A kind of anhydrous dyeing and finishing test glass of the supercritical fluid of movable type
Technical field
The present invention relates to pressure vessel and textile dyeing and finishing equipment manufacturing technology fields more particularly to a kind of the super of movable type to face
Boundary's liquid waterless dyeing and finishing test glass.
Background technique
The dyeing and printing process of traditional textile produces, and not only its process flow is long, and process is more, the quality of product often by
The combined influence of many factors, but the color of especially textile is processed.Thus, in the dyeing and printing process of textile, it usually needs
By beating sample, putting the links such as middle sample, trial production and production.And the test link such as wherein beat sample, be obtain factory formula and
The basis of technological parameter and premise.Therefore, the little sample testing device systems of research and development efficiently, reliable, applicable have mass production non-
Normal important role.
In general, the dyeing and printing process of textile produces, process is more, process flow is long, and product quality suffers from a variety of multiple
The combined influence of miscellaneous factor, especially in the color process segment of textile.Thus, the dyeing and printing process of textile, it usually needs warp
It crosses and beats sample, puts the links such as middle sample, trial production and production.Wherein, beating sample is to obtain the premise of production technology basic components.Cause
This, the sample proofing facility system of research and development efficiently, reliable, applicable, to the anhydrous dyeing and finishing technique of supercritical fluid be applied clinically and popularized and
Industrialization all has very important effect.
In recent years, due to ecological, environmental protective and shortage of fresh water etc., with supercritical CO2Equal fluids are the anhydrous of medium
Dyeing and finishing technique has obtained extensive concern and the attention of industry.Traditional water bath is replaced to carry out dyeing and finishing processing to textile with it, it can be from
Traditional dyeing and finishing is thoroughly eliminated on source processes the puzzlements such as brought energy consumption is high, environmental pollution is serious.Thus, research and develop shooting flow
The anhydrous change system of body, sustainable development and ecological environmental protection to textile printing and dyeing industry etc. all have important society
Meeting and realistic meaning.It wherein designs, develop the little sample testing device systems of hair efficiently, reliable, applicable, it is anhydrous to supercritical fluid
The popularization and application and industrialization of dyeing and finishing technique all have impetus very outstanding.
But in terms of presently disclosed document report and practical application, existing supercritical fluid dyeing and finishing Sample devices or its set
Standby system processes unit there is usually one fixed dyeing and finishing sample, a corresponding compression system, and in dyeing and finishing sample
Unit downstream configures a set of separation and recovery system, to realize the separation and recovery to machining medium and residual dye material.Thus, it is this kind of
Sample system generally can only once carry out sample processing to a sample, and must also carry out clearly to system after sample every time
It washes, just can be carried out test of drawing a design next time, especially in the color sample processing for carrying out textile, the thorough cleaning of system is just aobvious
It obtains particularly significant.However, existing majority Sample devices system or its processing unit, cleaning process is cumbersome, and is not easy to clean.
Meanwhile pressurization and the separation and recovery system of this kind of dyeing and finishing sample system configuration, vacancy rate is high, cannot obtain effectively sufficiently sharp
With.Thus, the low efficiency of these existing supercritical fluid dyeing and finishing sample systems, is far from satisfying actual production to sample at present
The wilderness demand of sample, to also largely effect on and delay the industrialization promotion and reality of the anhydrous dyeing and finishing technique of supercritical fluid
Using.
In view of the above shortcomings, the designer, is actively subject to research and innovation, to found a kind of the overcritical of movable type
Liquid waterless dyeing and finishing test glass makes it with more the utility value in industry.
Summary of the invention
In order to solve the above technical problems, the object of the present invention is to provide one kind have easy to operate, sample is high-efficient, it is reliable,
Convenient for cleaning, economical and practical, the mobile anhydrous dyeing and finishing test glass of supercritical fluid that has a wide range of application.
