CN106758311A - Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration - Google Patents

Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration Download PDF

Info

Publication number
CN106758311A
CN106758311A CN201611089514.4A CN201611089514A CN106758311A CN 106758311 A CN106758311 A CN 106758311A CN 201611089514 A CN201611089514 A CN 201611089514A CN 106758311 A CN106758311 A CN 106758311A
Authority
CN
China
Prior art keywords
parts
synthetic leather
preparation
fire
resin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611089514.4A
Other languages
Chinese (zh)
Inventor
黄小平
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NANPING BOSHIDA ENERGY-SAVING TECHNOLOGY Co Ltd
Original Assignee
NANPING BOSHIDA ENERGY-SAVING TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NANPING BOSHIDA ENERGY-SAVING TECHNOLOGY Co Ltd filed Critical NANPING BOSHIDA ENERGY-SAVING TECHNOLOGY Co Ltd
Priority to CN201611089514.4A priority Critical patent/CN106758311A/en
Publication of CN106758311A publication Critical patent/CN106758311A/en
Pending legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/142—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes mixture of polyurethanes with other resins in the same layer
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
    • C09D175/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/61—Additives non-macromolecular inorganic
    • C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/60—Additives non-macromolecular
    • C09D7/63—Additives non-macromolecular organic
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
    • C09D7/40—Additives
    • C09D7/65—Additives macromolecular
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
    • D06M15/03—Polysaccharides or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/53—Polyethers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
    • D06N3/0061—Organic fillers or organic fibrous fillers, e.g. ground leather waste, wood bark, cork powder, vegetable flour; Other organic compounding ingredients; Post-treatment with organic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
    • D06N3/0063—Inorganic compounding ingredients, e.g. metals, carbon fibres, Na2CO3, metal layers; Post-treatment with inorganic compounds
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/007—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by mechanical or physical treatments
    • D06N3/0077—Embossing; Pressing of the surface; Tumbling and crumbling; Cracking; Cooling; Heating, e.g. mirror finish
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/0086—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the application technique
    • D06N3/0095—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the application technique by inversion technique; by transfer processes
    • D06N3/0097—Release surface, e.g. separation sheets; Silicone papers
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
    • D06N3/12—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins
    • D06N3/14—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes
    • D06N3/145—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. gelatine proteins with polyurethanes two or more layers of polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/06—Properties of the materials having thermal properties
    • D06N2209/067—Flame resistant, fire resistant
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/10—Properties of the materials having mechanical properties
    • D06N2209/103—Resistant to mechanical forces, e.g. shock, impact, puncture, flexion, shear, compression, tear
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/12—Permeability or impermeability properties
    • D06N2209/126—Permeability to liquids, absorption
    • D06N2209/128—Non-permeable
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2209/00—Properties of the materials
    • D06N2209/16—Properties of the materials having other properties
    • D06N2209/1607—Degradability
    • D06N2209/1621—Water-soluble, water-dispersible
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2211/00—Specially adapted uses
    • D06N2211/12—Decorative or sun protection articles
    • D06N2211/14—Furniture, upholstery
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
    • D06N2211/00—Specially adapted uses
    • D06N2211/12—Decorative or sun protection articles
    • D06N2211/28—Artificial leather

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Treatment And Processing Of Natural Fur Or Leather (AREA)

Abstract

The invention discloses a kind of preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration, it is related to synthetic leather processing technical field, comprises the following steps：(1) treatment of synthetic leather base cloth, the treatment of (2) release liners, the processing of (3) synthetic leather semi-finished product, the processing of (4) synthetic leather products.The rich texture of the made synthetic leather of the present invention, flexible smooth, outward appearance is beautiful generous；The performance of made synthetic leather is excellent simultaneously, and fire-retardant soundproof effect is good, intensity is high, water proofing property and hydrolytic resistance are strong, so as to extend its service life as house decorative material.

