CN106957075A - A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing - Google Patents
A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing Download PDFInfo
- Publication number
- CN106957075A CN106957075A CN201710200215.1A CN201710200215A CN106957075A CN 106957075 A CN106957075 A CN 106957075A CN 201710200215 A CN201710200215 A CN 201710200215A CN 106957075 A CN106957075 A CN 106957075A
- Authority
- CN
- China
- Prior art keywords
- mother solution
- crystalline mother
- drying machine
- centrifugal spray
- air
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/02—Treatment of water, waste water, or sewage by heating
- C02F1/04—Treatment of water, waste water, or sewage by heating by distillation or evaporation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/14—Evaporating with heated gases or vapours or liquids in contact with the liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/22—Evaporating by bringing a thin layer of the liquid into contact with a heated surface
- B01D1/24—Evaporating by bringing a thin layer of the liquid into contact with a heated surface to obtain dry solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D46/00—Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
- B01D46/02—Particle separators, e.g. dust precipitators, having hollow filters made of flexible material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D50/00—Combinations of methods or devices for separating particles from gases or vapours
- B01D50/60—Combinations of devices covered by groups B01D46/00 and B01D47/00
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
- C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
- Y02A50/2351—Atmospheric particulate matter [PM], e.g. carbon smoke microparticles, smog, aerosol particles, dust
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Hydrology & Water Resources (AREA)
- Engineering & Computer Science (AREA)
- Environmental & Geological Engineering (AREA)
- Water Supply & Treatment (AREA)
- Organic Chemistry (AREA)
- Drying Of Solid Materials (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention discloses a kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing, including drying machine with centrifugal spray, the feed end of drying machine with centrifugal spray connects the crystalline element of saliferous crystalline mother solution by pipeline, connects heated air source by pipeline；The gas discharge end of drying machine with centrifugal spray is sequentially connected cyclone separator and sack cleaner by pipeline, and the gas discharge end of sack cleaner passes through Pipe installing Venturi scrubber and gas-liquid separator.The present invention is heated using hot-blast stove to air, crystalline mother solution is then atomized by spray dryer, and by with hot-air current contacting, rapid draing is carnallite, the device can be handled effectively crystalline mother solution in industrial wastewater, reduce the amount of subsequent treatment, it is to avoid pollution to environment.
Description
Technical field：
The present invention relates to Coal Chemical Industry draining technology field, a kind of particularly industrial brine waste crystalline mother solution of safe and low consumption processing
Process unit.
Background technology：
Coal Chemical Industry process is that coal is converted into gas, liquid and solid product or half product, be then further processed into chemical industry,
The industry of energy products.Meanwhile, the energy actual features of China are oil starvation, few gas, coal resources relative abundance, and coal valency
Lattice relative moderate, therefore coal chemical industry has the huge market demand and opportunity to develop in China.New Coal Chemical Industry will
Chinese energy it is sustainable during play the part of important role, the coal-fired environmental pollution caused, reduction are mitigated to China from now on
Dependence to Imported oil, domestic economy has great meaning.
But along with the often urgent problem to be solved of opportunity.New Coal Chemical water consumption is huge, year water consumption it is usual
Up to thousands of ten thousand stere even more highs, the fast development of Coal Chemical Industry has triggered the unbalance of regional water resources.Therefore Coal Chemical Industry is given up
Water zero discharge becomes the unique channel for solving this problem.In the development process of zero-discharge technology, increasing expert
Arrived with focus of attention, the difficult point of zero-discharge technology with emphasis often not in the recovery of water, but in the money of final solid abraum salt
Sourceization is utilized, and in the processing of useless Organic substance in water.
With regard to it is domestic at present in the Coal Chemical Engineering Project of operation for, existing two to three realize the " useless of Coal Chemical Engineering Project
Water zero discharge ", but equally exist major defect；For the Inner Mongol project of successful operation, have been realized in
The output of crystal salt.But the mother liquor discharged for crystallization apparatus is not well solved but.What the current project was taken
Measure is to direct cycle to mother liquor in front end system, causes plurality of impurities to be enriched with, fluctuation of service, reclaims condensate liquid water quality and reaches
Mark is difficult, while output crystal salt is brown, the phenomenon such as salt component is impure, it is impossible to complete the recycling of moisture and solid salt.This
If kind of a situation cannot rationally improve, while being impacted to environment, the economic benefit of factory can be also had a strong impact on.
