CN106900754A - Lawn-care galenical and preparation method thereof - Google Patents

Lawn-care galenical and preparation method thereof Download PDF

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Publication number
CN106900754A
CN106900754A CN201710046309.8A CN201710046309A CN106900754A CN 106900754 A CN106900754 A CN 106900754A CN 201710046309 A CN201710046309 A CN 201710046309A CN 106900754 A CN106900754 A CN 106900754A
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parts
lawn
care
preparation
galenical
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施春华
张美芬
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Shengzhou City Paitepu Technology Development Co Ltd
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Shengzhou City Paitepu Technology Development Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10Animals; Substances produced thereby or obtained therefrom
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08Magnoliopsida [dicotyledons]
    • A01N65/20Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05BPHOSPHATIC FERTILISERS
    • C05B7/00Fertilisers based essentially on alkali or ammonium orthophosphates
    • CCHEMISTRY; METALLURGY
    • C05FERTILISERS; MANUFACTURE THEREOF
    • C05GMIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
    • C05G3/00Mixtures of one or more fertilisers with additives not having a specially fertilising activity

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Dentistry (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Agronomy & Crop Science (AREA)
  • Wood Science & Technology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Pest Control & Pesticides (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Virology (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention provides a kind of lawn-care galenical and preparation method thereof, and bactericide is made up of following component and weight portion:22 ~ 28 parts of kuh-seng, 25 ~ 45 parts of dandelion, 60 ~ 70 parts of the root of langdu, 25 ~ 35 parts of Flos Artemisiae finitae, 15 ~ 25 parts of Chinese gall, 1 ~ 3 part of insecticides adjuvant, 0.7 ~ 1.5 part of eupatorine, 0.1 ~ 0.3 part of nutritional agents, present invention also offers the preparation method of bactericide, bactericide prepared by the present invention can not only kill bacterium on lawn, virus also has certain insecticidal effect, instant effect, excellent effect, effective time is long, low toxicity and low residue, to person poultry harmless, it is degradable, grass will not develop immunity to drugs, and can also provide nutriment for lawn, it is ensured that lawn healthy growth.

Description

Lawn-care galenical and preparation method thereof
Technical field
The invention belongs to bactericide technical field, and in particular to a kind of lawn-care galenical and preparation method thereof.
Background technology
The rise of Lawn Industry is the mark of human civilization and social progress, and China's Lawn Industry has stepped into extensive hair at present The new period of exhibition, turfgrass species is various, and characteristic is different.Classify by weather conditions and turfgrass Regional Distribution, can be by turfgrass It is divided into warm season turf and cold-season turfgrass.Warm season turf principally falls into grass family, and optimum growth temperature is 25~ 30℃.Cold-season turfgrass, originates in Northern Europe and Asia, and growth thermophilic is 15~25 DEG C, is mainly distributed on the North China and east of China Backlands area, harm that Diseases of Turfgrass is caused is big, is preventing and treating lawn disease at present using bactericide while prevent that difficulty is big, high cost Harmful important means, but the bactericide consumption of routine is big, but do not reach good bactericidal effect.
Prior art such as, Chinese invention granted patent document, the B of Authorization Notice No. CN 103875722, the disclosure of the invention A kind of Chinese herbal medicine merges the botanical fungicide for extracting, and its active ingredient is by the Chinese herbal medicine merging extraction of following weight ratio Into 20 ~ 30 parts of kuh-seng, 20 ~ 50 parts of dandelion, 50 ~ 80 parts of the root of langdu, 20 ~ 40 parts of Flos Artemisiae finitae, 10 ~ 30 parts of Chinese gall;Its system Preparation Method is, by each taste Chinese herbal medicine dried and crushed, to soak 2 ~ 8 hours in ethanol, is circulated extraction 2 ~ 8 times, is extracted every time About 40 ~ 60 minutes time, remove the dregs of a decoction, extract solution be placed in Rotary Evaporators be concentrated in vacuo, be concentrated into be quantitatively adding it is quantitative Insecticides adjuvant stirs prepared, and it has a preparation stabilization, and significantly, broad spectrum activity is good for bactericidal effect, the characteristics of to person poultry safety, but It is that the bactericide is only capable of playing bactericidal effect, unitary function lacks the nutritional ingredient beneficial to lawn, in terms of to lawn maintenance Also certain room for promotion.
