.05% and deionized water:Its surplus；First NMF is
Glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, 1,3 butylene glycol, PEG-400, Natrulon H-10, reed
Fragrant plant oil in two or more；Second NMF is carbohydrate isomer, oat beta-glucan, tetrahydrochysene methylpyrimidine carboxylic
Two or more in acid, Sodium Hyaluronate, mushroom glucan, yeast dextran, chitosan.
Preferably, by weight percentage, the facial mask liquid is made up of following components：Haematococcus pluvialis extract 0.1%,
Tetrahydrochysene methylpyrimidine carboxylic acid 0.05%, EDETATE SODIUM 0.02%, glycerine 3%, methyl propanediol 3%, glycerin polyether -262%, D-
Panthenol 0.1%, succinoglycan 0.08%, carbohydrate isomer 0.3%, oat beta-glucan 0.3%, Sodium Hyaluronate
0.03%th, anti wrinkling agent 0.2%, emollient 0.3%, thickener 0.1%, emulsifying agent 0.8%, preservative 0.9%, daily essence
0.02%th, pH adjusting agent 0.018% and deionized water：Its surplus.
Preferably, by weight percentage, the facial mask liquid is made up of following components：Haematococcus pluvialis extract 0.1%,
Tetrahydrochysene methylpyrimidine carboxylic acid 0.05%, EDETATE SODIUM 0.02%, glycerine 3%, methyl propanediol 3%, glycerin polyether -262%, D-
Panthenol 0.1%, succinoglycan 0.08%, carbohydrate isomer 0.3%, oat beta-glucan 0.3%, Sodium Hyaluronate
0.03%th, tocopherol acetate 0.2%, pentaerythrite four (thylhexoic acid) ester 0.3%, carbomer 0.1%, hydrolecithin
0.5%th, lysolecithin 0.3%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.4%, daily essence 0.02%,
NaOH0.018% and deionized water：Its surplus.
Further, the invention provides the preparation method of marine alga moisture saver mask liquid, including following preparation process：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tocopherol acetate, EDETATE SODIUM, the first moisturizing
Agent, the second NMF, anti wrinkling agent, emollient, thickener, emulsifying agent, preservative, daily essence, pH adjusting agent and deionized water；
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) tocopherol acetate, EDETATE SODIUM, the first NMF, emollient, thickener, emulsifying agent are added residue and gone
Stirred in ionized water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
Ball algae extract, the second NMF, preservative, daily essence and NaOH solution, produce the facial mask liquid after stirring.
Further, the invention provides a kind of marine alga moisture saver mask, the facial mask includes face mask substrate material, the facial mask base
Uniform adsorption has above-described facial mask liquid on material.
Preferably, the face mask substrate material is any one in cotton, silk, non-woven fabrics and biological fiber.
Beneficial effect
The marine alga moisture saver mask liquid of the present invention, its functional component haematococcus pluvialis extract, carbohydrate isomer, tetrahydrochysene
Synergy can be produced between methylpyrimidine carboxylic acid, Sodium Hyaluronate, oat beta-glucan, moistening effect can be strengthened, is continued
Water lock, desalinates microgroove, and without glutinous soapy feeling, while Ai Keduoyin (tetrahydrochysene methylpyrimidine carboxylic acid) addition can preferably protect skin
Skin cell, makes skin from environmental stimuli, moisturizing of releiving, and resists injury of the environmental stimuli to skin.