For the crystalline mother solution of coal chemical industrial waste water, more safe processing mode is carries out burning disposal at present.But by
Salt content is very high in coal chemical industrial waste water crystalline mother solution, and the characteristics of particularly chloride ion content is higher causes incinerator
Equipment material is higher, and investment cost is greatly promoted；Simultaneously because containing substantial amounts of COD impurity in crystalline mother solution, to avoid burning
During produce the formation secondary pollution of the noxious material such as bioxin, therefore cause the operation operating mode of incinerator extremely harsh, pole
The big operating cost for adding device.Therefore either investment cost, or operating cost, all serious limits burning work
Application of the skill in the disposal of coal chemical industrial waste water crystalline mother solution.
The content of the invention：
The invention aims to solve the deficiencies in the prior art, there is provided a kind of industrial brine waste knot of safe and low consumption processing
The process unit of brilliant mother liquor.
The technical solution adopted by the present invention is：
A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing, including drying machine with centrifugal spray, its feature
It is：
The feed end of the drying machine with centrifugal spray is connected the crystalline element of saliferous crystalline mother solution by pipeline, connected by pipeline
Heated air source；The gas discharge end of drying machine with centrifugal spray is sequentially connected cyclone separator and sack cleaner, cloth by pipeline
The gas discharge end of bag dust collector passes through Pipe installing Venturi scrubber and gas-liquid separator；
Hot-air enters after the air distributor at the top of drying machine with centrifugal spray in the shape of a spiral evenly into centrifugal spray drying
The high speed centrifugal atomization device that the hothouse of machine, saliferous crystalline mother solution enter at the top of drying machine with centrifugal spray forms imperceptible mist
Shape liquid pearl enters the hothouse of drying machine with centrifugal spray, and hot-air was contacted with vaporific saliferous crystalline mother solution and in the extremely short time
Interior to dry as carnallite, carnallite is continuously arranged by the bottom of drying machine with centrifugal spray bottom, cyclone dust collectors and sack cleaner
Go out and keep in, waste gas high altitude discharge up to standard after being washed by air-introduced machine through Venturi scrubber, a small amount of tail gas is through gas-liquid separator
Biochemical device is sent to handle by washings.
A kind of process unit of the described industrial brine waste crystalline mother solution of safe and low consumption processing, it is characterised in that：
The heated air source is produced by fuel gas hot-blast stove combustion gas, fuel gas hot-blast stove connection air blower and air filter, air
After air filter, heating feeding drying machine with centrifugal spray in fuel gas hot-blast stove is sent into through air blower.
A kind of process unit of the described industrial brine waste crystalline mother solution of safe and low consumption processing, it is characterised in that：
Air-introduced machine is set on pipeline between the sack cleaner and Venturi scrubber.
A kind of process unit of the described industrial brine waste crystalline mother solution of safe and low consumption processing, it is characterised in that：
The Venturi scrubber is presented lower structure arrangement, tail head with gas-liquid separator and connected.
A kind of process unit of the described industrial brine waste crystalline mother solution of safe and low consumption processing, it is characterised in that：
The atomizer sprayer of the drying machine with centrifugal spray is made using dual phase steel.
Compared with prior art, the beneficial effects of the present invention are：
Invention introduces spray drying technology, solving crystalline mother solution can not arrange outside, system can not stable operation shortcoming；
Scheme, the limitation of high operating cost with high investment, and the maturity of spray drying technology such as mother liquor burning are overcome, is also fully protected
The stability to crystalline mother solution processing is demonstrate,proved；
The present invention air is heated using hot-blast stove, crystalline mother solution is then atomized by spray dryer, and by with
Hot-air current contacting, rapid draing is carnallite, and the device can be handled effectively crystalline mother solution in industrial wastewater, reduction
The amount of subsequent treatment, it is to avoid pollution to environment.
Brief description of the drawings：
Fig. 1 is structural representation of the invention.