The content of the invention
The present invention provides a kind of excellent to lawn bactericidal effect and with insecticidal effect for above-mentioned technical problem, will not be dirty Dye environment, low toxicity and low residue improves tolerance, can also provide a kind of lawn-care that nutriment ensures careless healthy growth for grass With galenical and preparation method thereof.
It is of the invention to be for the scheme that above-mentioned technical problem is taken:Lawn-care galenical, bactericide is by following Composition and weight portion are constituted:22 ~ 28 parts of kuh-seng, 25 ~ 45 parts of dandelion, 60 ~ 70 parts of the root of langdu, 25 ~ 35 parts of Flos Artemisiae finitae, Chinese gall 15 ~ 25 parts, 1 ~ 3 part of insecticides adjuvant, 0.7 ~ 1.5 part of eupatorine, 0.1 ~ 0.3 part of nutritional agents, bactericide of the invention can not only be killed Bacterium, virus on weed eradication level ground also have certain insecticidal effect, and instant effect, excellent effect is degradable, can also be provided for lawn Nutriment, it is ensured that lawn healthy growth.
Preferably, insecticides adjuvant includes bleeding agent, preservative and amphoteric surfactant, bleeding agent is polyoxyethylene nonyl phenyl One or more mixture in vinethene, AEO, polysorbate60, Tween 80, makes bactericide effectively permeate Harmful bacteria and virus are killed in grass, preservative is Sodium Benzoate or potassium sorbate, prevents the medicinal herb componentses in bactericide from becoming Matter, reduces bactericidal effect, and amphoteric surfactant is made up of following component and weight portion:Myristyl dihydroxy ethyl amine oxide 3 ~ 5 parts, 3.5 ~ 4.5 parts of dodecyl alanine, 5 ~ 15 parts of water, 3.3 ~ 3.8 parts of ethanol, 0.2 ~ 0.3 part of vegetable oil, make preparation Sterilized reduction in surface tension, each composition is uniformly dispersed, and makes the bactericide also effect with easily biological-degradable.
Preferably, nutritional agents is made up of following component and weight portion:4 ~ 6 parts of polysaccharide, 0.2 ~ 0.6 part of calcium ammonium nitrate, partially 0.22 ~ 0.48 part of sodium metasilicate, 5 ~ 12 parts of ammonium humate, 2 ~ 4 parts of potassium dihydrogen phosphate, polysaccharide are many sucrose, glucose, Agricus blazei One or more in sugar, astragalus polyose, R- polysaccharide, after bactericide can be made to be sprayed on lawn, while bactericide is acted on For lawn provides nutriment, it is ensured that lawn healthy growth, except root, stem, leaf normal growth, sodium metasilicate and nitric acid can be promoted Ammonium calcium produces unexpected effect by polysaccharide, with the effect for stimulating lawn tolerance to improve, especially to harmful bacteria, Under adverse circumstances.
The preparation method of lawn-care galenical, preparation method is comprised the following steps:
It is prepared by eupatorine:By weight, fresh Eupatorium adenophorum is taken, is cleaned, dries pulverizing, soaked with extractant, it is ultrasonic-wave assisted Molten, filtering, revolving obtains Herba Lycopi's alkali extract;
Chinese herbal medicine is extracted:By weight, kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall are taken, is shredded, microwave disinfection, powder Broken sieving, is put into immersion in ethanol, and refluxing extraction, concentrated by rotary evaporation obtains concentrate, standby;
Merge:Eupatorine, insecticides adjuvant, nutritional agents are sequentially added in concentrate, is stirred, stood, obtain bactericide;The present invention is logical The effective insecticidal constituent extracted Invasive Alien Species in purple stem is crossed to mix with extracts of Chinese herbal medicine, insecticides adjuvant, nutritional agents again, The excellent bactericide of sterilized, insecticidal effect is obtained, also nutritional ingredient can be provided for grass, it is ensured that the healthy growth of grass.
