CN106903309A - A kind of hook and its manufacture method with novel wear resistant Rotating fields - Google Patents

A kind of hook and its manufacture method with novel wear resistant Rotating fields Download PDF

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Publication number
CN106903309A
CN106903309A CN201611097874.9A CN201611097874A CN106903309A CN 106903309 A CN106903309 A CN 106903309A CN 201611097874 A CN201611097874 A CN 201611097874A CN 106903309 A CN106903309 A CN 106903309A
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China
Prior art keywords
hook
laser
pin
hole
blank
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Pending
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CN201611097874.9A
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Chinese (zh)
Inventor
刘红宾
李旺
孙峰
李广生
潘宝珠
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Laser Technology Development (beijing) Co Ltd
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Laser Technology Development (beijing) Co Ltd
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Priority to CN201611097874.9A priority Critical patent/CN106903309A/en
Publication of CN106903309A publication Critical patent/CN106903309A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F10/00Additive manufacturing of workpieces or articles from metallic powder
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F10/00Additive manufacturing of workpieces or articles from metallic powder
    • B22F10/20Direct sintering or melting
    • B22F10/28Powder bed fusion, e.g. selective laser melting [SLM] or electron beam melting [EBM]
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F10/00Additive manufacturing of workpieces or articles from metallic powder
    • B22F10/30Process control
    • B22F10/36Process control of energy beam parameters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F10/00Additive manufacturing of workpieces or articles from metallic powder
    • B22F10/60Treatment of workpieces or articles after build-up
    • B22F10/64Treatment of workpieces or articles after build-up by thermal means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F10/00Additive manufacturing of workpieces or articles from metallic powder
    • B22F10/60Treatment of workpieces or articles after build-up
    • B22F10/66Treatment of workpieces or articles after build-up by mechanical means
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F5/00Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product
    • B22F5/10Manufacture of workpieces or articles from metallic powder characterised by the special shape of the product of articles with cavities or holes, not otherwise provided for in the preceding subgroups
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B23MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23PMETAL-WORKING NOT OTHERWISE PROVIDED FOR; COMBINED OPERATIONS; UNIVERSAL MACHINE TOOLS
    • B23P15/00Making specific metal objects by operations not covered by a single other subclass or a group in this subclass
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y10/00Processes of additive manufacturing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B33ADDITIVE MANUFACTURING TECHNOLOGY
    • B33YADDITIVE MANUFACTURING, i.e. MANUFACTURING OF THREE-DIMENSIONAL [3-D] OBJECTS BY ADDITIVE DEPOSITION, ADDITIVE AGGLOMERATION OR ADDITIVE LAYERING, e.g. BY 3-D PRINTING, STEREOLITHOGRAPHY OR SELECTIVE LASER SINTERING
    • B33Y80/00Products made by additive manufacturing
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C21/00Apparatus or processes specially adapted to the manufacture of reactors or parts thereof
    • G21C21/18Manufacture of control elements covered by group G21C7/00
    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21CNUCLEAR REACTORS
    • G21C7/00Control of nuclear reaction
    • G21C7/06Control of nuclear reaction by application of neutron-absorbing material, i.e. material with absorption cross-section very much in excess of reflection cross-section
    • G21C7/08Control of nuclear reaction by application of neutron-absorbing material, i.e. material with absorption cross-section very much in excess of reflection cross-section by displacement of solid control elements, e.g. control rods
    • G21C7/12Means for moving control elements to desired position
    • G21C7/14Mechanical drive arrangements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F3/00Manufacture of workpieces or articles from metallic powder characterised by the manner of compacting or sintering; Apparatus specially adapted therefor ; Presses and furnaces
    • B22F3/24After-treatment of workpieces or articles
    • B22F2003/248Thermal after-treatment
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E30/00Energy generation of nuclear origin
    • Y02E30/30Nuclear fission reactors
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/25Process efficiency

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Chemical & Material Sciences (AREA)
  • Materials Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Plasma & Fusion (AREA)
  • Thermal Sciences (AREA)
  • Automation & Control Theory (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Laser Beam Processing (AREA)

Abstract

The present invention discloses a kind of nuclear power station CRDM hook and its manufacture method with novel wear resistant Rotating fields.The hook structure is:The wearing layer profile of pin-and-hole is square;Briar tooth is plane with the faying face of matrix.The present invention uses laser 3D printing technology, and manufacturing step is as follows:S1:Set up blank three-dimensional digital-to-analogue;S2:Laser deposition fabrication scheme is formulated, and logarithmic mode carries out section and laser beam scan path planning;S3:Setting Fabrication parameter and basketry control program;S4:Complete preparation before manufacture;S5:Program according to setting carries out laser deposition manufacture;S6:Hook blank is separated from substrate cut, is then heat-treated;S7:Acquisition hook finished product is machined out to the hook blank after heat treatment.Hook produced by the present invention has mechanical property more more preferable than oxygen-acetylene repairing hook, and the fully automated control of production process is not influenceed by operating personnel, is adapted to batch production, can completely substitute oxygen-acetylene repairing hook.