A kind of anhydrous dyeing and finishing test glass of supercritical fluid of movable type proposed by the present invention, including high-potting cup cylinder,
High-potting Sealing cap for cup, high-pressure fluid diversion pipe, the first pressure piping, the second pressure piping, the first high-pressure stop valve and
Two high-pressure stop valves, it is characterised in that:
The inside bottom of the high-potting cup cylinder is in recessed arc-shaped, the mobile lid of the high-potting Sealing cap for cup
It is located at the upper end rim of a cup of the high-potting cup cylinder, is equipped at intervals with medium entrance and Jie on the high-potting Sealing cap for cup
Matter outlet;
One end of first pressure piping is connected at the medium entrance and is located at the high-potting Sealing cap for cup
Top, the other end of first pressure piping connects for external air source or tank charging system, the first high-pressure stop valve peace
On first pressure piping;
One end of second pressure piping is connected at the media outlet and is located at the high-potting Sealing cap for cup
Top, second pressure piping is connected to the high-potting cup cylinder, and the other end of second pressure piping is for outer
The connection of portion's separation and recovery system, second high-pressure stop valve are mounted on second pressure piping;
The high-pressure fluid diversion pipe connect with first pressure piping and is located at the high-potting Sealing cap for cup
Lower section, the high-pressure fluid diversion pipe are suspended on vertically in the high-potting cup cylinder;
It further include wireless pressure temperature integrated transducer and safety valve, the wireless pressure temperature integrated transducer peace
On first pressure piping or the second pressure piping, the safety valve is mounted on first pressure piping or second high
On pressure pipeline.
Further, the wireless pressure temperature integrated transducer and safety valve are installed in second pressure piping
On, four-way connection is installed, the four-way connection is located at the media outlet and described second high on second pressure piping
Between pressure cutoff valve, the wireless pressure temperature integrated transducer and safety valve are separately mounted to two phases of the four-way connection
Pair interface.
Further, the wireless pressure temperature integrated transducer and safety valve are installed in first pressure piping
On, four-way connection is installed, the four-way connection is located at the medium entrance and described first high on first pressure piping
Between pressure cutoff valve, the wireless pressure temperature integrated transducer and safety valve are separately mounted to two phases of the four-way connection
Pair interface.
Further, the wireless pressure temperature integrated transducer is mounted on first pressure piping, the peace
Full valve is mounted on second pressure piping, is equipped with the first three-way connection on first pressure piping, and the described 1st
Pass joint is between the medium entrance and first high-pressure stop valve, the wireless pressure temperature integrated transducer peace
At the intermediary interface of first three-way connection, the second three-way connection is installed on second pressure piping, described
For two three-way connections between institute's media outlet and second high-pressure stop valve, the safety valve is mounted on second threeway
At the intermediary interface of connector.
Further, the wireless pressure temperature integrated transducer is mounted on second pressure piping, the peace
Full valve is mounted on first pressure piping, is equipped with the first three-way connection on first pressure piping, and the described 1st
Between the medium entrance and first high-pressure stop valve, the safety valve is mounted on the described 1st and connects pass joint
At the intermediary interface of head, the second three-way connection is installed on second pressure piping, second three-way connection is located at and is situated between
Between matter outlet and second high-pressure stop valve, the wireless pressure temperature integrated transducer is mounted on second threeway
At the intermediary interface of connector.
Further, the upper end of the high-pressure fluid diversion pipe is high by screw thread and first on high-potting Sealing cap for cup
Pressure pipeline connection, distance of the lower end of the high-pressure fluid diversion pipe apart from the high-potting cup cylinder body bottom are 0.1-5cm.
Further, the medium entrance and media outlet are right centered on the axial line of the high-potting Sealing cap for cup
Claim setting.
