CN106939515A - The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of denim fabric production - Google Patents
The preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of denim fabric production Download PDFInfo
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- CN106939515A CN106939515A CN201710290518.7A CN201710290518A CN106939515A CN 106939515 A CN106939515 A CN 106939515A CN 201710290518 A CN201710290518 A CN 201710290518A CN 106939515 A CN106939515 A CN 106939515A
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- warp
- mercerization
- ball warp
- yarn
- denim fabric
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- 239000004744 fabric Substances 0.000 title claims abstract description 39
- 238000005517 mercerization Methods 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 26
- 230000000149 penetrating effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 29
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 21
- 238000004043 dyeing Methods 0.000 claims abstract description 19
- 230000008569 process Effects 0.000 claims abstract description 13
- 239000003513 alkali Substances 0.000 claims abstract description 10
- 238000007670 refining Methods 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 16
- 229920000742 Cotton Polymers 0.000 claims description 12
- 241000219146 Gossypium Species 0.000 claims description 12
- 238000006243 chemical reaction Methods 0.000 claims description 10
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- LNOPIUAQISRISI-UHFFFAOYSA-N n'-hydroxy-2-propan-2-ylsulfonylethanimidamide Chemical compound CC(C)S(=O)(=O)CC(N)=NO LNOPIUAQISRISI-UHFFFAOYSA-N 0.000 claims description 7
- 229920000056 polyoxyethylene ether Polymers 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 229920000433 Lyocell Polymers 0.000 claims description 4
- DBMJMQXJHONAFJ-UHFFFAOYSA-M Sodium laurylsulphate Chemical compound [Na+].CCCCCCCCCCCCOS([O-])(=O)=O DBMJMQXJHONAFJ-UHFFFAOYSA-M 0.000 claims description 4
- -1 butyl glycol ethers Chemical class 0.000 claims description 4
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims description 3
- 229940051841 polyoxyethylene ether Drugs 0.000 claims description 3
- 235000004879 dioscorea Nutrition 0.000 claims description 2
- 238000005303 weighing Methods 0.000 claims description 2
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims 9
- 235000011121 sodium hydroxide Nutrition 0.000 claims 3
- 150000003871 sulfonates Chemical class 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 8
- 238000005516 engineering process Methods 0.000 abstract description 4
- 230000009467 reduction Effects 0.000 abstract description 2
- 238000009992 mercerising Methods 0.000 description 15
- 239000000975 dye Substances 0.000 description 6
- 239000000047 product Substances 0.000 description 4
- 230000008595 infiltration Effects 0.000 description 3
- 238000001764 infiltration Methods 0.000 description 3
- 230000003647 oxidation Effects 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- 239000002351 wastewater Substances 0.000 description 3
- RCEAADKTGXTDOA-UHFFFAOYSA-N OS(O)(=O)=O.CCCCCCCCCCCC[Na] Chemical class OS(O)(=O)=O.CCCCCCCCCCCC[Na] RCEAADKTGXTDOA-UHFFFAOYSA-N 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 229910052788 barium Inorganic materials 0.000 description 2
- DSAJWYNOEDNPEQ-UHFFFAOYSA-N barium atom Chemical compound [Ba] DSAJWYNOEDNPEQ-UHFFFAOYSA-N 0.000 description 2
- 230000000740 bleeding effect Effects 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 239000012466 permeate Substances 0.000 description 2
- 150000003014 phosphoric acid esters Chemical class 0.000 description 2
- 238000009955 starching Methods 0.000 description 2
- 238000009976 warp beam dyeing Methods 0.000 description 2
- 238000009941 weaving Methods 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 239000012750 alkali resistant agent Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000009990 desizing Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000007306 functionalization reaction Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- COHYTHOBJLSHDF-BUHFOSPRSA-N indigo dye Chemical compound N\1C2=CC=CC=C2C(=O)C/1=C1/C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-BUHFOSPRSA-N 0.000 description 1
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 230000003204 osmotic effect Effects 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B7/00—Mercerising, e.g. lustring by mercerising
- D06B7/04—Mercerising, e.g. lustring by mercerising of yarns, threads or filaments
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/165—Ethers
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/256—Sulfonated compounds esters thereof, e.g. sultones
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/402—Amides imides, sulfamic acids
- D06M13/438—Sulfonamides ; Sulfamic acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
- Coloring (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Treatment Of Fiber Materials (AREA)
Abstract
The invention discloses the preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric, it is characterised in that in the preceding working procedure that denim fabric is produced, the warp thread after warping is made into Shu Jing, ball warp is prepared into a warp beam per beam;Without refining procedure, not dyed preceding alkali immerging process after mercerized finish, mercerization finish directly is carried out to ball warp, rope-dyeing is directly carried out.The production technology of the present invention, traditional denim fabric post-mercerizing is arranged and is improved in preceding working procedure carry out mercerization finish to warp thread in advance, on the premise of the denim fabric quality of production is ensured, eliminate 2 road dyeing and finishing manufacturing procedures, mercerization effect more preferably, dyeing after yarn lustrous surface it is good, coloured light is uniform, and suitable power saving emission reduction clean manufacturing.