Preferably, extractant be methyl alcohol, ethanol, ethylene glycol, propyl alcohol, petroleum ether, acetone, one or more of hexamethylene Mixture, Eupatorium adenophorum powder soaking temperature in extractant is 48 ~ 75 DEG C, and soak time is 1 ~ 3h, fully extracts Eupatorium adenophorum In effective insecticidal constituent, precipitated impurities.
Preferably, ultrasonic wave hydrotropy power is 100 ~ 400w, the time is 10 ~ 30min, and purple is fully dissolved beneficial to extractant Effective insecticidal constituent in stem Herba Lycopi, it is 0.7 ~ 0.9 that vacuum is rotated after filtering, and temperature is 45 ~ 55 DEG C, and extractant is removed, Avoid the effect of the bactericide of extractant reduction preparation.
Preferably, taking kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall, shred, microwave disinfection, microwave disinfection temperature It is 70 DEG C ~ 105 DEG C to spend, and the time is 90 ~ 180s, crushes the sieving of 150 mesh, it is to avoid the bacterium, virus in herbal raw material are to preparing The effective influence of bactericide.
Preferably, be put into Chinese herbal medicine after crushing soaking 2 ~ 8h in 85% ethanol, refluxing extraction 2 ~ 8 times is extracted every time 30 ~ 70min, concentrated by rotary evaporation extracts the soluble organic in Chinese herbal medicine, removes useless material, makes the bactericide of preparation Usage amount is few but effect is good.
Compared with prior art, beneficial effects of the present invention are:It is effective in purple stem by extracting to Invasive Alien Species Insecticidal constituent mixes with extracts of Chinese herbal medicine, insecticides adjuvant, nutritional agents again, obtains the excellent bactericide of sterilized, insecticidal effect, profit Preparing bactericide with Invasive Alien Species can slow down the invasion speed of Invasive Alien Species, and the nutritional agents added in bactericide can For lawn provides nutritional ingredient, it is ensured that the healthy growth of grass, bactericide prepared by the present invention can not only kill bacterium on lawn, Virus also has certain insecticidal effect, and instant effect, excellent effect, effective time is long, low toxicity and low residue, to person poultry harmless, can Degraded, grass will not develop immunity to drugs, and can also provide nutriment for lawn, it is ensured that lawn healthy growth.
Specific embodiment
It is described in further detail with reference to embodiments:
Embodiment 1
Lawn-care galenical, bactericide is made up of following component and weight portion:22 ~ 28 parts of kuh-seng, dandelion 25 ~ 45 Part, 60 ~ 70 parts of the root of langdu, 25 ~ 35 parts of Flos Artemisiae finitae, 15 ~ 25 parts of Chinese gall, 1 ~ 3 part of insecticides adjuvant, 0.7 ~ 1.5 part of eupatorine, battalion 0.1 ~ 0.3 part of agent is supported, bactericide of the invention can not only kill bacterium on lawn, virus also has certain insecticidal effect, Instant effect, excellent effect is degradable, can also provide nutriment for lawn, it is ensured that lawn healthy growth.
Insecticides adjuvant includes bleeding agent, preservative and amphoteric surfactant, and bleeding agent is NPE, fat One or more mixture in fat alcohol APEO, polysorbate60, Tween 80, makes bactericide be killed in effectively penetrating into grass Harmful bacteria and virus, preservative are Sodium Benzoate or potassium sorbate, prevent the medicinal herb componentses in bactericide from going bad, and reduce sterilized Effect, amphoteric surfactant is made up of following component and weight portion:3 ~ 5 parts of myristyl dihydroxy ethyl amine oxide, dodecane 3.5 ~ 4.5 parts of base alanine, 5 ~ 15 parts of water, 3.3 ~ 3.8 parts of ethanol, 0.2 ~ 0.3 part of vegetable oil, make the sterilized surface of preparation Power declines, and each composition is uniformly dispersed, and makes the bactericide also effect with easily biological-degradable.