Description

A kind of hook and its manufacture method with novel wear resistant Rotating fields
Technical field
The invention belongs to laser gain material manufacture field, it is related to for a kind of new of nuclear power station CRDM hook Structure and manufacture method.
Background technology
CRDM is the key equipment of nuclear power plant reactor, is also uniquely to move equipment on reaction reator body. Hook component is one of most crucial, most critical part in CRDM.The startup of reactor, power adjusting, power The feature operations such as holding, normal shutdown and breakdown, exactly enter to show mode by two groups of hooks according to the pendulum that sequential is moved Completing drive rod drives the lifting of reactor core control rod, underthrust to act to realize.
The development of nuclear power technology is proposed higher to the security of reactor system and equipment, reliability and economy It is required that.Used as consumable accessory, the characteristic such as the wear-resistant of hook, heat resistance, corrosion-resistant directly determines whole CRDM Service life.Overlaying-type hook is difficult to collapse tooth, fracture and fragmentation due to its superior impact resistance, corrosion resistance, amount containing cobalt it is low and More preferable wearability and be widely adopted.But the operation difficulty for carrying out oxy-acetylene manual build up welding in aperture due to it is high, technique Stability is poor, low production efficiency, product percent of pass are low, and the product of domestic relevant unit does not have practical engineering application to be worth.It is domestic This kind of hook almost all that nuclear power engineering is used uses import.Overlaying-type hook, connecting rod turn into CRDM in only One is not carried out the domestic part of mass.
Laser gain material is produced by deconstructing three-dimensional structure for recycling high energy laser beam carries out stacking manufacture after two dimension Technology.There is unique advantage for the processing and manufacturing of complex component, refractory material.The present invention is just to provide a kind of with new The hook and its laser deposition manufacture method of wear-resisting Rotating fields.
The content of the invention
The invention provides a kind of nuclear power station CRDM hook and its laser with novel wear resistant Rotating fields Deposition process method.
Nuclear power station CRDM hook novel wear resistant Rotating fields proposed by the present invention, it is characterized in that:Pin-and-hole it is resistance to Mill layer is the cylindrical tubular being serrated;Pin-and-hole wearing layer is zigzag with matrix faying face;The faying face of briar tooth and matrix It is zigzag.
The laser deposition system of the nuclear power station CRDM hook with novel wear resistant Rotating fields proposed by the present invention Method is made, is comprised the following steps:
S1:Set up hook blank three-dimensional digital model;
S2:Hook laser deposition fabrication scheme is formulated, and logarithmic mode carries out section and laser beam scan path planning;
S3:Setting laser deposition Fabrication parameter and basketry control program;
S4:Complete preparation before laser deposition manufacture;
S5:Program according to setting carries out laser deposition manufacture;
S6:Hook blank is separated from substrate cut it is right, after be heat-treated;
S7:Hook blank after heat treatment is machined out, hook finished product is obtained.
The cylindrical tubular hook jaw pin porose area wearing layer being serrated of the present invention, it is characterized in that:Pipe overall diameter is not Less than 10.5mm, no more than 19.0mm.
Hook laser deposition manufacture method S2 steps of the present invention, it is characterised in that:
S2-1:Hook blank is used to be given birth in horizontal lateral flat manner with plane where briar tooth face centre normal and its axis It is long;
S2-2:Hook blank digital-to-analogue is cut into slices;
S2-3:Subregion is carried out to section, and plans the laser beam scan path of each subregion;
S2-4:The section of establishment hook blank and laser deposition fabrication schedule file.