Description
Technical field:
The present invention relates to the preparation of ball warp mercerization and efficient silkete penetrating agent in a kind of production of denim fabric, belong to spinning
Knit dyeing and finishing technique field.
Background technology:
Since American invention jeans, cowboy is tight with its rough, bold and unconstrained, graceful, generous, natural style and structure
It is close it is abundant, wear the characteristics of soft comfortable, quality are firm wear-resisting, liked by numerous teenagers and numerous consumers, as generation
Most successful and the dress-goods being most widely known by the people, very huge market is occupied in International Textile in the market in boundary's rag trade history
Share.Cowboy's industry product forward direction is superior, personalized, functionalization, fashion-orientation direction are developed.
In recent years, it has been found that jean warp crosses the mill white effect of cloth cover comfortable feel, gloss preferably, distinct after mercerized finish
Fruit and clearly cloth style, impart denim fabric high added value, are the preferred fabrics of high-grade jeans.But in cowboy
In fabric production process be usually beam dyeing starching after weaved again with weft yarn, mercerized finish is carried out afterwards.Because of conventional cowboy
Fabric typically uses indigo dye and dyeing, and bipseudoindoxyl dye fastness is poor, and post-mercerizing, which is arranged, can make the lighter that cloth cover has contaminated,
Waste dyestuff and whard to control to color, mercerising liquid containing color because that can not be recycled, the increase of colorful wastewater discharge capacity is unfavorable
In energy-saving and emission-reduction clean manufacturing.And in existing denim fabric mercerized finish technology, a certain amount of bleeding agent need to be added.Use at present
Phosphoric acid ester alkali-resistant penetrant because of the composition of also phosphorus, its application is restricted under current environmental requirement;Also some
Bleeding agent is because of the alkali containing high concentration in mercerising liquid, and osmotic effect is not good in the short time so that glossiness is expected behind mercerising and soft
Softness is undesirable, and irregular colour is even aberration occurs, influences denim fabric quality.
The content of the invention:
The problem of existing for above-mentioned prior art, the first aspect of the present invention purpose is that a kind of mercerization effect of offer is good
Yarn lustrous surface is good after good, dyeing, and coloured light is uniform, and ball warp silk in the denim fabric production of suitable power saving emission reduction clean manufacturing
Light technique.
To achieve these goals, the technical solution adopted by the present invention is:
Ball warp mercerization in a kind of denim fabric production, it is characterised in that in the preceding working procedure that denim fabric is produced,
Shu Jing is made in warp thread after warping, ball warp is prepared into a warp beam per beam;Without refining procedure, directly to ball warp
Not dyed preceding alkali immerging process after mercerized finish, mercerization finish is carried out, i.e., directly carries out rope-dyeing.
The production technology of the present invention, traditional denim fabric post-mercerizing is arranged and is improved in preceding working procedure in advance to warp thread
Mercerization finish is carried out, is dyed afterwards, is weaved.On the premise of the denim fabric quality of production is ensured, 2 road dyeing and finishing processing are eliminated
Process, wherein:In preceding working procedure, Shu Jing is made in the warp thread after warping, ball warp is prepared into a warp beam per beam,
Mercerized finish directly is carried out to ball warp, traditional refining procedure is eliminated;After mercerization finish, beam dyeing work is directly carried out
Sequence, rope-dyeing is completed through multiple tracks oxidation operation, then through weaving into finished product, rear road eliminates alkali immerging work before traditional dyeing
Sequence.Meanwhile, the use of a big chunk dyestuff and auxiliary agent is saved, the discharge of waste water is reduced, the purpose of energy-saving and emission-reduction is reached,
Effectively reduce production cost.
