CN106750515A - A kind of rubber regeneration method - Google Patents

A kind of rubber regeneration method Download PDF

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Publication number
CN106750515A
CN106750515A CN201611135666.3A CN201611135666A CN106750515A CN 106750515 A CN106750515 A CN 106750515A CN 201611135666 A CN201611135666 A CN 201611135666A CN 106750515 A CN106750515 A CN 106750515A
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CN
China
Prior art keywords
rubber
regeneration method
reactor
slicing
stripping
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611135666.3A
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Chinese (zh)
Inventor
俞杨许
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Individual
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Individual
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Publication date
Application filed by Individual filed Critical Individual
Priority to CN201611135666.3A priority Critical patent/CN106750515A/en
Publication of CN106750515A publication Critical patent/CN106750515A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00Recovery or working-up of waste materials
    • C08J11/04Recovery or working-up of waste materials of polymers
    • C08J11/10Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • C08J11/12Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation by dry-heat treatment only
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00Recovery or working-up of waste materials
    • C08J11/04Recovery or working-up of waste materials of polymers
    • C08J11/10Recovery or working-up of waste materials of polymers by chemically breaking down the molecular chains of polymers or breaking of crosslinks, e.g. devulcanisation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2317/00Characterised by the use of reclaimed rubber
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/62Plastics recycling; Rubber recycling

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Processing Of Solid Wastes (AREA)
  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)

Abstract

The invention discloses a kind of rubber regeneration method, comprise the following steps:Waste old is selected first, cleaned successively, dried, stripping and slicing, pulverising step, then the rubber after crushing is placed in reactor and adds desulfurizing agent, stir so that reacting abundant, rubber is placed in cooling tower is again cooled down, rubber after cooling carries out compacting slice through the conche in moulding equipment, mill, is made reclaimed rubber finished product.The present invention has following advantages compared with prior art:The linear strand of rubber not being destroyed, feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, improving sizing material quality, non-environmental-pollution reduces the equipment requirement to producing, reduces production cost.