Nutritional agents is made up of following component and weight portion:4 ~ 6 parts of polysaccharide, 0.2 ~ 0.6 part of calcium ammonium nitrate, sodium metasilicate 0.22 ~ 0.48 part, 5 ~ 12 parts of ammonium humate, 2 ~ 4 parts of potassium dihydrogen phosphate, polysaccharide be sucrose, glucose, Agaricus Blazei Murrill polysaccharide, astragalus polyose, One or more in R- polysaccharide, after bactericide can be made to be sprayed on lawn, for lawn provides battalion while bactericide is acted on Support material, it is ensured that lawn healthy growth.
The preparation method of lawn-care galenical, preparation method is comprised the following steps:
1)It is prepared by eupatorine:By weight, fresh Eupatorium adenophorum is taken, is cleaned, dries pulverizing, soaked with extractant, ultrasonic wave Hydrotropy, filtering, revolving obtains Herba Lycopi's alkali extract;
2)Chinese herbal medicine is extracted:By weight, kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall are taken, are shredded, microwave disinfection, Pulverize and sieve, be put into immersion in ethanol, refluxing extraction, concentrated by rotary evaporation obtains concentrate, standby;
3)Merge:Eupatorine, insecticides adjuvant, nutritional agents are sequentially added in concentrate, is stirred, stood, obtain bactericide;The present invention Mixed with extracts of Chinese herbal medicine, insecticides adjuvant, nutritional agents again by extracting the effective insecticidal constituent in purple stem to Invasive Alien Species Close, obtain the excellent bactericide of sterilized, insecticidal effect, can also provide nutritional ingredient for grass, it is ensured that the healthy growth of grass.
Extractant is methyl alcohol, ethanol, ethylene glycol, propyl alcohol, petroleum ether, acetone, one or more mixture of hexamethylene, purple Stem Herba Lycopi's powder soaking temperature in extractant is 48 ~ 75 DEG C, and soak time is 1 ~ 3h, fully effectively killing in extraction Eupatorium adenophorum Worm composition, precipitated impurities.
Ultrasonic wave hydrotropy power is 100 ~ 400w, and the time is 10 ~ 30min, in fully dissolving Eupatorium adenophorum beneficial to extractant Effective insecticidal constituent, after filtering rotate vacuum be 0.7 ~ 0.9, temperature be 45 ~ 55 DEG C, extractant is removed, it is to avoid extract The effect of bactericide prepared by agent reduction.
Take kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall, shred, microwave disinfection, microwave disinfection temperature be 70 DEG C ~ 105 DEG C, the time is 90 ~ 180s, crushes the sieving of 150 mesh, it is to avoid bacterium, virus in herbal raw material have to the bactericide for preparing Influential effect.
2 ~ 8h of immersion in 85% ethanol is put into Chinese herbal medicine after crushing, refluxing extraction 2 ~ 8 times extracts 30 ~ 70min every time, Concentrated by rotary evaporation, the soluble organic in Chinese herbal medicine is extracted, remove useless material, make the bactericide usage amount of preparation few but Effect is good.
Embodiment 2
Lawn-care galenical, bactericide is made up of following component and preferred weight part:27 parts of kuh-seng, 33 parts of dandelion, 64 parts of the root of langdu, 28 parts of Flos Artemisiae finitae, 22 parts of Chinese gall, 2 parts of insecticides adjuvant, 1.2 parts of eupatorine, 0.2 part of nutritional agents.
Insecticides adjuvant includes bleeding agent, preservative and amphoteric surfactant, and bleeding agent is preferably Tween 80, and preservative is excellent Elect Sodium Benzoate as, the composition, or the present invention that certainly above-mentioned preservative and bleeding agent is not limited only to above-mentioned selection are matched somebody with somebody Fang Zhongtong crosses the composition that combination reaches effect same, and amphoteric surfactant is made up of following component and preferred weight part:14 4 parts of alkyl dihydroxy ethyl amine oxide, 4.2 parts of dodecyl alanine, 8 parts of water, 3.5 parts of ethanol, 0.22 part of vegetable oil.