Laser deposition manufacture hook blank S3 steps setting laser deposition Fabrication parameter of the present invention, it is characterised in that: Laser spot diameter is φ 2mm ~ φ 6mm, and laser power is 1kw ~ 5Kw, laser scanning speed 3mm/s ~ 30mm/s, laser scanning Overlapping rate is 30% ~ 50%, and slice thickness is 0.5mm ~ 2.0mm.
Laser deposition of the present invention manufactures hook blank S4 steps, it is characterised in that:
S4-1:To base material degreasing, surface polishing scale removal, then cleaning, drying;
S4-2:Base material is placed on the workbench in the laser deposition molding storehouse of argon atmospher protection and fixed, adjustment powder feeder To the distance of substrate surface, and set the beginning and end of laser scanning;
S4-3:Laser deposition manufacture hook blank is loaded into powder feeder with raw material powder;
S4-4:Carry out the reasonability of laser deposition fabrication schedule prerun, testing equipment operation accuracy and program operation;
Laser deposition of the present invention manufactures the heat treatment of hook blank S6 steps, it is characterised in that:Heat treatment temperature is 800 DEG C ~ 1075 DEG C, the type of cooling is furnace cooling.
The machining of S7 steps of the present invention, it is characterised in that:
S7-1:Datum level is processed --- and the depositional plane top surface and bottom cut surface of Milling Machining hook blank turn into processing datum;
S7-2:Pin-and-hole axle center positions --- the circular wear-resisting area's home position of lower pin-and-hole is orientated as pin-and-hole axle center, according still further to size It is required that positioning pin-and-hole axle center in the circular wear-resisting area's home position of upper pin-and-hole;
S7-3:Punching --- hole milling is carried out in pin-and-hole wearing layer area with the axle center set;
S7-4:Then the numerical programming procedure on the basis of upper and lower pin-and-hole axle center, completes the machining of hook.
S2-3 digital-to-analogues section of the present invention, it is characterised in that:At least it is divided into four scannings point in pin-and-hole layer slice plane Area --- matrix area, lower pin-and-hole high-abrasive material area and upper high-abrasive material area of pin-and-hole portion;Upper and lower pin-and-hole high-abrasive material area is with hook Circle centered on pin-and-hole axle center;The round diameter is between 10.5mm ~ 19mm;The circular high-abrasive material of adjacent two layers section Area's diameter differs 2mm ~ 4mm.
S2-4 laser beam scan paths planning of the present invention, it is characterised in that:The laser scanning of same section different zones Path can mutually be mutually perpendicular to, it is also possible to be parallel to each other;The laser beam scan path of adjacent two layers can be with identical, it is also possible in one Determine angle, such as 90 °.
The base material of S4-1 steps of the present invention, it is characterised in that:Base material is stainless steel, such as 12Cr17Mn6Ni5N, 12Cr18Ni9, Y12Cr18Ni9, Y12Cr18Ni9Cu3,06Cr19Ni10,00Cr18Ni9N.
S4-3 laser depositions of the present invention manufacture hook blank raw material powder, it is characterised in that:Hook matrix former material Feed powder end is this body stainless steel of 00Cr18Ni9N control nitrogen Austria;Wearing layer raw material powder is the cobalt-base alloys of Stellite 6.
S4-3 powder feeders of the present invention, it is characterised in that:Powder feeder at least possesses two powder feeding storehouses of sealing.
This body powder of stainless steel of 00Cr18Ni9N controls nitrogen Austria of the present invention, it is characterised in that:The manufacture of the material powder Method is rotary electrode method or gas atomization.
The Co-based alloy powders of Stellite of the present invention 6, it is characterised in that:The manufacture method of the material powder is rotation Turn electrode method or gas atomization.
The hook that the present invention is provided has crystal grain tiny, and mechanical property is good, and wearing layer hardness uniform, controllable, residual stress is small Etc. advantage.The laser deposition manufacture method that the present invention is provided is different from traditional-handwork oxygen-acetylene repairing technique dependence operator, Production process Automatic Control, laser deposition manufacture system is totally-enclosed, not by external environment and operating personnel's technical merit and work Make the influence of state, production yield rate is high, with product mass production advantage.