The production process of denim fabric after improvement is as follows:--- --- ball warp --- mercerising --- contaminates warping yarn
Color --- dividing sinker --- starching --- weaving ------- enzyme desizing --- Final finishing --- finished product of singing.
It is used as further setting:
Ball warp yams of the present invention are related to 10s, 12s, 16s cotton, cotton/viscous 80/20, cotton/tencel 80/
20th, 70/30,60/40 etc.;
Described each ball warp beam yarn contains 400-500 root warp thread;
Described ball warp mercerization formula is:
The second aspect of the present invention purpose is that there is provided a kind of efficient mercerising infiltration for being applicable above-mentioned ball warp mercerization
Agent, improves yarn mercerization effect, improves fabric quality.
A kind of efficient silkete penetrating agent, including following compositions by weight percentage:
A kind of preparation method of efficient silkete penetrating agent, it is characterised in that comprise the following steps:
A kind of preparation method of efficient silkete penetrating agent, comprises the following steps:
(1) the accurate isomerous tridecanol polyoxyethylene ether for weighing parts by weight is placed in three with thermometer mouthful being completely dried
In flask;
(2) agitating device is loaded onto, starts agitator, is started to warm up after stirring to 100-160 DEG C, then meter is added dropwise
Measured sulfamic acid, isothermal reaction 120min;
(3) system is cooled to 50 DEG C after reacting and adds a certain amount of butyl glycol ether and dodecyl sodium sulfate stirring
30min;
(4) system temperature is down to room temperature, adds after measured deionized water high-speed stirred 30min and discharge.
The beneficial effects of the present invention are:
1st, the present invention is right in preceding working procedure using New Processing on the basis of traditional denim manufacturing technique
Ball warp carries out mercerising, and dyed rear colour brightness, the more conventional yarn of depth are far better.Woven fabric has preferable light
Pool, distinct mill white effect, clearly cloth style and comfortable feel.Denim yarn mercerising is arranged with denim fabric post-mercerizing
Compare, final product quality is close, belong to medium-to-high grade fabric, improve added value;And the more traditional denim fabric processing of ball warp mercerising
Technique eliminates caustic dip process before one of refining procedure is dyed with together with so that once color success rate is improved, dyestuff is saved
And auxiliary agent, dye forecourt and be free of dyestuff in raffinate after mercerising, recoverable reduces wastewater discharge, reduces production
Cost, is conducive to energy-saving and emission-reduction clean manufacturing.
2nd, present invention also offers a kind of efficient silkete penetrating agent of new preparation, it instead of the infiltration of phosphoric acid ester alkali resistant
Agent, resisting high-concentration alkali lye is functional, makes the surface tension of alkali lye and reduces, and promotes the infiltration of alkali lye, makes mercerization uniform, contracting
The time of short mercerising.It can quickly be permeated in a short time to yarn interior after ball warp alkali immerging aborning, improve life
Speed is produced, and mercerization effect is good, dyed rear yarn lustrous surface is good, and coloured light irregularity is reduced, and improves finished product fabric
Quality stability.
With reference to embodiment, the present invention is described in further detail, but protection scope of the present invention is not limited
In this.
Embodiment:
Embodiment 1:
By 16s cottons/yarn of tencel 70/30 by warping, coiling in warp beam, by warp beam yarn apply some tension
Beam yarn is made, each beam yarn contains 400-500 one threads, after each beam yarn reel be wound in a warp beam be prepared into ball warp, will
Beam yarn overall alignment in 12-25 ball warp, while feeding cord roller, directly carries out mercerized finish, laggard axle of passing through to ball warp
Dyeing process, rope-dyeing is finally completed through multiple tracks oxidation operation.
Ball warp mercerization formula is in such scheme:
The preparation method of efficient silkete penetrating agent in such scheme is:
Accurately 30g isomerous tridecanol polyoxyethylene ethers are weighed to be placed in the there-necked flask with thermometer being completely dried;
Agitating device is loaded onto, starts agitator, stirring degree is that 800r/min is started to warm up to 100-160 DEG C after stirring, then by
It is added dropwise to 25g sulfamic acid, isothermal reaction 120min;After reaction by system cool to 50 DEG C add 5.5g butyl glycol ethers and
6.5g dodecyl sodium sulfates stir 30min;
System temperature is down to room temperature, adds after 33g deionized water high-speed stirreds 30min and discharges.
