CN106956000A - A kind of fast preparation method of TiAl-base alloy drip molding - Google Patents
A kind of fast preparation method of TiAl-base alloy drip molding Download PDFInfo
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- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
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- B22F10/00—Additive manufacturing of workpieces or articles from metallic powder
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- B22F12/00—Apparatus or devices specially adapted for additive manufacturing; Auxiliary means for additive manufacturing; Combinations of additive manufacturing apparatus or devices with other processing apparatus or devices
- B22F12/50—Means for feeding of material, e.g. heads
- B22F12/53—Nozzles
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- Y02P10/25—Process efficiency
Abstract
The invention discloses a kind of fast preparation method of TiAl-base alloy drip molding, step is as follows:The three-dimensional entity model of TiAl-base alloy drip molding is set up, the geological information of each cross section is obtained by hierarchy slicing, and is converted into numerical control table, NC table motion track information;Substrate is fixed on the numerical control table, NC table of five-axle linkage, substrate is partially melting to form molten bath in the presence of laser, while being allowed to melt by the heat affected area that TiAl-base alloy pre-alloyed powder sends into laser using synchronous powder feeding system method;Now numerical control table, NC table is moved according to the track of setting so that in substrate surface formation cladding layer;New sedimentary is frozen on the basis of first layer cladding layer, is successively accumulated afterwards, 3D solid drip molding is finally given, Milling Process finally is carried out to drip molding surface.The present invention achievable multi items, the quick manufacture of parts in small batch, have the advantages that stock utilization height, processing flexibility are high, and drip molding room-temperature mechanical property is excellent, easy to utilize.
Description
Technical field
The present invention relates to a kind of brittle metal material forming techniques, particularly a kind of quick system of TiAl-base alloy drip molding
Preparation Method.
Background technology
TiAl-base alloy has the advantages that low-density, high-melting-point, high elastic modulus and high specific strength, there is good at high temperature
Good creep resistant and antioxygenic property, it is considered to be preferably high-temperature structural material of future generation.But TiAl-base alloy room temperature is moulded
Property is poor, and the characteristics of shaping difficulty is the major obstacle of its development and application.
The traditional forming methods of TiAl-base alloy include ingot metallurgy, hot investment casting and powder metallurgic method.Ingot metallurgy
Method can obtain that even tissue is tiny, better performances TiAl-base alloy drip moldings, but its complex process, allowance are big, material
Expect that utilization rate is low.In addition, the forward and backward treatment process of ingot metallurgy is more, duration is processed, production cost is added.At present, cast
TiAl-base alloy has come into the commercial Application stage.Foundry engieering low cost, can direct forming, but common contracting in casting
Hole, shrinkage porosite, component segregation, organize the defect such as thick to be equally existed in TiAl-base alloy precision castings, have a strong impact on the power of alloy
Learn performance.Powder metallurgic method effectively prevent the casting flaws such as segregation, shrinkage porosite, shrinkage cavity, can prepare even tissue, tiny
TiAl-base alloy drip molding, and the near-net-shape of baroque part can be realized.However, alloy in preparation process easily by
The pollution of interstitial element, it is oxygen-containing to wait impurity more, cause plasticity lower.In addition, the control of porosity is also powder metallurgy legal system
The subject matter that standby TiAl-base alloy faces.
In order to further expand the application scale of TiAl-base alloy, it is necessary to improve combination property and the reduction of TiAl-base alloy
Production cost.All there is respective limitation in TiAl-base alloy traditional forming methods and difficulty has compared with quantum jump, Development of Novel in a short time
TiAl-base alloy forming technology is to solve the important directions that TiAl-base alloy shapes problem.The method that the present invention is used is one
Plant advanced near-net-shape technique.Compared to the traditional forming methods of TiAl-base alloy, the method that the present invention is used exists following
Advantage:(1) traditional mould and large scale industry facility is not needed, manufacturing procedure is few, stock utilization is high, follow-up machining is remaining
Amount is small, reduces production cost;(2) it is flexible high, multi items, the quick manufacture of parts in small batch can be achieved;(3) process material
The cooling velocity of material is fast, and the microscopic structure of drip molding is tiny, and it is scarce to avoid macrostructure common in traditional casting, forging
Fall into, mechanical property is preferable.
