CN106756094A - Zinc distillation furnace - Google Patents
Zinc distillation furnace Download PDFInfo
- Publication number
- CN106756094A CN106756094A CN201611226650.3A CN201611226650A CN106756094A CN 106756094 A CN106756094 A CN 106756094A CN 201611226650 A CN201611226650 A CN 201611226650A CN 106756094 A CN106756094 A CN 106756094A
- Authority
- CN
- China
- Prior art keywords
- zinc
- condensation chamber
- distillery
- slag
- distillation
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/04—Obtaining zinc by distilling
- C22B19/16—Distilling vessels
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/04—Obtaining zinc by distilling
- C22B19/16—Distilling vessels
- C22B19/18—Condensers, Receiving vessels
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/32—Refining zinc
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)
Abstract
The invention discloses a kind of zinc distillation furnace, including distillery, destilling tower, condensation chamber and pumped vacuum systems, distillery, destilling tower and condensation chamber are sequentially connected, and pumped vacuum systems is communicated in condensation chamber, the side of condensation chamber is provided with zinc outlet, and distillery is provided with slag-drip opening and charging aperture.This kind of zinc distillation furnace uses advanced slag making technology, while high temperature distillation zinc, iron aluminium impurity is set to form mobility slag and continuously exclude, continuous production can be realized, reduce the labour intensity of staff, the separating effect of iron and zinc is improved, the scope of application is larger, distillation smelting furnace is arranged together with refining furnace, energy consumption is relatively low in smelting process, workshop floor space is smaller, and metal recovery rate is high, can save production cost, simultaneously, this kind of zinc distillation furnace burn out rate is relatively low, is easy to operation, has broad application prospects.
Description
Technical field
The present invention relates to technical field of chemical, more particularly to a kind of zinc distillation furnace.
Background technology
At present, the preparation method of high-purity Zn is mainly distillation condensation method.A kind of typical zinc distillation equipment is tower zinc
Distillation equipment.
The impurity-eliminating effect of tower zinc distillation equipment is preferable, but, the energy consumption in removal of impurities is higher, and production cost is higher.
Therefore, how reducing energy consumption, reduce production cost, be those skilled in the art need at present solve technology ask
Topic.
The content of the invention
In view of this, it is an object of the invention to provide a kind of zinc distillation furnace, being capable of reducing energy consumption, reduction production cost.
To achieve the above object, the present invention provides following technical scheme：
A kind of zinc distillation furnace, including distillery, destilling tower, condensation chamber and pumped vacuum systems, the distillery, the distillation
Tower is sequentially connected with the condensation chamber, and the pumped vacuum systems is communicated in the condensation chamber, and the side of the condensation chamber is provided with out
Zinc mouthful, the distillery is provided with slag-drip opening and charging aperture.
Preferably, the U-shaped pipeline communication that the distillery passes through vertically-arranged with the condensation chamber, the destilling tower is located at described
Among U-tube road.
Preferably, the condensation chamber is thermostatic chamber.
Preferably, the distillery is provided with resistive heater.
Preferably, the pumped vacuum systems includes vacuum degree measuring equipment.
The zinc distillation furnace that the present invention is provided includes distillery, destilling tower, condensation chamber and pumped vacuum systems, distillery, distillation
Tower is sequentially connected with condensation chamber, and pumped vacuum systems is communicated in condensation chamber, and the side of condensation chamber is provided with zinc outlet, and distillery is provided with
Slag-drip opening and charging aperture.
Distillery is used to melt plating cadmia and makes iron aluminum slag, in practical operation, after plating cadmia material melting, by charging aperture
It is added directly into distillery, while adding a kind of slag former, makes slag former with foreign metal iron reactive aluminum, generation in plating cadmia
The iron aluminum slag of low melting point, separates with fused zinc.Metallic zinc becomes gaseous state zinc fume at high temperature, into destilling tower in remove height boiling
Point metallic iron, metallic iron due to than it is great, boiling point is high and sink to below liquid Zn so that iron tramp can from slag-drip opening discharge stove
Outward.Clean zinc fume is cooled down into condensation chamber, is obtained liquid Zn and is released stove ingot casting from zinc outlet.Wherein, can in distillery
To be put into efficient slag former, to improve the separating effect of zinc and iron, make slag low containing zinc, improve the rate of recovery of zinc.
