CN106746647A - A kind of low temperature fast firing ceramic glaze and preparation method thereof - Google Patents

A kind of low temperature fast firing ceramic glaze and preparation method thereof Download PDF

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Publication number
CN106746647A
CN106746647A CN201611272314.2A CN201611272314A CN106746647A CN 106746647 A CN106746647 A CN 106746647A CN 201611272314 A CN201611272314 A CN 201611272314A CN 106746647 A CN106746647 A CN 106746647A
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CN
China
Prior art keywords
parts
ceramic glaze
low temperature
temperature fast
raw material
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Pending
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CN201611272314.2A
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Chinese (zh)
Inventor
周满仓
刘麟沛
周帅
闫留增
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Zhengzhou Optimal Ceramic Co Ltd
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Zhengzhou Optimal Ceramic Co Ltd
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Priority to CN201611272314.2A priority Critical patent/CN106746647A/en
Publication of CN106746647A publication Critical patent/CN106746647A/en
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    • CCHEMISTRY; METALLURGY
    • C03GLASS; MINERAL OR SLAG WOOL
    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81Coating or impregnation
    • C04B41/85Coating or impregnation with inorganic materials
    • C04B41/86Glazes; Cold glazes

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Structural Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

The invention discloses a kind of low temperature fast firing ceramic glaze, it is made up of the raw material of following weight portion:Useless 26 parts of porcelain powder, 8 12 parts of ball clay, 59 parts of pine tag soil, 15 25 parts of feldspar, 17 22 parts of porcelain stone, 0.1 0.3 parts of waterglass, 0.15 0.5 parts of alkali face, 7 13 parts of Jiaozhuo soil, 6 12 parts of quartz sand, 25 35 parts of kaolin;The present invention discloses the preparation method of low temperature fast firing ceramic glaze.Low temperature fast firing ceramic glaze proportioning of the present invention is creative, and raw material is cheap and easy to get, substantially reduces ceramic glaze product firing temperature and shortens firing period, energy-saving effect is notable, also energy consumption cost is largely reduced, manpower and resource is saved, the production cost further saved;The inventive method is simple, can be completed using existing instrument, is greatly saved Productive statistics, is adapted to promote the use of.