Description

Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration
Technical field：
The present invention relates to synthetic leather processing technical field, and in particular to a kind of fire-retardant sound insulation synthesis suitable for interior decoration The preparation method of leather.
Background technology：
Synthetic leather is material common in living, and can be used for many design fields, such as clothes, jewellery, household.Leather There is comfortable softness, good durable, wear-resistant, rich texture, high resilience, give nature environmental protection, quality it is rough, return Return natural psychological feelingses.Synthetic leather passes through various processing technologys such as modern hollow out, laser engraving, is endowed a kind of novelty Type of service, i.e. interior decoration.Synthetic leather is used for indoor ornamentation and is broadly divided into classification：Leather interface, leather furniture and leather are old If wherein leather interface includes leather metope and leather ground, and the application of synthetic leather processing into leather metope is more extensive, Certain fire-retardant deadening can also be played while the compartment is played.
At present, conventional synthetic leather all has certain flame retardant effect substantially, but soundproof effect is small, need to such as improve sound insulation effect Really, generally realized by the way of synthetic leather thickness is increased, so increase cost, limit synthetic leather as wall Face decorate indoors in application.
The content of the invention：
The technical problems to be solved by the invention are to provide that a kind of rich texture, intensity are good and the feature of environmental protection is strong is applied to The preparation method of the fire-retardant sound insulation synthetic leather of interior decoration.
The technical problems to be solved by the invention are realized using following technical scheme：
Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration, comprise the following steps：
(1) treatment of synthetic leather base cloth：Raising base cloth is first passed through into impregnating groove with the speed of 5-10m/min, in impregnating groove Equipped with 55-60 DEG C of impregnation material, then curing process is carried out by coagulating basin, 5-10 DEG C of cold air is passed through in coagulating basin, then passed through Rinsing bowl carries out washing process, and rinsing bowl, most afterwards through 65-70 DEG C of slow drying, is obtained final product to be attached with and contained built with 30-35 DEG C of warm water Soak the synthetic leather base cloth of material；
(2) treatment of release liners：First with an applicator roll in release liners the shell fabric of even spread one, fabric is in 75- Slowly dried at 80 DEG C, recycle No. two applicator roll floor middle material of even spread one on release liners fabric, middle material is in 85-90 Slowly dried at DEG C, then using No. three applicator rolls, the floor of even spread one is then expected on release liners middle material, then expect in Rapid draing at 100-105 DEG C, obtains final product the release liners for being attached with fabric, middle material successively and then expecting；
(3) processing of synthetic leather semi-finished product：By the above-mentioned release liners through after treatment in 2-3min is preheated at 80-85 DEG C, so The synthetic leather base cloth that impregnation material will be attached with afterwards is laid in release liners, and 3-5min is pressed under pressure 0.5MPa, then through 65- 70 DEG C of slow drying, finally separate release liners, obtain final product synthetic leather semi-finished product；
(4) processing of synthetic leather products：By synthetic leather semi-finished product by embossing machine compacting line, polished after being cooled down through room temperature Treatment, obtains final product synthetic leather products；
The impregnation material is made up of the raw material of following parts by weight：Ethoxylated dodecyl alcohol 10-15 parts, polyethylene glycol oxide 5-10 parts, Sodium Polyacrylate 3-6 parts, poloxamer 2-4 parts, carbomer 2-4 parts, Brazil wax 1-2 parts, water soluble shells gather It is sugared 1-2 parts, polyethylene glycol 0.5-1 parts, asbestos wool 0.5-1 parts, poly-aspartic-acid 0.3-0.5 parts, water 100-150 parts；
The fabric is mixed by the raw material of following parts by weight：A expects 15-20 parts, 10-15 parts of B material；The middle material It is mixed by the raw material of following parts by weight：A expects 15-20 parts, 15-20 parts of B material；It is described then to expect by following parts by weight Raw material is mixed：A expects 15-20 parts, 20-25 parts of B material；
The A material are made up of the raw material of following parts by weight：Waterborne polyurethane resin 10-15 parts, water-soluble poly butadiene Resin 5-10 parts, cetanol 2-4 parts, 2-4 parts of hydrogenated rosin pentaerythritol ester, 1-2 parts of nanometer rubber powder, vaseline 1-2 parts, poly- season Ammonium salt 0.5-1 parts, ultra-fine polytetrafluorethylepowder powder 0.5-1 parts, maleic anhydride grafting 0.3-0.5 parts of compatilizer, water 100-150 Part；
The B material are made up of the raw material of following parts by weight：Waterborne polyurethane resin 15-20 parts, polyvinyl alcohol resin 3-6 Part, HPMA 2-4 parts, PAMC 2-4 parts, polyvinyl butyral resin 1-2 parts, PVPP 1- 2 parts, PNBR 1-2 parts, 0.5-1 parts of C5 hydrogenated petroleum resins, bipentaerythrite 0.5-1 parts, toner 0.5-1 parts, water 100-150 parts.