The content of the invention
It is an object of the invention to provide a kind of production cost is low, forming speed is fast, stock utilization is high, drip molding room temperature
The TiAl-base alloy preparation method of excellent in mechanical performance so that it is poor to solve current TiAl-base alloy material temperature-room type plasticity, tradition into
Shape method prepares the problem of difficulty is big.
Realize that the object of the invention technical solution is:A kind of fast preparation method of TiAl-base alloy drip molding, including
Following steps:
Step 1, the three-dimensional entity model of drip molding is set up, the geological information of each cross section is obtained by hierarchy slicing,
And it is converted into numerical control table, NC table motion track information;
Step 2, substrate is fixed on the numerical control table, NC table of five-axle linkage, substrate local melting in the presence of laser beam
Molten bath is formed, while being allowed to melt by the heat affected area that TiAl-base alloy pre-alloyed powder sends into laser using synchronous powder feeding system method;
Now numerical control table, NC table is moved according to the track obtained by step 1 so that in substrate surface formation first layer cladding layer;
Step 3, laser head and powder-feeding nozzle are risen to cladding layer thickness identical highly, laser beam will enter hot shadow
The powder for ringing area is heated and melted, and new sedimentary is frozen on the basis of first layer cladding layer, is successively accumulated afterwards, finally
Obtain 3D solid drip molding;
Step 4, Milling Process is carried out to drip molding outer surface, is met the drip molding of surface finish requirements.
Preferably, in step 2, described TiAl-base alloy pre-alloyed powder is particle size range between 50~150 μm
Spherical powder.
Preferably, in step 2, using argon gas as whole process protection atmosphere, wherein laser processing parameter is:Laser power
For:200~2200W, sweep speed is:80~1080mm/min, powder feeding rate be 0.8~5.7g/min, defocusing amount be 6~
10mm。
Preferably, in step 2, the generation equipment of laser beam is CO2Laser, Nd:YAG laser, optical fiber laser or
Semiconductor laser.
Compared with prior art, its remarkable advantage is the present invention:Traditional mould and large scale industry facility is not needed,
Manufacturing procedure is few, reduces production cost.(1) manufacturing process is quick, and stock utilization is high, low cost;(2) it is flexible high, can be real
Existing multi items, the quick manufacture of parts in small batch;(3) cooling velocity of process material is fast, drip molding fine microstructures, and keeps away
Macrostructure's defect common in traditional casting, forging is exempted from, mechanical property is preferable;(4) follow-up machining allowance is small, is easy to push away
Wide application.
Embodiment
The means that the present invention is combined based on laser melting coating and increasing material manufacturing, TiAl base prealloys are made using laser as thermal source
Powder fusing, cooling, solidification forming, so as to solve the processing problem of TiAl-base alloy.
A kind of fast preparation method of TiAl-base alloy drip molding, is comprised the following specific steps that:
Step 1, the three-dimensional entity model of TiAl-base alloy drip molding is set up, each cross section is obtained by hierarchy slicing
Geological information, and it is converted into numerical control table, NC table motion track information;
Step 2, substrate is fixed on the numerical control table, NC table of five-axle linkage, substrate local melting shape in the presence of laser
Into molten bath, while the heat affected area that TiAl-base alloy pre-alloyed powder sends into laser is allowed to melt using synchronous powder feeding system method;This
When numerical control table, NC table moved according to the track obtained by step 1 so that in substrate surface formation first layer cladding layer;Used by this step
TiAl-base alloy pre-alloyed powder be spherical powder of the particle size range between 50~150 μm.Process is made using argon gas
For protective atmosphere, wherein laser processing parameter is:Laser power is:200~2200W, sweep speed is:80~1080mm/
Min, powder feeding rate is 0.8~5.7g/min, and defocusing amount is 6~10mm.The generation equipment of the laser beam is CO2Laser,
Nd:YAG laser, optical fiber laser or semiconductor laser.