Brief description of the drawings
Drawings and Examples can be so that the present invention is further described, and accompanying drawing is as follows:
Fig. 1 oxygen-acetylene repairing hook structural representations;
Pin-and-hole wearing layer structural representation under Fig. 2 oxygen-acetylene repairing hooks;
Fig. 3 oxygen-acetylene repairing hook briar tooths and matrix faying face schematic diagram;
Fig. 4 laser depositions manufacture hook structural representation;
Pin-and-hole wearing layer structural representation under Fig. 5 laser depositions manufacture hook;
Fig. 6 laser depositions manufacture hook briar tooth and matrix faying face schematic diagram;
The zigzag faying face of Fig. 7 high-abrasive materials and matrix;
Fig. 8 laser depositions manufacture hook blahk structure schematic diagram;
Fig. 9 laser depositions manufacture hook blank pin-and-hole layer section schematic diagram;
Figure 10 laser depositions manufacture hook blank pin-and-hole layer section laser beam scan path planning chart;
6 heat treatment hardnesses of Figure 11 laser deposition Stellite-temperature curve;
Figure 12 laser deposition control nitrogen austenitic stainless steels heat treatment hardness-temperature curve;
Figure 13 laser depositions manufacture hook blank machining pin-and-hole axle center positioning schematic diagram.
Numbering explanation:1 --- oxygen-acetylene repairing hook matrix, 2 --- pin-and-hole and its wearing layer under oxygen-acetylene repairing hook, 3 --- pin-and-hole and its wearing layer, 4 on oxygen-acetylene repairing hook --- oxygen-acetylene repairing hook briar tooth wearing layers;5 --- laser sinks Product hook matrix, 6 --- pin-and-hole and its wearing layers, 7 under laser deposition hook --- pin-and-hole and its wear-resisting on laser deposition hook Layer, 8 --- laser deposition hook briar tooth wearing layer;9 --- pin-and-hole axle center, 10 --- laser under laser deposition manufacture hook blank Pin-and-hole axle center on deposit manufacture hook blank.
Specific embodiment
The manufacture method of oxygen-acetylene repairing hook is:It is machined to using 00Cr18Ni9N control nitrogen austenitic stainless steel forging rods Hook matrix 1, the pin hole processing on matrix;Pin-and-hole 2 is wherein descended to be processed into the symmetric pyramid hole with certain inclination angle, such as Fig. 2 institutes Show;Briar tooth facing cut processes groove surface, as shown in Figure 3;Then oxy-acetylene heap is carried out with the cobalt-base alloy welding wires of Stellite 6 again Weldering pin-and-hole wearing layer 2 and 3, in briar tooth surface build-up welding briar tooth 4;Then blank is made annealing treatment, finally carries out finished product machining. One of difficult point of the technique is the built-up welding of wearing layer in pin-and-hole.The pin-and-hole of hook is a kind of Small-deep Hole, main in the hole Built-up welding is carried out by manual operations.Although the cobalt-base alloys of Stellite 6 is with good wearability, but a kind of remnants should Power sensitive material, the faying face of wearing layer and matrix control nitrogen austenitic stainless steel is easily ftractureed due to the presence of residual stress;And During manual build up welding, the technical merit and working condition of operating personnel can influence the carburizing amount of wearing layer, cause abrasion hardness exceeded And skewness;Therefore the technique is stronger to the dependence of operating personnel, technology stability extreme difference.
Laser gain material manufacturing technology is that three-dimensional structure is decomposed into 2-d plane graph, recycles laser digitizing processing system Powder rapid melting is shaped X-Y scheme structure by system, successively piles up a kind of brand-new manufacturing process of manufacture product, and laser sinks Product manufacturing technology is the one kind in laser gain material manufacturing technology.The step of present invention is using laser deposition manufacturing technology manufacture hook Including:
A, set up hook blank three-dimensional digital model;
B, formulation hook laser deposition fabrication scheme, and logarithmic mode carries out section and laser beam scan path planning;
C, setting laser deposition Fabrication parameter, work out laser deposition manufacturing process control program;
Preparation before d, completion laser deposition manufacture;
E, carry out laser deposition manufacture according to process file;
F, hook blank is cut into separation from substrate, be then heat-treated;
G, roughing is carried out to the hook blank after heat treatment and Non-Destructive Testing is carried out;
H, the hook blank qualified to Non-Destructive Testing are finished, and manufacture finished product hook;
I, size and appearance test are carried out to finished product hook.
