CN106898505A - A kind of equipment for preparing Graphene electric capacity - Google Patents
A kind of equipment for preparing Graphene electric capacity Download PDFInfo
- Publication number
- CN106898505A CN106898505A CN201710029142.4A CN201710029142A CN106898505A CN 106898505 A CN106898505 A CN 106898505A CN 201710029142 A CN201710029142 A CN 201710029142A CN 106898505 A CN106898505 A CN 106898505A
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- China
- Prior art keywords
- equipment
- electric capacity
- shower nozzle
- frame
- graphene electric
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Classifications
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES OR LIGHT-SENSITIVE DEVICES, OF THE ELECTROLYTIC TYPE
- H01G13/00—Apparatus specially adapted for manufacturing capacitors; Processes specially adapted for manufacturing capacitors not provided for in groups H01G4/00 - H01G11/00
Abstract
A kind of equipment for preparing Graphene electric capacity, it includes organic frame, and workbench is provided with described frame；Drying equipment, addressable displacement mechanism in frame are also included, and graphene oxide solution coating equipment, dielectric diaphragms material application device, positive electrode coating equipment, high-energy ray irradiation apparatus, the cleaning equipment controlled by displacement mechanism.Desired trajectory coating, high-energy ray reduced graphene, the coating of dielectric diaphragms material and solidification, the coating of positive electrode and solidification by successively completing graphene oxide solution on organic film of the invention, so as to complete the manufacture of single Graphene electric capacity, it is capable of achieving single monomer Graphene electric capacity, multiple monomer Graphene electric capacity, or even manufactured while many specification polytypic monomer Graphene electric capacity, it is rational in infrastructure, it is flexibly controllable, it is simple to manufacture quick, low production cost, operating mode is gentle.
Description
【Technical field】
The invention belongs to carbon material technical field, a kind of equipment for preparing Graphene electric capacity is specifically related to.
【Background technology】
Graphene becomes carbon material, nanometer technology, Condensed Matter Physics and function due to its unique structure and photoelectric property
The study hotspot in the fields such as material.Graphene is used as the most strong one kind of the most thin, maximum intensity, electrical and thermal conductivity performance that have now been found that
Novel nano-material, Graphene is referred to as " dark fund ", is " king of new material ", and its theoretical specific surface area is up to 2630m2/g, can
For effect transistor, electrode material, composite, liquid crystal display material, sensor etc..
Graphene refers to mono-layer graphite in the narrow sense, and thickness is 0.335nm, only one layer carbon atom, but within actually 10 layers
Graphite-structure be also referred to as Graphene.And more than 10 layers are then referred to as graphite film.Each carbon atom of Graphene is
Sp2 hydridization, and a remaining hydridization is contributed, and contribute a remaining p orbital electron to form π keys, pi-electron can be moved freely,
Assign Graphene the excellent property led.Because former intermolecular forces are very strong, at normal temperatures, even if surrounding carbon atom collides, stone
The interference that electronics in black alkene is subject to also very little.Scattering, 140 times of electron mobility about in silicon are not susceptible in transmission.
Its electrical conductivity is the optimal material of electric conductivity under normal temperature up to 106s/m, may be used on the manufacture of various electronic components.
Graphene electric capacity, using the characteristic of lithium ion rapid, high volume shuttle between graphenic surface and electrode, opens
A kind of New-energy capacitance for sending, can realize the storage and powerful transmission of Large Copacity.But, existing Graphene electric capacity pair
Preparation condition and environmental requirement are higher, and volume production difficulty is big, high cost.
【The content of the invention】
For above-mentioned technical problem of the prior art, the invention provides a kind of equipment for preparing Graphene electric capacity, its
It is rational in infrastructure, it is flexibly controllable, it is simple to manufacture fast, low production cost, operating mode is gentle.
