CN106929157A - The uniform fir essential oil production alembic of one kind distillation - Google Patents
The uniform fir essential oil production alembic of one kind distillation Download PDFInfo
- Publication number
- CN106929157A CN106929157A CN201710265536.XA CN201710265536A CN106929157A CN 106929157 A CN106929157 A CN 106929157A CN 201710265536 A CN201710265536 A CN 201710265536A CN 106929157 A CN106929157 A CN 106929157A
- Authority
- CN
- China
- Prior art keywords
- tank body
- cavity volume
- distillation
- big
- permeability cell
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004821 distillation Methods 0.000 title claims abstract description 23
- 239000000341 volatile oil Substances 0.000 title claims abstract description 22
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 12
- 230000035699 permeability Effects 0.000 claims abstract description 29
- 239000002893 slag Substances 0.000 claims abstract description 26
- 239000012528 membrane Substances 0.000 claims abstract description 12
- 239000008246 gaseous mixture Substances 0.000 claims abstract description 8
- 238000007789 sealing Methods 0.000 claims abstract description 3
- 238000002156 mixing Methods 0.000 claims description 5
- 239000003818 cinder Substances 0.000 claims description 2
- 230000000694 effects Effects 0.000 abstract description 4
- 238000000034 method Methods 0.000 description 9
- 239000003921 oil Substances 0.000 description 7
- 238000001256 steam distillation Methods 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000010586 diagram Methods 0.000 description 3
- 239000000843 powder Substances 0.000 description 3
- 244000050510 Cunninghamia lanceolata Species 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- 238000005336 cracking Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 241000218645 Cedrus Species 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- IRAQOCYXUMOFCW-CXTNEJHOSA-N cedrene Chemical group C1[C@]23[C@H](C)CC[C@H]3C(C)(C)[C@H]1C(C)=CC2 IRAQOCYXUMOFCW-CXTNEJHOSA-N 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- IRAQOCYXUMOFCW-UHFFFAOYSA-N di-epi-alpha-cedrene Natural products C1C23C(C)CCC3C(C)(C)C1C(C)=CC2 IRAQOCYXUMOFCW-UHFFFAOYSA-N 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000001976 improved effect Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000003550 marker Substances 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
The invention discloses one kind uniform fir essential oil production alembic of distillation, including tank body；Breathable membrane being provided with by bottom in tank body, tank inner chamber is set to two up big and down small cavity volumes every setting up separately, tank body top surface is provided with charging aperture, the top of big cavity volume is provided with gaseous mixture outlet pipe, steam inlet pipe is inserted with small cavity volume, tank body side is provided with slag notch, the top of slag notch connects with big cavity volume, and the bottom of slag notch connects with small cavity volume, and slag notch is provided with slag door；It is big that many permeability cells through breathable membrane are provided with and communicated between cavity volume and small cavity volume；The top end face of permeability cell be sealing, bottom face be open；The pipe outer wall face of each permeability cell recline tank body internal face corresponding position set；Gathered on the tube wall of permeability cell and be provided with air-vent.Structure is more reasonable, and evenly, distillation efficiency is higher, and distillation time can substantially shorten, and using effect is more preferable for distillation.
Description
Technical field
The invention belongs to the extractive technique field of fir essential oil, it is related to a kind of uniform fir essential oil production of distillation to distill
Tank.
