CN106852328A - A kind of Pesticidal combination of the nitrile of worm containing acetyl and multiple killing teichomycin - Google Patents

A kind of Pesticidal combination of the nitrile of worm containing acetyl and multiple killing teichomycin Download PDF

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Publication number
CN106852328A
CN106852328A CN201510902391.0A CN201510902391A CN106852328A CN 106852328 A CN106852328 A CN 106852328A CN 201510902391 A CN201510902391 A CN 201510902391A CN 106852328 A CN106852328 A CN 106852328A
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multiple killing
killing teichomycin
nitrile
acetyl
worm
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张伟
高云
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Shaanxi Welch Crop Protection Co Ltd
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Shaanxi Welch Crop Protection Co Ltd
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/561,2-Diazoles; Hydrogenated 1,2-diazoles
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/22Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom rings with more than six members

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  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of nitrile of worm containing acetyl and the Pesticidal combination of multiple killing teichomycin, effective active composition is acetyl worm nitrile and multiple killing teichomycin, and the weight ratio of acetyl worm nitrile and multiple killing teichomycin is the ︰ 1 of 1 ︰ 80~80.The present composition has synergistic effect to the various pests for endangering agricultural production, reduces pesticide usage amount, reduces residual quantity of the agricultural chemicals on crop, alleviates environmental pollution, and to person poultry safety, Environmental compatibility is good, and insect is not likely to produce the resistance to the action of a drug.

Description

A kind of Pesticidal combination of the nitrile of worm containing acetyl and multiple killing teichomycin
Technical field
The invention belongs to technical field of pesticide, it is related to the Pesticidal combination of a kind of nitrile of worm containing acetyl and multiple killing teichomycin in farming Application on thing insect.
Background technology
Acetyl worm nitrile:Molecular formula:C13H10Cl2F3N3O2S, acetyl worm nitrile is a broad spectrum pesticide, and its insecticidal mechanism is Hinder the chloride metabolism of insect GABA (GABA) control.
Multiple killing teichomycin:Have to insect and quickly tag and stomach poison function, there is stronger osmosis to blade, can kill Subepidermal insect, the longevity of residure is more long, has certain ovicidal action to some insects, without systemic action.
But in the real process of agricultural production, pest control is easiest to generate the problem that the product of pest resistance to insecticide It is raw.Different cultivars composition is compounded, and is to prevent and treat the very common method of resistant insect.Heterogeneity is compounded, according to reality Application effect come judge certain compounding be synergy, plus and or antagonism.In most cases, the compounding effect of agricultural chemicals All it is additive effect, really has the compounding of synergistic effect seldom, especially synergistic effect is clearly, co-toxicity coefficient is very high answers With just less.Studied by inventor, find not yet to disclose the relevant report that acetyl worm nitrile and multiple killing teichomycin are compounded.
The content of the invention
The purpose of the present invention is to propose to a kind of with synergistic function, the nitrile of worm containing acetyl that use cost is low, preventive effect is good With the Pesticidal combination of multiple killing teichomycin.
The Pesticidal combination of the nitrile of worm containing acetyl proposed by the present invention and multiple killing teichomycin, acetyl worm nitrile and multiple killing teichomycin weight ratio For the ︰ 1 of 1 ︰ 80~80, acetyl worm nitrile and the preferred weight ratio of multiple killing teichomycin are the ︰ 1 of 1 ︰ 40~40;More preferably acetyl worm nitrile and many The weight ratio of killing teichomycin is 20:1~1:20.The Pesticidal combination of the nitrile of worm containing acetyl proposed by the present invention and multiple killing teichomycin is used to prevent Control the purposes of insect on crops, described crops include cereal crops, legume crop, fibre crops, sugar crop, melon Crop, fruits crop, dry fruit crop, hobby crop, root crop, oil crops, flower crop, medicinal crop, original Material crop, green manure pasture crop;Described insect is beetle, leafhopper, aphid, aleyrodid, beet armyworm, diamondback moth, cnaphalocrocis Snout moth's larva, striped rice borer, yellow rice borer, bollworm or thrips.
The weight ratio of acetyl worm nitrile and multiple killing teichomycin is the ︰ 1 of 1 ︰ 80~80.The weight percent of active component in usual composition Content is the 0.5%~90% of gross weight, preferably 5%~80%.According to different preparation types, active component content model Enclose different.Generally, liquid preparation contains by weight 1%~70% active material, preferably 5%~50%;Gu Body preparation contains by weight 5%~80% active material, preferably 10%~80%.
