CN106825459A - A kind of vacuum casting device of TiAl intermetallic compound ingot - Google Patents

A kind of vacuum casting device of TiAl intermetallic compound ingot Download PDF

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Publication number
CN106825459A
CN106825459A CN201611250119.XA CN201611250119A CN106825459A CN 106825459 A CN106825459 A CN 106825459A CN 201611250119 A CN201611250119 A CN 201611250119A CN 106825459 A CN106825459 A CN 106825459A
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CN
China
Prior art keywords
movable stand
mould
liquid outlet
support
base
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201611250119.XA
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Chinese (zh)
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CN106825459B (en
Inventor
张龙
潘龙
刘喜
李耀鹏
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Huizhou Hezhihua New Material Co ltd
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Qingdao Apulse Intellectual Property Management Co Ltd
QINGDAO R & D INSTITUTE XI'AN JIAOTONG UNIVERSITY
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Priority to CN201611250119.XA priority Critical patent/CN106825459B/en
Publication of CN106825459A publication Critical patent/CN106825459A/en
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Publication of CN106825459B publication Critical patent/CN106825459B/en
Expired - Fee Related legal-status Critical Current
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D7/00Casting ingots, e.g. from ferrous metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D27/00Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting
    • B22D27/15Treating the metal in the mould while it is molten or ductile ; Pressure or vacuum casting by using vacuum

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Crucibles And Fluidized-Bed Furnaces (AREA)

Abstract

The invention discloses a kind of vacuum casting device of TiAl intermetallic compound ingot, including vacuum induction melting furnace, crucible is provided with stove, crucible bottom is provided with the base sealed with crucible bottom, base center is provided with liquid outlet, foam ceramic filter is installed in liquid outlet, base has may move and pours set, the set upper surface of pouring is adjacent to base lower surface and can be moved left and right along base lower surface, pour set center and be provided with sprue gate, set is poured by movement, can make to pour set outer lining closing liquid outlet, or make sprue gate all or part section alignment liquid outlet;Pour set lower section and be provided with mould, mould outside is provided with movable stand, movable stand upper end connects first support, one layer of heat-preservation cotton of encirclement mould is fixed with first support, movable stand lower end connects second support, the cold shower nozzle of water smoke is connected with second support, the movable stand can be driven and moved in movable stand synchronization in process of setting with the upper shifting of solid liquid interface by cylinder.