Background technology
Contain substantial amounts of fir essential oil in China fir, its main component is cedrene, cedar wood alcohol etc., can be used for perfume industry
In.At present, the extraction processing of fir essential oil is main using solvent extraction method, cracking process, steam distillation.Using solvent extraction
The oil yield that method extracts fir essential oil is high compared with the oil yield of steam distillation, but needs substantial amounts of solvent, and subsequent treatment is complicated,
There is a problem of high energy consumption, dissolvent residual.The oil yield for extracting fir essential oil using cracking process is higher, but it is a chemical mistake
Journey, the essential oil for obtaining contains the materials such as substantial amounts of tar, phenol, aldehyde and ketone, has a strong impact on the quality of fir essential oil.Steam distillation
Preferably, clear, aroma of pure are best suitable for for blending the fir essential oil quality that method is extracted, and its extraction process is pure thing
Reason process, it is pollution-free, but oil yield is relatively low.Several techniques compare, and steam distillation is the production work of preferred environment-friendly type
Skill, but should also optimize to improve yield and further reducing energy consumption.The step of steam distillation extracts fir essential oil
It is：A, China fir is ground into fir powder；B, in fir powder add dispensing be stirred mixing；C, the fir powder that will be mixed send
Enter in destilling tower, distilled to superheated steam is passed through in destilling tower, distillation time is 9-11 hours；That is discharged after D, distillation is mixed
Close gas be delivered in cooling tower cooled down after obtain oil mixing with water liquid；E, oil mixing with water liquid are obtained after water-oil separating
Fir essential oil.
Alembic is the equipment of core in steam distillation, and distillation time generally need to be small up to 9-11 in whole technique
When, therefore the efficiency of alembic is related to the efficiency that whole fir essential oil is produced.The efficiency of alembic is set to improve it is necessary to protect
On the premise of the utilization rate of the volume for demonstrate,proving alembic, make the directly contact area of the overall border of material and water vapour in alembic
Can be as far as possible big, as far as possible uniformly, while also to ensure that scarfing cinder will be conveniently after the completion of distillation.
The structure of fir essential oil production alembic of the prior art as shown in Figure 1 and Figure 2, including tank body 2；In tank body 2
Breathable membrane 6 being provided with by bottom and the inner chamber of tank body 2 being set to two up big and down small cavity volumes every setting up separately, the top surface of tank body 2 is provided with charging
Mouth 1, the top of big cavity volume is provided with gaseous mixture outlet pipe 7, and steam inlet pipe 4 is inserted with small cavity volume, and the side of tank body 2 is provided with slag notch 3,
The top of slag notch 3 connects with big cavity volume, and the bottom of slag notch 3 connects with small cavity volume, and slag notch 3 is provided with slag door 5.
Using the alembic of such technology it is of course possible to use, but due to the overall border of material in alembic and water vapour
The size of directly contact area be equivalent to the area of breathable membrane 6, directly contact area is big not enough, and directly contact point is complete
Portion is located at the overall bottom surface of material, and distribution is not uniform enough, and distillation is not uniform enough, and distillation efficiency is not high enough, and distillation time is relatively
Long, using effect is preferable not enough.
The content of the invention
To overcome the deficiencies in the prior art, a kind of structure of present invention offer is more reasonable, and evenly, distillation efficiency is more for distillation
Height, the fir essential oil production alembic that distillation time can substantially shorten, using effect is more preferable.
The technical scheme that is used to reach above-mentioned technical purpose of the present invention is：The uniform fir essential oil production of one kind distillation
With alembic, including tank body；Breathable membrane being provided with by bottom in tank body, tank inner chamber is set to up big and down small two every setting up separately
Cavity volume, tank body top surface is provided with charging aperture, and the top of big cavity volume is provided with gaseous mixture outlet pipe, steam inlet pipe, tank body are inserted with small cavity volume
Side is provided with slag notch, and the top of slag notch connects with big cavity volume, and the bottom of slag notch connects with small cavity volume, is set on slag notch
There is slag door；It is big that many permeability cells through breathable membrane are provided with and communicated between cavity volume and small cavity volume；The top end face of permeability cell is
Seal, bottom face is open；The pipe outer wall face of each permeability cell recline tank body internal face corresponding position set；The pipe of permeability cell
Gathered on wall and be provided with air-vent.
The top end face of described permeability cell stretches into the mouth of pipe most lower edge of tank interior point less than gaseous mixture outlet pipe.
Described permeability cell is uniformly arranged along the inner circumferential of tank body by rotation axes of symmetry of the axis of tank body.
The advantage of the invention is that：
Due to being provided with and communicated with many permeability cells through breathable membrane between big cavity volume and small cavity volume；The top of permeability cell
Face be sealing, bottom face be open；The pipe outer wall face of each permeability cell recline tank body internal face corresponding position set；Permeability cell
Tube wall on gather be provided with air-vent.