The concrete mode of each step is introduced with example below:
A, set up hook blank mathematical model
According to hook finished product mathematical model, hook machining blank mathematical model is designed first;It is special further according to laser deposition technique Internal soundness of seeking peace detection requires that each machined surface all increases allowance, so as to obtain laser deposition manufacture hook blank Numerical model;
Finished product hook jaw pin bore dia is in the present inventionφ9.493mm, the cylindrical jagged tubular wearing layer tooth root section circle of layer With diameter greater than pin-and-hole diameter, less than the width 19mm of hook side.The wear-resisting area of the present invention be respectively adopted diameter 10.5mm, 14mm and 19mm, space width is respectively 0.5mm, 1mm, 1.5mm and 2.0mm and is manufactured and designed.
B, formulation hook laser deposition fabrication scheme, and logarithmic mode carries out section and laser beam scan path planning
Three-dimension Numerical Model structure and laser deposition manufacturing technical feature according to blank, design the forming arrangements of blank.According to The characteristics of hook blank is L-shaped, the present invention is laterally kept flat with plane where its axis using briar tooth face centre normal in horizontal, Along the forming arrangements of arrow meaning vertical direction successively accumulated growth, as shown in Figure 8;
When being cut into slices according to the program, hook slice plane inner structure will be identical, as shown in Figure 9.Each section is divided into Four regions:Matrix 5, lower pin-and-hole high-abrasive material area 6, upper pin-and-hole high-abrasive material area 7 and briar tooth area 8.The pin of adjacent two layers section Hole high-abrasive material area diameter difference 2mm ~ 4mm, makes high-abrasive material area form Sawtooth connection with matrix, as shown in Figure 7;
Laser beam scan path planning is carried out to section.In order to reduce and cutting down cumulative stress, the laser of adjacent two layers is typically required Scanning pattern is angled.In the present invention, the laser beam scan path of adjacent two layers section is vertical in 90 °;
When laser beam scan path planning is carried out, in addition to the laser beam scan path of adjacent two layers section is angled, with all The laser beam scan path in adjacent twoth area is also angled in piece.It is in 90 °, as shown in Figure 10, Figure 10 that the present invention is(a)With Figure 10(b)It is the laser beam scan path planning of two neighboring section;Now need to set sweep span, i.e. laser scanning overlap joint Rate, overlapping rate of the present invention be 30% ~ 50% between.
C, setting laser deposition Fabrication parameter simultaneously work out laser deposition manufacturing process control program
The 00Cr18Ni9N control nitrogen austenitic stainless steels of optimization and swashing for the cobalt-base alloys of Stellite 6 are obtained by system experimentation Light deposition fabrication process parameters.It is as shown in table 1 present invention optimizes three kinds of laser technical parameterses:
The hook laser deposition fabrication process parameters table of table 1
According to technological parameter and section scanning pattern, laser deposition manufacturing process control program is worked out.
Preparation before d, completion laser deposition manufacture
Preparation before laser deposition manufacture, is divided into four aspects:The first step, base material prepares;Second step, workbench prepares; 3rd step, raw material prepare;It is finally program prerun;
First it is that base material prepares.Due to laser deposition is control nitrogen austenitic stainless steel, and first-selected base material is exactly to control nitrogen austenitic not Rust steel board.In view of cost, can be replaced with other stainless steels, such as 12Cr17Mn6Ni5N(201 trades mark), 12Cr18Mn9Ni5N (202 trades mark), 12Cr18Ni9(302 trades mark), Y12Cr18Ni9(303 trades mark), 06Cr19Ni10(304 trades mark)Deng.The present invention Use 06Cr19Ni10 cut deals, thickness 30mm;
Base material is cleaned into degreasing and rust removal, in drying oven inner heating drying, 150 DEG C of drying temperature is incubated 60min.Then to base material Flash removed, the bright descaling of surface polishing are removed in corner angle polishing;
Second step, workbench prepares.The base material that will be dried and polish is placed on the workbench in laser deposition molding storehouse And fixed with fixture, argon gas is full of in the shaping storehouse.Laser deposition molding coaxial powder feeding device to the distance of substrate surface is adjusted, really Guarantor's substrate deposition surface is in the range of laser spot.The beginning and end that setting powder feeder is scanned on base material, limits sweep limits. Finally confirm the oxygen content in shaping storehouse, laser deposition manufacture could be started when only less than 50ppm;
3rd step, raw material prepare.Raw materials of the present invention be 00Cr18Ni9N control nitrogen austenitic stainless steel powder and The Co-based alloy powders of Stellite 6.00Cr18Ni9N is controlled nitrogen austenitic stainless steel powder and is prepared using rotation electrode technique, changes Study and point meet RCC-M standards, granularity is -60 mesh ~ 200 mesh.The Co-based alloy powders of Stellite 6 are prepared for gas atomization Built-up welding powder, chemical composition meets AWS A5.21 standards, mesh ~ 320 of powder size -100 mesh;
Powder is fitted into the powder feeder of laser deposition digital control system, the powder feeder at least has two powder feeding storehouses, it is possible to achieve Laser deposition manufacture while at least two dusty materials.Powder feeder used of the invention is carrier gas type powder feeder, and protective gas is High-purity argon gas, possess three powder feeding storehouses, it is possible to achieve laser deposition while three kinds of dusty materials.