Embodiment
Following examples are used to illustrate the present invention, but are not limited to the scope of the present invention.Unless otherwise specified, of the invention
Employed in each component can be obtained by way of market is bought.Wherein：
Haematococcus pluvialis extract, Sodium Hyaluronate produce for Fu Ruida；Reed fragrant plant oil is the production of ISP companies of the U.S.；PEG-
400th, hydroxyethyl cellulose produces for Tao Shi, and main component is polyethylene glycol；Oat beta-glucan is raw for fragrant (symrise) of moral
Production, mainly including water, glycerine, beta glucan, 1,2- hexylene glycols, pungent glycol, D-pantothenyl aleohol；Mushroom glucan is that the bright moral of South Korea hundred is public
Department's production；Pyrenomycetes acid, yeast dextran, C12-20 alkyl glucosides, Natrulon H-10 produce for BASF；Adenosine is sincerity
Medicine company is produced；Niacinamide produces for DSM (DSM) company；Collagen produces for France Luo Sailuo；Xanthans is model Derby
Er Te Mineralka D. O. O. produces；White Mineral Oil produces for Germany Shu Mei；Parahydroxyacet-ophenone produces for fragrant (symrise) of moral；
1,2- ethylene glycol produces for Bristol；Carbomer produces for Lu Borun；PEG-400 odium stearate is standing grain big (Croda) production, daily
Essence is fragrant kindness production.
Terminology used in the present invention " pentaerythrite four (thylhexoic acid) ester ", No. CAS be 7299-99-2, code name UN-219,
It is a kind of light emollient.
Terminology used in the present invention " C12-20 alkyl glucosides " be carbon chain lengths be 12-20 natural fatty alcohol with grape
A kind of material of sugar synthesis, commonly uses code name APG.
The term " PEG-400 odium stearate " of the present invention is conventional emulsifying agent, and PEG is the English name of poly- diethanol
Polyethylene glycol abbreviation, the chemical composition of poly- diethanol (PEG) class is generally used as different type area using numeral
Point, such as：PEG-4, PEG-100 etc., numeral are smaller, represent chemical composition and are more easily absorbed by the skin.
Terminology used in the present invention " PEG/PPG-14/7 dimethyl ethers " is methyl oxirane and oxirane dimethyl
The polymer of ether, alias has PEG/PPG-3/6 dimethyl ethers, PEG/PPG-9/2 dimethyl ethers, and No. CAS is 61419-46-3.
Terminology used in the present invention " DMDMH " is 1,3- dihydroxymethyl -5,5- dimethyl hydantoins, also known as
1,3- dihydroxymethyl -5,5- DMH, No. CAS is 6440-58-0, and DMDM is diformazan hydroxyl dimethyl (Dimethylol
Dimethyl abbreviation).
Haematococcus pluvialis belong to volvocales, haematococcus section.Haematococcus pluvialis are that content astaxanthin highest is micro- in nature
Biology, is the best natural origin of astaxanthin.Determination of Astaxanthin in Haematococcus Pluvialis content is 1.5%~3.0%, is counted as natural
" concentrate " of astaxanthin., can be effectively in scavenger-cell and astaxanthin is then one of most strong natural in the world
Oxygen radical, strengthen cytothesis ability, maintain organism balance and reduce senile cell accumulation, from inside to outside protect cell and
DNA health, so as to protect skin health.It is thin that haematococcus pluvialis extract rich in astaxanthin can penetrate into each skin
Born of the same parents, reconstructed collagen albumen and albumen substrate, remold elasticity of skin, and firm skin " insulation barrier " fully keeps moisture of skin, from
And play moisturizing, crease-resistant effect.
Tetrahydrochysene methylpyrimidine carboxylic acid, also referred to as Ai Keduoyin, English name is Ectoin, from high Halophiles
(Halomonas Elongata), the strain is found in Egyptian desert salt lake, therefore the composition is also referred to as " Facultative Halophiles extraction
Liquid ".Under high salt, high temperature, the extreme condition of high ultraviolet radiation, Ectoin makes Halophiles escape injury.Ectoin is a kind of
Amino acid derivativges, belong to extremolytes pressure protection factor classes, extremophile microorganism can be protected to resist extreme environment,
Such as salt lake, hot spring, desert, volcanic crater etc..Ection can build the molecular powerful protective layer of moisture in skin,
Protect skin not injured by inside and outside stimulating factor, prevent skin senescence and cellular damage.
