CN106714341A - Open-type heater manufacturing method used for synchronous-radiation in-situ test - Google Patents
Open-type heater manufacturing method used for synchronous-radiation in-situ test Download PDFInfo
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- CN106714341A CN106714341A CN201611185802.XA CN201611185802A CN106714341A CN 106714341 A CN106714341 A CN 106714341A CN 201611185802 A CN201611185802 A CN 201611185802A CN 106714341 A CN106714341 A CN 106714341A
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- good heat
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- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
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Abstract
The invention discloses an open-type heater manufacturing method used for a synchronous-radiation in-situ test. Center areas of a front side wall and a rear side wall of a heater are embedded with slices so as to form thin sidewalls. A ray incidence hole and a ray outgoing hole are arranged on the thin sidewalls of the heater. An upper portion and a lower portion of a good heat conduction block of the heater are provided with a plurality of vent hole channels. According to the vent hole channels, through alternatively arranging ventilation channels between adjacent vent hole channel ports on a front end surface and a rear end surface, and using two end socket plugging blocks with flat surfaces to plug two end sockets of the good heat conduction block of the heater which is provided with the vent hole channels, the vent hole channels are unidirectionally connected. By using the method, connection among ventilation pipelines is convenient to realize, a flowing path and heating time of a gas in the good heat conduction block of the heater can be prolonged several times, and a sample heating rate and a highest temperature can be obviously increased; a thin sidewall sample chamber is realized, a condition that rays touch the heater so as to form an interference signal is avoided; and loading and unloading of the sidewalls of a sample chamber are convenient so that sample replacing operation is convenient and sample replacing time is greatly saved.
Description
Technical field
The invention belongs to synchrotron radiation in-situ test field, more particularly to a kind of opening for synchrotron radiation in-situ test
Formula heater preparation method.
Background technology
The existing device for synchronizing radiation in-situ test in a heated condition, is all placed in airtight cavity by sample
In, to ensure to isolate with air, realization in a heated condition prevents sample oxidized.But, it is this to use closed sample cavity
Synchrotron radiation test device have the following disadvantages：First, using the synchrotron radiation test device of closed sample cavity, because being penetrated
Linear window encapsulant resistant to elevated temperatures can not be limited, it is impossible to realize the miniaturization of synchrotron radiation in-situ testing device, give temperature control dress
Put in the installation at synchrotron radiation line station and test process applied stress, magnetic field etc. test parameter applying and control bring it is tired
It is difficult；Second, it is also not fully transparent to ray so far in order to realize that sample cavity is sealed, it is necessary to which ray window is sealed
Window material, window aperture seal material is inevitably produced to ray and absorbed and interference diffraction maximum；3rd, using closed sample
The synchrotron radiation test device in chamber, it is closed due to sample cavity, need to survey test device from line station when test sample is changed
Disassembled on examination platform, opening closed sample cavity could change sample, re-test device reinstalls the test of line station after changing sample
Platform, then re-start the alignment regulation of ray light path.The sample of this closed sample cavity synchrotron radiation test device changes behaviour
Not only make program very complicated, it is necessary to when wasting valuable machine very long, and be difficult to ensure that the strict of front and rear sample test condition
Unanimously.
Existing method makes open synchrotron radiation in-situ testing device can run into problems with：
Firstth, heating plate is set using side outer patch mode so that the half surface exposure of heating plate in atmosphere, is heated
The heat that piece is produced has nearly half to be slatterned in being dispersed into air, causes heating rate and the highest temperature that heater to be reached
Degree is all severely impacted；
Secondth, the entrance aperture of setting ray and the heater sidewall thickness of perforation hole is thicker, easily makes in test process
Ray encounters heater and causes interference with signal and be mixed into test signal；
3rd, manufacture difficulty is big, causes the gas passage quantity that can be set can only be in units, it is difficult to which guarantee is through flue
The gas temperature that road flows into sample cavity reaches heating deblocking temperature, limits the heating rate and maximum temperature of heater；
4th, fitted using two pieces of good heat-conducting blocks of heater, i.e., set in the good heat-conducting block medial surface of radiation-incident side heater
Put exposed coil-shape vent line, surveying the method that the good heat-conducting block of heater fits with diffraction makes heater, this method due to
It is required that closely sealed Area comparison is big, easy gas leakage, in addition, sample cavity only has single sided entry, is stopped by sample, can cause sample cavity
Non-uniform temperature, furthermore, heater sidewall thickness is blocked up, it is easy to allow ray to encounter heater.
In sum, there is problems with prior art：
1st, it is not easy to realize UNICOM between breather line, gas flows through distance and heated time in the good heat-conducting block of heater
Short, sample heating rate is slow, and maximum temperature is low；
2nd, ray touches heater and forms interference signal；
3rd, sample cavity side wall unloads inconvenience.