Nutritional agents is made up of following component and preferred weight part:5 parts of polysaccharide, 0.4 part of calcium ammonium nitrate, sodium metasilicate 0.33 Part, 7 parts of ammonium humate, 3.4 parts of potassium dihydrogen phosphate, polysaccharide is preferably sucrose and glucose, and certainly above-mentioned polysaccharide is not limited only to The composition of effect same is reached in sucrose and glucose, or inventive formulation by combination.
The preparation method of lawn-care galenical, preparation method includes following preferred steps:
1)It is prepared by eupatorine:By weight, fresh Eupatorium adenophorum is taken, is cleaned, dries pulverizing, soaked with 90% ethanol, immersion temperature Degree is preferably 49 DEG C, and soak time is preferably 2h, ultrasonic-wave assisted molten during immersion, and ultrasonic wave hydrotropy power is preferably 300w, when Between be preferably 12min, filtering, revolving, revolving vacuum be preferably 0.78, temperature is preferably 50 DEG C, obtains Herba Lycopi's alkali extract;
2)Chinese herbal medicine is extracted:By weight, kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall are taken, are shredded, microwave disinfection, Microwave disinfection temperature is preferably 100 DEG C, and the time is preferably 120s, crushes the sieving of 150 mesh, is put into 85% ethanol and soaks 4h, flows back Extract 5 times, 35min is extracted every time, extract solution is placed in Rotary Evaporators and is concentrated in vacuo, and obtains concentrate, standby;
3)Merge:Eupatorine, insecticides adjuvant, nutritional agents are sequentially added in concentrate, is stirred, stood, obtain bactericide.
Extractant in above-mentioned steps 1 is not limited only to 90% ethanol, can also be methyl alcohol, ethanol, ethylene glycol, propyl alcohol, oil Ether, acetone, one or more mixture of hexamethylene, some routine operations in above-mentioned steps 1 ~ 3 are as crushed, filtering, flow back The technologies such as extraction are existing known technology, in the prior art that those skilled in the art know, therefore do not remake narration in detail herein.
Bactericide prepared by the present invention is tested on lawn:
One piece of football pitch is chosen, football pitch is divided into trisection, blank control group is set respectively(Not spraying fungicide), control group (Sprinkling lawn-care soil bactericide specially PCNB, consumption is 340 grams/ha)And test group(Prepared by the sprinkling present invention kills Microbial inoculum, consumption is 280 grams/ha), spray 1 time, to be checked after 1 month, structure is shown in Table 1.
The result of the test table of table 1
Group Rot number on lawn Lawn rotting rate Turf injures number Sod quality
Blank group 81.0 35.3% 12 4.8
Control group 78.2 34.1% 9 4.7
Test group 3.1 0.3% 5 5.8
As can be seen from Table 1 using sterilized turf quality of the invention substantially due to common lawn bactericide lawn matter Amount.
Embodiment of above is merely to illustrate the present invention, and not limitation of the present invention, the ordinary skill people of this area Member, without departing from the spirit and scope of the present invention, can also make a variety of changes and modification.Therefore, it is all equivalent Technical scheme fall within scope of the invention, scope of patent protection of the invention should be defined by the claims.

Claims (8)

1. lawn-care galenical, it is characterised in that:The bactericide is made up of following component and weight portion:Kuh-seng 22 ~ 28 parts, 25 ~ 45 parts of dandelion, 60 ~ 70 parts of the root of langdu, 25 ~ 35 parts of Flos Artemisiae finitae, 15 ~ 25 parts of Chinese gall, 1 ~ 3 part of insecticides adjuvant, pool 0.7 ~ 1.5 part of blue alkali, 0.1 ~ 0.3 part of nutritional agents.