Therefore, water vapour is obviously just bigger than traditional circular cross-section with the area of material directly contact, and directly contact
That puts is more evenly distributed, therefore distillation is evenly, and distillation efficiency is higher, and distillation time can substantially shorten, and using effect is more preferable.
Brief description of the drawings
The invention will be further described with reference to the accompanying drawings and examples.Wherein：
Fig. 1 is the schematic diagram of the alembic of prior art；
Fig. 2 is the local subdivision schematic diagram of the alembic of prior art；
Fig. 3 is local subdivision schematic diagram of the invention.
Marker number in accompanying drawing is described as follows：Charging aperture 1, tank body 2, slag notch 3, steam inlet pipe 4, slag door 5, breathable membrane
6th, gaseous mixture outlet pipe 7, permeability cell 8
Specific embodiment
Embodiments of the invention, as shown in figure 3, a kind of uniform fir essential oil production alembic of distillation, including tank body
2；Breathable membrane 6 being provided with by bottom in tank body 2, the inner chamber of tank body 2 is set to two up big and down small cavity volumes, the top surface of tank body 2 every setting up separately
Charging aperture 1 is provided with, the top of big cavity volume is provided with gaseous mixture outlet pipe 7, and steam inlet pipe 4 is inserted with small cavity volume, and the side of tank body 2 is provided with
Slag notch 3, the top of slag notch 3 connects with big cavity volume, and the bottom of slag notch 3 connects with small cavity volume, and slag notch 3 is provided with slag door
5；It is big that many permeability cells 8 through breathable membrane 6 are provided with and communicated between cavity volume and small cavity volume；The top end face of permeability cell 8 is envelope
Mouthful, bottom face be open；The pipe outer wall face of each permeability cell 8 recline tank body 2 internal face corresponding position set；Permeability cell 8
Gathered on tube wall and be provided with air-vent.
The top end face of described permeability cell 8 stretches into the mouth of pipe most lower edge of part in tank body 2 less than gaseous mixture outlet pipe 7.
Described permeability cell 8 is uniformly arranged along the inner circumferential of tank body 2 by rotation axes of symmetry of the axis of tank body 2.Thoroughly
Tracheae 8 sets that improved effect very little is not obvious enough, and permeability cell 8 sets the too many dischargeable capacity that can then take too many alembic,
The quantity of permeability cell 8 is preferably 4-8 roots.
Claims (3)
1. a kind of uniform fir essential oil production alembic of distillation, including tank body；Being provided with breathable membrane by bottom in tank body will
Tank inner chamber is set to two up big and down small cavity volumes every setting up separately, and tank body top surface is provided with charging aperture, and the top of big cavity volume is provided with mixing
Gas outlet pipe, is inserted with steam inlet pipe in small cavity volume, tank body side is provided with slag notch, and the top of slag notch connects with big cavity volume, goes out
The bottom of cinder notch connects with small cavity volume, and slag notch is provided with slag door；It is characterized in that：Setting is connected between cavity volume and small cavity volume greatly
There are many permeability cells through breathable membrane；The top end face of permeability cell be sealing, bottom face be open；The pipe of each permeability cell
Outside wall surface recline tank body internal face corresponding position set；Gathered on the tube wall of permeability cell and be provided with air-vent.
2. one kind according to claim 1 distills uniform fir essential oil production alembic, it is characterised in that：Described
The top end face of permeability cell stretches into the mouth of pipe most lower edge of tank interior point less than gaseous mixture outlet pipe.