Ectoin protects mechanism：Ectoin is a kind of Kosmotropic regularization materials of strength, and small molecule amino acid spreads out
Biology can fetter the hydrone of surrounding, be formed " ectoin water complex ".Then, this layer of complex parcel again can cell,
Around enzyme, protein and other biomolecule, the Hydration Shell with protection, nourishing and stabilization is formed.Due to containment vessel
In the presence of can reduce skin and not injured by ultraviolet radioactive, pollution particle, the stress factor such as cold and hot, dry.
Carbohydrate isomer is referred to as " water lock magnetite ", is a kind of natural moisture preserving extracted from sugarcane carbohydrate synthesis
Agent, assists the keratin in moisture content combined with stratum corneum, with up to moistening effect.Water lock magnetite is used as a kind of good water-loss reducer and soft
Moisten agent, have effects that to repair epidermal layer cells, lifting skin moisturizing ability.The isomerization D- manufactured via Measurement for Biochemistry
Glucan, with the composition structure close with human keratinous layer, can be combined using on skin with epsilon-amino acid functional group, just as
Firmly combined as magnetite, long-acting can maintain the hydromagnetic field energy power of skin.
Sodium Hyaluronate is also known as sodium hyaluronate sodium, and basic structure is by two dissacharide units D-Glucose aldehydic acid and N- acetyl Portugal
The large-scale polysaccharide of osamine composition.It is different from other mucopolysaccharides, its not sulfur-bearing.Its hyalomitome molecule can carry more than 500 times
Moisture, be it is current recognized by optimal moisturizing ingredient, be widely applied in skin care products and cosmetics.
Oat beta-glucan is a kind of SNSP for being present in oat endosperm and gluten cell wall, can improve skin
Texture, lifts skin elasticity, with excellent moisture-keeping function and repair.
Haematococcus pluvialis extract, carbohydrate isomer, tetrahydrochysene methylpyrimidine carboxylic acid, Sodium Hyaluronate, oat Portugal gather
Synergy can be produced between sugar, moistening effect can be strengthened, continues water lock, desalinates microgroove, and without glutinous soapy feeling, while Ai Ke
More because the addition of (tetrahydrochysene methylpyrimidine carboxylic acid) can preferably protect Skin Cell, make skin from environmental stimuli, releive guarantor
It is wet, resist injury of the environmental stimuli to skin.
Embodiment 1
A kind of marine alga moisture saver mask liquid, by weight percentage, it is made up of following components:Haematococcus pluvialis extract
0.03%th, tetrahydrochysene methylpyrimidine carboxylic acid 0.01%, EDETATE SODIUM 0.01%, glycerine 3%, 1,3 butylene glycol 3%, PEG-
4000.1%th, succinoglycan 0.01%, carbohydrate isomer 0.03%, yeast dextran 0.03%, Sodium Hyaluronate
0.001%th, collagen 0.01%, pentaerythrite (thylhexoic acid) ester 0.1%, carbomer 0.05%, PEG-100 stearates
2%th, parahydroxyacet-ophenone 0.2%, 1,2- hexylene glycols 0.1%, daily essence 0.01%, NaOH 0.01% and deionized water:Its
Surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tetrahydrochysene methylpyrimidine carboxylic acid, EDETATE SODIUM, glycerine,
1,3 butylene glycol, PEG-400, succinoglycan, carbohydrate isomer, yeast dextran, Sodium Hyaluronate, collagen,
Pentaerythrite (thylhexoic acid) ester, carbomer, lysolecithin, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence, NaOH
And deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, 1,3 butylene glycol, PEG-400, succinoglycan, collagen, pentaerythrite (second
Base caproic acid) ester, carbomer, lysolecithin add and stirred in remaining deionized water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
Ball algae extract, tetrahydrochysene methylpyrimidine carboxylic acid, carbohydrate isomer, yeast dextran, Sodium Hyaluronate, para hydroxybenzene second
Ketone, 1,2- hexylene glycols, daily essence and NaOH solution, produce the facial mask liquid after stirring.