It is described impregnation material preparation method be：Xiang Shuizhong adds polyethylene glycol oxide, poloxamer and polyethylene glycol, with 5 DEG C/ The programming rate of min is warming up to reflux state insulation mixing 30min, adds Sodium Polyacrylate, carbomer and babassu Wax, continues the insulation mixing 15min that flows back, and is then cooled to 5-10 DEG C of insulation mixing 30min with the cooling rate of 5 DEG C/min, then Ethoxylated dodecyl alcohol, water soluble chitosan, asbestos wool and poly-aspartic-acid are added, 15min is stood after being sufficiently mixed, with Reflux state insulation mixing 10min is warming up to the programming rate of 10 DEG C/min afterwards, last natural cooling cooling obtains final product impregnation Material.
The preparation method of A material is：Xiang Shuizhong adds cetanol, hydrogenated rosin pentaerythritol ester, nanometer rubber powder and all Intellectual circle, fully dispersed rear standing 10min, then reflux state insulation mixing 15min is warming up to the programming rate of 5 DEG C/min, and Polyquaternium, ultra-fine polytetrafluorethylepowder powder and maleic anhydride grafting compatilizer are added, continues the insulation mixing 30min that flows back, so Add waterborne polyurethane resin and water-soluble poly butadiene resin while hot afterwards, be sufficiently mixed uniform, last natural cooling cooling, i.e., Obtain A material.
The preparation method of B material is：Xiang Shuizhong adds PAMC, polyvinyl butyral resin, powder fourth Nitrile rubber and C5 hydrogenated petroleum resins, fully dispersed rear standing 10min, then backflow shape is warming up to the programming rate of 10 DEG C/min State insulation mixing 20min, and polyvinyl alcohol resin, PVPP and bipentaerythrite are added, continue the insulation mixing that flows back 15min, then adds waterborne polyurethane resin, HPMA and toner while hot, is sufficiently mixed uniformly, last naturally cold But lower the temperature, obtain final product B material.
The nanometer rubber powder is made up of the raw material of following parts by weight：Dcpd resin 5-10 parts, bismaleimide Polyimide resin 3-6 parts, chlorinated polyethylene rubber 2-4 parts, hydrophobic nano-silica 2-4 parts, Tissuemat E 1-2 parts, vulcanization pig Oily 1-2 parts, super fine magnesia 1-2 parts, hexadecyltrimethylammonium chloride 0.5-1 parts, coal tar 0.5-1 parts, lanthana 0.1- 0.3 part.
The preparation method of the nanometer rubber powder is：To addition bimaleimide resin, chlorination in dcpd resin Polyethylene rubber and coal tar, utilize microwave treater microwave treatment 5min after being sufficiently mixed, continue at microwave after standing 15min Reason 5min, and adds Tissuemat E, sulfurized lard and hexadecyltrimethylammonium chloride, microwave treatment again after being well mixed 5min, then add hydrophobic nano-silica, super fine magnesia and lanthana while hot, be sufficiently mixed it is uniform, then with 10 DEG C/ The cooling rate cooling of min, is incubated mixing 15min after temperature is down to 0-5 DEG C, is then heated up with the programming rate of 5 DEG C/min, Mixing 30min, gained mixture natural cooling cooling, after temperature is down to 35-40 DEG C are incubated after temperature rises to 125-130 DEG C In feeding nano-level grinder, a nanometer rubber powder is obtained final product after being fully ground.
The condition of work of the microwave treater is microwave frequency 2450MHz, power 700W.
The particle mean size of the nanometer rubber powder is 20nm.
The beneficial effects of the invention are as follows：Preparation method of the present invention is applied to processing indoor decoration synthetic leather, has Processing cost is low and the characteristics of the strong feature of environmental protection, using water as coating solvents, it is to avoid prepare what synthetic leather was present using organic solvent The problem of health is influenceed after volatilization；And the rich texture of made synthetic leather, flexible smooth, outward appearance is beautiful generous；Simultaneously The performance of made synthetic leather is excellent, and fire-retardant soundproof effect is good, intensity is high, water proofing property and hydrolytic resistance are strong, so as to extend it As the service life of house decorative material.
Specific embodiment：
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) treatment of synthetic leather base cloth：Raising base cloth is first passed through into impregnating groove with the speed of 5m/min, impregnating groove built with 55-60 DEG C of impregnation material, then curing process is carried out by coagulating basin, 5-10 DEG C of cold air is passed through in coagulating basin, then by washing Groove carries out washing process, and rinsing bowl is most obtained final product and be attached with impregnation material through 65-70 DEG C of slow drying afterwards built with 30-35 DEG C of warm water Synthetic leather base cloth；
(2) treatment of release liners：First with an applicator roll in release liners the shell fabric of even spread one, fabric is in 75- Slowly dried at 80 DEG C, recycle No. two applicator roll floor middle material of even spread one on release liners fabric, middle material is in 85-90 Slowly dried at DEG C, then using No. three applicator rolls, the floor of even spread one is then expected on release liners middle material, then expect in Rapid draing at 100-105 DEG C, obtains final product the release liners for being attached with fabric, middle material successively and then expecting；
