CN106865544A - A kind of repeatable medical activated carbon for utilizing and its production method - Google Patents
A kind of repeatable medical activated carbon for utilizing and its production method Download PDFInfo
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- CN106865544A CN106865544A CN201710186737.0A CN201710186737A CN106865544A CN 106865544 A CN106865544 A CN 106865544A CN 201710186737 A CN201710186737 A CN 201710186737A CN 106865544 A CN106865544 A CN 106865544A
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- eucommia
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Abstract
The invention discloses a kind of repeatable medical activated carbon for utilizing and its generation method, including shell, the bark of eucommia, corn ear and grape pip are used as raw material, and are matched according to following number：15 parts of 16 parts of shell, 30 50 parts of the bark of eucommia, 35 40 parts of corn ear and grape pip, are then customized medical active carbon powder, and the active carbon powder is filled into capsule for medicine according to corresponding method.A kind of repeatable medical activated carbon for utilizing that the present invention is obtained, there is perfect removing toxic substances in medical use, simultaneously because inside with the addition of the bark of eucommia, the small part for making it also remain with the bark of eucommia is medicinal and health-care components, and the anti-oxidation function in a small number of grape pips, compared with the activated carbon that existing wood materials are made, the porosity is higher, the more preferable function of effect of ejecting poison, so that it can also carry out reusable function using the later stage by reclaiming.
Description
Technical field
The present invention relates to the activated carbon in a kind of medical medicine field, especially a kind of repeatable medical activated carbon for utilizing and
Its production method.
Background technology
Medicinal carbon is a kind of dedicated for pharmacy, used as medical accessory, the sp act charcoal of the medical domain such as removing toxic substances.
It is mainly used in impurity and small molecule heavy metal in the decolouring and adsorbent solution of solution in pharmacy procedure, is the most frequently used depyrogenation
Means.This activated carbon is generally applied to medicinal applications, so being referred to as " medicinal carbon " by people.The characteristics of it is maximum
It is exactly decolorization rate fast, high adsorption capacity, endoporus gap structure is flourishing, the features such as hole is thick, in can effectively adsorbing liquid medicine
Pigment, just and reduce liquid medicine impurity, without influence liquid medicine other constituent concentrations and the property of medicine.Medicinal carbon is with high-quality
Timber is raw material, and profile is powdered, is refined through high temperature carbonization, activation and working procedures and forms wood activated charcoal, with than table
Area is big, and activity is high, and micropore is flourishing, and decolorizing ability is strong, and the features such as pore structure is larger, pore structure is big, can have compared with adsorptive liquid
In larger various materials, the impurity such as color.
But currently used for medicinal carbon service efficiency it is poor, and due to medical active carbon surface be easy to oxidation, lead
Cause shelf-life short life, it is therefore desirable to improve.
The content of the invention
There is provided the invention aims to solve above-mentioned the deficiencies in the prior art it is a kind of repeatable utilize it is medical
Activated carbon and its production method.
To achieve these goals, a kind of repeatable medical activated carbon for utilizing designed by the present invention, including shell, Du
Secondary, corn ear and grape pip are matched as raw material according to following number：Shell 1-6 parts, bark of eucommia 30-50 parts, corn
Rod 35-40 parts and grape pip 1-5 parts, then it is customized medical active carbon powder according to corresponding method, and by the activity
Carbon powder is filled into capsule for medicine.
Preferably, the shell is coconut husk.
Preferably, the raw material also includes redwood, the number of the redwood is 3-5 parts.