4th step, program prerun.After above-mentioned preparation is completed, under conditions of laser is not opened, operation process The program of control, accuracy, integrality and reliability that each equipment such as inspection numerical control program, lathe, protection gas and powder feeder is run Property, it is ensured that stablizing for hook manufacturing process is controllable.If it find that problem, revision program or equipment, are then carried out pre- again immediately Operation, untill confirming without any exception.
E, according to setting program file carry out laser deposition manufacture
The present invention has carried out the laser deposition of hook blank according to the process control procedure that the laser technical parameterses of table 1 are worked out respectively Manufacture.In laser deposition manufacturing process, note observing forming quality, note abnormalities and want instant adjusting process, it is ensured that laser deposition Process is smoothed out.
F, hook blank is cut into separation from substrate, be then heat-treated
Laser deposition manufacturing technology is due to being that high energy beam transient prediction melts and unstable state solidification forming, and its residual stress is larger, Stress relief annealing must be carried out.
Nitrogen austenitic stainless steel and Stellite 6 are controlled to laser deposition 00Cr18Ni9N carries out heat treatment experiment, obtains two Temperature-the hardness curve of person, as is illustrated by figs. 11 and 12, Figure 11 is 6 hardness of laser deposition Stellite-temperature curve, figure 12 is laser deposition 00Cr18Ni9N control nitrogen austenitic stainless steels hardness-temperature curve.According to hardness-temperature curve, the present invention It is preferred that the heat treatment temperature of the hook blank for determining is 800 DEG C ~ 1075 DEG C.According to the temperature of selection, it is incubated respectively 30min, 45min, 60min, 75min and 90min are contrasted.
To being drawn through 00Cr18Ni9N control nitrogen austenitic stainless steels and the cobalt-base alloys of Stellite 6 after Overheating Treatment Performance test is stretched, test result is as shown in table 2:
Laser deposition 00Cr18Ni9N controls nitrogen austenitic stainless steel and the cobalt-base alloys mechanical property of Stellite 6 after table 2 is heat-treated Energy
As can be seen that the cobalt-base alloys of Stellite 6 of laser deposition manufacture and 00Cr18Ni9N control nitrogen austenitic stainless steels, nothing By be laser deposition state or heat treatment after, its comprehensive mechanical property all be higher than RCC-M standards;
According to above-mentioned Tensile Test Results, currently preferred hook Technology for Heating Processing is:Heat treatment temperature:800℃~1075 DEG C, soaking time 45min ~ 75min, the type of cooling is with stove Slow cooling.
G, roughing is carried out to the hook blank after heat treatment and Non-Destructive Testing is carried out
Hook blank to completing heat treatment is machined out, and hook shaped top and bottom surface are processed first(Two sides of hook) Into datum level, smooth bright and clean surface, surface roughness≤1.6 μm are obtained.Then water logging ultrasonic wave C-scan inspections are carried out to it Test, confirm blank internal soundness.The Rockwell of the wearing layers of Stellite 6 is tested in briar tooth area 8, lower pin-and-hole area 6 and upper pin-and-hole area 7 Hardness, each area test is no less than 3 points.In the present invention, the Rockwell hardness of trizonal Stellite 6 is identical, is HRC43 ±2。
H, the hook blank qualified to Non-Destructive Testing are machined out, and obtain hook finished product
To checking qualified hook blank to finish.Two sides of processing hook first turn into processing datum, processing When be necessary to ensure that two sides are vertical with wearing layer faying face, then the datum level bottom 6 regions of Stellite 6 position under Pin-and-hole axle center 9, then with axle center 9 as basic point, positions pin-and-hole axle center 10, in theory axle in 6 regions of Stellite 7 on top The heart 10 should also be the center of circle of the circle of region 7, but have deviation in practice, as shown in figure 13.Numerical programming procedure, respectively On the basis of axle center 9 and axle center 10, punching and finished product machining are completed.