Description

A kind of vacuum casting device of TiAl intermetallic compound ingot
Technical field
The invention belongs to materials processing technology field, more particularly, to a kind of vacuum pressing and casting of TiAl intermetallic compound ingot Device.
Background technology
Intermatallic Ti-Al compound density is small, and intensity is big, hardness is big, and resistance to elevated temperatures is strong, its corrosion resistance and antifriction Wipe performance high, especially TiAl intermetallic compound is because having high specific strength, high specific stiffness, anti-corrosion, wear-resisting, high temperature resistant and excellent The advantages of different antioxygenic property, the good candidates structural wood as fields such as contemporary aerospace industry, civilian industries One of material, particularly has broad application prospects in blade of aviation engine field.3D printing, or increasing material manufacturing is used as near A kind of quick shaping process risen over year, using successively powdering, laser or electron beam melt the mode being molded, and realize precision The finishing shaping of part, and the defects such as the shrinkage cavity shrinkage porosity of casting process appearance are avoided, add as a kind of emerging material Work means.
Powder used by current 3D printing, typically by vacuum pouring after melting into ingot casting, subsequent secondary smelting is simultaneously used The mode for being atomized legal system powder is obtained, and in vacuum melting and casting process, melting is protected typically in vacuum induction melting furnace Be poured into mould after temperature, due to needed after mould preheating experience be put into induction furnace, vacuumize, melting, the process, temperature such as cast Can decline, while alloy pig center easily the problems such as shrinkage cavity, gross segregation occurs, cause ingot casting utilization rate to decline, and rear In continuous cutting process, it is easy to adhere to dirt in shrinkage cavity, and is difficult to clean off, while Intermatallic Ti-Al compound in the liquid state anti- Should be active very high, easily reacted with mould, powder processed is impacted, thus find a kind of reduction ingot casting shrinkage cavity and avoid The casting device reacted with mould has great importance.
The content of the invention
In order to solve the above technical problems, the invention provides a kind of vacuum casting device of TiAl intermetallic compound ingot.
The complete technical scheme of the present invention includes:
A kind of vacuum casting device of TiAl intermetallic compound ingot, including vacuum induction melting furnace, are provided with crucible in stove, Crucible bottom is provided with the base sealed with crucible bottom, and base center is provided with liquid outlet, foam ceramic filter is provided with liquid outlet, Base has may move and pours set, and the set upper surface of pouring is adjacent to base lower surface and can be moved left and right along base lower surface, pours Set center is provided with sprue gate, and set is poured by movement, can make to pour set outer lining closing liquid outlet, or make sprue gate all or part Section is directed at liquid outlet;
Pour set lower section and be provided with mould, the mould is composite die, including alumina outer and with to be poured into a mould ingot casting phase With the internal layer of component;Mould outside is provided with movable stand, and movable stand connects cylinder by cylinder rod, and movable stand upper end connects first Frame, is fixed with one layer of heat-preservation cotton of encirclement mould in first support, connection second support in movable stand lower end is connected in second support There is the cold shower nozzle of water smoke, the movable stand can be driven in movable stand synchronization in process of setting with the upper shifting of solid liquid interface by cylinder Move.
The present invention is relative to the advantage of prior art:
1. by way of additional heat-preservation cotton, the speed of mould cooling is reduced, reduce casting flaw incidence.
2. by the carrying out of process of setting, cylinder drives the mode moved on movable stand, is incubated mould upstream fast with bottom Quickly cooling but, forms effective thermograde, makes the freezing interface of aluminium alloy flat, and feeding angle increase, upper metal liquid energy is enough filled Divide feeding, prevent the generation of ingot casting central pipe shrinkage defect.
3. mould inside use with the internal layer to be poured into a mould ingot casting same composition, belonged to the titanium-aluminium alloy for avoiding high reaction activity Between compound and mould reaction, improve purity.
Brief description of the drawings
Fig. 1 is present invention casting device structural representation used.
In figure:1- induction melting furnaces, 2- crucibles, 3- bases, 4- liquid outlets, 5- may move and pour set, 6- moulds, 7- outer layers, 8- internal layers, 9- movable stands, 10- first supports, 11- heat-preservation cottons, 12- second supports, the cold shower nozzle of 13- water smokes, 14- cylinders.
Specific embodiment
The present invention will be further described with reference to the accompanying drawings and detailed description.
The alloy compositions of selection are to include Al by atomic percent:39-40%, Cr:1.2-1.5-%, Nb:1.6- 1.8%, Si:0.05-0.11%, Mo:0.2-0.3%, V:2.2-2.8%, B:0.03-0.04%, La:0.02-0.04%, it is remaining It is Ti to measure.
A kind of vacuum casting device of TiAl intermetallic compound ingot, including vacuum induction melting furnace, are provided with crucible in stove, Crucible bottom is provided with the base sealed with crucible bottom, and base center is provided with liquid outlet, foam ceramic filter is provided with liquid outlet, Base has may move and pours set, and the set upper surface of pouring is adjacent to base lower surface and can be moved left and right along base lower surface, pours Set center is provided with sprue gate, and set is poured by movement, can make to pour set outer lining closing liquid outlet, or make sprue gate all or part Section is directed at liquid outlet;
Pour set lower section and be provided with mould, the mould is composite die, including alumina outer and with to be poured into a mould ingot casting phase With the internal layer of component;Mould outside is provided with movable stand, and movable stand connects cylinder by cylinder rod, and movable stand upper end connects first Frame, is fixed with one layer of heat-preservation cotton of encirclement mould in first support, connection second support in movable stand lower end is connected in second support There is the cold shower nozzle of water smoke, the movable stand can be driven in movable stand synchronization in process of setting with the upper shifting of solid liquid interface by cylinder Move.
Casting method is:The raw material of the Intermatallic Ti-Al compound component of melting is wanted in selection, including titanium sponge, aluminium block with Remaining trace element;It is put into the crucible 2 of vacuum induction melting furnace 1, crucible bottom is provided with the base 3 sealed with crucible bottom, Base center is provided with the liquid outlet 4 of a diameter of 10cm, and the foam ceramic filter that thickness is 1cm is provided with liquid outlet, and base is divided into Have may move and pour set 5, the set upper surface of pouring is adjacent to base lower surface and can be moved left and right along base lower surface, pours set center and sets Have the sprue gate of a diameter of 10cm, set poured by movement, can make to pour set outer lining closing liquid outlet, or make sprue gate whole or Partial cross section is directed at liquid outlet, so as to control the aperture of liquid outlet.
It is put into vacuum induction melting furnace after mould 6 is preheating into 600-800 DEG C, crucible lower section, mould therefor is compound Mould, including alumina outer 7 and with the internal layer 8 to be poured into a mould ingot casting same composition, alumina outer thickness be 3-5cm, it is interior Thickness degree is 0.2-0.5cm, mold height 50cm, die cavity diameter of section 10cm.
Mould outside is provided with movable stand 9, and movable stand connects cylinder 14, movable stand upper end connection first support by cylinder rod 10, one layer of heat-preservation cotton 11 of encirclement mould, movable stand lower end connection second support 12, in second support are fixed with first support The cold shower nozzle 13 of water smoke is connected with,
Induction melting furnace is closed, sealing is evacuated down to 10-5-10-6Pa, opens molten when induction heating apparatus is heated Alloy, heating power is 250-300KW, and smelting temperature is 1750-1830 DEG C, is promoted after 5-10min is incubated after being completely melt It is removable to pour set, make the part or all of section alignment liquid outlet in sprue gate, molten metal outflow carries out bottom pouring type pouring.
The time of the cast full of mould is 120-180s, and after cast, with the carrying out of process of setting, cylinder drives and moves Moved in moving frame, the heat-preservation cotton of its middle and upper part is incubated to mould, reduce mould to dispersed heat around, reduce cooling velocity, subtracted The setting time of slow top aluminium alloy, the cold shower nozzle of water smoke of bottom promotes the aluminium alloy of bottom by cooling water spray painting to mould Quick solidification, with the upper shifting of solid liquid interface, moves in movable stand synchronization, is incubated by top and bottom cools down, and makes aluminium alloy Freezing interface is flat, and feeding angle increase, the enough abundant feeding of upper metal liquid energy prevents the product of ingot casting central pipe shrinkage defect Raw, according to specific setting time, upper shifting speed is 20-25cm/min.
Solidification terminates rear natural cooling, and vacuum breaker takes out ingot casting.
The above, is only presently preferred embodiments of the present invention, and not the present invention is imposed any restrictions, every according to the present invention Any simple modification, change and equivalent structure change that technical spirit is made to above example, still fall within skill of the present invention In the protection domain of art scheme.