The invention also discloses a kind of production method of the repeatable medical activated carbon for utilizing, mainly include the following steps that：
1) choose fresh bark of eucommia greenery piece to be cleaned up with clear water, it is added by the way of mechanical expression then
Work, squeezing material cake and juice that collection is obtained are stand-by；
2) choose the bark of eucommia limb after peeling, be crushed to 25-28 mesh after cleaning, and be dipped into mass concentration for 30-32%,
Temperature is 4h in 35 degrees Celsius of sodium hydroxide solution, and immersion finishes backward its and applies ultrasonic wave, and the applying mode of ultrasonic wave is：
The ultrasonic wave 1min that first applies frequency 350-370KHz to it simultaneously stops 0.5min, then apply the ultrasound that frequency is 100-120KHz
Ripple 1min simultaneously stops 0.5min, the applying process of circulation above-mentioned ultrasonic wave 2-3 times, is filtrated to get the first reactive powder powder, treats
With；
3) by step 1) in squeezing material cake, step 2) in solid powder and clean up the bark of eucommia fallen leaves with step 1)
In the juice that obtains be 8-10 according to weight ratio:Temperature is deposited in after 1 ratio mix for 45 degrees Celsius, relative humidity are 95%
Greenhouse in 50h, it is stand-by；
4) by step 3) through stacking treatment mixture according to weight ratio be 1:The ratio of 2-1.4 is added to mass concentration
To be impregnated in 45% phosphoric acid solution, dipping temperature is 65-70 degrees Celsius, and dip time is 1-2h, stand-by；
5) will impregnate during the mixture for finishing sends into activation furnace and be activated, during activation, first be warming up to 200-220 Celsius
Degree, and temperature 2-3h is kept, then it is further continued for being warming up to 500-520 degrees Celsius, and temperature 1-2h is kept, washed after cooling
To neutrality, crushed after being dried is stand-by to 300 mesh；
6) by the corn ear after threshing, shell, be put into retort and completely cut off air and heated, temperature control at 250 DEG C,
After heating 3.5 hours, power off and cooled down, obtain primary carbide；Then primary carbide is placed in retort
650 DEG C are warmed up to, after carrying out naked light burning 35~50 minutes, turning off naked light carries out natural cooling, obtain carbonizing block；Grind：Will
The charing block pulverization for obtaining, sieving, obtains powdered carbon powder；Activation process is carried out again, obtains activation charcoal end, and be dried
Treatment, obtains final product the second active carbon powder, stand-by；
7) grape pip powder is broken to 40~60 mesh, obtains grape pip powder；
8) isolation air is heated in being put into retort, and temperature control after heating 3.5 hours, is powered off at 250 DEG C
Cooled down, obtained primary carbide；Then primary carbide is placed on and 650 DEG C is warmed up in retort, carry out naked light combustion
After burning 35~50 minutes, turning off naked light carries out natural cooling, obtains carbonizing block；Grind：The charing block pulverization that will be obtained, mistake
Sieve, obtains powdered carbon powder；Activation process is carried out again, activation charcoal end is obtained, and carries out dried process, obtain final product the 3rd activated carbon powder
End, it is stand-by；
9) finally above-mentioned first active carbon powder, the second active carbon powder and the 3rd active carbon powder are entered by mixer
Row stirs, and is then packaged into capsule by packing machine.
A kind of repeatable medical activated carbon for utilizing and its production method that the present invention is obtained, have in medical use
Perfect removing toxic substances, simultaneously because inside with the addition of the bark of eucommia, the small part for making it also remain with the bark of eucommia is medicinal and health-care components, and
Anti-oxidation function in a small number of grape pips, compared with the activated carbon that existing wood materials are made, the porosity is higher, and effect of ejecting poison is more
Good function, so that it can also carry out reusable function using the later stage by reclaiming.
Specific embodiment
With reference to embodiment, the present invention is further described.
Embodiment 1：
A kind of repeatable medical activated carbon for utilizing that the present embodiment is provided, including shell, the bark of eucommia, corn ear and grape
Seed is matched as raw material according to following number：Shell 1-6 parts, bark of eucommia 30-50 parts, corn ear 35-40 parts and grape
Seed 1-5 parts, medical active carbon powder then is customized according to corresponding method, and the active carbon powder is filled into glue,medicinal
It is intracapsular.3 parts of described in the present embodiment 3 parts of shell, bark of eucommia 30- parts, 35 parts of corn ear and grape pip.
Preferably, the shell is coconut husk.
Preferably, the raw material also includes redwood, the number of the redwood is 3-5 parts.It is described in the present embodiment
Redwood is 3 parts.