(3) processing of synthetic leather semi-finished product：By the above-mentioned release liners through after treatment in 3min is preheated at 80-85 DEG C, then The synthetic leather base cloth that impregnation material will be attached with is laid in release liners, and 3min is pressed under pressure 0.5MPa, then through 65-70 DEG C Slow drying, finally separates release liners, obtains final product synthetic leather semi-finished product；
(4) processing of synthetic leather products：By synthetic leather semi-finished product by embossing machine compacting line, polished after being cooled down through room temperature Treatment, obtains final product synthetic leather products.
It is impregnated with the preparation of material：To 8 parts of polyethylene glycol oxides, 2 parts of poloxamers and 0.5 part of polyethylene glycol of addition in 150 parts of water, Reflux state insulation mixing 30min is warming up to the programming rate of 5 DEG C/min, 3 parts of Sodium Polyacrylates, 2 parts of Ka Boshu are added Fat and 1 part of Brazil wax, continue the insulation mixing 15min that flows back, and are then cooled to 5-10 DEG C of guarantor with the cooling rate of 5 DEG C/min Temperature mixing 30min, adds 10 parts of ethoxylated dodecyl alcohols, 1 part of water soluble chitosan, 0.5 part of asbestos wool and 0.3 part of poly- day L-aminobutanedioic acid, stands 15min after being sufficiently mixed, be then warming up to reflux state insulation mixing with the programming rate of 10 DEG C/min 10min, last natural cooling cooling, obtains final product impregnation material.
The preparation of fabric：It is prepared by fully mixing by 20 parts of A material and 15 parts of B material.
The preparation of middle material：It is prepared by fully mixing by 15 parts of A material and 15 parts of B material.
Then the preparation expected：It is prepared by fully mixing by 20 parts of A material and 25 parts of B material.
The preparation of A material：To 2 parts of cetanols, 2 parts of hydrogenated rosin pentaerythritol esters, 1 part of nanometer rubber powder of addition in 150 parts of water With 1 part of vaseline, it is fully dispersed after stand 10min, then with the programming rate of 5 DEG C/min be warming up to reflux state insulation mixing 15min, and 1 part of polyquaternium, 0.5 part of ultra-fine polytetrafluorethylepowder powder and 0.3 part of maleic anhydride grafting compatilizer are added, continue Backflow insulation mixing 30min, then adds 15 parts of waterborne polyurethane resins and 5 parts of water-soluble poly butadiene resins, fully while hot Well mixed, last natural cooling cooling obtains final product A material.
The preparation of B material：To 2 parts of PAMCs, 2 parts of polyvinyl butyral resins, 1 part of powder of addition in 150 parts of water Last nitrile rubber and 0.5 part of C5 hydrogenated petroleum resin, fully dispersed rear standing 10min, then with the programming rate liter of 10 DEG C/min Temperature adds 3 parts of polyvinyl alcohol resins, 2 parts of PVPPs and 0.5 part of double Ji Wusi to reflux state insulation mixing 20min Alcohol, continue flow back insulation mixing 15min, then while hot add 20 parts of waterborne polyurethane resins, 2 parts of HPMAs and 0.5 part of toner, is sufficiently mixed uniform, last natural cooling cooling, obtains final product B material.
The preparation of nanometer rubber powder：To 5 parts of bimaleimide resins, 2 parts of chlorinations of addition in 10 parts of dcpd resins Polyethylene rubber and 0.5 part of coal tar, the microwave treater after being sufficiently mixed using microwave frequency 2450MHz, power 700W are micro- Ripple processes 5min, and microwave treatment 5min, and 2 parts of Tissuemat Es of addition, 1 part of sulfurized lard and 0.5 part ten are continued after standing 15min Six alkyl trimethyl ammonium chlorides, microwave treatment 5min again after being well mixed, then 3 parts of hydrophobic nano titanium dioxides are added while hot Silicon, 2 parts of super fine magnesias and 0.2 part of lanthana, are sufficiently mixed uniformly, are then lowered the temperature with the cooling rate of 10 DEG C/min, treat temperature Degree is incubated mixing 15min after being down to 0-5 DEG C, then heated up with the programming rate of 5 DEG C/min, after temperature rises to 125-130 DEG C Insulation mixing 30min, gained mixture natural cooling cooling, after temperature is down to 35-40 DEG C in feeding nano-level grinder, through filling The nanometer rubber powder that particle mean size is 20nm is obtained final product after dividing grinding.
Embodiment 2
(1) treatment of synthetic leather base cloth：Raising base cloth is first passed through into impregnating groove with the speed of 5m/min, impregnating groove built with 55-60 DEG C of impregnation material, then curing process is carried out by coagulating basin, 5-10 DEG C of cold air is passed through in coagulating basin, then by washing Groove carries out washing process, and rinsing bowl is most obtained final product and be attached with impregnation material through 65-70 DEG C of slow drying afterwards built with 30-35 DEG C of warm water Synthetic leather base cloth；