Step 3, laser head and powder-feeding nozzle are risen to cladding layer thickness identical highly, laser beam will enter hot shadow
The powder for ringing area is heated and melted, and new sedimentary is frozen on the basis of first layer cladding layer, is successively accumulated afterwards, finally
Obtain TiAl-base alloy 3D solid drip molding;It is consistent wherein in laser processing parameter, powder feeding rate and step 2.
Step 4, Milling Process is carried out to drip molding outer surface, is met the TiAl-base alloy shaping of surface finish requirements
Part.
In order that present disclosure is more easily understood, the present invention is explained below by specific embodiment
Release.
Embodiment 1
A kind of fast preparation method of TiAl-base alloy drip molding, its preparation process is as follows:
(1) 50~150 μm of Ti-46Al-2Nb-2Cr alloy spherical powder is put into 100 DEG C of drying in vacuum drying chamber
20h, removes the moisture in powder.
(2) using TC4 titanium alloy sheets as matrix material, and 60mm*60mm*10mm size is cut into, will with sand paper
The oxide-film of substrate surface is removed, and clean with alcohol washes.
(3) three-dimensional CAD model of part is pressed into certain thickness hierarchy slicing, is converted to a series of two-dimensional geometry information,
According to these information, and it is converted into numerical control table, NC table motion track information.
(4) substrate is fixed on the numerical control table, NC table of five-axle linkage, source, laser apparatus is used as using 200W optical fiber laser
Standby, process is used as protective atmosphere using argon gas.Base material is partially melting to form molten bath in the presence of laser, while using same
Walk in the heat affected area that powder-feeding method makes TiAl-base alloy pre-alloyed powder enter laser with certain speed and in superlaser
Effect is lower to melt, and forms cooled and solidified after molten drop is fallen into molten bath.Now workbench according to CAD give each layer cross section track
Information is moved in X, Y direction.So that forming cladding layer in the specific region of substrate surface;Machined parameters are:Laser power
200W, sweep speed 80mm/min, powder feeding rate 0.8g/min, defocusing amount 6mm, carrier gas flux is 13L/min.
(5) laser head and powder-feeding nozzle are risen to previous cladding layer thickness identical highly, it is ensured that cladding it is new one
Layer when defocusing amount with it is consistent before.In the presence of high energy laser beam, layer segment fusing is deposited, while into laser heat affecting
The powder in area melt to be formed molten drop fall into molten bath and with molten bath together cooled and solidified, solidified on the basis of first layer cladding layer
Cheng Xin sedimentary, successively accumulates afterwards, is completed until prepared by whole TiAl-base alloy drip molding.
(6) Milling Process is carried out to drip molding outer surface, is met the TiAl-base alloy drip molding of surface finish requirements.
Embodiment 2
A kind of fast preparation method of TiAl-base alloy drip molding, its preparation process is as follows:
(1) 50~150 μm of Ti-46Al-2Nb-2Cr alloy powders are dried according to the methods described of embodiment 1.
(2) three-dimensional CAD model of part is pressed into certain thickness hierarchy slicing, is converted to a series of two-dimensional geometry information,
According to these information, and it is converted into numerical control table, NC table motion track information.
(3) it will be fixed on the numerical control table, NC table of five-axle linkage, adopt after TC4 titanium alloy substrate surface treateds thick 20mm
With 4kW semiconductor laser as laser equipment, process is used as protective atmosphere using argon gas.Effect of the base material in laser
Under be partially melting to form molten bath, swash while using synchronous powder feeding system method TiAl-base alloy pre-alloyed powder is entered with certain speed
Melted in the heat affected area of light and in the presence of superlaser, form cooled and solidified after molten drop is fallen into molten bath.Workbench is pressed
Moved according to the trace information of the given each layer cross sections of CAD in X, Y direction.So that forming molten in the specific region of substrate surface
Coating;Machined parameters are:Laser power 2200W, sweep speed 600mm/min, powder feeding rate 5.7g/min, defocusing amount 10mm,
Carrier gas flux is 20L/min.