In order to solve above-mentioned technical problem, the present invention uses following technical proposals：
A kind of equipment for preparing Graphene electric capacity, it includes organic frame, and workbench is provided with described frame；Also wrap
Include graphene oxide solution coating equipment in frame, dielectric diaphragms material application device, positive electrode coating equipment,
High-energy ray irradiation apparatus, cleaning equipment, and drying equipment；Also include the addressable displacement mechanism in frame, institute
Graphene oxide solution coating equipment, dielectric diaphragms material application device, positive electrode coating equipment, the high-energy ray irradiation stated
Any position that equipment, cleaning equipment are connected with displacement mechanism and can be moved under displacement mechanism control above workbench
Put；Described drying equipment can be on heat radiation to workbench.
In further improvement project, described displacement mechanism includes control device, and is connected with control device
By the mobile movable stand of control device control；Described movable stand is included can be along one end of workbench in frame
The lengthwise movement frame moved back and forth in stroke and the other end between, and motion can be transversely to the machine direction on lengthwise movement frame
The reciprocating flattened pallet of the conduct route of frame.
In further improvement project, described graphene oxide solution coating equipment is included for storing oxidation stone
First container and graphene oxide solution shower nozzle of black alkene solution, between the first described container and graphene oxide solution shower nozzle
Connected by pipeline, described graphene oxide solution shower nozzle is on flattened pallet.
In further improvement project, described dielectric diaphragms material application device is included for storing dielectric diaphragms
The second container and dielectric diaphragms material shower nozzle of material, pass through pipeline between described second container and dielectric diaphragms material shower nozzle
Connection, described dielectric diaphragms material shower nozzle is on flattened pallet.
In further improvement project, described positive electrode coating equipment include for store positive electrode
Three containers and positive electrode shower nozzle, are connected, described positive pole between the 3rd described container and positive electrode shower nozzle by pipeline
Material shower nozzle is on flattened pallet.
In further improvement project, described drying equipment includes drying machine and the dry wind being connected with drying machine
Mouth shower nozzle, the described air port shower nozzle that dries is located on flattened pallet.
In further improvement project, described high-energy ray irradiation apparatus is high-energy ray transmitter, and it is located at flat
Stretch on pallet.
In further improvement project, described cleaning equipment include for the 4th container that stores cleaning solvent and
Cleaning sprayer, is connected between the 4th described container and cleaning sprayer by pipeline, and described cleaning sprayer is located at flattened pallet
On.
In further improvement project, film device is also included, described upper film device is included located at frame one
The bin for placing electrode base-material volume of side, and located at the lay-on roll at the top of workbench.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention on organic film by successively completing oxidation
The desired trajectory coating of graphene solution, high-energy ray reduced graphene, the coating of dielectric diaphragms material and solidification, positive electrode
Coating and solidification, so as to complete the manufacture of single Graphene electric capacity, be capable of achieving single monomer Graphene electric capacity, multiple monomer stones
Black alkene electric capacity, or even manufactured while many specification polytypic monomer Graphene electric capacity, it is rational in infrastructure, it is flexibly controllable, it is simple to manufacture
Fast, low production cost, is manufactured by the way of solvent solution, and its operating mode is gentle pollution-free.
The present invention is described in further detail with specific embodiment below in conjunction with the accompanying drawings：
【Brief description of the drawings】
Fig. 1 is the schematic perspective view of the embodiment of the present invention；
Fig. 2 is the schematic perspective view of displacement mechanism in the embodiment of the present invention；
Fig. 3 is graphene oxide solution shower nozzle, dielectric diaphragms material shower nozzle, positive electrode shower nozzle, high energy in the embodiment of the present invention
The schematic perspective view of ray emitter, cleaning sprayer.
