CN106811349A - A kind of emulsifying cleaning agent and preparation method - Google Patents
A kind of emulsifying cleaning agent and preparation method Download PDFInfo
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- CN106811349A CN106811349A CN201510845437.XA CN201510845437A CN106811349A CN 106811349 A CN106811349 A CN 106811349A CN 201510845437 A CN201510845437 A CN 201510845437A CN 106811349 A CN106811349 A CN 106811349A
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Abstract
A kind of raw material the invention provides emulsifying cleaning agent and preparation method, including following weight portion is constituted：Sodium citrate 0.1-10；EDETATE SODIUM 0.1-10；Potassium hydroxide 0.01-5；Triethanolamine 1-20；Neopelex 1-20；Butyl 0.1-10；Tetrachloro-ethylene 0.1-10；Surfactant 0.1-10；Phenylpropyl alcohol triazole 0.01-1；Sodium metasilicate 0.1-10；Bleeding agent 0.1-10；Water surplus, it is emulsifying cleaning agent the invention provides a kind of cleaning agent, emulsifying cleaning agent is a kind of between waterborne cleaning agent and the osculant cleaning agent of leaning solvent, there is stronger cleansing power than waterborne cleaning agent, use cost simultaneously lower than leaning solvent, safer, more environmentally friendly, more energy efficient novel detergent.
Description
Technical field
This patent is related to cleaning agent field, more particularly to a kind of emulsifying cleaning agent and preparation method.
Background technology
General waterborne cleaning agent needs heating and different cleaning agents is required for when non-ferrous metal and ferrous metal is cleaned at present, and during common solvent type cleaning agent cleaning plastics, rubber has destroyed dissolving.Common solvent type cleaning agent cannot also dissolve cleaning vegetable and animals oils, and general waterborne cleaning agent also is difficult to cleaning polishing wax, rosin, adhesive and inorganic pigment.And typically all there is corrosivity to the healthy unfavorable of human body in cleaning agent conventional on the market.
The content of the invention
It is emulsifying cleaning agent the invention provides a kind of cleaning agent, emulsifying cleaning agent is a kind of between waterborne cleaning agent and the osculant cleaning agent of leaning solvent, there is stronger cleansing power than waterborne cleaning agent, use cost simultaneously lower than leaning solvent, it is safer, more environmentally friendly, more energy efficient novel detergent.
A kind of cleaning agent scheme that the present invention is provided is as follows, including the raw material of following weight portion is constituted：Sodium citrate 0.1-10；EDETATE SODIUM 0.1-10；Potassium hydroxide 0.01-5；Triethanolamine 1-20；Neopelex 1-20；Butyl 0.1-10；Tetrachloro-ethylene 0.1-10；Surfactant 0.1-10；Phenylpropyl alcohol triazole 0.01-1；Sodium metasilicate 0.1-10；Bleeding agent 0.1-10；Water surplus.
Above-mentioned cleaning agent, wherein, including following weight portion raw material composition：Sodium citrate 1-3；EDETATE SODIUM 0.5-2；Potassium hydroxide 0.05-1；Triethanolamine 5-12；Neopelex 8-12；Butyl 1-3；Tetrachloro-ethylene 0.5-1；Surfactant 2-5；Phenylpropyl alcohol triazole 0.05-0.2；Sodium metasilicate 1-3；Bleeding agent 2-5；Water surplus.
Above-mentioned cleaning agent, wherein, including following weight portion raw material composition：Sodium citrate 2；EDETATE SODIUM 1；Potassium hydroxide 0.06；Triethanolamine 10；Neopelex 10；Butyl 2；Tetrachloro-ethylene 0.8；Surfactant 3；Phenylpropyl alcohol triazole 0.1；Sodium metasilicate 2；Bleeding agent 4；Water surplus.
Above-mentioned cleaning agent, wherein, the sodium metasilicate is non-hydrate sodium metasilicate, and the surfactant is nonionic surfactant, and the nonionic surfactant is AEO-7, and the bleeding agent is penetrating agent JFC.