Performance detection:
Respectively to the embodiment of above-mentioned process ball warp mercerising, with being contrasted without the yarn of mercerized finish, contrast knot
Fruit is as shown in table 1.
Table 1, properties test result:
As can be seen from Table 1:
The efficient silkete penetrating agent of addition can quickly permeate in 8s to yarn interior, by 16s cottons/tencel of mercerising
70/30, mercerizing barium value obtains preferable gloss up to 136%, and dyed rear colour brightness, the more conventional yarn of depth good will be obtained
It is many.Woven denim fabric obtains preferable gloss, distinct mill white effect, clearly cloth style and comfortable feel.
Embodiment 2:
12s cottons/viscous 80/20 yarn in warp beam, the yarn in warp beam is applied into certain tension force by warping, coiling
Beam yarn is made, each beam yarn contains 400-500 one threads, after each beam yarn reel be wound in a warp beam be prepared into ball warp, will
Beam yarn overall alignment in 12-25 ball warp, while feeding cord roller, directly carries out mercerized finish, laggard axle of passing through to ball warp
Dyeing process, rope-dyeing is finally completed through multiple tracks oxidation operation.
Ball warp mercerization formula is in such scheme:
The preparation method of efficient silkete penetrating agent in such scheme is:
Accurately 36g isomerous tridecanol polyoxyethylene ethers are weighed to be placed in the there-necked flask with thermometer being completely dried;
Agitating device is loaded onto, starts agitator, stirring degree is that 800r/min is started to warm up to 100-160 DEG C after stirring, then by
It is added dropwise to 28g sulfamic acid, isothermal reaction 120min;After reaction by system cool to 50 DEG C add 6.5g butyl glycol ethers and
7g dodecyl sodium sulfates stir 30min;
System temperature is down to room temperature, adds after 22.5g deionized water high-speed stirreds 30min and discharges.
Performance detection:
Respectively by the embodiment of above-mentioned process mercerising, with being contrasted without the yarn arranged at mercerising, comparing result
As shown in table 2.
The properties test result of table 2:
As can be seen from Table 2:
The efficient silkete penetrating agent of addition can quickly permeate in 10s to yarn interior, by the 16s of ball warp mercerising
Cotton/viscous 80/20, mercerizing barium value obtains preferable gloss up to 118%, and dyed rear colour brightness, the more conventional yarn of depth will
It is much better.Woven denim fabric obtains preferable gloss, distinct mill white effect, clearly cloth style and comfortable hand
Sense.
Obviously, the above embodiment of the present invention is only to clearly demonstrate examples of the invention, not to of the invention real
Apply the restriction of mode.For those of ordinary skill in the field, other can also be made on the basis of the above description
Various forms of changes or variation.Here all embodiments can not be exhaustive.Every technical side for belonging to the present invention
Row of the obvious change or variation that case is extended out still in protection scope of the present invention.
Claims (8)
1. ball warp mercerization in a kind of denim fabric production, it is characterised in that in the preceding working procedure that denim fabric is produced, will
Shu Jing is made in warp thread after warping, and ball warp is prepared into a warp beam per beam;Without refining procedure, directly ball warp is entered
Not dyed preceding alkali immerging process, directly carries out rope-dyeing after row mercerized finish, mercerization finish.
2. ball warp mercerization in a kind of denim fabric production according to claim 1, it is characterised in that:Described ball warp
Yams are related to 10s, 12s, 16s cotton, cotton/viscous 80/20, one kind of cotton/tencel 80/20,70/30,60/40.
3. ball warp mercerization in a kind of denim fabric production according to claim 1, it is characterised in that:Described is each
Ball warp beam yarn contains 400-500 root warp thread.
4. ball warp mercerization in a kind of denim fabric production according to claim 1, it is characterised in that:Described ball warp
Mercerization formula is:
Caustic soda 100-200g/L,
Efficient silkete penetrating agent 1-5g/L,
60-90 DEG C of temperature,
Speed 10-35m/min.
