CN106838607A - Solid ammonia storage tank fills ammonia method - Google Patents

Solid ammonia storage tank fills ammonia method Download PDF

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Publication number
CN106838607A
CN106838607A CN201611159717.6A CN201611159717A CN106838607A CN 106838607 A CN106838607 A CN 106838607A CN 201611159717 A CN201611159717 A CN 201611159717A CN 106838607 A CN106838607 A CN 106838607A
Authority
CN
China
Prior art keywords
ammonia
storage tank
solid
air inlet
ammonia storage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611159717.6A
Other languages
Chinese (zh)
Inventor
王吉
徐贯军
郭秀强
夏秀明
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JILIN ZHONGXIN AUTOMOBILE EQUIPMENT CO Ltd
Original Assignee
JILIN ZHONGXIN AUTOMOBILE EQUIPMENT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JILIN ZHONGXIN AUTOMOBILE EQUIPMENT CO Ltd filed Critical JILIN ZHONGXIN AUTOMOBILE EQUIPMENT CO Ltd
Priority to CN201611159717.6A priority Critical patent/CN106838607A/en
Publication of CN106838607A publication Critical patent/CN106838607A/en
Pending legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C11/00Use of gas-solvents or gas-sorbents in vessels
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2221/00Handled fluid, in particular type of fluid
    • F17C2221/01Pure fluids
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2223/00Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel
    • F17C2223/01Handled fluid before transfer, i.e. state of fluid when stored in the vessel or before transfer from the vessel characterised by the phase
    • F17C2223/0107Single phase
    • F17C2223/013Single phase liquid

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Filling Or Discharging Of Gas Storage Vessels (AREA)

Abstract

Ammonia method is filled the present invention relates to a kind of solid ammonia storage tank, it is characterised in that specifically fill ammonia step, there are ammonia path, i.e. air inlet and gas outlet in the solid ammonia storage tank top and bottom for filling ammonia;Solid ammonia storage tank is laid using hanging device is filled on ammonia frame, 45 ° of angle of inclination, while air inlet direction is downward;End flanges connect cooling liquid water inlet pipe road under solid ammonia storage tank, and connection outlet pipeline in upper end makes coolant temperature be maintained between 10 15 DEG C;Solid ammonia storage tank lower end air inlet connection air inlet pipeline, solid ammonia storage tank upper end gas outlet is connected by outlet pipe with ammonia recycling device, is then turned on air inlet and gas outlet, carries out filling ammonia;After filling ammonia 5h, ammonia storage tank is carried out into 20 25 DEG C of cold baths, staticaccelerator adsorption 10h 15h.It can be reduced and fill the ammonia time, and ammonia speed is filled in quickening, and ammonia efficiency is filled in raising, it is ensured that fill ammonia quality.