(4) laser head and powder-feeding nozzle are risen to previous cladding layer thickness identical highly.In high energy laser beam
Under effect, layer segment fusing is deposited, while the powder into laser heat affected area melts and to form molten drop and fall into molten bath, the
New sedimentary is frozen on the basis of one layer of cladding layer.
(5) (3)~(4) step is repeated, is completed until prepared by whole TiAl-base alloy drip molding.
(6) Milling Process is carried out to drip molding outer surface, is met the TiAl-base alloy drip molding of surface finish requirements.
Embodiment 3
A kind of fast preparation method of TiAl-base alloy drip molding, its preparation process is as follows:
(1) 50~150 μm of Ti-43Al-9V-Y alloy powders are dried according to step described in embodiment 1.
(2) three-dimensional CAD model of part is pressed into certain thickness hierarchy slicing, is converted to a series of two-dimensional geometry information,
According to these information, and it is converted into numerical control table, NC table motion track information.
(3) it will be fixed on the numerical control table, NC table of five-axle linkage, adopt after TC4 titanium alloy substrate surface treateds thick 10mm
With 200W optical fiber laser as laser equipment, process is used as protective atmosphere using argon gas.Effect of the base material in laser
Under be partially melting to form molten bath, swash while using synchronous powder feeding system method TiAl-base alloy pre-alloyed powder is entered with certain speed
Melted in the heat affected area of light and in the presence of superlaser, form cooled and solidified after molten drop is fallen into molten bath.Workbench is pressed
Moved according to the trace information of the given each layer cross sections of CAD in X, Y direction.So that forming molten in the specific region of substrate surface
Coating;Machined parameters are:Laser power 200W, sweep speed 80mm/min, powder feeding rate 0.8g/min, defocusing amount 6mm, carrier gas
Flow is 13L/min.
(4) laser head and powder-feeding nozzle are risen to previous cladding layer thickness identical highly.In high energy laser beam
Under effect, layer segment fusing is deposited, while the powder into laser heat affected area melts and to form molten drop and fall into molten bath, the
New sedimentary is frozen on the basis of one layer of cladding layer.
(5) (3)~(4) step is repeated, is completed until prepared by whole TiAl-base alloy drip molding.
(6) Milling Process is carried out to drip molding outer surface, is met the TiAl-base alloy drip molding of surface finish requirements.
Embodiment 4
A kind of fast preparation method of TiAl-base alloy drip molding, its preparation process is as follows:
(1) 50~150 μm of Ti-43Al-9V-Y alloy powders are dried according to step described in embodiment 1.
(2) three-dimensional CAD model of part is pressed into certain thickness hierarchy slicing, is converted to a series of two-dimensional geometry information,
According to these information, and it is converted into numerical control table, NC table motion track information.
(3) it will be fixed on the numerical control table, NC table of five-axle linkage, adopt after TC4 titanium alloy substrate surface treateds thick 20mm
With 4kW semiconductor laser as laser equipment, process is used as protective atmosphere using argon gas.Effect of the base material in laser
Under be partially melting to form molten bath, swash while using synchronous powder feeding system method TiAl-base alloy pre-alloyed powder is entered with certain speed
Melted in the heat affected area of light and in the presence of superlaser, form cooled and solidified after molten drop is fallen into molten bath.Workbench is pressed
Moved according to the trace information of the given each layer cross sections of CAD in X, Y direction.So that forming molten in the specific region of substrate surface
Coating;Machined parameters are:Laser power 2200W, sweep speed 600mm/min, powder feeding rate 5.7g/min, defocusing amount 10mm,
Carrier gas flux is 20L/min.