Description

A kind of low temperature fast firing ceramic glaze and preparation method thereof
Technical field
The invention belongs to ceramic glaze technical field, and in particular to a kind of low temperature fast firing ceramic glaze and preparation method thereof.
Background technology
From in terms of current world wide construction sanitary ceramic production of articles benefit cost ratio, fuel cost is shared in production cost Ratio is maximum, reaches more than 40% in the total energy consumption of various countries' ceramic industry.At present, global construction sanitary ceramic Industrial expansion is constantly subjected to the restriction of high energy consumption.Due to the price continuous rise of oily, electric, combustion gas and coal over nearly 20 years, Contain the development speed of ceramics.Really domestic many Ceramics Enterprises due to energy consumption cost it is high, cause product price Raise up, reduce the market competitiveness and also have some enterprises because energy prices raise up, it is impossible to undertake product cost higher and be on the point of Face bankruptcy;Some developed countries, some enterprises Cost Problems surging due to energy prices cannot be digested abroad, and gradually contract Small Production of Ceramics, or returned home to developing china and founded the factory as far as possible.
Existing ceramic glaze firing temperature is high, and what is carried also has firing time problem long, and domestic ceramic glaze layer burns till Cycle was needed for up to 40 hours, and low production efficiency is significant wastage to manpower and resource.Therefore firing temperature is reduced with contracting Short firing period is the certainty of ceramic glaze development.
The content of the invention
It is an object of the invention to provide a kind of low temperature fast firing ceramic glaze, while providing the preparation method of the ceramic glaze.
To achieve the above object, the present invention is adopted the following technical scheme that:
A kind of low temperature fast firing ceramic glaze, is made up of the raw material of following weight portion:Useless 2-6 parts of porcelain powder, ball clay 8-12 parts, pine tag It is native 5-9 parts, feldspar 15-25 parts, porcelain stone 17-22 parts, waterglass 0.1-0.3 parts, 0.15-0.5 parts of alkali face, 7-13 parts of Jiaozhuo soil, Quartz sand 6-12 parts, kaolin 25-35 parts.
Preferably, the low temperature fast firing ceramic glaze, is made up of the raw material of following weight portion:Useless 4 parts of porcelain powder, 10 parts of ball clay, pine 7 parts of hair soil, 20 parts of feldspar, 19 parts of porcelain stone, 0.21 part of waterglass, 0.24 part of alkali face, 10 parts of Jiaozhuo soil, 9 parts of quartz sand, kaolin 29 parts.
The preparation method of above-mentioned low temperature fast firing ceramic glaze, comprises the following steps:
(1) 200-300 mesh sieves are crossed after each raw material is crushed, ball mill ball milling is added after being then well mixed, added after ball milling Water stirs, and crosses 100-200 mesh sieves, except standby after iron;Wherein the abrasive media of ball mill is ballstone, ballstone, raw material, moisture Ratio be 1.5-3: 1-1.5: 1, ballstone particle diameter be 2-4 centimetres;
(2) by glaze slip even application to green compact top layer;Then enter kiln to be burnt till at 1000-1145 DEG C, firing period is 8- 10h。
Preferably, the thickness of ceramic glaze layer is 1-1.5mm in step (2).
Low temperature fast firing ceramic glaze proportioning of the present invention is creative, and raw material is cheap and easy to get, substantially reduces ceramic glaze product burning Significantly, energy consumption cost is also largely reduced, save manpower and money with firing period, energy-saving effect is shortened into temperature Source, the production cost further saved.
The inventive method is simple, can be completed using existing instrument, is greatly saved Productive statistics, and suitable popularization makes With.
Specific embodiment
With reference to embodiment, the present invention is further illustrated, but protection scope of the present invention is not limited to that.
Embodiment 1
A kind of low temperature fast firing ceramic glaze, is made up of the raw material of following weight portion:Useless 2 parts of porcelain powder, 8 parts of ball clay, pine tag soil 5 Part, 15 parts of feldspar, 17 parts of porcelain stone, 0.1 part of waterglass, 0.15 part of alkali face, 7 parts of Jiaozhuo soil, 6 parts of quartz sand, 25 parts of kaolin.
The preparation method of low temperature fast firing ceramic glaze, comprises the following steps:
(1) 200 mesh sieves are crossed after each raw material is crushed, ball mill ball milling is added after being then well mixed, added water after ball milling and stirred Mix uniform, cross 100 mesh sieves, except standby after iron;Wherein the abrasive media of ball mill is ballstone, and ballstone, raw material, the ratio of moisture are 1.5: 1.5: 1, ballstone particle diameter is 2-3 centimetres;
(2) by glaze slip even application to green compact top layer, the thickness of ceramic glaze layer is 1mm;Then enter kiln to be burnt at 1000 DEG C Into firing period is 10h.
Embodiment 2
A kind of low temperature fast firing ceramic glaze, it is characterised in that be made up of the raw material of following weight portion:Useless 6 parts of porcelain powder, ball clay 12 Part, 9 parts of pine tag soil, 25 parts of feldspar, 22 parts of porcelain stone, 0.3 part of waterglass, 0.5 part of alkali face, 13 parts of Jiaozhuo soil, 12 parts of quartz sand, height 35 parts of ridge soil.
The preparation method of low temperature fast firing ceramic glaze, comprises the following steps:
(1) 300 mesh sieves are crossed after each raw material is crushed, ball mill ball milling is added after being then well mixed, added water after ball milling and stirred Mix uniform, cross 200 mesh sieves, except standby after iron;Wherein the abrasive media of ball mill is ballstone, and ballstone, raw material, the ratio of moisture are 3: 1: 1, ballstone particle diameter is 3-4 centimetres;
(2) by glaze slip even application to green compact top layer, the thickness of ceramic glaze layer is 1.5mm;Then kiln is entered at 1145 DEG C Burn till, firing period is 8h.
Embodiment 3
A kind of low temperature fast firing ceramic glaze, is made up of the raw material of following weight portion:Useless 4 parts of porcelain powder, 10 parts of ball clay, pine tag soil 7 Part, 20 parts of feldspar, 19 parts of porcelain stone, 0.21 part of waterglass, 0.24 part of alkali face, 10 parts of Jiaozhuo soil, 9 parts of quartz sand, 29 parts of kaolin.
The preparation method of low temperature fast firing ceramic glaze, comprises the following steps:
(1) 250 mesh sieves are crossed after each raw material is crushed, ball mill ball milling is added after being then well mixed, added water after ball milling and stirred Mix uniform, cross 150 mesh sieves, except standby after iron;Wherein the abrasive media of ball mill is ballstone, and ballstone, raw material, the ratio of moisture are 2: 1.2: 1, ballstone particle diameter is 2-4 centimetres;
(2) by glaze slip even application to green compact top layer, the thickness of ceramic glaze layer is 1.2mm;Then kiln is entered at 1100 DEG C Burn till, firing period is 9h.
Embodiment 4
A kind of low temperature fast firing ceramic glaze, it is characterised in that be made up of the raw material of following weight portion:Useless 3 parts of porcelain powder, ball clay 11 Part, 8 parts of pine tag soil, 23 parts of feldspar, 18 parts of porcelain stone, 0.26 part of waterglass, 0.4 part of alkali face, 12 parts of Jiaozhuo soil, 7 parts of quartz sand, height 32 parts of ridge soil.
The preparation method of low temperature fast firing ceramic glaze, comprises the following steps:
(1) 280 mesh sieves are crossed after each raw material is crushed, ball mill ball milling is added after being then well mixed, added water after ball milling and stirred Mix uniform, cross 180 mesh sieves, except standby after iron;Wherein the abrasive media of ball mill is ballstone, and ballstone, raw material, the ratio of moisture are 2.5: 1.3: 1, ballstone particle diameter is 2-4 centimetres;
(2) by glaze slip even application to green compact top layer, the thickness of ceramic glaze layer is 1.4mm;Then kiln is entered at 1090 DEG C Burn till, firing period is 9.5h.
Embodiment 1-4 fires the every instruction of products obtained therefrom and is met the requirements by GB/T6952-2005 " sanitary ceramics " detections.