Description

A kind of rubber regeneration method
Technical field
The present invention relates to a kind of rubber regeneration method.
Background technology
Because world's oil resources are in short supply, all kinds of rubber prices are caused to rise steadily, therefore rationally using regenerated resources, drop Low production cost will be inevitable choice.The coming years, rubber sources is in short supply will always to perplex countries in the world, and China also formulates Strategy on recycling economy development, therefore rubber sources recycling also seems more and more important.
With the development of modern society, the increase of rubber-consumer amount, the yield of scrap rubber is also more and more, but waste and old rubber Glue has to pass through regeneration and can recycle, and regeneration causes that waste old is turned waste into wealth, and improves its use value.With the world Environmental consciousness is improved constantly, the outlet that all reclaimed rubbers for making softening agent with coal tar of publicity are all refused in the world.And China regenerates Glue producer is typically used with using common sizing material, product quality is lifted.Due to using coal tar in reclaimed rubber production process Used as softening agent, there is strong foul odour production scene to oil, there is very big pollution to environment.
Therefore, active demand now is had become to sub- rubber environmental protection regeneration techniques.
The content of the invention
It is an object of the invention to provide a kind of rubber regeneration method.
To reach above-mentioned purpose, the technical solution adopted by the present invention is:
A kind of rubber regeneration method, comprises the following steps:Waste old is selected first, is cleaned successively, dried, cut , then be placed in the rubber after crushing in reactor and desulfurizing agent is added by block, pulverising step, stirs so that reaction is filled Point, then rubber is placed in cooling tower is cooled down, the rubber after cooling is pressed through the conche in moulding equipment, mill Piece is made, reclaimed rubber finished product is made.
The relevant content of above-mentioned technical proposal is explained as follows:
In above-mentioned technical proposal, clean, dry, stripping and slicing, pulverising step are carried out at normal temperatures, it is in small, broken bits after rubber fineness extremely Below 40 mesh.
Preferably, at 250-600 DEG C, heating rate is 50-80 DEG C/h to the temperature control in reactor.
Preferably, it is additionally added softening agent in reactor.
Preferably, softening agent is aliphatic acid.
Because above-mentioned technical proposal is used, the present invention has following advantages compared with prior art:
The linear strand of rubber is not destroyed, and feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, improves sizing material Quality, non-environmental-pollution reduces the equipment requirement to producing, and reduces production cost.
Specific embodiment
Following embodiments are merely to illustrate the present invention, but can not limit protection scope of the present invention.
Embodiment 1
A kind of rubber regeneration method of the invention, comprises the following steps:Waste old is selected first, cleaned successively, Dry, stripping and slicing, pulverising step, clean, dry, stripping and slicing, pulverising step are carried out at normal temperatures, it is in small, broken bits after rubber fineness to 40 , then be placed in the rubber after crushing in reactor and desulfurizing agent is added by mesh, stirs so that reacting fully, in reactor Softening agent is additionally added, softening agent is aliphatic acid, the initial temperature in reactor is 250 DEG C, and heating rate is 80 DEG C/h, then rubber Glue is placed in cooling tower and is cooled down, and the rubber after cooling carries out compacting slice through the conche in moulding equipment, mill, system Into reclaimed rubber finished product, the linear strand of rubber is not destroyed, feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, Sizing material quality is improved, non-environmental-pollution reduces the equipment requirement to producing, reduces production cost.
Embodiment 2
A kind of rubber regeneration method of the invention, comprises the following steps:Waste old is selected first, cleaned successively, Dry, stripping and slicing, pulverising step, clean, dry, stripping and slicing, pulverising step are carried out at normal temperatures, it is in small, broken bits after rubber fineness to 35 , then be placed in the rubber after crushing in reactor and desulfurizing agent is added by mesh, stirs so that reacting fully, in reactor Softening agent is additionally added, softening agent is aliphatic acid, the initial temperature in reactor is 300 DEG C, and heating rate is 60 DEG C/h, then rubber Glue is placed in cooling tower and is cooled down, and the rubber after cooling carries out compacting slice through the conche in moulding equipment, mill, system Into reclaimed rubber finished product, the linear strand of rubber is not destroyed, feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, Sizing material quality is improved, non-environmental-pollution reduces the equipment requirement to producing, reduces production cost.
Embodiment 3
A kind of rubber regeneration method of the invention, comprises the following steps:Waste old is selected first, cleaned successively, Dry, stripping and slicing, pulverising step, clean, dry, stripping and slicing, pulverising step are carried out at normal temperatures, it is in small, broken bits after rubber fineness to 30 , then be placed in the rubber after crushing in reactor and desulfurizing agent is added by mesh, stirs so that reacting fully, in reactor Softening agent is additionally added, softening agent is aliphatic acid, the initial temperature in reactor is 400 DEG C, and heating rate is 55 DEG C/h, then rubber Glue is placed in cooling tower and is cooled down, and the rubber after cooling carries out compacting slice through the conche in moulding equipment, mill, system Into reclaimed rubber finished product, the linear strand of rubber is not destroyed, feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, Sizing material quality is improved, non-environmental-pollution reduces the equipment requirement to producing, reduces production cost.
Embodiment 4
A kind of rubber regeneration method of the invention, comprises the following steps:Waste old is selected first, cleaned successively, Dry, stripping and slicing, pulverising step, clean, dry, stripping and slicing, pulverising step are carried out at normal temperatures, it is in small, broken bits after rubber fineness to 25 , then be placed in the rubber after crushing in reactor and desulfurizing agent is added by mesh, stirs so that reacting fully, in reactor Softening agent is additionally added, softening agent is aliphatic acid, the initial temperature in reactor is 350 DEG C, and heating rate is 70 DEG C/h, then rubber Glue is placed in cooling tower and is cooled down, and the rubber after cooling carries out compacting slice through the conche in moulding equipment, mill, system Into reclaimed rubber finished product, the linear strand of rubber is not destroyed, feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, Sizing material quality is improved, non-environmental-pollution reduces the equipment requirement to producing, reduces production cost.
Embodiment 5
A kind of rubber regeneration method of the invention, comprises the following steps:Waste old is selected first, cleaned successively, Dry, stripping and slicing, pulverising step, clean, dry, stripping and slicing, pulverising step are carried out at normal temperatures, it is in small, broken bits after rubber fineness to 28 , then be placed in the rubber after crushing in reactor and desulfurizing agent is added by mesh, stirs so that reacting fully, in reactor Softening agent is additionally added, softening agent is aliphatic acid, the initial temperature in reactor is 600 DEG C, and heating rate is 50 DEG C/h, then rubber Glue is placed in cooling tower and is cooled down, and the rubber after cooling carries out compacting slice through the conche in moulding equipment, mill, system Into reclaimed rubber finished product, the linear strand of rubber is not destroyed, feeding and operation are safe, and environmental protection is tasteless, saves petroleum resources, Sizing material quality is improved, non-environmental-pollution reduces the equipment requirement to producing, reduces production cost.
The above embodiments merely illustrate the technical concept and features of the present invention, its object is to allow person skilled in the art Scholar will appreciate that present disclosure and implement according to this that it is not intended to limit the scope of the present invention.It is all according to the present invention The equivalent change or modification that Spirit Essence is made, should all be included within the scope of the present invention.