(4) laser head and powder-feeding nozzle are risen to previous cladding layer thickness identical highly.In high energy laser beam
Under effect, layer segment fusing is deposited, while the powder into laser heat affected area melts and to form molten drop and fall into molten bath, the
New sedimentary is frozen on the basis of one layer of cladding layer.
(5) (3)~(4) step is repeated, is completed until prepared by whole TiAl-base alloy drip molding.
(6) Milling Process is carried out to drip molding outer surface, is met the TiAl-base alloy drip molding of surface finish requirements.
Comparative example 1
The TiAl-base alloy drip molding prepared for the TiAl-base alloy drip molding relatively more of the invention prepared with conventional method
Difference on room-temperature mechanical property, is compressed, tensile sample using wire cutting machine cutting, grinds off wire cutting trace after cutting with sand paper
Mark simultaneously carries out cleaning removing surface smut in alcohol with ultrasonic activation.Carried out on omnipotent mechanics machine room temperature compression,
Tension test, test result is listed in table 1.It can be found that the TiAl-base alloy drip molding prepared using the present invention is compared to casting
Method, room-temperature mechanical property has obtained obvious improvement.
TiAl-base alloy room-temperature mechanical property test result prepared by the differing formed method of table 1
In summary, TiAl-base alloy shaping can be effectively solved using present invention preparation TiAl-base alloy drip molding to ask
Topic, and entirely forming process is carried out under the control of computer and precision machine tool, obtained size of formed part high precision, and tool
Have that production cost is low, curring time is short, stock utilization is high, it is easy to utilize the advantages of drip molding excellent in mechanical performance.
Claims (4)
1. a kind of fast preparation method of TiAl-base alloy drip molding, it is characterised in that comprise the following steps:
Step 1, the three-dimensional entity model of drip molding is set up, the geological information of each cross section is obtained by hierarchy slicing, and turn
Turn to numerical control table, NC table motion track information;
Step 2, substrate is fixed on the numerical control table, NC table of five-axle linkage, substrate is partially melting to form in the presence of laser beam
Molten bath, while being allowed to melt by the heat affected area that TiAl-base alloy pre-alloyed powder sends into laser using synchronous powder feeding system method so that
In substrate surface formation first layer cladding layer;
Step 3, laser head and powder-feeding nozzle are risen to cladding layer thickness identical highly, laser beam will enter heat affected area
Powder heat and melt, new sedimentary is frozen on the basis of first layer cladding layer, is successively accumulated afterwards, is finally given
3D solid drip molding;
Step 4, Milling Process is carried out to drip molding outer surface, is met the drip molding of surface finish requirements.
2. the method as described in claim 1, it is characterised in that in step 2, TiAl-base alloy pre-alloyed powder is particle size range
Spherical powder between 50~150 μm.
3. the method as described in claim 1, it is characterised in that in step 2, using argon gas as whole process protection atmosphere, wherein
Laser processing parameter is:Laser power is:200~2200W, sweep speed is:80~1080mm/min, powder feeding rate is 0.8
~5.7g/min, defocusing amount is 6~10mm.
4. the method as described in claim 1, it is characterised in that in step 2, the generation equipment of laser beam is CO2Laser, Nd:
YAG laser, optical fiber laser or semiconductor laser.
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Cited By (3)
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CN112872364A (en) * | 2021-01-11 | 2021-06-01 | 上海大学 | Method and device for 3D printing of gamma-TiAl alloy in static magnetic field |
CN115261658A (en) * | 2022-08-19 | 2022-11-01 | 北京理工大学 | Additive manufacturing method of high-performance titanium-aluminum alloy with fine-grain full-lamellar structure |
CN115491673A (en) * | 2022-09-30 | 2022-12-20 | 无锡市江南橡塑机械有限公司 | Preparation method and repair method of self-lubricating wear-resistant coating of rubber mechanical screw |
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