At least contain a kind of surfactant in Pesticidal combination of the invention, active component is in water when being beneficial to administration Dispersion.Surface-active contents are the 5%~30% of total formulation weight, balance of solid or liquid diluent.
Pesticidal combination of the invention can by user using it is preceding through dilute or directly use.Its preparation can be by usual Processing method known in those skilled in the art prepare, will after active material mixes with liquid flux or solid carrier, Add the one kind in surfactant such as dispersant, stabilizer, wetting agent, binding agent, defoamer, disintegrant, antifreeze Or it is several.
Pesticidal combination of the invention, can on demand be processed into acceptable formulation on any agricultural chemicals, wherein more preferably Formulation for wettable powder, water dispersible granules, suspending agent, suspension emulsion, aqueous emulsion, microemulsion, microcapsule suspending agent, micro-capsule hang Floating-suspending agent, can also be made effervescent tablet, seed coat agent, ultra-low-volume formulation, aqua, soluble liquid, soluble powder, heat Mist agent.
Composition is when being made wettable powder comprising following constituent content:Acetyl worm nitrile 0.1%~80%, multiple killing teichomycin 0.1%~80%, dispersant 2%~10%, wetting agent 2%~10%, filler surplus.
Composition includes following constituent content when being made water dispersible granules:Acetyl worm nitrile 0.1%~80%, multiple killing teichomycin 0.1%~80%, dispersant 3%~12%, wetting agent 1%~8%, disintegrant 1%~10%, binding agent 0~8%, filler Surplus.
Composition includes following constituent content when being made suspending agent:Acetyl worm nitrile 0.1%~50%, multiple killing teichomycin 0.1% ~50%, dispersant 2%~10%, wetting agent 2%~10%, defoamer 0.01%~2%, thickener 0~2%, antifreeze 0 ~8%, deionized water adds to 100%.
Composition includes following constituent content when being made suspension emulsion:Acetyl worm nitrile 0.1%~50%, multiple killing teichomycin 0.1% ~50%, dispersant 2%~10%, defoamer 0.01%~2%, solvent 1%~15%, thickener 0~2%, emulsifying agent 2% ~12%, antifreeze 0~8%, deionized water adds to 100%.
Composition is when being made aqueous emulsion comprising following constituent content:Acetyl worm nitrile 0.1%~50%, multiple killing teichomycin 0.1% ~50%, solvent 1%~30%, emulsifying agent 1%~15%, antifreeze 0~8%, thickener 0~2%, defoamer 0.01%~ 2%th, deionized water supplies surplus.
Composition includes following constituent content when being made microcapsule suspending agent:Acetyl worm nitrile 0.1%~50%, multiple killing teichomycin 0.1%~50%, macromolecule cyst material 2%~10%, dispersant 1%~10%, organic solvent 1%~10%, defoamer 0.01%~2%, emulsifying agent 1%~7%, pH adjusting agent 0.01%~5%, deionized water add to 100%.
Composition includes following constituent content when being made microcapsule suspension-suspendinagent agent:Acetyl worm nitrile 0.1%~50%, kill more Mycin 0.1%~50%, macromolecule cyst material 2%~10%, dispersant 1%~12%, wetting agent 1%~8%, You Jirong Agent 1%~15%, emulsifying agent 1%~6%, defoamer 0.01%~2%, thickener 0~2%, pH adjusting agent 0.01%~ 5%th, deionized water adds to 100%.
Wettable powder the key technical indexes of the invention:
Water dispersible granules the key technical indexes of the invention:
Suspending agent the key technical indexes of the invention:
Suspension emulsion the key technical indexes of the invention:
Aqueous emulsion the key technical indexes of the invention:
Microcapsule suspending agent the key technical indexes of the invention:
Microcapsule suspension-suspendinagent agent the key technical indexes of the invention:
The advantage of the invention is that:
(1) after acetyl worm nitrile is compounded with multiple killing teichomycin, with obvious synergy and lasting effect;(2) to cereal crops, beans Class crop, fibre crops, sugar crop, melon crop, fruits crop, dry fruit crop, hobby crop, root crop, Oil crops, flower crop, medicinal crop, crop, green manure pasture crop insect have greater activity;(3) agriculture is reduced Medicinal dose, reduces residual quantity of the agricultural chemicals on crop, alleviates environmental pollution;(4) to person poultry safety, Environmental compatibility It is good;And preparation adhesion strength strengthens, resistance of rainwater washing against.