Claims (1)

1. a kind of vacuum casting device of TiAl intermetallic compound ingot, including vacuum induction melting furnace, is provided with crucible, earthenware in stove Crucible bottom is provided with the base sealed with crucible bottom, and base center is provided with liquid outlet, foam ceramic filter, bottom are provided with liquid outlet Seat has may move and pours set, and the set upper surface of pouring is adjacent to base lower surface and can be moved left and right along base lower surface, pours set Center is provided with sprue gate, and set is poured by movement, can make to pour set outer lining closing liquid outlet, or make sprue gate completely or partially cut In face of quasi- liquid outlet;
Pour set lower section and be provided with mould, the mould is composite die, including alumina outer and identical with to be poured into a mould ingot casting group The internal layer for dividing;Mould outside is provided with movable stand, and movable stand connects cylinder by cylinder rod, and movable stand upper end connects first support, One layer of heat-preservation cotton of encirclement mould is fixed with first support, connection second support in movable stand lower end is connected with second support The cold shower nozzle of water smoke, the movable stand can be driven and moved in movable stand synchronization in process of setting with the upper shifting of solid liquid interface by cylinder.
CN201611250119.XA 2016-12-29 2016-12-29 A kind of vacuum casting device of TiAl intermetallic compound ingot Expired - Fee Related CN106825459B (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB618824A (en) * 1945-11-13 1949-02-28 British Thomson Houston Co Ltd Improvements in and relating to methods of casting electrodes for x-ray tubes and casting moulds therefor
CN1169124A (en) * 1994-08-08 1997-12-31 西门子公司 Method and device for directionally solidifying a melt liquid
CN1473679A (en) * 2003-08-11 2004-02-11 西安交通大学 Method for producing copper-chromium contact material by vacuum directional solidification and single side water cooling cast mold
RU2267380C1 (en) * 2004-05-24 2006-01-10 Федеральное государственное унитарное предприятие "Всероссийский научно-исследовательский институт авиационных материалов" (ФГУП "ВИАМ") Apparatus for making castings with directed and monocrystalline structure
CN101844222A (en) * 2010-05-28 2010-09-29 北京科技大学 Controllable temperature gradient unidirectional solidification device and method
CN102139279A (en) * 2010-12-15 2011-08-03 北京科技大学 Method for producing oriented high-silicon steel cold-rolled sheet by using directional solidification plate blank

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB618824A (en) * 1945-11-13 1949-02-28 British Thomson Houston Co Ltd Improvements in and relating to methods of casting electrodes for x-ray tubes and casting moulds therefor
CN1169124A (en) * 1994-08-08 1997-12-31 西门子公司 Method and device for directionally solidifying a melt liquid
CN1473679A (en) * 2003-08-11 2004-02-11 西安交通大学 Method for producing copper-chromium contact material by vacuum directional solidification and single side water cooling cast mold
RU2267380C1 (en) * 2004-05-24 2006-01-10 Федеральное государственное унитарное предприятие "Всероссийский научно-исследовательский институт авиационных материалов" (ФГУП "ВИАМ") Apparatus for making castings with directed and monocrystalline structure
CN101844222A (en) * 2010-05-28 2010-09-29 北京科技大学 Controllable temperature gradient unidirectional solidification device and method
CN102139279A (en) * 2010-12-15 2011-08-03 北京科技大学 Method for producing oriented high-silicon steel cold-rolled sheet by using directional solidification plate blank

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Effective date of registration: 20190110

Address after: 518000 R&D Building, Shenglongxing Industrial Park, 22 Huanping Road, Pingdi Street, Longgang District, Shenzhen City, Guangdong Province, 11 and 12 floors

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Address before: 518000 11, 12 floor, Sheng Longxing Industrial Park R & D building, 22 Ping Ping Road, Longgang District, Shenzhen, Guangdong.

Patentee before: SHENZHEN XINSHEN NEW MATERIAL TECHNOLOGY Co.,Ltd.

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Granted publication date: 20190219