Preparing marine alga moisture saver mask then needs to proceed following step：
(5) face mask substrate material cut out (such as silk) is immersed in step (4) in the facial mask liquid of gained, wherein facial mask base
Material (such as silk) and the mass volume ratio of facial mask liquid are 1g:25ml, soak time is 30 minutes, and marine alga moisturizing face is produced after immersion
Film.
Embodiment 2
A kind of marine alga moisture saver mask liquid, by weight percentage, it is made up of following components:Haematococcus pluvialis extract
1%th, tetrahydrochysene methylpyrimidine carboxylic acid 0.5%, EDETATE SODIUM 0.03%, glycerine 5%, methyl propanediol 3%, Natrulon H-10 1%,
Reed fragrant plant oil 0.2%, Scleroglucan 1%, mushroom glucan 1.5%, adenosine 1%, dimethyl silicone polymer 1.8%, carbomer
0.4%th, hydrolecithin 1.8%, lysolecithin 2%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.5%, daily perfume (or spice)
Essence 0.2%, NaOH 0.1% and deionized water:Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tetrahydrochysene methylpyrimidine carboxylic acid, EDETATE SODIUM, glycerine,
Methyl propanediol, Natrulon H-10, reed fragrant plant oil, pyrenomycetes acid, mushroom glucan, adenosine, dimethyl silicone polymer, carbomer, hydrogen
Change lecithin, lysolecithin, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence, NaOH and deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, methyl propanediol, Natrulon H-10, reed fragrant plant oil, adenosine, dimethyl silicone polymer, card
Ripple nurse, hydrolecithin, lysolecithin are added to stir in remaining deionized water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
It is ball algae extract, tetrahydrochysene methylpyrimidine carboxylic acid, pyrenomycetes acid, mushroom glucan, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily
Essence and NaOH solution, produce the facial mask liquid after stirring.
Preparing marine alga moisture saver mask then needs to proceed following step：
(5) face mask substrate material cut out (such as silk) is immersed in step (4) in the facial mask liquid of gained, wherein facial mask base
Material (such as silk) and the mass volume ratio of facial mask liquid are 1g:25ml, soak time is 30 minutes, and marine alga moisturizing face is produced after immersion
Film.
Embodiment 3
A kind of marine alga moisture saver mask liquid, by weight percentage, it is made up of following components：Haematococcus pluvialis extract
0.06%th, tetrahydrochysene methylpyrimidine carboxylic acid 0.03%, EDETATE SODIUM 0.02%, glycerine 4%, methyl propanediol 2%, glycerin polyether-
261%th, D-pantothenyl aleohol 0.1%, succinoglycan 0.01%, carbohydrate isomer 0.1%, oat beta-glucan 0.1%, hyalomitome
Sour sodium 0.01%, niacinamide 0.1%, White Mineral Oil 0.1%, xanthans 0.1%, hydrolecithin 1%, parahydroxyacet-ophenone
0.3%th, 1,2- hexylene glycols 0.3%, daily essence 0.01%, NaOH 0.01% and deionized water:Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tetrahydrochysene methylpyrimidine carboxylic acid, EDETATE SODIUM, glycerine,
Methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, carbohydrate isomer, oat beta-glucan, hyaluronic acid
Sodium, niacinamide, White Mineral Oil, xanthans, hydrolecithin, parahydroxyacet-ophenone, 1,2- hexylene glycols, daily essence, NaOH and go
Ionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, niacinamide, white
Dormant oils, xanthans, hydrolecithin are added to stir in remaining deionized water at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
Ball algae extract, tetrahydrochysene methylpyrimidine carboxylic acid, carbohydrate isomer, oat beta-glucan, Sodium Hyaluronate, para hydroxybenzene second
Ketone, 1,2- hexylene glycols, daily essence and NaOH solution, produce the facial mask liquid after stirring.