Embodiment：
Below in conjunction with the accompanying drawings, the present invention is described in further detail by embodiment：
A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing, including drying machine with centrifugal spray 1, centrifugation spray
The feed end of mist drying machine 1 is connected the crystalline element of saliferous crystalline mother solution by pipeline, connects heated air source by pipeline；Centrifugation
The gas discharge end of spray dryer 1 is sequentially connected cyclone separator 2 and sack cleaner 3 by pipeline, sack cleaner 3
Gas discharge end passes through Pipe installing Venturi scrubber 4 and gas-liquid separator 5；
Hot-air enters after the air distributor at the top of drying machine with centrifugal spray 1 in the shape of a spiral evenly into centrifugal spray drying
The high speed centrifugal atomization device that the hothouse of machine 1, saliferous crystalline mother solution enter the top of drying machine with centrifugal spray 1 forms imperceptible
Vaporific liquid pearl enters the hothouse of drying machine with centrifugal spray 1, and hot-air is contacted and extremely short with vaporific saliferous crystalline mother solution
It can be dried in time as carnallite, carnallite is continuously by the bottom of drying machine with centrifugal spray 1, cyclone dust collectors 2 and sack cleaner 3
Bottom is discharged and kept in, waste gas high altitude discharge up to standard after being washed by air-introduced machine through Venturi scrubber 4, and a small amount of tail gas is through gas-liquid
Separator 5 send biochemical device to handle by washings.
Heated air source is produced by the combustion gas of fuel gas hot-blast stove 6, the connection air blower 7 of fuel gas hot-blast stove 6 and air filter 8,
Air is sent into after being heated in fuel gas hot-blast stove 6 through air blower 7 after air filter 8 and sends into drying machine with centrifugal spray 1.
Air-introduced machine 9 is set on the pipeline between sack cleaner 3 and Venturi scrubber 4.
Venturi scrubber 4 is connected with gas-liquid separator 5 in up-down structure arrangement, tail head.
The outer row's mother liquor of Coal Chemical Engineering Industry brine waste crystallization is handled using above technical scheme, it is truly complete
It has been apt to the final step of zero discharge of industrial waste water technology.It is relatively low with its while ensureing that impurity does not influence on front end process
Equipment investment and operating cost, have fully demonstrated its feasibility applied in technique of zero discharge.
The innovative point of the present invention is as follows：
Spray drying technology is introduced, the new method of processing Coal Chemical Industry brine waste crystalline mother solution is used as.The process unit is solved
Saliferous crystalline mother solution can not arranged outside, system can not stable operation shortcoming；Also overcome the schemes, height with high investment such as mother liquor burning
The limitation of operating cost, and the maturity of spray drying technology, have also fully ensured that the stabilization to the processing of saliferous crystalline mother solution
Property；
For Coal Chemical Industry brine waste water quality characteristicses, the atomizer sprayer of drying machine with centrifugal spray 1 uses dual phase steel, prevents dense salt
Corrosion of the water to equipment；Simultaneously its sprayer make injection liquid in small angular cone shape spray, can prevent crystalline mother solution and
Equipment inner wall is directly contacted, it is to avoid crystal salt is lumpd on equipment inner wall；Equipment material uses two-phase steel composite board, reduces equipment
Investment；
For the actual conditions containing organic matter in strong brine, strict control desiccation temperature reduces organic matter volatilization；
Increase Venturi scrubber 4 is washed to tail gas, it is ensured that no pollution of the crystalline mother solution to surrounding environment；Use and draw simultaneously
Blower fan 9 is pressurized to tail gas, reduces subsequent wash system scale.
Above-described embodiment is only the preferably embodiment of the present invention, and in addition, the present invention can also have other realizations
Mode.It should be noted that on the premise of without departing from present inventive concept, any conspicuously improved and modification all should fall
Enter within protection scope of the present invention.
Claims (5)
1. a kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing, including drying machine with centrifugal spray, it is special
Levy and be：
The feed end of the drying machine with centrifugal spray is connected the crystalline element of saliferous crystalline mother solution by pipeline, connected by pipeline
Heated air source；The gas discharge end of drying machine with centrifugal spray is sequentially connected cyclone separator and sack cleaner, cloth by pipeline
The gas discharge end of bag dust collector passes through Pipe installing Venturi scrubber and gas-liquid separator；
Hot-air enters after the air distributor at the top of drying machine with centrifugal spray in the shape of a spiral evenly into centrifugal spray drying
The high speed centrifugal atomization device that the hothouse of machine, saliferous crystalline mother solution enter at the top of drying machine with centrifugal spray forms imperceptible mist
Shape liquid pearl enters the hothouse of drying machine with centrifugal spray, and hot-air was contacted with vaporific saliferous crystalline mother solution and in the extremely short time
Interior to dry as carnallite, carnallite is continuously arranged by the bottom of drying machine with centrifugal spray bottom, cyclone dust collectors and sack cleaner
Go out and keep in, waste gas high altitude discharge up to standard after being washed by air-introduced machine through Venturi scrubber, a small amount of tail gas is through gas-liquid separator
Biochemical device is sent to handle by washings.