5. ball warp mercerization in a kind of denim fabric production according to claim 1, it is characterised in that:By 16s cottons/day
Yarn in warp beam in warp beam, is applied some tension and beam yarn is made, each beam yarn contains by 70/30 yarn of silk by warping, coiling
Have 400-500 one threads, after each beam yarn reel be wound in a warp beam be prepared into ball warp, by the beam yarn in 12-25 ball warp
Overall alignment, while feeding cord roller, directly carries out mercerized finish, laggard axle dyeing process of passing through is aoxidized through multiple tracks to ball warp
Process is finally completed rope-dyeing;
Ball warp mercerization formula is in such scheme:
Caustic soda 180g/L,
Efficient silkete penetrating agent 3g/L,
85 DEG C of temperature,
Speed 20m/min;
The preparation method of efficient silkete penetrating agent in such scheme is:
Accurately 30g isomerous tridecanol polyoxyethylene ethers are weighed to be placed in the there-necked flask with thermometer being completely dried;Load onto
Agitating device, starts agitator, stirring degree is that 800r/min is started to warm up to 100-160 DEG C after stirring, then adds dropwise
Enter 25g sulfamic acid, isothermal reaction 120min;System is cooled to 50 DEG C after reaction and adds 5.5g butyl glycol ethers and 6.5g
Dodecyl sodium sulfate stirs 30min;
System temperature is down to room temperature, adds after 33g deionized water high-speed stirreds 30min and discharges.
6. ball warp mercerization in a kind of denim fabric production according to claim 1, it is characterised in that:12s cottons/viscous
Yarn in warp beam in warp beam, is applied certain tension force and beam yarn is made, each beam yarn contains by 80/20 yarn by warping, coiling
Have 400-500 one threads, after each beam yarn reel be wound in a warp beam be prepared into ball warp, by the beam yarn in 12-25 ball warp
Overall alignment, while feeding cord roller, directly carries out mercerized finish, laggard axle dyeing process of passing through is aoxidized through multiple tracks to ball warp
Process is finally completed rope-dyeing;
Ball warp mercerization formula is in such scheme:
Caustic soda 160g/L
Efficient silkete penetrating agent 2.5g/L
85 DEG C of temperature
Speed 20m/min;
The preparation method of efficient silkete penetrating agent in such scheme is:
Accurately 36g isomerous tridecanol polyoxyethylene ethers are weighed to be placed in the there-necked flask with thermometer being completely dried;Load onto
Agitating device, starts agitator, stirring degree is that 800r/min is started to warm up to 100-160 DEG C after stirring, then adds dropwise
Enter 28g sulfamic acid, isothermal reaction 120min;System is cooled to 50 DEG C after reaction and adds 6.5g butyl glycol ethers and 7g ten
Dialkyl sulfonates stir 30min;
System temperature is down to room temperature, adds after 22.5g deionized water high-speed stirreds 30min and discharges.
7. the efficient silkete penetrating agent described in a kind of claim 4, it is characterised in that:Including following groups by weight percentage
Into:
Isomerous tridecanol polyoxyethylene ether 30-40%
Sulfamic acid 30-35%
Butyl glycol ether 1-5%
Dodecyl sodium sulfate 1-10%
Deionized water surplus.
8. the preparation method of efficient silkete penetrating agent described in a kind of claim 7, it is characterised in that:Comprise the following steps:
(1) the accurate isomerous tridecanol polyoxyethylene ether for weighing parts by weight is placed in the there-necked flask with thermometer being completely dried
In;
(2) agitating device is loaded onto, starts agitator, is started to warm up after stirring to 100-160 DEG C, then metering is added dropwise
Good sulfamic acid, isothermal reaction 120min;
(3) system is cooled to 50 DEG C after reacting and adds butyl glycol ether and dodecyl sodium sulfate stirring 30min;
(4) system temperature is down to room temperature, adds after deionized water high-speed stirred 30min and discharge.
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CN108796895A (en) * | 2018-06-21 | 2018-11-13 | 浙江美欣达纺织印染科技有限公司 | It is a kind of based on the tencel production technology for padding silkete penetrating agent |
CN109023646A (en) * | 2018-08-21 | 2018-12-18 | 中纺院(浙江)技术研究院有限公司 | A kind of Lyocell polyethylene cool feeling denim fabric and its processing technology |
CN113668262A (en) * | 2021-08-02 | 2021-11-19 | 浙江鑫兰纺织有限公司 | Production process of anti-aging jean fabric |
CN113668119A (en) * | 2021-08-02 | 2021-11-19 | 浙江鑫兰纺织有限公司 | Processing method of double-layer warm-keeping jean fabric |
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