Preparing marine alga moisture saver mask then needs to proceed following step：
(5) face mask substrate material cut out (such as silk) is immersed in step (4) in the facial mask liquid of gained, wherein facial mask base
Material (such as silk) and the mass volume ratio of facial mask liquid are 1g:25ml, soak time is 30 minutes, and marine alga moisturizing face is produced after immersion
Film.
Embodiment 4
A kind of marine alga moisture saver mask liquid, by weight percentage, it is made up of following components:Haematococcus pluvialis extract
0.13%th, tetrahydrochysene methylpyrimidine carboxylic acid 0.1%, EDETATE SODIUM 0.04%, glycerine 5%, methyl propanediol 5%, glycerin polyether-
264%th, D-pantothenyl aleohol 1%, succinoglycan 0.1%, carbohydrate isomer 0.5%, oat beta-glucan 0.5%, hyaluronic acid
Sodium 0.05%, tocopherol acetate 0.8%, pentaerythrite (thylhexoic acid) ester 1%, hydroxyethyl cellulose 0.3%, C12-20 alkane
Base glucoside 2%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.5%, daily essence 0.1%, NaOH 0.05% and go from
Sub- water:Its surplus.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tetrahydrochysene methylpyrimidine carboxylic acid, EDETATE SODIUM, glycerine,
Methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, carbohydrate isomer, oat beta-glucan, hyaluronic acid
Sodium, tocopherol acetate, pentaerythrite (thylhexoic acid) ester, hydroxyethyl cellulose, C12-20 alkyl glucosides, para hydroxybenzene second
Ketone, 1,2- hexylene glycols, daily essence, NaOH and deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, tocopherol second
Acid esters, pentaerythrite (thylhexoic acid) ester, hydroxyethyl cellulose, C12-20 alkyl glucosides add in remaining deionized water in
Stirred at 80-85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
Ball algae extract, tetrahydrochysene methylpyrimidine saccharide carboxylic acid isomer, oat beta-glucan, Sodium Hyaluronate, parahydroxyacet-ophenone,
1,2- hexylene glycol, daily essence and NaOH solution, produce the facial mask liquid after stirring.
Preparing marine alga moisture saver mask then needs to proceed following step：
(5) face mask substrate material cut out (such as silk) is immersed in step (4) in the facial mask liquid of gained, wherein facial mask base
Material (such as silk) and the mass volume ratio of facial mask liquid are 1g:25ml, soak time is 30 minutes, and marine alga moisturizing face is produced after immersion
Film.
Embodiment 5
A kind of marine alga moisture saver mask liquid, by weight percentage, it is made up of following components:Haematococcus pluvialis extract
0.1%th, tetrahydrochysene methylpyrimidine carboxylic acid 0.05%, EDETATE SODIUM 0.02%, glycerine 3%, methyl propanediol 3%, glycerin polyether-
262%th, D-pantothenyl aleohol 0.1%, succinoglycan 0.08%, carbohydrate isomer 0.3%, oat beta-glucan 0.3%, hyalomitome
Sour sodium 0.03%, tocopherol acetate 0.2%, pentaerythrite four (thylhexoic acid) ester 0.3%, carbomer 0.1%, hydrogenation lecithin
Fat 0.5%, lysolecithin 0.3%, parahydroxyacet-ophenone 0.5%, 1,2- hexylene glycols 0.4%, (daily) essence 0.02%,
Its surplus of NaOH 0.018%, deionized water.
By said components and percentage by weight, the preparation process of the facial mask liquid includes：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tetrahydrochysene methylpyrimidine carboxylic acid, EDETATE SODIUM, glycerine,
Methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, carbohydrate isomer, oat beta-glucan, hyaluronic acid
Sodium, tocopherol acetate, pentaerythrite (thylhexoic acid) ester, carbomer, hydrolecithin, lysolecithin, para hydroxybenzene second
Ketone, 1,2- hexylene glycols, daily essence, NaOH and deionized water.