2. lawn-care galenical according to claim 1, it is characterised in that:The insecticides adjuvant includes infiltration Agent, preservative and amphoteric surfactant, the bleeding agent are NPE, AEO, tween 60th, one or more mixture in Tween 80, the preservative is Sodium Benzoate or potassium sorbate, the amophoteric surface active Agent is made up of following component and weight portion:3 ~ 5 parts of myristyl dihydroxy ethyl amine oxide, dodecyl alanine 3.5 ~ 4.5 Part, 5 ~ 15 parts of water, 3.3 ~ 3.8 parts of ethanol, 0.2 ~ 0.3 part of vegetable oil.
3. lawn-care galenical according to claim 1, it is characterised in that:The nutritional agents by following component and Weight portion is constituted:4 ~ 6 parts of polysaccharide, 0.2 ~ 0.6 part of calcium ammonium nitrate, 0.22 ~ 0.48 part of sodium metasilicate, 5 ~ 12 parts of ammonium humate, phosphorus 2 ~ 4 parts of acid dihydride potassium;The polysaccharide is one or more in sucrose, glucose, Agaricus Blazei Murrill polysaccharide, astragalus polyose, R- polysaccharide.
4. the preparation method of lawn-care galenical, it is characterised in that:The preparation method is comprised the following steps:
1) prepared by eupatorine:By weight, fresh Eupatorium adenophorum is taken, is cleaned, dries pulverizing, soaked with extractant, ultrasonic wave Hydrotropy, filtering, revolving obtains Herba Lycopi's alkali extract;
2)Chinese herbal medicine is extracted:By weight, kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall are taken, are shredded, microwave disinfection, Pulverize and sieve, be put into immersion in ethanol, refluxing extraction, concentrated by rotary evaporation obtains concentrate, standby;
3)Merge:Eupatorine, insecticides adjuvant, nutritional agents are sequentially added in concentrate, is stirred, stood, obtain bactericide.
5. the preparation method of lawn-care galenical according to claim 4, it is characterised in that:In the step 1 Extractant is methyl alcohol, ethanol, ethylene glycol, propyl alcohol, petroleum ether, acetone, one or more mixture of hexamethylene, Eupatorium adenophorum powder Soaking temperature is 48 ~ 75 DEG C in extractant, and soak time is 1 ~ 3h.
6. the preparation method of lawn-care galenical according to claim 4, it is characterised in that:In the step 1 Ultrasonic wave hydrotropy power is 100 ~ 400w, and the time is 10 ~ 30min, and it is 0.7 ~ 0.9 that vacuum is rotated after filtering, and temperature is 45 ~ 55 ℃。
7. the preparation method of lawn-care galenical according to claim 4, it is characterised in that:In the step 2 Kuh-seng, dandelion, the root of langdu, Flos Artemisiae finitae, Chinese gall are taken, is shredded, microwave disinfection, microwave disinfection temperature is 70 DEG C ~ 105 DEG C, when Between be 90 ~ 180s, crush 150 mesh sieving.
8. the preparation method of lawn-care galenical according to claim 4, it is characterised in that:In the step 2 It is put into the Chinese herbal medicine after crushing and 2 ~ 8h is soaked in 85% ethanol, refluxing extraction 2 ~ 8 times is extracted 30 ~ 70min, rotated dense every time Contracting.
CN201710046309.8A 2017-01-22 2017-01-22 Lawn-care galenical and preparation method thereof Pending CN106900754A (en)

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CN107344890A (en) * 2017-07-24 2017-11-14 张剑秋 A kind of special fertilizer and preparation method thereof of enlarging afforested area of garden lawn
CN113163760A (en) * 2018-10-16 2021-07-23 耐遏赛公司 Method for fungal inhibition on living plants using carboxylic acids and salts thereof
CN113994851A (en) * 2021-08-11 2022-02-01 华艺生态园林股份有限公司 Maintenance method for preventing lawn alopecia areata in summer

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Application publication date: 20170630