The content of the invention
It is an object of the invention to provide a kind of open heater preparation method for synchrotron radiation in-situ test, purport
Solve that prior art is present be not easy to realize breather line between UNICOM, gas flows through distance in the good heat-conducting block of heater
Short with heated time, sample heating rate is slow, and maximum temperature is low, and ray touches heater and forms interference signal, sample cavity side wall
Load and unload inconvenient problem.
The present invention is achieved in that a kind of open heater preparation method bag for synchrotron radiation in-situ test
Include：
In heater front side wall thin slice into thin sidewalls, ray entrance aperture 16 and ray outgoing is embedded in rear wall central area
Hole 9 is arranged on the thin sidewalls of heater；
In the upper and lower part of the good heat-conducting block 4 of heater, multiple vent caps 12, the vent cap 12, by preceding are set
The ventilation raceway groove between the port of adjacent vent holes road 12 is arranged alternately on end face and rear end face, and it is stifled with two pieces of terminations of surfacing
Block blocks two terminations of the good good heat-conducting block of heater of heating for being provided with vent cap, unidirectional UNICOM's vent cap 12；
Further, thin slice is flush-mounted in the good heat-conducting block 4 of heater of heater to ray and back reflection Xian Liangge center sides area
The inner side in domain constitutes heater sample cavity thin sidewalls, and the good heat-conducting block 4 of heater of heater is used to be embedded in the window size of thin slice
More than the size of the beam orifice opened up on thin slice, it is to avoid the ray touching good heat-conducting block of heater produces interference signal.
Further, it is identical with the material of the good heat-conducting block of heater for the thin slice material being embedded in.
Further, the thickness of setting-in thin slice is less than 0.5 millimeter, is embedded in thin slice towards the surface of sample and the good heat conduction of heater
The flush of sample cavity other positions in block.
Further, the diameter of vent cap is less than 2 millimeters, and vent cap is smaller than 1 millimeter.
Further, gas enters from air admission hole 1, unidirectionally flow through be arranged on it is logical in the good heat-conducting block 4 of the heater of heater
After stomata road 12 is heated, sample cavity 11, gas are entered from the stomata for being arranged on the upper side of sample cavity 11 and downside center
After heat is transmitted to sample by body contact sample, from ray entrance aperture 16, ray perforation hole 9 and the left port of sample cavity 11 and right output port
Outflow.
Further, several heating plates inserting groove is set in the top of the good heat-conducting block 4 of heater of heater, bottom
10, heating plate inserting groove 10 is arranged in the good heat-conducting block 4 of heater, is around provided with vent cap 12.
Further, sample cavity 11 is provided with the middle of the good heat-conducting block of heater, the heater of composition sample cavity trailing flank is good to lead
Hot block is easy to handling.
Further, the inside of the good heat-conducting block of heater is provided with breather line, can conduct the heat of the good heat-conducting block of heater
To the gas in breather line.Heated gas flows into sample cavity by the venthole for being arranged on breather line end.
Further, heating plate is fitted with the good heat-conducting block of heater, sample is controlled by the heating power for adjusting heating plate
The temperature of sample in product chamber, the temperature of sample is by being close to the thermocouple monitoring of sample.
Further, sample cavity 11 is the rectangle sample chamber of left and right opening, and the sample for in-situ test can be passed freely through
Sample cavity 11, it is possible to which tensile stress is applied by the sample termination for extending sample cavity 11 from left and right opening.
Further, the sample cavity rear wall for being embedded with the thin sidewalls for setting ray perforation hole can be loaded and unloaded easily.
Further, heated through breather line, the gas for flowing into sample cavity by breather line end venthole is inert gas,
Beam orifice and left and right are opened from before and after sample cavity after being contacted with sample through the heating and continuous inert gas for flowing into sample cavity of breather line
Mouthful outflow, protects sample while being heated to sample, prevents sample and air contact and aoxidizes.
Further, ray entrance aperture 16 and ray perforation hole 9, ray are opened up on heating plate and the good heat-conducting block 4 of heater
Perforation hole 9 is horn opening, and 120 ° are more than towards the horn flare angle of ray exit direction.
Compared to existing technology, the present invention has the advantage that：
1. UNICOM between breather line is easy to implement, distance can be flowed through in the good heat-conducting block of heater with several times extension gas
And heated time, hence it is evident that lifting sample heating rate and maximum temperature；
2. thin sidewalls sample cavity is realized, it is to avoid ray touches heater and forms interference signal；
3. sample cavity side wall unloads convenient, significantly facilitates sample replacement operation, saves significantly on the time of sample replacing.