(2) portions of de-ionized water is taken, NaOH is added in deionized water and configures NaOH solution；
(3) by EDETATE SODIUM, glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, tocopherol second
Acid esters, pentaerythrite (thylhexoic acid) ester, carbomer, hydrolecithin, lysolecithin are added in remaining deionized water in 80-
Stirred at 85 DEG C；
(4) component mixture in step (3) is cooled to 45-50 DEG C, and it is red to add the rain life of above-mentioned percentage by weight
Ball algae extract, tetrahydrochysene methylpyrimidine carboxylic acid, carbohydrate isomer, oat beta-glucan, Sodium Hyaluronate, para hydroxybenzene second
Ketone, 1,2- hexylene glycols, daily essence and NaOH solution, produce the facial mask liquid after stirring.
Preparing marine alga moisture saver mask then needs to proceed following step：
(5) face mask substrate material cut out (such as silk) is immersed in step (4) in the facial mask liquid of gained, wherein facial mask base
Material (such as silk) and the mass volume ratio of facial mask liquid are 1g:25ml, soak time is 30 minutes, and marine alga moisturizing face is produced after immersion
Film.
Embodiment 6
Respectively by marine alga moisture saver mask liquid made from embodiment 1-5, filling, unlimited bottle cap is carried out with dark brown vial,
It is placed in the environment of 40 DEG C of environment temperature, relative humidity 60%, continuous observation is simultaneously tested, and concrete outcome see the table below 1.Detect micro- life
Thing level, specific detection project, detection method and examination criteria are carried out according to QB/T2872-2007.
The preservative efficacy testing of the marine alga moisture saver mask of table 1
| Observe phenomenon | |
| Embodiment 1 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 2 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 3 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 4 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
| Embodiment 5 | No abnormality seen after 60 days, pure in smell does not detect microorganism |
Embodiment 7
1st, skin care test short run effect
Randomly select female volunteers of 150 ages in 18-45 one full year of life to be tested, be randomly divided into 6 groups, every group 25
People, volunteer signs voluntary book before test.After the cleaned arm of volunteer, constant temperature and humidity (22-25 DEG C of indoor temperature, it is wet
Degree 40-60%) environmental balance position after 30 minutes, with skinanalysis apparatus measure moisture content of skin.Then by present invention implementation
Sample in example 1-5 is applied in corresponding region to 5 groups of volunteers by positioning respectively, respectively after applying 20 minutes, and assessment uses face
The using effect of the area skin after membrane sample.6th group of volunteer does not deal with as blank control.
Evaluation criteria is set to：Humidity of skin is measured assessment using moisture of skin tester, and skin is to film sample
The using effects such as glutinous soapy feeling and smoothness after infiltration rate, use are assessed using sensory evaluation method, i.e., volunteer is according to oneself
Feel be estimated.Final to assess using 3 points of system scorings, humidity does not increase by 1 point, and it is 1 point to absorb slow, and it is 1 point to have glutinous soapy feeling,
With rear skin it is astringent it is rough be 1 point；It is 2 points to absorb very fast, and glutinous soapy feeling is not by force 2 points, and relatively smooth with rear skin is 2 points；
Humidity increases by 3 points, and is easily absorbed as 3 points, is 3 points without glutinous soapy feeling, very smooth with rear skin is 3 points.Score more high effect is better,
Experiment test fractional result is shown in Table 2.
The marine alga moisture saver mask liquid short-period used effect of table 2
| Effect | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | Control group |
| Humidity increase | 67 | 69 | 71 | 75 | 75 | 35 |
| Easily absorb | 75 | 73 | 57 | 55 | 71 | - |
| Glutinous soapy feeling | 72 | 70 | 42 | 43 | 64 | - |
| Smoothness | 54 | 56 | 68 | 69 | 68 | - |
| Total score | 268 | 268 | 238 | 242 | 278 | - |
Test result shows that facial mask of the present invention has obvious moisture-keeping efficacy, the film sample of embodiment 5 in a short time for use
Comprehensive using effect preferably, be more easy to absorb while efficient moisture-retention, glutinous soapy feeling it is less, more smooth using rear skin.