This kind of zinc distillation furnace uses advanced slag making technology, while high temperature distillation zinc, iron aluminium impurity is formed flowing
Property slag and continuously exclude, continuous production can be realized, reduce the labour intensity of staff, improve iron and effect separated with zinc
Really, the scope of application is larger, and distillation smelting furnace is arranged together with refining furnace, and energy consumption is relatively low in smelting process, and face is taken up an area in workshop
Product is smaller, and metal recovery rate is high, can save production cost, meanwhile, this kind of zinc distillation furnace burn out rate is relatively low, is easy to operation, tool
Have broad application prospects.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing
The accompanying drawing to be used needed for having technology description is briefly described, it should be apparent that, drawings in the following description are only this
Inventive embodiment, for those of ordinary skill in the art, on the premise of not paying creative work, can also basis
The accompanying drawing of offer obtains other accompanying drawings.
Fig. 1 is the sectional view of the specific embodiment of zinc distillation furnace provided by the present invention.
In figure, 1 is zinc outlet, and 2 is condensation chamber, and 3 is pumped vacuum systems, and 4 is charging aperture, and 5 is destilling tower, and 6 is distillery,
7 is plating cadmia material, and 8 is resistive heater, and 9 is slag-drip opening.
Specific embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
Core of the invention is to provide a kind of zinc distillation furnace, being capable of reducing energy consumption, reduction production cost.
Fig. 1 is refer to, Fig. 1 is the sectional view of the specific embodiment of zinc distillation furnace provided by the present invention.
In a kind of specific embodiment of zinc distillation furnace provided by the present invention, including distillery 6, destilling tower 5, the and of condensation chamber 2
Pumped vacuum systems 3, distillery 6, destilling tower 5 are sequentially connected with condensation chamber 2, and pumped vacuum systems 3 is communicated in condensation chamber 2, condensation chamber 2
Side be provided with zinc outlet 1, distillery 6 is provided with slag-drip opening 9 and charging aperture 4.Wherein, the quantity of destilling tower 5 can be according to reality
Border needs to be selected.
Distillery 6 is used to melt plating cadmia and makes iron aluminum slag, in practical operation, after plating cadmia material 7 melts, by charging
Mouth 4 is added directly into distillery 6, while adding a kind of slag former, makes slag former and foreign metal iron reactive aluminum in plating cadmia,
The iron aluminum slag of low melting point is generated, is separated with fused zinc.Metallic zinc becomes gaseous state zinc fume at high temperature, is gone into destilling tower 5 is interior
Except higher boiling metallic iron, metallic iron due to than it is great, boiling point is high and sinks to below liquid Zn, so that iron tramp can be from slag-drip opening
9 discharge out of the furnace.Clean zinc fume is cooled down into condensation chamber 2, is obtained liquid Zn and is released stove ingot casting from zinc outlet 1.Wherein, steaming
Evaporate and can be put into efficient slag former in room 6, to improve the separating effect of zinc and iron, make slag low containing zinc, improve the rate of recovery of zinc.
It can be seen that, this kind of zinc distillation furnace uses advanced slag making technology, while high temperature distillation zinc, forms iron aluminium impurity
Mobility slag and continuously exclude, continuous production can be realized, reduce the labour intensity of staff, improve iron and separated with zinc
Effect, distillation smelting furnace is arranged together with refining furnace, and energy consumption is relatively low in smelting process, and workshop floor space is smaller, metal
The rate of recovery is high, can save production cost, meanwhile, this kind of zinc distillation furnace burn out rate is relatively low, is easy to operation, with wide application
Prospect.
In above-described embodiment, distillery 6 can be located at U-shaped with condensation chamber 2 by the U-shaped pipeline communication of vertically-arranged, destilling tower 5
Among pipeline, be conducive to saving to take up room, and be prevented from during iron tramp ascends into condensation chamber 2 with zinc fume.Certainly, steam
Evaporating room 6 can also be by the pipeline communication of other shapes with condensation chamber 2.