Specific embodiment
With reference to embodiment to further instruction of the present invention, the percentage in embodiment is weight percentage, but The invention is not limited in this.
Application Example one
The wettable powder of embodiment 1~4
Acetyl worm nitrile, multiple killing teichomycin, dispersant, wetting agent, filler are well mixed in mixed cylinder, through airslide disintegrating mill Remixed after crushing uniform, you can wettable powder product of the present invention is obtained, 1 is specifically shown in Table.
The each component of 1 embodiment of table 1~4 and weight portion
The water dispersible granules of embodiment 5~8
Acetyl worm nitrile, multiple killing teichomycin, dispersant, wetting agent, disintegrant, filler etc. are needed through air-flow crushing together Particle diameter, add other auxiliary agents such as binding agent (can add to be not added with), obtain pelletize materials.Item is quantitatively sent into fluid bed system By after granulation and drying in grain drying machine, you can water dispersible granules product of the present invention is obtained, 2 are specifically shown in Table.
The each component of 2 embodiment of table 5~8 and weight portion
The suspending agent of embodiment 9~12
By dispersant, wetting agent, defoamer, thickener (can add to be not added with), antifreeze (can add to be not added with), by a high speed Shear-mixed is uniform, adds acetyl worm nitrile, multiple killing teichomycin, and ball milling 2~3 hours in ball mill make diameter of particle all at 5 μm Hereinafter, surplus is supplied with deionized water, you can suspending agent product of the present invention is obtained, 3 are specifically shown in Table.
The each component of 3 embodiment of table 9~12 and weight portion
The suspension emulsion of embodiment 13~15
Dispersant, defoamer, thickener (can add to be not added with), antifreeze (can add to be not added with) are mixed by high speed shear Uniformly, acetyl worm nitrile is added, ball milling 2~3 hours in ball mill make diameter of particle all below 5 μm, multiple killing teichomycin is obtained Suspending agent, then directly emulsifies multiple killing teichomycin, solvent (can add to be not added with), emulsifying agent and various auxiliary agent high speed agitators In suspending agent, surplus is supplied with deionized water, and suspension emulsion product of the present invention is obtained, and is specifically shown in Table 4.
The each component of 4 embodiment of table 13~15 and weight portion
The aqueous emulsion of embodiment 16~18
Acetyl worm nitrile, multiple killing teichomycin, solvent, emulsifying agent are added together, make to be dissolved into homogeneous oil phase;By deionized water, Antifreeze (can add to be not added with), thickener (can add to be not added with), defoamer are mixed, into homogeneous water phase.In high-speed stirred Under, water is added to oil phase, surplus is supplied with deionized water;Aqueous emulsion product of the present invention is can be prepared by, is specifically shown in Table 5。
The each component of 5 embodiment of table 16~18 and weight portion
The microemulsion of embodiment 19~21
Acetyl worm nitrile, multiple killing teichomycin are dissolved in the homogenizer equipped with solvent, by emulsifying agent, antifreeze, (can add can not Plus), defoamer be added in the homogenizer equipped with above-mentioned solution, surplus deionized water give after supplying strongly mixing and it is even Change, finally obtain the transparent microemulsion product of the present invention of clear appearance, be specifically shown in Table 6.
The each component of 6 embodiment of table 19~21 and content
Embodiment 22,23 microcapsule suspending agents
Acetyl worm nitrile, multiple killing teichomycin, macromolecule cyst material, solvent, defoamer are mixed, make to be dissolved into homogeneous oil phase, In a shear condition, oil phase is added to containing in emulsifying agent, pH adjusting agent, the aqueous phase solution of dispersant, surplus deionization Water is supplied, and two kinds of materials react in oil-water interfaces, forms high score ascus wall, is made well dispersed micro- of the present composition Capsule suspending agent product, is specifically shown in Table 7.