According to the above aspect of the present invention, the present invention has at least the following advantages: the present invention both can be by high-potting cup and shooting flow
Body booster jar is filled to be attached with separation and recovery system, realizes that the tank of machining medium fills the separation and recovery of the medium with after;Together
When can also carry out separating disconnection with above system, so that the fixed dyeing and finishing of traditional supercritical fluid unit of drawing a design has been become one kind
The test glass of packaged type realizes and multiple test glasses are separately or concurrently carried out to medium tank fills, and then concentrates while being risen
The purpose of temperature test processing.It draws a design processing efficiency and its medium to substantially increase the anhydrous dyeing and finishing of high-pressure supercritical fluid
Booster jar fills the utilization efficiency with separation and recovery system, and it is a large amount of to what is drawn a design effectively to have adapted to the anhydrous dyeing and finishing actual production of textile
Demand.
More importantly the present invention is integrated by medium entrance, outlet and its corresponding shut-off valve and wireless pressure temperature
Change sensor and safety valve concentrated setting is ipsilateral on high-potting Sealing cap for cup, advantageously reduces setting for high-potting cup cylinder
Meter and difficulty of processing are also more convenient for concentrate heating sample processing.And it is arranged another on high-potting Sealing cap for cup
Side, the high-pressure fluid diversion pipe being suspended from test glass can then be realized by the flow velocity and pressure of tank filling medium to bottom of a cup dyestuff etc.
The stirring hydrotropy of chemicals, and purging or the suction to chemicals such as bottom dyestuffs can also be effectively realized in wash phase, it improves
Cleaning efficiency.Meanwhile the wireless pressure temperature integrated transducer being arranged on test glass can be by pressure medium, temperature in test glass
It is real-time transmitted to the external record and real time monitoring for receiving system, realizing to pressure medium, temperature in test glass.It is set on test glass
The safety valve set can effectively ensure that test glass under condition of high voltage using safe.To overcome existing fixed supercritical fluid
Dyeing and finishing Sample devices or its device systems utilization efficiency it is low, cleaning it is cumbersome, be not able to satisfy actual production to draw a design demand the disadvantages of.
Thus, the technology of the present invention is remarkably improved the sample efficiency of the anhydrous dyeing and finishing production of supercritical fluid, and has equipment
System operatio is easy, sample is high-efficient, it is reliable, convenient for cleaning, it is economical and practical, have a wide range of application the advantages that.It is solved to from source
Ecology, the greenization clean manufacturing of textile printing and dyeing industry are realized in the certainly generation and discharge of textile printing and dyeing industry pollutant, are had non-
Normal wide application prospect and important practical significance.
The above description is only an overview of the technical scheme of the present invention, in order to better understand the technical means of the present invention,
And can be implemented in accordance with the contents of the specification, the following is a detailed description of the preferred embodiments of the present invention and the accompanying drawings.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the anhydrous dyeing and finishing test glass of supercritical fluid mobile in the embodiment of the present invention one;
Fig. 2 is the structural schematic diagram of the anhydrous dyeing and finishing test glass of supercritical fluid mobile in the embodiment of the present invention two;
Fig. 3 is the structural schematic diagram of the anhydrous dyeing and finishing test glass of supercritical fluid mobile in the embodiment of the present invention three;
Fig. 4 is the structural schematic diagram of the anhydrous dyeing and finishing test glass of supercritical fluid mobile in the embodiment of the present invention four;
Wherein: the first high-pressure stop valve of 1-;2- wireless pressure temperature integrated transducer;3- safety valve;4- high-potting
Sealing cap for cup;The second high-pressure stop valve of 5-;6- high-potting cup cylinder;7- high-pressure fluid diversion pipe;The first pressure piping of 8-;9-
Second pressure piping;10- medium entrance;11- media outlet;12- four-way connection;The first three-way connection of 13-;The second threeway of 14-
Connector.
Specific embodiment
With reference to the accompanying drawings and examples, specific embodiments of the present invention will be described in further detail.Implement below
Example is not intended to limit the scope of the invention for illustrating the present invention.