2nd, skin care test long-term effect
Randomly select female volunteers of 125 ages in 18-45 one full year of life to be tested, be randomly divided into 5 groups, every group 25
People, volunteer signs voluntary book before test.After the cleaned arm of volunteer, constant temperature and humidity (22-25 DEG C of indoor temperature, it is wet
Degree 40-60%) environmental balance position after 30 minutes, with skinanalysis apparatus determine skin (including water content, elasticity, carefully
Line), and carry out mark in test position.Sample in 1-5 of the embodiment of the present invention is connected to 5 groups of volunteers by mark position respectively
Continuous application one month.After one month, test badge position skin, each Parameters variation situation before and after contrast assesses long-term
Use the using effect of the area skin after film sample.Experimental result is shown in Table 3.
The marine alga moisture saver mask liquid permanence operation of table 3
| Effect | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Humidity increase | 21 | 22 | 23 | 24 | 25 |
| Elasticity increase | 18 | 20 | 21 | 20 | 22 |
| Microgroove is reduced | 15 | 17 | 19 | 20 | 22 |
Test result shows that facial mask of the present invention has effects that long-acting moisturizing, can increase the water content and elasticity of skin, together
When can also effectively desalinate microgroove.The film sample of embodiment 5, which contrasts other samples, has more preferable effect.
3rd, outdoor test
Volunteer of 150 ages in the outdoor hot operation of 18-45 one full year of life long campaigns is chosen, 6 groups, every group are randomly divided into
25 people, volunteer signs voluntary book before test.Test position is the skin of volunteer's exposure outside.It is (indoor in constant temperature and humidity
22-25 DEG C of temperature, humidity 40-60%) environmental balance positioned after 30 minutes, with skinanalysis apparatus determine moisture content of skin.Will
Sample in 1-5 of the embodiment of the present invention is applied in corresponding region to three groups of volunteers by positioning respectively, respectively after applying 20 minutes,
Test badge position moisture content of skin situation, the 6th group of volunteer is dealt with using other moisturizers.Then 150 volunteers
Hot operation is engaged in open air, after a hour, test badge position moisture content of skin situation, it is average that moisture content of skin rounds group
Value, the unit of moisture content of skin is au, and the situation of change before and after contrast assesses protecting effect of the film sample to skin.Experiment knot
Fruit is shown in Table 4.
The marine alga moisture saver mask liquid outdoor test effect of table 4
It can be seen that, facial mask of the present invention in addition to moistening effect, than similar moisturizer have more preferably resist high temperature, it is high ultraviolet
Injury of the line to skin, protects skin not by environmental stimuli.
In addition, facial mask liquid produced by the present invention, which can not only be applied directly to face, carries out skin nursing, it is also adsorbable in each
Kind of face mask substrate material, such as non-woven fabrics, cotton, silk, on biological fiber, patch formula facial mask is made and uses.By the facial mask liquid of the present invention
Patch formula facial mask is made and carries out face's nursing, it is similar with the above results using result.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, belong to the scope of protection of present invention without departing from theon the basis of the spirit of the present invention.
Claims (10)
1. a kind of preserving moisture and protecting skin composition, it is characterised in that count by weight, it includes：
2. composition as claimed in claim 1, it is characterised in that first NMF is glycerine, methyl propanediol, glycerine
Polyethers -26, D-pantothenyl aleohol, succinoglycan, 1,3 butylene glycol, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite and
One or more in PEG/PPG-14/7 dimethyl ethers；Second NMF be carbohydrate isomer, oat beta-glucan,
One in Sodium Hyaluronate, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, chitosan and trehalose
Plant or a variety of.
3. composition as claimed in claim 1, it is characterised in that the composition also includes：Anti wrinkling agent, emollient, thickening
Agent, emulsifying agent, preservative, pH adjusting agent and/or daily essence.