(2) treatment of release liners：First with an applicator roll in release liners the shell fabric of even spread one, fabric is in 75- Slowly dried at 80 DEG C, recycle No. two applicator roll floor middle material of even spread one on release liners fabric, middle material is in 85-90 Slowly dried at DEG C, then using No. three applicator rolls, the floor of even spread one is then expected on release liners middle material, then expect in Rapid draing at 100-105 DEG C, obtains final product the release liners for being attached with fabric, middle material successively and then expecting；
(3) processing of synthetic leather semi-finished product：By the above-mentioned release liners through after treatment in 3min is preheated at 80-85 DEG C, then The synthetic leather base cloth that impregnation material will be attached with is laid in release liners, and 3min is pressed under pressure 0.5MPa, then through 65-70 DEG C Slow drying, finally separates release liners, obtains final product synthetic leather semi-finished product；
(4) processing of synthetic leather products：By synthetic leather semi-finished product by embossing machine compacting line, polished after being cooled down through room temperature Treatment, obtains final product synthetic leather products.
It is impregnated with the preparation of material：To 8 parts of polyethylene glycol oxides, 4 parts of poloxamers and 0.5 part of polyethylene glycol of addition in 150 parts of water, Reflux state insulation mixing 30min is warming up to the programming rate of 5 DEG C/min, 5 parts of Sodium Polyacrylates, 2 parts of Ka Boshu are added Fat and 1 part of Brazil wax, continue the insulation mixing 15min that flows back, and are then cooled to 5-10 DEG C of guarantor with the cooling rate of 5 DEG C/min Temperature mixing 30min, adds 10 parts of ethoxylated dodecyl alcohols, 2 parts of water soluble chitosans, 0.5 part of asbestos wool and 0.3 part of poly- day L-aminobutanedioic acid, stands 15min after being sufficiently mixed, be then warming up to reflux state insulation mixing with the programming rate of 10 DEG C/min 10min, last natural cooling cooling, obtains final product impregnation material.
The preparation of fabric：It is prepared by fully mixing by 20 parts of A material and 15 parts of B material.
The preparation of middle material：It is prepared by fully mixing by 15 parts of A material and 15 parts of B material.
Then the preparation expected：It is prepared by fully mixing by 20 parts of A material and 25 parts of B material.
The preparation of A material：To 3 parts of cetanols, 2 parts of hydrogenated rosin pentaerythritol esters, 1 part of nanometer rubber powder of addition in 150 parts of water With 1 part of vaseline, it is fully dispersed after stand 10min, then with the programming rate of 5 DEG C/min be warming up to reflux state insulation mixing 15min, and 0.5 part of polyquaternium, 0.5 part of ultra-fine polytetrafluorethylepowder powder and 0.3 part of maleic anhydride grafting compatilizer are added, after Continuous backflow insulation mixing 30min, then adds 15 parts of waterborne polyurethane resins and 7 parts of water-soluble poly butadiene resins while hot, fills Divide well mixed, last natural cooling cooling obtains final product A material.
The preparation of B material：To 4 parts of PAMCs, 1 part of polyvinyl butyral resin, 1 part of powder of addition in 150 parts of water Last nitrile rubber and 0.5 part of C5 hydrogenated petroleum resin, fully dispersed rear standing 10min, then with the programming rate liter of 10 DEG C/min Temperature adds 5 parts of polyvinyl alcohol resins, 1 part of PVPP and 0.5 part of double Ji Wusi to reflux state insulation mixing 20min Alcohol, continue flow back insulation mixing 15min, then while hot add 20 parts of waterborne polyurethane resins, 3 parts of HPMAs and 0.5 part of toner, is sufficiently mixed uniform, last natural cooling cooling, obtains final product B material.
The preparation of nanometer rubber powder：Gather to 5 parts of bimaleimide resins, 3 parts of chlorinations are added in 8 parts of dcpd resins Ethylene rubber and 0.5 part of coal tar, utilize microwave frequency 2450MHz, the microwave treater microwave of power 700W after being sufficiently mixed Treatment 5min, microwave treatment 5min, and 1 part of Tissuemat E of addition, 1 part of sulfurized lard and 0.5 part 16 are continued after standing 15min Alkyl trimethyl ammonium chloride, microwave treatment 5min again after being well mixed, then 4 parts of hydrophobic nano-silicas, 1 are added while hot Part super fine magnesia and 0.2 part of lanthana, are sufficiently mixed uniformly, are then lowered the temperature with the cooling rate of 10 DEG C/min, treat that temperature drops Mixing 15min is incubated after to 0-5 DEG C, is then heated up with the programming rate of 5 DEG C/min, be incubated after temperature rises to 125-130 DEG C Mixing 30min, gained mixture natural cooling cooling, after temperature is down to 35-40 DEG C in feeding nano-level grinder, through fully grinding The nanometer rubber powder that particle mean size is 20nm is obtained final product after mill.
Embodiment 3
Embodiment 1 and preparation method described in embodiment 2 are used to prepare indoor decoration synthetic leather, and are used for performance Tested, as a result as shown in table 1.
The performance of the made synthetic leather of table 1
General principle of the invention and principal character and advantages of the present invention has been shown and described above.The technology of the industry Personnel it should be appreciated that the present invention is not limited to the above embodiments, simply explanation described in above-described embodiment and specification this The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appending claims and its Equivalent thereof.