In above-mentioned each embodiment, condensation chamber 2 is thermostatic chamber, to ensure condensation efficiency.Can specifically be set in condensation chamber 2
Thermocouple and controller are put, the temperature in condensation chamber 2 is observed and control.
In above-mentioned each embodiment, distillery 6 is provided with resistive heater 8, is easy to control the heating-up temperature of distillery 6
Precision, it is ensured that the accuracy of vapo(u)rizing temperature.Wherein, the quantity of resistive heater 8 can be selected according to actual needs.When
So, the setting not limited to this of the heater in distillery 6.
In above-mentioned each embodiment, pumped vacuum systems 3 can include vacuum degree measuring equipment, real-time monitoring condensation chamber 2
Vacuum, it is ensured that zinc fume enters the efficiency of condensation chamber 2.
Each embodiment is described by the way of progressive in this specification, and what each embodiment was stressed is and other
The difference of embodiment, between each embodiment identical similar portion mutually referring to.
Zinc distillation furnace provided by the present invention is described in detail above.Specific case used herein is to this hair
Bright principle and implementation method is set forth, the explanation of above example be only intended to help understand the method for the present invention and its
Core concept.It should be pointed out that for those skilled in the art, not departing from the premise of the principle of the invention
Under, some improvement and modification can also be carried out to the present invention, these are improved and modification also falls into the protection of the claims in the present invention
In the range of.
Claims (5)
1. a kind of zinc distillation furnace, it is characterised in that including distillery (6), destilling tower (5), condensation chamber (2) and pumped vacuum systems
(3), the distillery (6), the destilling tower (5) and the condensation chamber (2) are sequentially connected, pumped vacuum systems (3) connection
In the condensation chamber (2), the side of the condensation chamber (2) is provided with zinc outlet (1), and the distillery (6) is provided with slag-drip opening (9)
With charging aperture (4).
2. zinc distillation furnace according to claim 1, it is characterised in that the distillery (6) passes through with the condensation chamber (2)
The U-shaped pipeline communication of vertically-arranged, the destilling tower (5) is among the U-tube road.
3. zinc distillation furnace according to claim 1, it is characterised in that the condensation chamber (2) is thermostatic chamber.
4. zinc distillation furnace according to claim 1, it is characterised in that the distillery (6) is provided with resistive heater
(8)。
5. the zinc distillation furnace according to Claims 1-4 any one, it is characterised in that the pumped vacuum systems (3) includes
Vacuum degree measuring equipment.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611226650.3A CN106756094B (en) | 2016-12-27 | 2016-12-27 | Zinc distillation furnace |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611226650.3A CN106756094B (en) | 2016-12-27 | 2016-12-27 | Zinc distillation furnace |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106756094A true CN106756094A (en) | 2017-05-31 |
| CN106756094B CN106756094B (en) | 2018-10-23 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611226650.3A Active CN106756094B (en) | 2016-12-27 | 2016-12-27 | Zinc distillation furnace |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106756094B (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107460326A (en) * | 2017-10-10 | 2017-12-12 | 湖南金马有邻环保科技有限公司 | A kind of zinc-nickel skin continuous vacuum smelts retort |
| CN107457409A (en) * | 2017-10-10 | 2017-12-12 | 湖南金马有邻环保科技有限公司 | One kind plating cadmia melting continuously zinc powder furnace |
| CN110524002A (en) * | 2019-09-26 | 2019-12-03 | 湖南新威凌新材料有限公司 | A kind of environmental protection electric heating zinc powder furnace |