Description

Solid ammonia storage tank fills ammonia method
Technical field
Ammonia method is filled the present invention relates to a kind of solid ammonia storage tank, belongs to vehicle maintenance service systems technology field.
Background technology
With the progress of economic society, auto industry is fast-developing, the increasing number of automobile, the environment that vehicle exhaust is caused Pollution is also increasingly serious.Therefore the purifying problem of vehicle exhaust, is increasingly subject to the attention of people.
Vehicle maintenance service system is to store ammonia and to discharge when needed with solid particulate matter, with catalyst reaction after go Except NOx hazardous materials, the purpose of cleaning of off-gas has been reached.The method is safe and reliable, low cost, course continuation mileage are long.
But during solid ammonia storage tank fills ammonia, there is that to fill the ammonia time long, speed is slow, and efficiency is low, fills the difficult control of ammonia amount Situations such as, the quality of solid ammonia storage tank is have impact on, be not suitable for batch production.
Original technology is filled using gaseous state ammonia, is filled the ammonia time and is fixed on 20-25h, because ammonia is close with respect to liquefied ammonia Degree is larger, therefore under same volume, amount of the liquefied ammonia in ammonia storage tank is more, and liquid ammonia gasification needs heat absorption, while playing cold But effect.
In sum, reduce and fill the ammonia time, ammonia speed is filled in quickening, ammonia efficiency is filled in raising, it is ensured that it is current sheet to fill ammonia quality Field personnel's urgent problem.
The content of the invention
Ammonia method is filled it is an object of the invention to provide a kind of solid ammonia storage tank, it can reduce and fill the ammonia time, ammonia is filled in quickening Ammonia efficiency is filled in speed, raising, it is ensured that fill ammonia quality.
The technical proposal of the invention is realized in this way:Solid ammonia storage tank fills ammonia method, it is characterised in that specifically fill ammonia Step,
1)There are ammonia path, i.e. air inlet and gas outlet in the solid ammonia storage tank top and bottom for filling ammonia;
2)Solid ammonia storage tank is laid using hanging device is filled on ammonia frame, 45 ° of angle of inclination, while air inlet direction is downward;
3)End flanges connect cooling liquid water inlet pipe road under solid ammonia storage tank, and connection outlet pipeline in upper end protects coolant temperature Hold between 10-15 DEG C;
4)Solid ammonia storage tank lower end air inlet connection air inlet pipeline, solid ammonia storage tank upper end gas outlet passes through outlet pipe and ammonia Retracting device is connected, and is then turned on air inlet and gas outlet, carries out filling ammonia;
5)After filling ammonia 5h, ammonia storage tank is carried out into 20-25 DEG C of cold bath, staticaccelerator adsorption 10h-15h.
The positive effect of the present invention is farthest to reduce to fill the ammonia time, saves manpower and materials, convenient, fast, Effectively, large-scale production is more suitable for fill.The present invention is to allow ammonia to be converted into liquefied ammonia, by liquid by way of inhaling additional storage Ammonia is stayed in ammonia storage tank, then carries out staticaccelerator adsorption, which save the time of filling, it is to avoid that fills that ammonia brought for a long time is bad Consequence, more accelerates the rate of adsorption of material.
Brief description of the drawings
Fig. 1 fills ammonia schematic diagram for solid ammonia storage tank.
Specific embodiment
Below in conjunction with accompanying drawing, the present invention will be further described with embodiment:As shown in figure 1, solid ammonia storage tank fills ammonia Method, it is characterised in that specifically fill ammonia step:
1)Filling the top and bottom of solid ammonia storage tank 1 of ammonia has ammonia path, i.e. air inlet 2 and gas outlet 3;
2)Solid ammonia storage tank 1 is laid using hanging device is filled on ammonia frame, 45 ° of angle of inclination, while air inlet direction is downward;
3)1 time end flanges of solid ammonia storage tank connect cooling liquid water inlet pipe road 4, and connection outlet pipeline 5 in upper end makes coolant temperature It is maintained between 10-15 DEG C;
4)1 lower end air inlet of solid ammonia storage tank 2 connects air inlet pipeline, the upper end gas outlet 3 of solid ammonia storage tank 1 by outlet pipe with Ammonia recycling device is connected, and is then turned on air inlet 2 and gas outlet 3, carries out filling ammonia;
5)After filling ammonia 5h, ammonia storage tank is carried out into 20-25 DEG C of cold bath, staticaccelerator adsorption 10h-15h.
Embodiment 1
A solid ammonia storage tank 1 is made, is placed on static shelf, as shown in figure 1, connection cooling water pipeline, cooling water temperature 12 DEG C, ammonia pipeline is connected, determine No leakage point, now proceed by and fill ammonia, terminate to fill after 1h, it is put into 12 DEG C of waters bath with thermostatic control In, cooling absorption 7-8h, pressure inside the tank is that this fills end for 0Mpa.