Embodiment one:
As shown in Figure 1, a kind of anhydrous dyeing and finishing test glass of the supercritical fluid of movable type, including high-potting cup cylinder 6, height
Pressure test Sealing cap for cup 4, high-pressure fluid diversion pipe 7, the first pressure piping 8, the second pressure piping 9,1 and of the first high-pressure stop valve
Second high-pressure stop valve 5, the inside bottom of the high-potting cup cylinder is in recessed arc-shaped, the high-potting cup sealing
The mobile lid of lid is located at the upper end rim of a cup of the high-potting cup cylinder, is equipped at intervals with medium on the high-potting Sealing cap for cup
Import 10 and media outlet 11;
Mobile high-pressure tests high pressure sealing of the Sealing cap for cup realization to medium in cup.
One end of first pressure piping is connected at the medium entrance and is located at the high-potting Sealing cap for cup
Top, the other end of first pressure piping connects for external air source or tank charging system, the first high-pressure stop valve peace
On first pressure piping;
First high-pressure stop valve, which can be realized, fills the medium tank of test glass, and disconnected with the separation of gas source or tank charging system
It opens.
One end of second pressure piping is connected at the media outlet and is located at the high-potting Sealing cap for cup
Top, second pressure piping is connected to the high-potting cup cylinder, and the other end of second pressure piping is for outer
The connection of portion's separation and recovery system, second high-pressure stop valve are mounted on second pressure piping;
Second high-pressure stop valve, which can be realized, carries out decompression output to the medium in test glass, and with separation and recovery system
Separation disconnects.
The high-pressure fluid diversion pipe connect with first pressure piping and is located at the high-potting Sealing cap for cup
Lower section, the high-pressure fluid diversion pipe are suspended on vertically in the high-potting cup cylinder;
It further include wireless pressure temperature integrated transducer 2 and safety valve 3, the wireless pressure temperature integrated transducer
It is installed on second pressure piping with safety valve, four-way connection 12 is installed on second pressure piping, described four
Pass joint between the media outlet and second high-pressure stop valve, the wireless pressure temperature integrated transducer and
Safety valve is separately mounted to two opposite interfaces of the four-way connection.
Wireless pressure temperature integrated transducer can realize the remote transmission to medium air pressure in test glass, and safety valve then may be used
It realizes and carries out emergency decompression when pressure is more than safe pressure in cup.
The upper end of the high-pressure fluid diversion pipe is connected by the first pressure piping on screw thread and high-potting Sealing cap for cup
It connects, distance of the lower end of the high-pressure fluid diversion pipe apart from the high-potting cup cylinder body bottom is 0.1-5cm.
The medium entrance and media outlet are symmetrical arranged centered on the axial line of the high-potting Sealing cap for cup.
Test glass is being carried out to realize the stirring hydrotropy to chemicals such as bottom of a cup dyestuffs when medium tank is filled, it is clear in test glass
The stage of washing can also effectively realize the purging to chemicals such as bottom dyestuffs, improve cleaning efficiency.
The installation site of certain wireless pressure temperature integrated transducer and safety valve is not limited to institute in embodiment one
It states, also mountable in other positions, following embodiment gives the other of wireless pressure temperature integrated transducer and safety valve
Installation site.
Embodiment two:
As shown in Fig. 2, the wireless pressure temperature integrated transducer and safety valve are installed in first high-voltage tube
On road, four-way connection 12 is installed on first pressure piping, the four-way connection is located at the medium entrance and described the
Between one high-pressure stop valve, the wireless pressure temperature integrated transducer and safety valve are separately mounted to the four-way connection two
A opposite interface.
Embodiment three:
As shown in figure 3, the wireless pressure temperature integrated transducer is mounted on first pressure piping, the peace
Full valve is mounted on second pressure piping, is equipped with the first three-way connection 13 on first pressure piping, and described first
Three-way connection is between the medium entrance and first high-pressure stop valve, the wireless pressure temperature integrated transducer
It is mounted at the intermediary interface of first three-way connection, the second three-way connection 14, institute is installed on second pressure piping
The second three-way connection is stated between institute's media outlet and second high-pressure stop valve, the safety valve is mounted on described second
At the intermediary interface of three-way connection.