Claims (5)

1. a kind of rubber regeneration method, it is characterised in that comprise the following steps:Waste old is selected first, cleaned successively, Dry, stripping and slicing, pulverising step, then the rubber after crushing is placed in reactor and desulfurizing agent is added, stir so that Reaction is abundant, then rubber is placed in cooling tower is cooled down, and the rubber after cooling is through the conche in moulding equipment, mill Compacting slice is carried out, reclaimed rubber finished product is made.
2. a kind of rubber regeneration method according to claim 1, it is characterised in that:The cleaning, dry, stripping and slicing, crushing Step is carried out at normal temperatures, it is in small, broken bits after rubber fineness to 40 mesh below.
3. a kind of rubber regeneration method according to claim 1, it is characterised in that:Temperature control in the reactor exists 250-600 DEG C, heating rate is 50-80 DEG C/h.
4. a kind of rubber regeneration method according to claim 1, it is characterised in that:Softening is additionally added in the reactor Agent.
5. a kind of rubber regeneration method according to claim 4, it is characterised in that:The softening agent is aliphatic acid.
CN201611135666.3A 2016-12-09 2016-12-09 A kind of rubber regeneration method Pending CN106750515A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611135666.3A CN106750515A (en) 2016-12-09 2016-12-09 A kind of rubber regeneration method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201611135666.3A CN106750515A (en) 2016-12-09 2016-12-09 A kind of rubber regeneration method

Publications (1)

Publication Number Publication Date
CN106750515A true CN106750515A (en) 2017-05-31

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107488270A (en) * 2017-08-17 2017-12-19 安徽微威环保科技有限公司 A kind of scrap tire rubber regeneration technology

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102962907A (en) * 2012-10-29 2013-03-13 南通回力橡胶有限公司 Rubber regeneration process
CN103770244A (en) * 2013-11-25 2014-05-07 简玉君 Rubber regeneration technology
CN104610570A (en) * 2015-01-30 2015-05-13 柳州市中配橡塑配件制造有限公司 Regeneration method of rubber

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102962907A (en) * 2012-10-29 2013-03-13 南通回力橡胶有限公司 Rubber regeneration process
CN103770244A (en) * 2013-11-25 2014-05-07 简玉君 Rubber regeneration technology
CN104610570A (en) * 2015-01-30 2015-05-13 柳州市中配橡塑配件制造有限公司 Regeneration method of rubber

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107488270A (en) * 2017-08-17 2017-12-19 安徽微威环保科技有限公司 A kind of scrap tire rubber regeneration technology

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Application publication date: 20170531