Claims (1)

1. solid ammonia storage tank fills ammonia method, it is characterised in that specifically fill ammonia step,
1)There are ammonia path, i.e. air inlet and gas outlet in the solid ammonia storage tank top and bottom for filling ammonia;
2)Solid ammonia storage tank is laid using hanging device is filled on ammonia frame, 45 ° of angle of inclination, while air inlet direction is downward;
3)End flanges connect cooling liquid water inlet pipe road under solid ammonia storage tank, and connection outlet pipeline in upper end protects coolant temperature Hold between 10-15 DEG C;
4)Solid ammonia storage tank lower end air inlet connection air inlet pipeline, solid ammonia storage tank upper end gas outlet passes through outlet pipe and ammonia Retracting device is connected, and is then turned on air inlet and gas outlet, carries out filling ammonia;
5)After filling ammonia 5h, ammonia storage tank is carried out into 20-25 DEG C of cold bath, staticaccelerator adsorption 10h-15h.
CN201611159717.6A 2016-12-15 2016-12-15 Solid ammonia storage tank fills ammonia method Pending CN106838607A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611159717.6A CN106838607A (en) 2016-12-15 2016-12-15 Solid ammonia storage tank fills ammonia method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611159717.6A CN106838607A (en) 2016-12-15 2016-12-15 Solid ammonia storage tank fills ammonia method

Publications (1)

Publication Number Publication Date
CN106838607A true CN106838607A (en) 2017-06-13

Family

ID=59139352

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611159717.6A Pending CN106838607A (en) 2016-12-15 2016-12-15 Solid ammonia storage tank fills ammonia method

Country Status (1)

Country Link
CN (1) CN106838607A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107504367A (en) * 2017-06-27 2017-12-22 中国第汽车股份有限公司 Ammonia recycle is filled with system and its ammonia recycle filling method

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100294195A1 (en) * 2007-10-05 2010-11-25 Mitsubishi Chemical Corporation Method for charging with liquefied ammonia, method for producing nitride crystal, and reactor for growth of nitride crystal
CN202884466U (en) * 2012-10-16 2013-04-17 苏州金宏气体股份有限公司 Ultra-pure liquid ammonia filling equipment
CN103541794A (en) * 2013-10-30 2014-01-29 中国第一汽车股份有限公司 Circulation ammonia filling method for solid ammonia storing system
CN103672391A (en) * 2013-12-27 2014-03-26 吉林省众鑫汽车装备有限公司 Movable ammonia filling equipment
US20150300573A1 (en) * 2012-11-02 2015-10-22 International Engine Intellectual Property Company, Llc Power modulation for ammonia delivery system
CN205278765U (en) * 2015-12-08 2016-06-01 河南晋开集团雨露复合肥有限公司 Liquid ammonia fills device of dress
CN106015918A (en) * 2016-07-08 2016-10-12 吉林省众鑫汽车装备有限公司 Ammonia charging method for solid ammonia storage tank

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100294195A1 (en) * 2007-10-05 2010-11-25 Mitsubishi Chemical Corporation Method for charging with liquefied ammonia, method for producing nitride crystal, and reactor for growth of nitride crystal
CN202884466U (en) * 2012-10-16 2013-04-17 苏州金宏气体股份有限公司 Ultra-pure liquid ammonia filling equipment
US20150300573A1 (en) * 2012-11-02 2015-10-22 International Engine Intellectual Property Company, Llc Power modulation for ammonia delivery system
CN103541794A (en) * 2013-10-30 2014-01-29 中国第一汽车股份有限公司 Circulation ammonia filling method for solid ammonia storing system
CN103672391A (en) * 2013-12-27 2014-03-26 吉林省众鑫汽车装备有限公司 Movable ammonia filling equipment
CN205278765U (en) * 2015-12-08 2016-06-01 河南晋开集团雨露复合肥有限公司 Liquid ammonia fills device of dress
CN106015918A (en) * 2016-07-08 2016-10-12 吉林省众鑫汽车装备有限公司 Ammonia charging method for solid ammonia storage tank

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107504367A (en) * 2017-06-27 2017-12-22 中国第汽车股份有限公司 Ammonia recycle is filled with system and its ammonia recycle filling method
CN107504367B (en) * 2017-06-27 2020-06-16 中国第一汽车股份有限公司 Ammonia gas circulating charging system and ammonia gas circulating charging method thereof

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Application publication date: 20170613

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