The invention also discloses a kind of production method of the repeatable medical activated carbon for utilizing, mainly include the following steps that：
1) choose fresh bark of eucommia greenery piece to be cleaned up with clear water, it is added by the way of mechanical expression then
Work, squeezing material cake and juice that collection is obtained are stand-by；
2) choose the bark of eucommia limb after peeling, be crushed to 25-28 mesh after cleaning, and be dipped into mass concentration for 30-32%,
Temperature is 4h in 35 degrees Celsius of sodium hydroxide solution, and immersion finishes backward its and applies ultrasonic wave, and the applying mode of ultrasonic wave is：
The ultrasonic wave 1min that first applies frequency 350-370KHz to it simultaneously stops 0.5min, then apply the ultrasound that frequency is 100-120KHz
Ripple 1min simultaneously stops 0.5min, the applying process of circulation above-mentioned ultrasonic wave 2-3 times, is filtrated to get the first reactive powder powder, treats
With；
3) by step 1) in squeezing material cake, step 2) in solid powder and clean up the bark of eucommia fallen leaves with step 1)
In the juice that obtains be 8-10 according to weight ratio:Temperature is deposited in after 1 ratio mix for 45 degrees Celsius, relative humidity are 95%
Greenhouse in 50h, it is stand-by；
4) by step 3) through stacking treatment mixture according to weight ratio be 1:The ratio of 2-1.4 is added to mass concentration
To be impregnated in 45% phosphoric acid solution, dipping temperature is 65-70 degrees Celsius, and dip time is 1-2h, stand-by；
5) will impregnate during the mixture for finishing sends into activation furnace and be activated, during activation, first be warming up to 200-220 Celsius
Degree, and temperature 2-3h is kept, then it is further continued for being warming up to 500-520 degrees Celsius, and temperature 1-2h is kept, washed after cooling
To neutrality, crushed after being dried is stand-by to 300 mesh；
6) by the corn ear after threshing, shell, be put into retort and completely cut off air and heated, temperature control at 250 DEG C,
After heating 3.5 hours, power off and cooled down, obtain primary carbide；Then primary carbide is placed in retort
650 DEG C are warmed up to, after carrying out naked light burning 35~50 minutes, turning off naked light carries out natural cooling, obtain carbonizing block；Grind：Will
The charing block pulverization for obtaining, sieving, obtains powdered carbon powder；Activation process is carried out again, obtains activation charcoal end, and be dried
Treatment, obtains final product the second active carbon powder, stand-by；
7) grape pip powder is broken to 40~60 mesh, obtains grape pip powder；
8) isolation air is heated in being put into retort, and temperature control after heating 3.5 hours, is powered off at 250 DEG C
Cooled down, obtained primary carbide；Then primary carbide is placed on and 650 DEG C is warmed up in retort, carry out naked light combustion
After burning 35~50 minutes, turning off naked light carries out natural cooling, obtains carbonizing block；Grind：The charing block pulverization that will be obtained, mistake
Sieve, obtains powdered carbon powder；Activation process is carried out again, activation charcoal end is obtained, and carries out dried process, obtain final product the 3rd activated carbon powder
End, it is stand-by；
9) finally above-mentioned first active carbon powder, the second active carbon powder and the 3rd active carbon powder are entered by mixer
Row stirs, and is then packaged into capsule by packing machine.
Embodiment 2：
A kind of repeatable medical activated carbon for utilizing that the present embodiment is provided, described 5 parts of shell, 50 parts of the bark of eucommia, corn
4 parts of 40 parts of rod and grape pip, are then fabricated to product according to method in embodiment 1.
After tested, a kind of repeatable medical activated carbon for utilizing that the present embodiment is obtained, antioxidant effect is good, makes its later stage
It is higher by recycling rate of waterused after recycling.
Embodiment 3：
A kind of repeatable medical activated carbon for utilizing that the present embodiment is provided, described 2 parts of shell, 45 parts of the bark of eucommia, corn
2 parts of 35 parts of rod and grape pip, are then fabricated to product according to method in embodiment 1.
After tested, a kind of repeatable medical activated carbon for utilizing that the present embodiment is obtained, antioxidant effect is good, makes its later stage
It is higher by recycling rate of waterused after recycling.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding can carry out various changes, modification, replacement to these embodiments without departing from the principles and spirit of the present invention
And modification, the scope of the present invention be defined by the appended.
Claims (4)
1. a kind of repeatable medical activated carbon for utilizing, it is characterized in that：Including shell, the bark of eucommia, corn ear and grape pip conduct
Raw material, and matched according to following number：Shell 1-6 parts, bark of eucommia 30-50 parts, corn ear 35-40 parts and grape pip 1-5
Part, medical active carbon powder then is customized according to corresponding method, and the active carbon powder is filled into capsule for medicine.
2. according to a kind of repeatable medical activated carbon for utilizing according to claim 1, it is characterized in that：The shell is coconut palm
Shell.