The embodiment 22 of table 7,23 each components and weight portion
Embodiment 24,25 microcapsule suspension-suspendinagent agents
Multiple killing teichomycin, macromolecule cyst material, solvent are mixed, makes to be dissolved into homogeneous oil phase, by oil phase in shearing condition Under be added to containing emulsifying agent, the aqueous phase solution of pH adjusting agent, be made well dispersed microcapsule suspending agent.By dispersant, wet Profit agent, defoamer, thickener (can add to be not added with) are well mixed by high speed shear, add acetyl worm nitrile, the ball in ball mill Mill 2~3 hours, makes diameter of particle all below 5 μm, and suspending agent is obtained, and suspending agent then is added into micro-capsule suspension Aqueous phase solution in, deionized water supplies surplus, is made the well dispersed microcapsule suspension-suspendinagent agent product of the present composition, Specifically it is shown in Table 8.
The embodiment 24 of table 8,25 each components and weight portion
The embodiment of the present invention is the method being combined using Toxicity Determination and field test.First pass through indoor virulence survey Calmly, the co-toxicity coefficient (CTC) after clear and definite two kinds of medicaments are compounded by a certain percentage, CTC < 80 are antagonism, 80≤CTC≤120 It is summation action, CTC > 120 are synergistic effect, on this basis, then carry out field test.
Test method:The mother liquor of each mixed agent is diluted to five series concentrations respectively during experiment, is respectively placed in beaker It is standby.Using the first leaching leaf method that is followed by worm, by not in contact with the blade of the same size of any medicament in the liquid for having configured Taken out after immersion 5s, dried naturally, be put into insect box, then connected for examination larva, raised under the conditions of 25 DEG C, often process 3 Secondary repetition, often repeats test worm number used for 50, while setting blank, dead borer population is checked in 72h, calculates the death rate and correction The death rate, tries to achieve virulence regression equation and calculates LC50Value.If the control death rate is more than 10%, it is considered as invalid experiment.Calculate public Formula is as follows:
Insect corrected mortality is converted into probit value (y), concentration for the treatment of (μ g/ml) is converted into logarithm value (x), with minimum Square law draws virulence regression equation, and thus calculates the value of every kind of medicament, and common poison system is calculated according to the abundant equations of Sun Yun Number CTC.Computing formula is following, and (with acetyl worm nitrile as standard agent, its toxicity index is for 100):
TI × the P of the theoretical toxicity index (TTI) of M=acetyl worm nitrileAcetyl worm nitrile+TI × the P of multiple killing teichomycinMultiple killing teichomycin
In formula:M is the mixture of different ratio
PMultiple killing teichomycinIt is multiple killing teichomycin ratio shared in the composition
PAcetyl worm nitrileIt is acetyl worm nitrile ratio shared in the composition
Application Example two:
For examination insect:Brassicaceous vegetable diamondback moth
Test medicine is provided by Shaanxi Welch Crop Protection Co., Ltd..
Experimental design:Determine having for acetyl worm nitrile and multiple killing teichomycin active compound and the two different ratio mixture by pilot study Effect lethasl concentration scope.
Toxicity test result
The acetyl worm nitrile of table 9 compounds the toxicity test analysis of results table to brassicaceous vegetable diamondback moth with multiple killing teichomycin
Reagent agent Proportioning Co-toxicity coefficient (CTC)
Acetyl worm nitrile 1.58
Multiple killing teichomycin 0.63
Acetyl Chong Jing ︰ multiple killing teichomycins 80:1 0.81 191.50
Acetyl Chong Jing ︰ multiple killing teichomycins 60:1 0.75 205.58
Acetyl Chong Jing ︰ multiple killing teichomycins 40:1 0.72 211.66
Acetyl Chong Jing ︰ multiple killing teichomycins 20:1 0.65 226.79
Acetyl Chong Jing ︰ multiple killing teichomycins 9:1 0.59 232.71
Acetyl Chong Jing ︰ multiple killing teichomycins 4:1 0.49 247.74
Acetyl Chong Jing ︰ multiple killing teichomycins 2:1 0.41 256.46
Acetyl Chong Jing ︰ multiple killing teichomycins 1:1 0.36 250.23
Acetyl Chong Jing ︰ multiple killing teichomycins 1:4 0.29 246.94