I, size and appearance test are carried out to hook
Dimension control is carried out to hook finished product using high precision three-dimensional coordinates measurement instrument.The thick of each machined surface is tested using extra coarse degree instrument Rugosity.Whether there is crackle using osmosis inspection finished product hook.Sight check hook outward appearance is complete under high-brightness environment Property.During visual detection, hook surface is not allow for any pit, cracking, crackle, incomplete fusion and slag inclusion.Liquid penetrating inspection When, not in there is any linear display on wear-resisting area and interface(It is a length of wide 3 times);It is not allow for circular more than 1.5mm It has been shown that, if the minimum thickness required after final machining is less than 1.5mm, the maximum allowable size of circle display is the thickness; A Liquid Penetrant has been allowed to show.
The hook manufactured by above-mentioned steps can fully meet the use requirement of nuclear power station CRDM hook.It is logical Ultrasonic NDT and penetrating inspection are crossed, any excessive defect is not found, wearing layer hardness HRC43 ± 2 meet product technology and want Ask, and than oxygen-acetylene repairing hook wearing layer hardness evenly.The hook of this method manufacture, laser deposition 00Cr18Ni9N control nitrogen Austenite stainless steel matrix has and has more preferable comprehensive mechanical property than oxygen-acetylene repairing hook matrix.Production process of the present invention Fully automated control, manufacturing process and quality are not influenceed by operating personnel, are adapted to batch production, can completely substitute oxy-acetylene heap Weldering hook.

Claims (15)

1. the nuclear power station CRDM hook that a kind of utilization laser gain material manufacturing technology is manufactured, it is characterised in that:Pin-and-hole Wearing layer be the cylindrical tubular being serrated;Pin-and-hole wearing layer is zigzag with matrix faying face;The knot of briar tooth and matrix Conjunction face is zigzag.
2. the laser gain material manufacturer of the nuclear power station CRDM hook of the novel wear resistant Rotating fields described in claim 1 Method, comprises the following steps:
S1:Set up hook blank three-dimensional digital model;
S2:Hook laser gain material fabrication scheme is formulated, and logarithmic mode carries out section and laser beam scan path planning;
S3:Setting laser gain material Fabrication parameter and basketry control program;
S4:Complete preparation before laser gain material manufacture;
S5:Program according to setting carries out laser gain material manufacture;
S6:Hook blank is separated from substrate cut, is then heat-treated;
S7:Hook blank after heat treatment is machined out, hook finished product is obtained.
3. the cylindrical tubular hook jaw pin porose area wearing layer being serrated described in claim 1, it is characterized in that:Pipe overall diameter is not Less than 10.5mm, no more than 19.0mm.
4. hook laser gain material manufacture method S2 steps described in claim 2, it is characterised in that:
S2-1:Hook blank is used to be grown in horizontal lateral flat manner with plane where briar tooth face center method and its axis;
S2-2:Hook blank digital-to-analogue is cut into slices;
S2-3:Subregion is carried out to section, and plans the laser beam scan path of each subregion;
S2-4:The section of establishment hook blank and laser gain material fabrication schedule file.
5. laser gain material manufacture hook blank S3 steps set laser gain material Fabrication parameter described in claim 2, it is characterised in that: Laser spot diameter is φ 2mm ~ φ 6mm, and laser power is 1kw ~ 5Kw, laser scanning speed 3mm/s ~ 30mm/s, laser scanning Overlapping rate is 30% ~ 50%, and slice thickness is 0.5mm ~ 2.0mm.
6. laser gain material described in claim 2 manufactures hook blank S4 steps, it is characterised in that:
S4-1:To base material degreasing, surface polishing scale removal, then cleaning, drying;
S4-2:Base material is placed on the workbench in the laser deposition molding storehouse of argon atmospher protection and fixed, adjustment powder feeder To the distance of substrate surface, and set the beginning and end of laser scanning;
S4-3:Laser gain material manufacture hook blank is loaded into powder feeder with raw material powder;
S4-4:Carry out the reasonability of laser gain material fabrication schedule prerun, testing equipment operation accuracy and program operation.