Example IV:
As shown in figure 4, the wireless pressure temperature integrated transducer is mounted on second pressure piping, the peace
Full valve is mounted on first pressure piping, is equipped with the first three-way connection 13 on first pressure piping, and described first
For three-way connection between the medium entrance and first high-pressure stop valve, the safety valve is mounted on first threeway
At the intermediary interface of connector, the second three-way connection 14 is installed on second pressure piping, second three-way connection is located at
Between institute's media outlet and second high-pressure stop valve, the wireless pressure temperature integrated transducer is mounted on described second
At the intermediary interface of three-way connection.
When a kind of anhydrous dyeing and finishing test glass of the supercritical fluid of movable type of the invention works, it need to carry out first overcritical
The quantitative textile fabrics of liquid waterless dyeing and finishing sample pretreating and material is quantitatively contaminated, is placed in high-potting cup cylinder 6.It is tried with high pressure
It tests Sealing cap for cup 4 and seals high-potting cup cylinder, and other component is accordingly connected or assembled.It is then shut off the second high pressure
Shut-off valve 5 connects the first pressure piping connecting with the first high-pressure stop valve 1 and machining medium gas source or medium tank charging system
It is logical, and the first high-pressure stop valve 1 of unlatching carries out quantitative medium tank to test glass system and fills.Tank is closed the first high pressure after the completion of filling and is cut
Only valve 1, and test glass system is separated with tank charging system.Aforesaid operations are repeated, by the campaign cup for the processing that need to draw a design
Medium tank is carried out to fill.Then it is placed in ready in heating system or other heating baths wait the test glass concentration drawn a design that heats up,
And it carries out concentrating processing of drawing a design according to predetermined temperature program and proofing condition.
After drawing a design, each test glass can separately or concurrently be passed through to the second high pressure of 5 outboard end of the second high-pressure stop valve
Pipeline accesses dedicated separation and recovery system, separates and recovers to dyeing medium.Meanwhile according to demand of actually drawing a design, test
Cup can also be connected to by the first pressure piping that the first high-pressure stop valve 1 connects with machining medium gas source or medium tank charging system,
With using high-pressure fluid diversion pipe 7 in clean fluid medium and cup to the loose colour drawn a design on product in test glass or other residual dyeizations
Remaining dye material is purged, is cleaned in material and cup.The medium and residual dye material of cleaning are sealed by high-potting cup
Media outlet 11 is handled through above-mentioned separation and recovery system again on lid 4.In addition, when necessary can also be by the first high-pressure stop valve 1
First pressure piping of connection is connect with dedicated separation and recovery system, by the second high pressure of 5 outboard end of the second high-pressure stop valve
Pipeline is connected to machining medium gas source or medium tank charging system, to be situated between using high-pressure fluid diversion pipe 7 in cup and clean fluid
Draw a design in confrontation test glass the loose colour on product or other residual dye materials and cup in remaining dye material aspirated, cleaned,
The cleaning efficiency of certain samples is provided.
Under normal conditions, after separating and recovering or/and clean, make the first high-pressure stop being arranged on each test glass first
Valve 1 is in close state, and is then sufficiently recycled using the gas pump that separation and recovery system configures to medium in each test glass
And decompression.When the pressure that wireless pressure temperature integrated transducer 2 is shown is equal to or less than atmospheric pressure, separation and recovery system
Gas pump stops working.Then the dedicated machining medium gas source or medium tank charging system that will be connect with test glass, and separate back
Receipts system is each turned off separation.High-potting Sealing cap for cup 4 is finally opened, sample of drawing a design is taken out, completes drawing a design for anhydrous dyeing and finishing
Test.Aforesaid operations are repeated, can continue to realize that the sample of the anhydrous dyeing and finishing of supercritical fluid of next round is drawn a design.
The above is only a preferred embodiment of the present invention, it is not intended to restrict the invention, it is noted that for this skill
For the those of ordinary skill in art field, without departing from the technical principles of the invention, can also make it is several improvement and
Modification, these improvements and modifications also should be regarded as protection scope of the present invention.