Acetyl Chong Jing ︰ multiple killing teichomycins 1:9 0.28 239.40
Acetyl Chong Jing ︰ multiple killing teichomycins 1:20 0.29 223.65
Acetyl Chong Jing ︰ multiple killing teichomycins 1:40 0.30 213.13
Acetyl Chong Jing ︰ multiple killing teichomycins 1:60 0.31 205.25
Acetyl Chong Jing ︰ multiple killing teichomycins 1:80 0.32 198.35
As shown in Table 9, acetyl worm nitrile is matched in 1 80~80 ︰ 1 of ︰, altogether with multiple killing teichomycin to brassicaceous vegetable diamondback moth Malicious coefficient is all higher than 120, illustrate both in the range of the ︰ 1 of 1 ︰ 80~80 mixture show synergistic effect, when acetyl worm nitrile with it is many The proportioning of killing teichomycin is 1:20~20:When 1, synergistic effect becomes apparent protruding, and co-toxicity coefficient is all higher than 220.Tried through applicant Issue after examination and approval the optimum ratio of existing acetyl worm nitrile and multiple killing teichomycin for 20 ︰ 1,19 ︰ 1,18 ︰ 1,17 ︰ 1,16 ︰ 1,15 ︰ 1,14 ︰ 1,13 ︰ 1, 12 ︰ 1,11 ︰ 1,10 ︰ 1,9 ︰ 1,8 ︰ 1,7 ︰ 1,6 ︰ 1,5 ︰ 1,4 ︰ 1,3 ︰ 1,2 ︰ 1,1 ︰ 1,1 ︰ 2,1 ︰ 3,1 ︰ 4,1 ︰ 5,1 ︰ 6,1 ︰ 7,1 ︰ 8th, 1 ︰ 9,1 ︰ 10,1 ︰ 11,1 ︰ 12,1 ︰ 13,1 ︰ 14,1 ︰ 15,1 ︰ 16,1 ︰ 17,1 ︰ 18,1 ︰ 19,1 ︰ 20, wherein when acetyl worm nitrile with Multiple killing teichomycin weight ratio is 2:Co-toxicity coefficient is maximum when 1, and synergistic effect is the most obvious, to the beetle in various crop, leafhopper, aphid The preventing and treating of worm, aleyrodid, beet armyworm, diamondback moth, rice leaf roller, striped rice borer, yellow rice borer, bollworm or thrips has significantly Synergistic effect, co-toxicity coefficient is more than 120.
Effect experiment part:Test medicine is researched and developed by Shaanxi Welch Crop Protection Co., Ltd., provided, comparison medicament 10% acetyl worm nitrile suspending agent (autogamy), 5% multiple killing teichomycin suspending agent (purchased in market).
Application Example triacetyl worm nitrile and multiple killing teichomycin and its compounding preventing and treating cabbage aphid test of pesticide effectiveness
This test arrangement investigates cabbage aphid insect pest index in Shaanxi Province Weinan City Dali County before medicine, occur just in insect pest Phase dispenser, 3 days after dispenser, investigates insect pest indexes and calculates preventive effect for 10 days, 20 days.Result of the test is as follows:
The acetyl worm nitrile of table 10 and multiple killing teichomycin and its compounding preventing and treating cabbage aphid test of pesticide effectiveness
As can be seen from Table 10, cabbage aphid can be effectively prevented and treated after acetyl worm nitrile and multiple killing teichomycin compounding, is tried through inventor Cabbage flea beetle, diamondback moth can also be effectively prevented and treated after verifying bright acetyl worm nitrile and multiple killing teichomycin compounding, prevention effect is above 96%, better than the preventive effect of single dose, and preventive effect phase is long.Target crop is had no adverse effects in experiment scope of medication.
The acetyl worm nitrile of Application Example four prevents and treats the paddy rice rice leaf roller test of pesticide effectiveness with multiple killing teichomycin and its compounding
This test arrangement investigates paddy rice rice leaf roller insect pest index in Shaanxi Province Hanzhong suburban area before medicine, in insect pest hair Raw initial stage dispenser, 3 days after dispenser, investigates insect pest indexes and calculates preventive effect for 10 days, 20 days.Result of the test is as follows:
The acetyl worm nitrile of table 11 prevents and treats the paddy rice rice leaf roller test of pesticide effectiveness with multiple killing teichomycin and its compounding
As can be seen from Table 11, paddy rice rice leaf roller can be effectively prevented and treated after acetyl worm nitrile and multiple killing teichomycin compounding, through hair Person of good sense's experiment can also effectively prevent and treat rice-stem borer, yellow rice borer, prevention effect after proving acetyl worm nitrile and multiple killing teichomycin compounding 96% is above, better than the preventive effect of single dose, and preventive effect phase is long.Target crop is had no adverse effects in experiment scope of medication.