Claims (8)

1. the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration is applied to, it is characterised in that comprised the following steps：
(1) treatment of synthetic leather base cloth：Raising base cloth is first passed through into impregnating groove with the speed of 5-10m/min, impregnating groove built with 55-60 DEG C of impregnation material, then curing process is carried out by coagulating basin, 5-10 DEG C of cold air is passed through in coagulating basin, then by washing Groove carries out washing process, and rinsing bowl is most obtained final product and be attached with impregnation material through 65-70 DEG C of slow drying afterwards built with 30-35 DEG C of warm water Synthetic leather base cloth；
(2) treatment of release liners：First with an applicator roll in release liners the shell fabric of even spread one, fabric is in 75-80 DEG C It is lower slow dry, No. two applicator roll floor middle material of even spread one on release liners fabric are recycled, middle material is at 85-90 DEG C Slow to dry, then using No. three applicator rolls, the floor of even spread one is then expected on release liners middle material, is then expected in 100-105 Rapid draing at DEG C, obtains final product the release liners for being attached with fabric, middle material successively and then expecting；
(3) processing of synthetic leather semi-finished product：By the above-mentioned release liners through after treatment in 2-3min is preheated at 80-85 DEG C, then will The synthetic leather base cloth for being attached with impregnation material is laid in release liners, and 3-5min is pressed under pressure 0.5MPa, then through 65-70 DEG C Slow drying, finally separates release liners, obtains final product synthetic leather semi-finished product；
(4) processing of synthetic leather products：By synthetic leather semi-finished product by embossing machine compacting line, after being cooled down through room temperature at polishing Reason, obtains final product synthetic leather products；
The impregnation material is made up of the raw material of following parts by weight：Ethoxylated dodecyl alcohol 10-15 parts, polyethylene glycol oxide 5-10 Part, Sodium Polyacrylate 3-6 parts, poloxamer 2-4 parts, carbomer 2-4 parts, Brazil wax 1-2 parts, water soluble chitosan 1- 2 parts, polyethylene glycol 0.5-1 parts, asbestos wool 0.5-1 parts, poly-aspartic-acid 0.3-0.5 parts, water 100-150 parts；
The fabric is mixed by the raw material of following parts by weight：A expects 15-20 parts, 10-15 parts of B material；The middle material is by such as The raw material of lower parts by weight is mixed：A expects 15-20 parts, 15-20 parts of B material；It is described then to expect by the raw material of following parts by weight It is mixed：A expects 15-20 parts, 20-25 parts of B material；
The A material are made up of the raw material of following parts by weight：Waterborne polyurethane resin 10-15 parts, water-soluble poly butadiene resin 5-10 parts, cetanol 2-4 parts, 2-4 parts of hydrogenated rosin pentaerythritol ester, 1-2 parts of nanometer rubber powder, vaseline 1-2 parts, polyquaternium 0.5-1 parts, ultra-fine polytetrafluorethylepowder powder 0.5-1 parts, maleic anhydride 0.3-0.5 parts, water 100-150 parts of compatilizer of grafting；
The B material are made up of the raw material of following parts by weight：Waterborne polyurethane resin 15-20 parts, polyvinyl alcohol resin 3-6 parts, HPMA 2-4 parts, PAMC 2-4 parts, polyvinyl butyral resin 1-2 parts, PVPP 1-2 Part, PNBR 1-2 parts, 0.5-1 parts of C5 hydrogenated petroleum resins, bipentaerythrite 0.5-1 parts, toner 0.5-1 parts, water 100-150 parts.
2. the preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration according to claim 1, it is characterised in that It is described impregnation material preparation method be：Xiang Shuizhong adds polyethylene glycol oxide, poloxamer and polyethylene glycol, with the liter of 5 DEG C/min Warm speed is warming up to reflux state insulation mixing 30min, adds Sodium Polyacrylate, carbomer and Brazil wax, continues Backflow insulation mixing 15min, is then cooled to 5-10 DEG C of insulation mixing 30min with the cooling rate of 5 DEG C/min, adds bay Alcohol APEO, water soluble chitosan, asbestos wool and poly-aspartic-acid, stand 15min, then with 10 after being sufficiently mixed DEG C/programming rate of min is warming up to reflux state insulation mixing 10min, last natural cooling cooling obtains final product impregnation material.
3. the preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration according to claim 1, it is characterised in that The preparation method of A material is：Xiang Shuizhong adds cetanol, hydrogenated rosin pentaerythritol ester, nanometer rubber powder and vaseline, fully 10min is stood after dispersion, then reflux state insulation mixing 15min is warming up to the programming rate of 5 DEG C/min, and add polyquaternary amine Salt, ultra-fine polytetrafluorethylepowder powder and maleic anhydride grafting compatilizer, continue the insulation mixing 30min that flows back, and then add while hot Waterborne polyurethane resin and water-soluble poly butadiene resin, are sufficiently mixed uniform, last natural cooling cooling, obtain final product A material.
4. the preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration according to claim 1, it is characterised in that The preparation method of B material is：Xiang Shuizhong add PAMC, polyvinyl butyral resin, PNBR and C5 hydrogenated petroleum resins, it is fully dispersed after stand 10min, then to be warming up to reflux state insulation with the programming rate of 10 DEG C/min mixed 20min is closed, and adds polyvinyl alcohol resin, PVPP and bipentaerythrite, continue the insulation mixing 15min that flows back, then Waterborne polyurethane resin, HPMA and toner are added while hot, are sufficiently mixed uniform, last natural cooling cooling, i.e., Obtain B material.
5. the preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration according to claim 1, it is characterised in that The nanometer rubber powder is made up of the raw material of following parts by weight：Dcpd resin 5-10 parts, bimaleimide resin 3-6 Part, chlorinated polyethylene rubber 2-4 part, hydrophobic nano-silica 2-4 parts, Tissuemat E 1-2 parts, sulfurized lard 1-2 parts, surpass Thin 1-2 parts, hexadecyltrimethylammonium chloride 0.5-1 parts, coal tar 0.5-1 parts, lanthana 0.1-0.3 parts of magnesia.
6. the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration is applied to according to claim 1 or 5, and its feature exists In the preparation method of the nanometer rubber powder is：To addition bimaleimide resin, haloflex in dcpd resin Rubber and coal tar, utilize microwave treater microwave treatment 5min after being sufficiently mixed, microwave treatment is continued after standing 15min 5min, and add Tissuemat E, sulfurized lard and hexadecyltrimethylammonium chloride, microwave treatment again after being well mixed 5min, then add hydrophobic nano-silica, super fine magnesia and lanthana while hot, be sufficiently mixed it is uniform, then with 10 DEG C/ The cooling rate cooling of min, is incubated mixing 15min after temperature is down to 0-5 DEG C, is then heated up with the programming rate of 5 DEG C/min, Mixing 30min, gained mixture natural cooling cooling, after temperature is down to 35-40 DEG C are incubated after temperature rises to 125-130 DEG C In feeding nano-level grinder, a nanometer rubber powder is obtained final product after being fully ground.
7. the preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration according to claim 6, it is characterised in that： The condition of work of the microwave treater is microwave frequency 2450MHz, power 700W.
8. the preparation method of the fire-retardant sound insulation synthetic leather suitable for interior decoration according to claim 6, it is characterised in that： The particle mean size of the nanometer rubber powder is 20nm.
CN201611089514.4A 2016-12-01 2016-12-01 Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration Pending CN106758311A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611089514.4A CN106758311A (en) 2016-12-01 2016-12-01 Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611089514.4A CN106758311A (en) 2016-12-01 2016-12-01 Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration

Publications (1)

Publication Number Publication Date
CN106758311A true CN106758311A (en) 2017-05-31

Family

ID=58915390

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201611089514.4A Pending CN106758311A (en) 2016-12-01 2016-12-01 Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration

Country Status (1)

Country Link
CN (1) CN106758311A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018193659A (en) * 2017-05-22 2018-12-06 株式会社クラレ Leather-like sheet and production method thereof
CN110527305A (en) * 2019-09-11 2019-12-03 烟台大学 Utilize the method for the ash of buffing containing chromium production particle board
CN114808479A (en) * 2022-05-19 2022-07-29 福建华夏合成革有限公司 Preparation method of water-based earphone sleeve leather

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1050577A (en) * 1989-09-25 1991-04-10 蒋和平 Wet polyvingl butyral synthetic leather
US20060272770A1 (en) * 2004-08-24 2006-12-07 San Fang Chemical Industry Co., Ltd. Method for making artificial leather with superficial texture
CN101525846A (en) * 2009-03-27 2009-09-09 福建兰峰制革有限公司 Method for producing crease-free leathers
CN102234937A (en) * 2010-05-07 2011-11-09 福建兰峰制革有限公司 Production process of top layer leather-simulated super-fibre synthetic leather
CN103031744A (en) * 2011-09-29 2013-04-10 昆山协兴合成革有限公司 Manufacture method of half microfiber sports shoe leather
CN104389192A (en) * 2014-12-02 2015-03-04 福建华阳超纤有限公司 Manufacturing method of soft fine-creased artificial super-fiber leather