A kind of another side of the invention, preparation method of cleaning agent, comprises the following steps：
A certain amount of water is taken to be heated to sequentially add sodium citrate, EDETATE SODIUM and non-hydrate sodium metasilicate after 45-60 degree and be uniformly mixing to obtain the first mixture；
Triethanolamine and neopelex are added in the first mixture and the second mixture is uniformly mixing to obtain；
Second mixture and tetrachloro-ethylene, AEO-7 and penetrating agent JFC are uniformly mixing to obtain 0/w solution；
Phenylpropyl alcohol triazole and butyl are well mixed and obtain solution B；
Above-mentioned solution B is slowly added to be stirred in above-mentioned 0/w solution.
Above-mentioned preparation method, wherein, the preparation method also includes, mixing speed is 200-300r/min during the first mixture and the second mixture is prepared.
Above-mentioned preparation method, wherein, the preparation method also includes, 0/w solution is uniformly mixing to obtain with tetrachloro-ethylene, AEO-7 and penetrating agent JFC again after the second mixture temperature is cooled into 35-40 degree.
Above-mentioned preparation method, wherein, the preparation method also includes, the second mixture and tetrachloro-ethylene, AEO-7 and penetrating agent JFC are uniformly mixing to obtain into 0/w solution, wherein the speed of the stirring is 600-800r/min.
Above-mentioned preparation method, wherein, the preparation method also includes, is well mixed phenylpropyl alcohol triazole and butyl obtains solution B at normal temperatures.
Above-mentioned preparation method, wherein, the preparation method also includes, is slowly added in 0/w solution to be uniformly mixing to obtain described cleaning agent by solution B at normal temperatures and in whipping process controls cleaning agent in the range of alkalescent.
It is emulsifying cleaning agent the invention provides a kind of cleaning agent, emulsifying cleaning agent is a kind of between waterborne cleaning agent and the osculant cleaning agent of leaning solvent, there is stronger cleansing power than waterborne cleaning agent, use cost simultaneously lower than leaning solvent, it is safer, more environmentally friendly, more energy efficient novel detergent；Specifically, with powerful oil removing cleansing power, can cleaning solvent type cleaning agent cannot dissolve the vegetable and animals oils of cleaning, the buffing wax that general aqueous cleaning cannot be cleaned, rosin, adhesive and inorganic pigment can be cleaned again；And without flash-point, safer, comfortable operating environment is harmless；It is suitable for various cleaning ways, puts examination cleaning on the skin by hand, cleaning showers, soaking and washing and supersonic wave cleaning machine is cleaned；Can be cleaned with normal temperature, it is easy to operate；Non-ferrous metal capable of washing and ferrous metal and various plastics, rubber；Cleaning agent of the invention is weak neutral cleaners, and product is gentle, does not corrode hand.
Specific embodiment
In the following description, a large amount of concrete details are given to provide more thorough understanding of the invention.It is, however, obvious to a person skilled in the art that the present invention can be carried out without one or more of these details.In other examples, in order to avoid obscuring with the present invention, it is not described for some technical characteristics well known in the art.
In order to thoroughly understand the present invention, detailed step and detailed structure will be proposed in following description, to explain technical scheme.Presently preferred embodiments of the present invention is described in detail as follows, but in addition to these detailed descriptions, the present invention can also have other embodiment.
The raw material composition of embodiment 1, a kind of cleaning agent, including following weight portion：Sodium citrate 0.1Kg；EDETATE SODIUM 0.1Kg；Potassium hydroxide 0.01Kg；Triethanolamine 1Kg；Neopelex 1Kg；Butyl 0.1Kg；Tetrachloro-ethylene 0.1Kg；Surfactant 0.1Kg；Phenylpropyl alcohol triazole 0.01Kg；Sodium metasilicate 0.1Kg；Bleeding agent 0.1Kg；The amount of water 45Kg, wherein potassium hydroxide is adjusted according to the PH of product, and the amount of the potassium hydroxide required for making product PH control near 8.5 is standard.