【Specific embodiment】
A kind of equipment for preparing Graphene electric capacity, as shown in Figure 1, 2, 3, it includes organic frame 10, in described frame 10
It is provided with workbench 20；The graphene oxide solution coating equipment in frame 10, dielectric diaphragms material is also included to apply
Coating equipment, positive electrode coating equipment, high-energy ray irradiation apparatus, cleaning equipment, and drying equipment；Also include located at machine
Addressable displacement mechanism on frame 10, described graphene oxide solution coating equipment, dielectric diaphragms material application device, positive pole
Material application device, high-energy ray irradiation apparatus, cleaning equipment are connected with displacement mechanism and can be moved down in displacement mechanism control
Move the optional position to above workbench；Described drying equipment can be on heat radiation to workbench；Film is also included to set
Standby, described upper film device is included rolls up 50 bin 30 located at the side of frame 10 for placing electrode base-material, and is located at
The lay-on roll 40 at the top of workbench 20.
In specific works, electrode base-material uses organic film 80, and one organic film 80 first is placed in into work as matrix
On platform 20, in the present embodiment, it is rolled into the organic film of tubular volume 50 and is laid on workbench 20 by the feeding of lay-on roll 40；
Then displacement mechanism controls graphene oxide solution coating equipment in coating work is carried out on organic film 80, by graphene oxide
Solution is coated on organic film 80；After coating is completed, the graphene oxide solution on the surface of organic film 80 is subject to drying to set
Graphene oxide layer is dried to after standby heat radiation；Then, oxygen of the displacement mechanism control irradiation apparatus to the surface of organic film 80
Graphite alkene layer is irradiated according to default route to graphene oxide layer, and the graphene oxide in certain track is reduced into
Graphene, shaping is portrayed this completes the graphene layer to negative electrode and lug, form Graphene state negative electrode layer and
Lug layer, because the track form of negative electrode and lug can preset, therefore, it can complete different on organic film 80
The shaping of model electric capacity is portrayed, while the shaping that multiple monomer electric capacity can also be completed on organic film 80 is portrayed；In negative pole
After layer and lug layer portray shaping, displacement mechanism control cleaning equipment washes graphene oxide unnecessary on organic film 80
Layer；Afterwards, displacement mechanism control dielectric diaphragms material application device carries out the painting of dielectric diaphragms material to the surface of organic film 80
Cover, graphene layer surface and non-graphite alkene layer surface are coated with dielectric diaphragms material so on organic film 80；Then again
The surface of organic film 80 is irradiated by displacement mechanism control high-energy ray irradiation apparatus, the track of irradiation is along negative electrode and pole
The course bearing of ear, so Graphene state negative electrode layer and lug layer on dielectric diaphragms material irradiated by high-energy ray after quilt
It is fixed up, forms dielectric layer；Then the surface of organic film 80 is cleaned by displacement mechanism control cleaning equipment again, by liquid
State, uncured dielectric diaphragms material clean is complete；Then, positive electrode coating equipment is controlled along default by displacement mechanism
The course bearing of negative electrode and lug is coated, and positive electrode is coated in into dielectric layer, then is controlled by displacement mechanism high
Energy radiation exposure equipment is irradiated to positive electrode, and positive electrode is solidified on dielectric layer, forms anode layer, by this,
One monomer Graphene electric capacity has just manufactured completion.
The present invention controls graphene oxide solution coating equipment, dielectric diaphragms material by the travel mechanism that can arbitrarily address
Coating equipment, positive electrode coating equipment, high-energy ray irradiation apparatus, cleaning equipment successively complete oxidation on organic film 80
The desired trajectory coating of graphene solution, high-energy ray reduced graphene, the coating of dielectric diaphragms material and solidification, positive electrode
Coating and solidification, so as to complete the manufacture of Graphene electric capacity, be capable of achieving single monomer Graphene electric capacity, multiple monomer Graphenes
Electric capacity, or even manufactured while many specification polytypic monomer Graphene electric capacity, it is rational in infrastructure, it is flexibly controllable, it is simple to manufacture fast,
Low production cost, is manufactured by the way of solvent solution, and its operating mode is gentle pollution-free.