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1050577A (en) * 1989-09-25 1991-04-10 蒋和平 Wet polyvingl butyral synthetic leather
US20060272770A1 (en) * 2004-08-24 2006-12-07 San Fang Chemical Industry Co., Ltd. Method for making artificial leather with superficial texture
CN101525846A (en) * 2009-03-27 2009-09-09 福建兰峰制革有限公司 Method for producing crease-free leathers
CN102234937A (en) * 2010-05-07 2011-11-09 福建兰峰制革有限公司 Production process of top layer leather-simulated super-fibre synthetic leather
CN103031744A (en) * 2011-09-29 2013-04-10 昆山协兴合成革有限公司 Manufacture method of half microfiber sports shoe leather
CN104389192A (en) * 2014-12-02 2015-03-04 福建华阳超纤有限公司 Manufacturing method of soft fine-creased artificial super-fiber leather

Non-Patent Citations (6)

* Cited by examiner, † Cited by third party
Title
夏征农: "《大辞海 化工轻工纺织卷》", 31 August 2009, 上海：上海辞书出版社 *
宋小平等: "《石油工业用添加剂生产与应用技术》", 31 March 2014, 中国石化出版社 *
方亮: "《药用高分子材料学》", 31 August 2015, 中国医药科技出版社 *
李广宇等: "《胶黏剂原材料手册》", 31 August 2004, 北京：国防工业出版社 *
陆启玉: "《油脂化工产品生产技术》", 31 March 2004, 北京：化学工业出版社 *
陈开勋: "《新领域精细化工》", 31 March 1999, 中国石化出版社 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2018193659A (en) * 2017-05-22 2018-12-06 株式会社クラレ Leather-like sheet and production method thereof
CN110527305A (en) * 2019-09-11 2019-12-03 烟台大学 Utilize the method for the ash of buffing containing chromium production particle board
CN114808479A (en) * 2022-05-19 2022-07-29 福建华夏合成革有限公司 Preparation method of water-based earphone sleeve leather

Similar Documents

Publication Publication Date Title
CN103696274B (en) A kind of foaming synthetic leather manufacture method based on water-base resin and TPU resin
CN106758311A (en) Suitable for the preparation method of the fire-retardant sound insulation synthetic leather of interior decoration
CN106400597B (en) Suitable for the four sides elasticity synthetic leather making release liners coating material of clothes
CN107059420A (en) Aqueous dry method foaming clothing leather and preparation method thereof
CN106867341A (en) A kind of construction wall insulation water-thinned nanometer paint
CN105155297B (en) A kind of preparation method of aqueous polyurethane impregnation superfine fiber chemical leather bass
CN103147312A (en) PU (Polyurethane) synthetic leather and preparation method thereof
CN107354760B (en) Low-temperature-deflection-resistant perforated breathable polyvinyl chloride artificial leather and preparation method thereof
WO2016086719A1 (en) Process for producing automotive interior leather
CN108068426A (en) A kind of production technology of high-strength cow nonwoven skin cloth
CN107011788A (en) Artificial leather inorganic agent, artificial polyvinyl chloride leather, preparation method and the usage
CN1228500C (en) Post finishing process for superfine fiber artificial leather
CN105133367A (en) Aqueous polyurethane shoe lining leather production process
CN106087438B (en) A kind of environment-friendlyfoamed foamed artificial leather and preparation method thereof
CN105603831B (en) A kind of high-strength waterproof vegetable fibre board and its production technology
CN106637926A (en) Waterborne synthetic leather surface treatment agent and preparation method thereof
CN105178053A (en) Production process of waterborne polyurethane instep leather
CN110344276A (en) A kind of pure plain leather of biology base high gloss and its manufacturing method
CN105926304B (en) A kind of manufacture method of water-based PU on-slip material
CN106758532A (en) Suitable for the heat accumulation thermal synthetic leather making release liners coating material of clothes
CN106758414A (en) A kind of efficient levelling type leather dye fixation auxiliary agent
US20150159321A1 (en) Suede-like synthetic leather and method of making the same
WO2016086717A1 (en) Process for producing color-changed leather
CN106758273A (en) Suitable for the preparation method of the environmentally friendly super fiber leather of automotive trim
CN106752208A (en) A kind of open type electric tricycle seat processing outside leather substance

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20170531

RJ01 Rejection of invention patent application after publication