7. laser gain material described in claim 2 manufactures the heat treatment of hook blank S6 steps, it is characterised in that:Heat treatment temperature is situated between Between 800 DEG C ~ 1075 DEG C, soaking time 45min ~ 75min, the type of cooling is furnace cooling.
8. the machining of S7 steps described in claim 2, it is characterised in that:
S7-1:Datum level is processed --- and the depositional plane top surface and bottom cut surface of Milling Machining hook blank turn into processing datum;
S7-2:Pin-and-hole axle center positions --- the circular wear-resisting area's home position of lower pin-and-hole is orientated as pin-and-hole axle center, according still further to size It is required that positioning pin-and-hole axle center in the circular wear-resisting area's home position of upper pin-and-hole;
S7-3:Punching --- hole milling is carried out in pin-and-hole wearing layer area with the axle center set;
S7-4:Then the numerical programming procedure on the basis of upper and lower pin-and-hole axle center, completes the machining of hook.
9. S2-3 digital-to-analogues section described in claim 4, it is characterised in that:At least it is divided into four scannings point in pin-and-hole layer slice plane Area --- matrix area, lower pin-and-hole wearing layer area, upper pin-and-hole wearing layer area and briar tooth area;Upper and lower pin-and-hole high-abrasive material area is with hook Circle centered on pin-and-hole axle center;The round diameter is between 10.5mm ~ 19mm;The circular high-abrasive material of adjacent two layers section Area's diameter differs 2mm ~ 4mm.
10. S2-4 laser beam scan paths planning described in claim 4, it is characterised in that:The laser of same section different zones is swept Retouching path can mutually be mutually perpendicular to, it is also possible to be parallel to each other;The laser beam scan path of adjacent two layers section can also may be used with identical With at an angle, such as 90 °.
The base material of S4-1 steps described in 11. claims 6, it is characterised in that:Base material is stainless steel, such as 12Cr17Mn6Ni5N, 12Cr18Ni9, Y12Cr18Ni9, Y12Cr18Ni9Cu3,06Cr19Ni10,00Cr18Ni9N.
S4-3 laser gain materials manufacture hook blank raw material powder described in 12. claims 6, it is characterised in that:Raw matrix materials Powder is this body stainless steel of 00Cr18Ni9-N control nitrogen Austria;Wearing layer raw material powder is the cobalt-base alloys of Stellite 6.
The powder feeder of S4-3 steps described in 13. claims 6, it is characterised in that:Powder device at least possesses two powder feeding storehouses of sealing.
This body powder of stainless steel of 00Cr18Ni9-N controls nitrogen Austria described in 14. claims 13, it is characterised in that:The material powder Manufacture method is rotary electrode method or gas atomization.
The Co-based alloy powders of Stellite 6 described in 15. claims 13, it is characterised in that:The manufacture method of the material powder is Rotary electrode method or gas atomization.
CN201611097874.9A 2016-12-03 2016-12-03 A kind of hook and its manufacture method with novel wear resistant Rotating fields Pending CN106903309A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108480927A (en) * 2018-04-04 2018-09-04 鑫精合激光科技发展(北京)有限公司 A kind of preparation method with metallurgical binding abrasion resistant layer nuclear power hook
CN108962412A (en) * 2018-07-27 2018-12-07 中国核动力研究设计院 A kind of manufacturing process of in-pile component monoblock type guide cylinder
CN111299576A (en) * 2019-12-31 2020-06-19 北京航空航天大学合肥创新研究院 Multi-component material laser additive manufacturing method for precision component

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108480927A (en) * 2018-04-04 2018-09-04 鑫精合激光科技发展(北京)有限公司 A kind of preparation method with metallurgical binding abrasion resistant layer nuclear power hook
CN108962412A (en) * 2018-07-27 2018-12-07 中国核动力研究设计院 A kind of manufacturing process of in-pile component monoblock type guide cylinder
CN111299576A (en) * 2019-12-31 2020-06-19 北京航空航天大学合肥创新研究院 Multi-component material laser additive manufacturing method for precision component

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