In an embodiment of the present invention, as shown in Figure 1, Figure 2, Figure 3 shows, described displacement mechanism includes control device, with
And be connected with control device by the mobile movable stand of control device control；Described movable stand is included in frame 10
Can be along the lengthwise movement frame 60 moved back and forth in the stroke between one end of workbench 20 and the other end, and located at longitudinal fortune
The reciprocating flattened pallet 70 of the conduct route of movement frame 60 can be transversely to the machine direction in moving frame 60, the present invention is transported by longitudinal direction
The motion of moving frame 60 and flattened pallet 70 coordinates X, Y the addressable displacement for realizing movable stand.Described graphene oxide solution
Coating equipment includes the first container and graphene oxide solution shower nozzle 71 for storing graphene oxide solution, described
Connected by pipeline between one container and graphene oxide solution shower nozzle 71, described graphene oxide solution shower nozzle 71 is located at flat
Stretch on pallet 70.Described dielectric diaphragms material application device includes second container and Jie for storing dielectric diaphragms material
Electric separator material shower nozzle 72, is connected, described Jie between described second container and dielectric diaphragms material shower nozzle 72 by pipeline
Electric separator material shower nozzle 72 is on flattened pallet 70.Described positive electrode coating equipment is included for storing positive electrode
The 3rd container and positive electrode shower nozzle 73, between the 3rd described container and positive electrode shower nozzle 73 by pipeline connect, institute
The positive electrode shower nozzle 73 stated is on flattened pallet 70, here, positive electrode is LiFePO4.Described drying equipment includes
Have drying machine and be connected with drying machine dry air port shower nozzle 74, it is described to dry air port shower nozzle 74 on flattened pallet 70.
Described high-energy ray irradiation apparatus is generating laser 75, and it is located on flattened pallet 70, additionally, high-energy ray irradiation apparatus
But also X-ray emitter or particle beams transmitter.Described cleaning equipment includes the 4th appearance for storing cleaning solvent
Device and cleaning sprayer 76, are connected between the 4th described container and cleaning sprayer 76 by pipeline, and described cleaning sprayer 76 sets
In on flattened pallet 70, in the present embodiment, cleaning solvent can be polar solvent or organic solvent.
It is aobvious for those skilled in the art by the disclosure although the present invention is described in detail with reference to above example
And be clear to, and in the case of the principle of the invention and scope for not departing from described claim restriction, can be right
The present invention makes a variety of changes or changes.Therefore, the detailed description of the embodiment of the present disclosure is only used for explaining, rather than for limiting
The present invention, but it is defined by the subject-matter of the claims the scope of protection.
Claims (9)
1. a kind of equipment for preparing Graphene electric capacity, it is characterised in that it includes organic frame, is provided with described frame
Workbench；Also include graphene oxide solution coating equipment, dielectric diaphragms material application device, positive pole in frame
Material application device, high-energy ray irradiation apparatus, cleaning equipment, and drying equipment；Also include seeking in frame
Location displacement mechanism, described graphene oxide solution coating equipment, dielectric diaphragms material application device, positive electrode are applied and covered
Standby, high-energy ray irradiation apparatus, cleaning equipment are connected with displacement mechanism and work can be moved under displacement mechanism control and put down
Optional position above platform；Described drying equipment can be on heat radiation to workbench.
2. a kind of equipment for preparing Graphene electric capacity according to claim 1, it is characterised in that described displacement machine
Structure includes control device, and is connected with control device by the mobile movable stand of control device control；Described mobile station
Frame include in frame can along the lengthwise movement frame moved back and forth in the stroke between one end of workbench and the other end,
And the reciprocating flattened pallet of conduct route of movement frame can be transversely to the machine direction on lengthwise movement frame.
3. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that described oxidation stone
Black alkene solution coating equipment includes the first container and graphene oxide solution shower nozzle for storing graphene oxide solution, institute
Connected by pipeline between the first container and graphene oxide solution shower nozzle stated, described graphene oxide solution shower nozzle is located at
On flattened pallet.
4. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that described dielectric every
Membrane material coating equipment includes the second container and dielectric diaphragms material shower nozzle for storing dielectric diaphragms material, described
Connected by pipeline between two containers and dielectric diaphragms material shower nozzle, described dielectric diaphragms material shower nozzle is located at flattened pallet
On.
5. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that described positive pole material
Material coating equipment includes the 3rd container and positive electrode shower nozzle for storing positive electrode, the 3rd described container and positive pole
Connected by pipeline between material shower nozzle, described positive electrode shower nozzle is on flattened pallet.
6. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that described drying sets
It is standby include drying machine and be connected with drying machine dry air port shower nozzle, the described air port shower nozzle that dries is located on flattened pallet.
7. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that described high energy is penetrated
Line irradiation apparatus is generating laser, and it is located on flattened pallet.
8. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that described cleaning sets
Standby the 4th container and cleaning sprayer included for storing cleaning solvent, passes through between the 4th described container and cleaning sprayer
Pipeline is connected, and described cleaning sprayer is on flattened pallet.
9. a kind of equipment for preparing Graphene electric capacity according to claim 2, it is characterised in that also include film
Equipment, described upper film device includes the bin for placing electrode base-material volume located at frame side, and located at work
The lay-on roll at the top of platform.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710029142.4A CN106898505A (en) | 2017-01-16 | 2017-01-16 | A kind of equipment for preparing Graphene electric capacity |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710029142.4A CN106898505A (en) | 2017-01-16 | 2017-01-16 | A kind of equipment for preparing Graphene electric capacity |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106898505A true CN106898505A (en) | 2017-06-27 |
Family
ID=59199116
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710029142.4A Pending CN106898505A (en) | 2017-01-16 | 2017-01-16 | A kind of equipment for preparing Graphene electric capacity |
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| Country | Link |
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| CN (1) | CN106898505A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108270038A (en) * | 2018-01-30 | 2018-07-10 | 黑龙江聚拢华玺智能科技有限公司 | A kind of production system of graphene battery |
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| CN102646795A (en) * | 2012-04-21 | 2012-08-22 | 吉林大学 | Organic electroluminescence device for reducing patterning graphene electrodes based on laser and manufacturing method therefor |
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| CN105271209A (en) * | 2015-11-05 | 2016-01-27 | 北京旭碳新材料科技有限公司 | Graphene film and method and device for continuously producing graphene film |
| CN105895853A (en) * | 2016-04-20 | 2016-08-24 | 清华大学深圳研究生院 | Power storage device and preparation method thereof |
| CN205709875U (en) * | 2016-04-11 | 2016-11-23 | 南京纳清建筑科技有限公司 | The device of graphene-based film is prepared in a kind of scale |
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- 2017-01-16 CN CN201710029142.4A patent/CN106898505A/en active Pending
Patent Citations (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2120634U (en) * | 1992-04-13 | 1992-11-04 | 天津市自动化仪表成套设计所 | Multi spray nozzle self-convert film flame plating machine |
| CN1387277A (en) * | 2001-05-23 | 2002-12-25 | 可卡姆工程有限公司 | Automatic production system of secondary lithium cell |
| CN102553753A (en) * | 2011-12-31 | 2012-07-11 | 暨南大学 | Thin film spray coating machine and thin film preparation method |
| CN102646795A (en) * | 2012-04-21 | 2012-08-22 | 吉林大学 | Organic electroluminescence device for reducing patterning graphene electrodes based on laser and manufacturing method therefor |
| CN103508447A (en) * | 2012-06-26 | 2014-01-15 | 海洋王照明科技股份有限公司 | Preparation method of graphene |
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| CN105271209A (en) * | 2015-11-05 | 2016-01-27 | 北京旭碳新材料科技有限公司 | Graphene film and method and device for continuously producing graphene film |
| CN205709875U (en) * | 2016-04-11 | 2016-11-23 | 南京纳清建筑科技有限公司 | The device of graphene-based film is prepared in a kind of scale |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108270038A (en) * | 2018-01-30 | 2018-07-10 | 黑龙江聚拢华玺智能科技有限公司 | A kind of production system of graphene battery |
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Application publication date: 20170627 |