3. one kind according to claim 2 distills uniform fir essential oil production alembic, it is characterised in that：Described
Permeability cell is uniformly arranged along the inner circumferential of tank body by rotation axes of symmetry of the axis of tank body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710265536.XA CN106929157A (en) | 2017-04-21 | 2017-04-21 | The uniform fir essential oil production alembic of one kind distillation |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710265536.XA CN106929157A (en) | 2017-04-21 | 2017-04-21 | The uniform fir essential oil production alembic of one kind distillation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106929157A true CN106929157A (en) | 2017-07-07 |
Family
ID=59437032
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710265536.XA Pending CN106929157A (en) | 2017-04-21 | 2017-04-21 | The uniform fir essential oil production alembic of one kind distillation |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106929157A (en) |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87205155U (en) * | 1987-09-03 | 1988-05-25 | 成都科技大学 | Ventilating type distil |
| RU2032723C1 (en) * | 1991-09-11 | 1995-04-10 | Научно-производственное коллективное предприятие "Полет" | Device for steam-based distillation of essential oils |
| CN202030729U (en) * | 2011-04-28 | 2011-11-09 | 成都永泰制药化工机械厂 | Plant distillation separating device |
| CN203462025U (en) * | 2013-08-19 | 2014-03-05 | 昆明朗盛生物科技有限公司 | Distillation tank for extracting vegetable oil |
| CN103740469A (en) * | 2014-02-07 | 2014-04-23 | 郭永来 | Steam distillation aromatic essential oil device |
| CN104278453A (en) * | 2014-09-24 | 2015-01-14 | 张家港市华益纺织有限公司 | Interlayer fining barrel for refining |
| CN105126378A (en) * | 2015-09-05 | 2015-12-09 | 腾冲明馨生物技术开发有限公司 | Aromatic-plant distilling extracting pot |
| CN105176690A (en) * | 2015-08-14 | 2015-12-23 | 福建鑫绿林产品开发有限公司 | Method for extracting cunninghamia lanceolata essential oil by utilization of cunninghamia lanceolata three remains |
| CN205035347U (en) * | 2015-09-23 | 2016-02-17 | 罗定市兴伟香料有限公司 | Cinnamon essential oil boiling bulb |
| CN206014822U (en) * | 2016-08-29 | 2017-03-15 | 罗定市骏达香料有限公司 | A kind of cinnamon essential oil boiler |
| CN206706053U (en) * | 2017-04-21 | 2017-12-05 | 福建鑫绿林产品开发有限公司 | One kind distills uniform fir essential oil production alembic |
-
2017
- 2017-04-21 CN CN201710265536.XA patent/CN106929157A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87205155U (en) * | 1987-09-03 | 1988-05-25 | 成都科技大学 | Ventilating type distil |
| RU2032723C1 (en) * | 1991-09-11 | 1995-04-10 | Научно-производственное коллективное предприятие "Полет" | Device for steam-based distillation of essential oils |
| CN202030729U (en) * | 2011-04-28 | 2011-11-09 | 成都永泰制药化工机械厂 | Plant distillation separating device |
| CN203462025U (en) * | 2013-08-19 | 2014-03-05 | 昆明朗盛生物科技有限公司 | Distillation tank for extracting vegetable oil |
| CN103740469A (en) * | 2014-02-07 | 2014-04-23 | 郭永来 | Steam distillation aromatic essential oil device |
| CN104278453A (en) * | 2014-09-24 | 2015-01-14 | 张家港市华益纺织有限公司 | Interlayer fining barrel for refining |
| CN105176690A (en) * | 2015-08-14 | 2015-12-23 | 福建鑫绿林产品开发有限公司 | Method for extracting cunninghamia lanceolata essential oil by utilization of cunninghamia lanceolata three remains |
| CN105126378A (en) * | 2015-09-05 | 2015-12-09 | 腾冲明馨生物技术开发有限公司 | Aromatic-plant distilling extracting pot |
| CN205035347U (en) * | 2015-09-23 | 2016-02-17 | 罗定市兴伟香料有限公司 | Cinnamon essential oil boiling bulb |
| CN206014822U (en) * | 2016-08-29 | 2017-03-15 | 罗定市骏达香料有限公司 | A kind of cinnamon essential oil boiler |
| CN206706053U (en) * | 2017-04-21 | 2017-12-05 | 福建鑫绿林产品开发有限公司 | One kind distills uniform fir essential oil production alembic |
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| PB01 | Publication | ||
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Application publication date: 20170707 |