The raw material composition of embodiment 2, a kind of cleaning agent, including following weight portion：Sodium citrate 10Kg；EDETATE SODIUM 10Kg；Potassium hydroxide 5Kg；Triethanolamine 20Kg；Neopelex 20Kg；Butyl 10Kg；Tetrachloro-ethylene 10Kg；Surfactant 10Kg；Phenylpropyl alcohol triazole 1Kg；Sodium metasilicate 10Kg；Bleeding agent 10Kg；The amount of water 65Kg, wherein potassium hydroxide is adjusted according to the PH of product, and the amount of the potassium hydroxide required for making product PH control near 8.5 is standard.
The raw material composition of embodiment 3, a kind of cleaning agent, including following weight portion：Sodium citrate 1Kg；EDETATE SODIUM 0.5Kg；Potassium hydroxide 0.05Kg；Triethanolamine 5Kg；Neopelex 8Kg；Butyl 1Kg；Tetrachloro-ethylene 0.5Kg；Surfactant 2Kg；Phenylpropyl alcohol triazole 0.05Kg；Sodium metasilicate 1Kg；Bleeding agent 2Kg；The amount of water 45Kg, wherein potassium hydroxide is adjusted according to the PH of product, and the amount of the potassium hydroxide required for making product PH control near 8.5 is standard.
The raw material composition of embodiment 4, a kind of cleaning agent, including following weight portion：Sodium citrate 3Kg；EDETATE SODIUM 2Kg；Potassium hydroxide 1Kg；Triethanolamine 12Kg；Neopelex 12Kg；Butyl 3Kg；Tetrachloro-ethylene 1Kg；Surfactant 5Kg；Phenylpropyl alcohol triazole 0.2Kg；Sodium metasilicate 3Kg；Bleeding agent 5Kg；The amount of water 65Kg, wherein potassium hydroxide is adjusted according to the PH of product, and the amount of the potassium hydroxide required for making product PH control near 8.5 is standard.
The raw material composition of embodiment 5, a kind of cleaning agent, including following weight portion：Sodium citrate 2Kg；EDETATE SODIUM 1Kg；Potassium hydroxide 0.06Kg；Triethanolamine 10Kg；Neopelex 10Kg；Butyl 2Kg；Tetrachloro-ethylene 0.8Kg；Surfactant 3Kg；Phenylpropyl alcohol triazole 0.1Kg；Sodium metasilicate 2Kg；Bleeding agent 4Kg；The amount of water 50Kg, wherein potassium hydroxide is adjusted according to the PH of product, and the amount of the potassium hydroxide required for making product PH control near 8.5 is standard.
In the present invention to illustrate that potassium hydroxide is used as pH value conditioning agent, for controlling the PH scopes of product, the pH value of cleaning agent of the invention has compatibility near 8.5 with the skin of human body, does not hurt hands；Surfactant is nonionic surfactant, preferably AEO-7；Sodium metasilicate is non-hydrate sodium metasilicate；Bleeding agent is penetrating agent JFC.
In the present invention by nonionic surfactant and anion surfactant compatibility as the emulsifying agent in the present invention, the stability with more preferable emulsifying effectiveness and product, wherein neopelex are anion surfactant；Phenylpropyl alcohol triazole in the present invention has lipophile and hydrophily, and then cleaning agent of the invention all has very strong cleaning performance to cleaning oiliness and aqueous spot；It is emulsification initiator that triethanolamine is used in the present invention, fast with reaction speed, and consumption is small and product of emulsification has the advantages that good stability；Butyl and tetrachloro-ethylene have good lipophile in the present invention, and the vegetable and animals oils to that cannot dissolve cleaning have very strong cleansing power.