3. according to a kind of repeatable medical activated carbon for utilizing according to claim 1 and 2, it is characterized in that：The raw material
Also include redwood, the number of the redwood is 3-5 parts.
4. a kind of production method of the repeatable medical activated carbon for utilizing, including using any shown in claims 1 to 3
The repeatable medical activated carbon for utilizing, it is characterized in that：Specifically use following steps：
1) choose fresh bark of eucommia greenery piece to be cleaned up with clear water, it be processed by the way of mechanical expression then,
Squeezing material cake and juice that collection is obtained, it is stand-by；
2) bark of eucommia limb after peeling is chosen, 25-28 mesh is crushed to after cleaning, and be dipped into mass concentration for 30-32%, temperature
It is 4h in 35 degrees Celsius of sodium hydroxide solutions, immersion finishes backward its and applies ultrasonic wave, and the applying mode of ultrasonic wave is：First to
Its ultrasonic wave 1min for applying frequency 350-370KHz simultaneously stops 0.5min, then applies the ultrasonic wave that frequency is 100-120KHz
1min simultaneously stops 0.5min, the applying process of circulation above-mentioned ultrasonic wave 2-3 times, is filtrated to get the first reactive powder powder, stand-by；
3) by step 1) in squeezing material cake, step 2) in solid powder and clean up the bark of eucommia fallen leaves with step 1) in
The juice for arriving is 8-10 according to weight ratio:The temperature that temperature is 45 degrees Celsius, relative humidity is 95% is deposited in after 1 ratio mix
Indoor 50h, it is stand-by；
4) by step 3) through stacking treatment mixture according to weight ratio be 1:The ratio of 2-1.4 is added to mass concentration
Impregnated in 45% phosphoric acid solution, dipping temperature is 65-70 degrees Celsius, and dip time is 1-2h, stand-by；
5) will impregnate activated in the mixture feeding activation furnace for finishing, and during activation, first be warming up to 200-220 degrees Celsius, and
Temperature 2-3h is kept, is then further continued for being warming up to 500-520 degrees Celsius, and keep temperature 1-2h, in being washed to after cooling
Property, crushed after being dried to 300 mesh is stand-by；
6) by the corn ear after threshing, shell, isolation air is heated in being put into retort, and temperature control is heated at 250 DEG C
After 3.5 hours, power off and cooled down, obtain primary carbide；Then primary carbide is placed in retort and is heated up
To 650 DEG C, after carrying out naked light burning 35~50 minutes, turning off naked light carries out natural cooling, obtains carbonizing block；Grind：To obtain
Charing block pulverization, sieving, obtain powdered carbon powder；Activation process is carried out again, obtains activation charcoal end, and be dried place
Reason, obtains final product the second active carbon powder, stand-by；
7) grape pip powder is broken to 40~60 mesh, obtains grape pip powder；
8) isolation air is heated in being put into retort, and at 250 DEG C, after heating 3.5 hours, power off is carried out temperature control
Cooling, obtains primary carbide；Then primary carbide is placed on and 650 DEG C is warmed up in retort, carry out naked light burning 35
After~50 minutes, turning off naked light carries out natural cooling, obtains carbonizing block；Grind：The charing block pulverization that will be obtained, sieving,
Obtain powdered carbon powder；Activation process is carried out again, activation charcoal end is obtained, and carries out dried process, obtain final product the 3rd active carbon powder, treat
With；
9) finally above-mentioned first active carbon powder, the second active carbon powder and the 3rd active carbon powder are stirred by mixer
Mix uniform, be then packaged into capsule by packing machine.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107827105A (en) * | 2017-12-05 | 2018-03-23 | 程庸堂 | A kind of activated carbon for treating hyperlipemia |
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|---|---|---|---|---|
| CN101643208A (en) * | 2009-01-16 | 2010-02-10 | 徐克文 | Composite biological activated carbon and rapid preparation method thereof |
| CN101913603A (en) * | 2010-08-16 | 2010-12-15 | 西北农林科技大学 | Method for preparing activated carbon from peeled branch wood of initiated branches in eucommia bark leaf forest |
| CN103043661A (en) * | 2012-12-12 | 2013-04-17 | 承德鑫永晟炭业有限公司 | Method for preparing active carbon for relieving or neutralizing effect of alcohol |
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Application publication date: 20170620 |