4. composition as claimed in claim 3, it is characterised in that the anti wrinkling agent is tocopherol acetate, adenosine, niacinamide
With the one or more in collagen；The emollient is pentaerythrite four (thylhexoic acid) ester, White Mineral Oil, poly dimethyl silicon
One or more in oxygen alkane, ring five dimethyl silicone polymer, Miglyol 812N；The thickener is carbomer, Huang
Virgin rubber, hydroxyethyl cellulose, PAA/sodium acryloyldimethyl taurate copolymers, the crosslinking of C10-30 alkylol acrylamides acid esters
One or more in polymer and the hard ester alcohol of spermaceti；The emulsifying agent is hydrolecithin, lysolecithin, PEG-100 hard
One or more in resin acid ester, C12-20 alkyl glucosides and ethylene glycol palmitate；The preservative is para hydroxybenzene second
Ketone, 1,2- hexylene glycols, methyl hydroxybenzoate, ethyl hydroxy benzoate, Nipasol, imidazolidinyl urea, double imidazolidinyl urea, Phenoxyethanol, first
Base OIT, methylchloroisothiazandnone, BIT, iodine propilolic alcohol butyl mephenesin Carbamate, acyl in DMDM second
One kind in the bromo- 2- nitropropanes -1,3- glycol of urea, 2-, potassium sorbate, sodium benzoate, Chlorphenesin and Sensiva SC50
Or it is a variety of.
5. a kind of marine alga moisture saver mask liquid, it is characterised in that by weight percentage, it is made up of following components：
6. facial mask liquid as claimed in claim 5, it is characterised in that first NMF is glycerine, methyl propanediol, glycerine
Polyethers -26, D-pantothenyl aleohol, succinoglycan, 1,3 butylene glycol, pungent glycol, PEG-400, Natrulon H-10, reed fragrant plant oil, sorbierite and
One or more in PEG/PPG-14/7 dimethyl ethers；Second NMF be carbohydrate isomer, oat beta-glucan,
Tetrahydrochysene methylpyrimidine carboxylic acid, Sodium Hyaluronate, Scleroglucan, mushroom glucan, yeast dextran, Aloe Vera Gel, glycine betaine, shell gather
One or more in sugar and trehalose.
7. facial mask liquid as claimed in claim 5, it is characterised in that by weight percentage, it is made up of following components：
First NMF be glycerine, methyl propanediol, glycerin polyether -26, D-pantothenyl aleohol, succinoglycan, 1,3 butylene glycol,
PEG-400, Natrulon H-10, reed fragrant plant oil in two or more；Second NMF is carbohydrate isomer, oat Portugal
Two kinds or several in glycan, tetrahydrochysene methylpyrimidine carboxylic acid, Sodium Hyaluronate, mushroom glucan, yeast dextran, pyrenomycetes acid
Kind.
8. facial mask liquid as claimed in claim 7, it is characterised in that by weight percentage, it is made up of following components：
9. facial mask liquid as claimed in claim 8, it is characterised in that by weight percentage, it is made up of following components：
10. the preparation method of a kind of facial mask liquid as described in one of claim 5-9, it is characterised in that prepare step including following
Suddenly：
(1) each component is weighed in proportion：Haematococcus pluvialis extract, tocopherol acetate, EDETATE SODIUM, the first NMF,
Two NMFs, anti wrinkling agent, emollient, thickener, emulsifying agent, preservative, daily essence, pH adjusting agent and deionized water；
(2) by EDETATE SODIUM, the first NMF, anti wrinkling agent, emollient, thickener, emulsifying agent add in remaining deionized water in
Stirred at 80-85 DEG C；
(3) component mixture in step (2) is cooled to 45-50 DEG C, and adds the haematococcus pluvialis of above-mentioned percentage by weight
Extract, the second NMF, preservative, daily essence and pH adjusting agent, produce the facial mask liquid after stirring.
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