The acetyl worm nitrile of Application Example five and multiple killing teichomycin and its compounding preventing and treating brassicaceous vegetable flea beetle test of pesticide effectiveness
This test arrangement investigates brassicaceous vegetable flea beetle insect pest index, in insect pest in Shaanxi Province Hanzhong suburban area before medicine Early period of origination dispenser, 3 days after dispenser, investigates insect pest indexes and calculates preventive effect for 10 days, 20 days.Result of the test is as follows:
The acetyl worm nitrile of table 12 and multiple killing teichomycin and its compounding preventing and treating brassicaceous vegetable flea beetle test of pesticide effectiveness
As can be seen from Table 12, brassicaceous vegetable flea beetle can be effectively prevented and treated after acetyl worm nitrile and multiple killing teichomycin compounding, is passed through Inventor's experiment prove can also effectively to prevent and treat after acetyl worm nitrile and multiple killing teichomycin compounding brassicaceous vegetable diamondback moth, aphid, Beet armyworm, prevention effect is above 96%, and better than the preventive effect of single dose, and preventive effect phase is long.To target in experiment scope of medication Crop has no adverse effects.
The acetyl worm nitrile of Application Example six and multiple killing teichomycin and its compounding preventing and treating cucumber aleyrodid test of pesticide effectiveness
This test arrangement investigates cucumber powder mite evil index in Shaanxi Province Weinan City Dali County, before medicine, occurs just in insect pest Phase dispenser, 3 days after dispenser, investigates insect pest indexes and calculates preventive effect for 10 days, 20 days.Result of the test is as follows:
The acetyl worm nitrile of table 13 and multiple killing teichomycin and its compounding preventing and treating cucumber aleyrodid test of pesticide effectiveness
As can be seen from Table 13, cucumber aleyrodid can be effectively prevented and treated after acetyl worm nitrile and multiple killing teichomycin compounding, is tried through inventor Cucumber blight can also be effectively prevented and treated after verifying bright acetyl worm nitrile and multiple killing teichomycin compounding, prevention effect is above 96%, is better than The preventive effect of single dose, and preventive effect phase is long.Target crop is had no adverse effects in experiment scope of medication.
Drawn by the experiment of different places throughout the country afterwards, to various crop after acetyl worm nitrile and multiple killing teichomycin compounding On beetle, leafhopper, aphid, aleyrodid, beet armyworm, diamondback moth, rice leaf roller, striped rice borer, yellow rice borer, bollworm or thrips More than 96%, better than single dose preventive effect, synergistic effect is obvious for preventive effect Deng common insect pests.

Claims (6)

1. the Pesticidal combination of a kind of nitrile of worm containing acetyl and multiple killing teichomycin, it is characterised in that:Active ingredient is acetyl worm nitrile and many The weight ratio of killing teichomycin, acetyl worm nitrile and multiple killing teichomycin is the ︰ 1 of 1 ︰ 80~80.
2. the Pesticidal combination of the nitrile of worm containing acetyl according to claim 1 and multiple killing teichomycin, it is characterised in that:Acetyl worm nitrile It is the ︰ 1 of 1 ︰ 40~40 with the weight ratio of multiple killing teichomycin.
3. the Pesticidal combination of the nitrile of worm containing acetyl according to claim 2 and multiple killing teichomycin, it is characterised in that:Acetyl worm nitrile It is 20 with the weight ratio of multiple killing teichomycin:1~1:20.
4. the Pesticidal combination of the nitrile of worm containing acetyl according to any one of claim 1 to 3 and multiple killing teichomycin, its feature exists In:Composition is made wettable powder, water dispersible granules, suspending agent, suspension emulsion, aqueous emulsion, microemulsion, microcapsule suspending agent, micro- Capsule suspension-suspending agent, thermal fog, ultra-low-volume formulation.
5. the Pesticidal combination of the nitrile of worm containing acetyl according to claim 4 and multiple killing teichomycin is used to prevent and treat insect on crops Purposes.
6. purposes according to claim 5, it is characterised in that:Described insect is beetle, leafhopper, aphid, aleyrodid, beet Noctuid, diamondback moth, rice leaf roller, striped rice borer, yellow rice borer, bollworm or thrips.
CN201510902391.0A 2015-12-09 2015-12-09 A kind of Pesticidal combination of the nitrile of worm containing acetyl and multiple killing teichomycin Pending CN106852328A (en)

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Application publication date: 20170616