A kind of another side of the invention, preparation method of cleaning agent, comprises the following steps：
Step S1：A certain amount of water is taken to be heated to sequentially add sodium citrate, EDETATE SODIUM and non-hydrate sodium metasilicate after 45-60 degree and be uniformly mixing to obtain the first mixture；
Step S2：Triethanolamine and neopelex are added in the first mixture and the second mixture is uniformly mixing to obtain, mixing speed is 200-300r/min during the first mixture and the second mixture is prepared；
Step S3：Second mixture and tetrachloro-ethylene, AEO-7 and penetrating agent JFC are uniformly mixing to obtain 0/w solution, triethanolamine and neopelex is added to be uniformly mixing to obtain the emulsion of oil-in-water form with tetrachloro-ethylene, AEO-7 and penetrating agent JFC again by the first mixture, for follow-up further emulsification is prepared, 0/w solution is uniformly mixing to obtain with tetrachloro-ethylene, AEO-7 and penetrating agent JFC again after the second mixture temperature wherein is cooled into 35-40 degree, wherein the speed of the stirring is 600-800r/min；That is under certain mixing speed and under reaction temperature, the more preferably more preferable oil-in-water emulsion of stability could be formed；
Step S4：Phenylpropyl alcohol triazole and butyl are well mixed and obtain solution B, phenylpropyl alcohol triazole and butyl are well mixed at normal temperatures specially and obtains solution B；
Step S5：Above-mentioned solution B is slowly added to be stirred in above-mentioned 0/w solution, solution B is specially slowly added in 0/w solution to be uniformly mixing to obtain described cleaning agent at normal temperatures and in whipping process cleaning agent is controlled in the range of alkalescent, to illustrate that in solution B is slowly added into 0/w solution at normal temperatures, wherein mixing speed is 100r/min, the product for obtaining under such condition is more preferably stablized, product needs control in the range of alkalescent, and PH is preferably 8.5.
In sum, it is emulsifying cleaning agent the invention provides a kind of cleaning agent, emulsifying cleaning agent is a kind of between waterborne cleaning agent and the osculant cleaning agent of leaning solvent, there is stronger cleansing power than waterborne cleaning agent, use cost simultaneously lower than leaning solvent, safer, more environmentally friendly, more energy efficient novel detergent；Specifically, with powerful oil removing cleansing power, can cleaning solvent type cleaning agent cannot dissolve the vegetable and animals oils of cleaning, the buffing wax that general aqueous cleaning cannot be cleaned, rosin, adhesive and inorganic pigment can be cleaned again；And without flash-point, safer, comfortable operating environment is harmless；It is suitable for various cleaning ways, puts examination cleaning on the skin by hand, cleaning showers, soaking and washing and supersonic wave cleaning machine is cleaned；Can be cleaned with normal temperature, it is easy to operate；Non-ferrous metal capable of washing and ferrous metal and various plastics, rubber；Cleaning agent of the invention is weak neutral cleaners, and product is gentle, does not corrode hand.
Presently preferred embodiments of the present invention is described above.It is to be appreciated that the present invention is not limited to the above specific embodiments, wherein the equipment and structure that do not describe in detail to the greatest extent are construed as being practiced with the common mode in this area；Any those of ordinary skill in the art, in the case where technical solution of the present invention ambit is not departed from, many possible variations and modification are all made to technical solution of the present invention using the methods and techniques content of the disclosure above, or the Equivalent embodiments of equivalent variations are revised as, this has no effect on substance of the invention.Therefore, every content without departing from technical solution of the present invention, according to technical spirit of the invention to any simple modification, equivalent variation and modification made for any of the above embodiments, still falls within the range of technical solution of the present invention protection.
Claims (10)
1. a kind of cleaning agent, it is characterised in that the raw material composition including following weight portion：Sodium citrate 0.1-10；EDETATE SODIUM 0.1-10；Potassium hydroxide 0.01-5；Triethanolamine 1-20；Neopelex 1-20；Butyl 0.1-10；Tetrachloro-ethylene 0.1-10；Surfactant 0.1-10；Phenylpropyl alcohol triazole 0.01-1；Sodium metasilicate 0.1-10；Bleeding agent 0.1-10；Water surplus.
2. a kind of cleaning agent as claimed in claim 1, it is characterised in that the raw material composition including following weight portion：Sodium citrate 1-3；EDETATE SODIUM 0.5-2；Potassium hydroxide 0.05-1；Triethanolamine 5-12；Neopelex 8-12；Butyl 1-3；Tetrachloro-ethylene 0.5-1；Surfactant 2-5；Phenylpropyl alcohol triazole 0.05-0.2；Sodium metasilicate 1-3；Bleeding agent 2-5；Water surplus.