2. a kind of process unit of industrial brine waste crystalline mother solution of safe and low consumption processing according to claim 1, it is special
Levy and be：
The heated air source is produced by fuel gas hot-blast stove combustion gas, fuel gas hot-blast stove connection air blower and air filter, air
After air filter, heating feeding drying machine with centrifugal spray in fuel gas hot-blast stove is sent into through air blower.
3. a kind of process unit of industrial brine waste crystalline mother solution of safe and low consumption processing according to claim 1, it is special
Levy and be：
Air-introduced machine is set on pipeline between the sack cleaner and Venturi scrubber.
4. a kind of process unit of industrial brine waste crystalline mother solution of safe and low consumption processing according to claim 1, it is special
Levy and be：
The Venturi scrubber is presented lower structure arrangement, tail head with gas-liquid separator and connected.
5. a kind of process unit of industrial brine waste crystalline mother solution of safe and low consumption processing according to claim 1, it is special
Levy and be：
The atomizer sprayer of the drying machine with centrifugal spray is made using dual phase steel.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710200215.1A CN106957075A (en) | 2017-03-30 | 2017-03-30 | A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710200215.1A CN106957075A (en) | 2017-03-30 | 2017-03-30 | A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing |
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| Publication Number | Publication Date |
|---|---|
| CN106957075A true CN106957075A (en) | 2017-07-18 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710200215.1A Pending CN106957075A (en) | 2017-03-30 | 2017-03-30 | A kind of process unit of the industrial brine waste crystalline mother solution of safe and low consumption processing |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108178217A (en) * | 2018-01-08 | 2018-06-19 | 华电水务工程有限公司 | A kind of high slat-containing wastewater is evaporated system and technique |
| CN109569163A (en) * | 2018-12-31 | 2019-04-05 | 阮氏化工（常熟）有限公司 | The method of high-concentration metallic ions acid-bearing wastewater recycling metal salt product |
| CN110803821A (en) * | 2019-12-20 | 2020-02-18 | 安徽金禾实业股份有限公司 | Method for deep treatment of concentrated liquid of sucralose high-salinity wastewater |
| CN114229871A (en) * | 2021-12-06 | 2022-03-25 | 宜宾海丰和锐有限公司 | Method for improving stability of ketone method hydrazine hydrate byproduct salt water evaporation system |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4882009A (en) * | 1987-07-13 | 1989-11-21 | Four Nines, Inc. | Apparatus for concentrating brine waters or dewatering brines generated in well drilling operation |
| CN202315347U (en) * | 2011-11-23 | 2012-07-11 | 四川康源医疗设备有限公司 | Centrifugal spray drying system with deduster |
| CN106315719A (en) * | 2015-06-23 | 2017-01-11 | 李全跃 | Antibiotic organic wastewater and drug residue treatment process |
-
2017
- 2017-03-30 CN CN201710200215.1A patent/CN106957075A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4882009A (en) * | 1987-07-13 | 1989-11-21 | Four Nines, Inc. | Apparatus for concentrating brine waters or dewatering brines generated in well drilling operation |
| CN202315347U (en) * | 2011-11-23 | 2012-07-11 | 四川康源医疗设备有限公司 | Centrifugal spray drying system with deduster |
| CN106315719A (en) * | 2015-06-23 | 2017-01-11 | 李全跃 | Antibiotic organic wastewater and drug residue treatment process |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108178217A (en) * | 2018-01-08 | 2018-06-19 | 华电水务工程有限公司 | A kind of high slat-containing wastewater is evaporated system and technique |
| CN109569163A (en) * | 2018-12-31 | 2019-04-05 | 阮氏化工（常熟）有限公司 | The method of high-concentration metallic ions acid-bearing wastewater recycling metal salt product |
| CN110803821A (en) * | 2019-12-20 | 2020-02-18 | 安徽金禾实业股份有限公司 | Method for deep treatment of concentrated liquid of sucralose high-salinity wastewater |
| CN114229871A (en) * | 2021-12-06 | 2022-03-25 | 宜宾海丰和锐有限公司 | Method for improving stability of ketone method hydrazine hydrate byproduct salt water evaporation system |
| CN114229871B (en) * | 2021-12-06 | 2024-02-13 | 宜宾海丰和锐有限公司 | Method for improving stability of evaporation system of byproduct brine of ketone hydrazine hydrate |
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Application publication date: 20170718 |