| CN112391068A (en) * | 2019-08-16 | 2021-02-23 | 烁元新材料(东营)股份有限公司 | Device for carrying out high-temperature treatment on carbon black in oxygen-free state |
| CN117230319A (en) * | 2023-11-14 | 2023-12-15 | 兴化市鹏鼎锌品厂 | Distillation method circulation extraction device for zinc material |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1145688A (en) * | 1967-06-16 | 1969-03-19 | Cie Metaux Doverpelt Lommel | Improvements in and relating to the purification of zinc by fractional distillation |
| CN101469372A (en) * | 2007-12-28 | 2009-07-01 | 鞍钢实业集团有限公司 | Method and apparatus for purifying zincilate |
| CN202415654U (en) * | 2011-12-31 | 2012-09-05 | 北京北矿锌业有限责任公司 | Distillation furnace for preparing high-purity zinc products directly by hot-galvanized slags |
| CN203751336U (en) * | 2014-02-27 | 2014-08-06 | 赵志强 | Device for producing nanoscale high-purity zinc powder through distillation method |
| CN206408276U (en) * | 2016-12-27 | 2017-08-15 | 湖南金马冶金技术开发有限公司 | Zinc distillation furnace |
-
2016
- 2016-12-27 CN CN201611226650.3A patent/CN106756094B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1145688A (en) * | 1967-06-16 | 1969-03-19 | Cie Metaux Doverpelt Lommel | Improvements in and relating to the purification of zinc by fractional distillation |
| CN101469372A (en) * | 2007-12-28 | 2009-07-01 | 鞍钢实业集团有限公司 | Method and apparatus for purifying zincilate |
| CN202415654U (en) * | 2011-12-31 | 2012-09-05 | 北京北矿锌业有限责任公司 | Distillation furnace for preparing high-purity zinc products directly by hot-galvanized slags |
| CN203751336U (en) * | 2014-02-27 | 2014-08-06 | 赵志强 | Device for producing nanoscale high-purity zinc powder through distillation method |
| CN206408276U (en) * | 2016-12-27 | 2017-08-15 | 湖南金马冶金技术开发有限公司 | Zinc distillation furnace |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107460326A (en) * | 2017-10-10 | 2017-12-12 | 湖南金马有邻环保科技有限公司 | A kind of zinc-nickel skin continuous vacuum smelts retort |
| CN107457409A (en) * | 2017-10-10 | 2017-12-12 | 湖南金马有邻环保科技有限公司 | One kind plating cadmia melting continuously zinc powder furnace |
| CN107457409B (en) * | 2017-10-10 | 2023-12-22 | 湖南金马冶金技术开发有限公司 | Zinc powder furnace for continuously smelting galvanized slag |
| CN112391068A (en) * | 2019-08-16 | 2021-02-23 | 烁元新材料(东营)股份有限公司 | Device for carrying out high-temperature treatment on carbon black in oxygen-free state |
| CN112391068B (en) * | 2019-08-16 | 2024-01-30 | 烁元新材料(东营)股份有限公司 | Device for carrying out high-temperature treatment on carbon black in anaerobic state |
| CN110524002A (en) * | 2019-09-26 | 2019-12-03 | 湖南新威凌新材料有限公司 | A kind of environmental protection electric heating zinc powder furnace |
| CN117230319A (en) * | 2023-11-14 | 2023-12-15 | 兴化市鹏鼎锌品厂 | Distillation method circulation extraction device for zinc material |
| CN117230319B (en) * | 2023-11-14 | 2024-02-09 | 兴化市鹏鼎锌品厂 | Distillation method circulation extraction device for zinc material |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106756094B (en) | 2018-10-23 |
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| TR01 | Transfer of patent right |
Effective date of registration: 20220303 Address after: 410000 room 1410, building 15, North Tower office building, Jinmao Plaza, fangmaoyuan (phase II), No. 1177, Huanhu Road, Tianding street, Yuelu District, Changsha City, Hunan Province Patentee after: Hunan ASMI Technology Co.,Ltd. Address before: 410015 complex building, No. 48, Xiaoguang Road, Yuhua District, Changsha City, Hunan Province Patentee before: HUNAN JINMA METALLURGICAL TECHNOLOGY DEVELOPMENT CO.,LTD. |
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| TR01 | Transfer of patent right | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Zinc distillation furnace Effective date of registration: 20230621 Granted publication date: 20181023 Pledgee: Hunan Ningxiang Rural Commercial Bank Co.,Ltd. Industrial Park sub branch Pledgor: Hunan ASMI Technology Co.,Ltd. Registration number: Y2023980045094 |
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| PE01 | Entry into force of the registration of the contract for pledge of patent right |