3. a kind of cleaning agent as claimed in claim 1, it is characterised in that the raw material composition including following weight portion：Sodium citrate 2；EDETATE SODIUM 1；Potassium hydroxide 0.06；Triethanolamine 10；Neopelex 10；Butyl 2；Tetrachloro-ethylene 0.8；Surfactant 3；Phenylpropyl alcohol triazole 0.1；Sodium metasilicate 2；Bleeding agent 4；Water surplus.
4. a kind of cleaning agent as described in claim 1-3 is any, it is characterised in that the sodium metasilicate is non-hydrate sodium metasilicate, the surfactant is nonionic surfactant, and the nonionic surfactant is AEO-7, and the bleeding agent is penetrating agent JFC.
5. a kind of preparation method of cleaning agent, it is characterised in that comprise the following steps：
A certain amount of water is taken to be heated to sequentially add sodium citrate, EDETATE SODIUM and non-hydrate sodium metasilicate after 45-60 degree and be uniformly mixing to obtain the first mixture；
Triethanolamine and neopelex are added in the first mixture and the second mixture is uniformly mixing to obtain；
Second mixture and tetrachloro-ethylene, AEO-7 and penetrating agent JFC are uniformly mixing to obtain 0/w solution；
Phenylpropyl alcohol triazole and butyl are well mixed and obtain solution B；
Above-mentioned solution B is slowly added to be stirred in above-mentioned 0/w solution.
6. a kind of preparation method of cleaning agent as claimed in claim 5, it is characterised in that the preparation method also includes that mixing speed is 200-300r/min during the first mixture and the second mixture is prepared.
7. a kind of preparation method of cleaning agent as claimed in claim 5, it is characterised in that the preparation method also includes, 0/w solution is uniformly mixing to obtain after the second mixture temperature is cooled into 35-40 degree with tetrachloro-ethylene, AEO-7 and penetrating agent JFC again.
8. a kind of preparation method of cleaning agent as claimed in claim 7, it is characterized in that, the preparation method also includes, the second mixture and tetrachloro-ethylene, AEO-7 and penetrating agent JFC are uniformly mixing to obtain into 0/w solution, wherein the speed of the stirring is 600-800r/min.
9. a kind of preparation method of cleaning agent as claimed in claim 5, it is characterised in that the preparation method also includes, obtains solution B by phenylpropyl alcohol triazole and butyl are well mixed at normal temperatures.
10. the preparation method of a kind of cleaning agent as described in claim 5-9 is any, it is characterized in that, the preparation method also includes, is slowly added in 0/w solution to be uniformly mixing to obtain described cleaning agent by solution B at normal temperatures and in whipping process controls cleaning agent in the range of alkalescent.
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Cited By (5)
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| CN108034530A (en) * | 2017-12-29 | 2018-05-15 | 镇江程灿科技服务有限公司 | A kind of environment-friendly type fruits and vegetables cleaning agent |
| CN108587805A (en) * | 2018-04-23 | 2018-09-28 | 杭州鼎好新材料有限公司 | A kind of polyvinyl cleaning agent and preparation method thereof |
| CN112226300A (en) * | 2020-10-09 | 2021-01-15 | 如皋市雨润纤维科技有限公司 | Preparation process of green high-efficiency environment-friendly oil agent |
| CN112961738A (en) * | 2021-02-05 | 2021-06-15 | 上海佐航新材料科技有限公司 | Novel alkaline hard floor cleaning agent and preparation method thereof |
| CN113509456A (en) * | 2020-04-09 | 2021-10-19 | 宁海德宝立新材料有限公司 | Diethylene glycol monobutyl ether litholytic agent |
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| CN112226300A (en) * | 2020-10-09 | 2021-01-15 | 如皋市雨润纤维科技有限公司 | Preparation process of green high-efficiency environment-friendly oil agent |
| CN112961738A (en) * | 2021-02-05 | 2021-06-15 | 上海佐航新材料科技有限公司 | Novel alkaline hard floor cleaning agent and preparation method thereof |
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Application publication date: 20170609 |