Claims (4)

1. a kind of low temperature fast firing ceramic glaze, it is characterised in that be made up of the raw material of following weight portion:Useless 2-6 parts of porcelain powder, ball clay 8- 12 parts, 5-9 parts of pine tag soil, feldspar 15-25 parts, porcelain stone 17-22 parts, waterglass 0.1-0.3 parts, 0.15-0.5 parts of alkali face, Jiaozhuo It is native 7-13 parts, quartz sand 6-12 parts, kaolin 25-35 parts.
2. a kind of low temperature fast firing ceramic glaze as claimed in claim 1, it is characterised in that be made up of the raw material of following weight portion: Useless 4 parts of porcelain powder, 10 parts of ball clay, 7 parts of pine tag soil, 20 parts of feldspar, 19 parts of porcelain stone, 0.21 part of waterglass, 0.24 part of alkali face, Jiaozhuo soil 10 parts, 9 parts of quartz sand, 29 parts of kaolin.
3. the preparation method of any described low temperature fast firing ceramic glazes of claim 1-2, it is characterised in that comprise the following steps: (1) 200-300 mesh sieves are crossed after each raw material is crushed, ball mill ball milling is added after being then well mixed, the stirring that added water after ball milling is equal It is even, 100-200 mesh sieves are crossed, except standby after iron;Wherein the abrasive media of ball mill is ballstone, and ballstone, raw material, the ratio of water are 1.5-3: 1-1.5: 1, ballstone particle diameter is 2-4 centimetres;
(2) glaze slip even application to green compact top layer is obtained into ceramic glaze layer;Then enter kiln to be burnt till at 1000-1145 DEG C, burn till Cycle is 8-10h.
4. the preparation method of low temperature fast firing ceramic glaze as claimed in claim 3, it is characterised in that in step (2), ceramic glaze layer Thickness be 1-1.5mm.
CN201611272314.2A 2016-12-30 2016-12-30 A kind of low temperature fast firing ceramic glaze and preparation method thereof Pending CN106746647A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1911855A (en) * 2006-08-17 2007-02-14 林伟河 Glaze coloured decoration daily use poocelain and its production method
CN103232222A (en) * 2013-05-16 2013-08-07 漳州汇宜陶瓷有限公司 Low-temperature stoneware formula
CN105924131A (en) * 2016-04-25 2016-09-07 福建科福材料有限公司 Slurry for craft ceramic and composition for preparation of slurry
CN106146043A (en) * 2016-07-07 2016-11-23 秦皇岛日福陶瓷有限公司 A kind of Bone China and sintering process thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1911855A (en) * 2006-08-17 2007-02-14 林伟河 Glaze coloured decoration daily use poocelain and its production method
CN103232222A (en) * 2013-05-16 2013-08-07 漳州汇宜陶瓷有限公司 Low-temperature stoneware formula
CN105924131A (en) * 2016-04-25 2016-09-07 福建科福材料有限公司 Slurry for craft ceramic and composition for preparation of slurry
CN106146043A (en) * 2016-07-07 2016-11-23 秦皇岛日福陶瓷有限公司 A kind of Bone China and sintering process thereof

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Application publication date: 20170531

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