Brief description of the drawings
Fig. 1 is the open heater schematic diagram for synchrotron radiation in-situ test provided in an embodiment of the present invention；
Fig. 2 is each part of the open heater for synchrotron radiation in-situ test provided in an embodiment of the present invention
Structure explosion diagram；
Fig. 3 is the heating heater of the open heater for synchrotron radiation in-situ test provided in an embodiment of the present invention
Good heat-conducting block and the good heat-conducting block schematic diagram of sample cavity trailing flank heater；
Fig. 4 is the heating heater of the open heater for synchrotron radiation in-situ test provided in an embodiment of the present invention
Good heat-conducting block and front/rear end schematic diagram；
Fig. 5 is the center cross-sectional of the open heater for synchrotron radiation in-situ test provided in an embodiment of the present invention
Profile；
Fig. 6 is the center longitudinal section of the open heater for synchrotron radiation in-situ test provided in an embodiment of the present invention
Profile；
In figure：1st, air admission hole；2nd, the first screw hole；3rd, the first sealing end block；4th, the good heat-conducting block of heater；5th, the second sealing
End block；6th, the second screw hole；7th, sample cavity back side panel；8th, thin sidewalls after sample cavity；9th, ray perforation hole；10th, heating plate inserting
Groove；11st, sample cavity；12nd, vent cap；13rd, ventilation groove；14th, the passage of UNICOM's vent cap end and sample cavity；
15th, thin sidewalls before sample cavity；16th, ray entrance aperture.
Specific embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Structure of the invention is explained in detail below in conjunction with the accompanying drawings.
Refer to Fig. 1 to Fig. 6：
A kind of open heater preparation method for synchrotron radiation in-situ test, including：
In heater front side wall thin slice into thin sidewalls, ray entrance aperture 16 and ray outgoing is embedded in rear wall central area
Hole 9 is arranged on the thin sidewalls of heater；
In the upper and lower part of the good heat-conducting block 4 of heater, multiple vent caps 12, the vent cap 12, by preceding are set
The ventilation raceway groove between the port of adjacent vent holes road 12 is arranged alternately on end face and rear end face, and it is stifled with two pieces of terminations of surfacing
Block blocks two terminations of the good good heat-conducting block of heater of heating for being provided with vent cap, unidirectional UNICOM's vent cap 12；
Further, thin slice is flush-mounted in the good heat-conducting block 4 of heater of heater to ray and back reflection Xian Liangge center sides area
The inner side in domain constitutes heater sample cavity thin sidewalls, and the good heat-conducting block 4 of heater of heater is used to be embedded in the window size of thin slice
More than the size of the beam orifice opened up on thin slice, it is to avoid the ray touching good heat-conducting block of heater produces interference signal.
Further, it is identical with the material of the good heat-conducting block of heater for the thin slice material being embedded in.
Further, the thickness of setting-in thin slice is less than 0.5 millimeter, is embedded in thin slice towards the surface of sample and the good heat conduction of heater
The flush of sample cavity other positions in block.
Further, the diameter of vent cap is less than 2 millimeters, and vent cap is smaller than 1 millimeter.
Further, gas enters from air admission hole 1, unidirectionally flow through be arranged on it is logical in the good heat-conducting block 4 of the heater of heater
After stomata road 12 is heated, sample cavity 11, gas are entered from the stomata for being arranged on the upper side of sample cavity 11 and downside center
After heat is transmitted to sample by body contact sample, from ray entrance aperture 16, ray perforation hole 9 and the left port of sample cavity 11 and right output port
Outflow.
Further, several heating plates inserting groove is set in the top of the good heat-conducting block 4 of heater of heater, bottom
10, heating plate inserting groove 10 is arranged in the good heat-conducting block 4 of heater, is around provided with vent cap 12.
Further, sample cavity 11 is provided with the middle of the good heat-conducting block of heater, the heater of composition sample cavity trailing flank is good to lead
Hot block is easy to dismounting.
Further, the inside of the good heat-conducting block of heater is provided with breather line, can conduct the heat of the good heat-conducting block of heater
To the gas in breather line.Heated gas flows into sample cavity by the venthole for being arranged on breather line end.
Further, heating plate is fitted with the good heat-conducting block of heater, sample is controlled by the heating power for adjusting heating plate
The temperature in the hot chamber of product.The temperature of sample cavity is by being close to the thermocouple monitoring of sample.
Further, sample cavity 11 is the rectangular cross section sample cavity of left and right opening, and the sample for in-situ test can be certainly
By through sample cavity 11, it is possible to apply tensile stress by the sample termination for extending sample cavity 11 from left and right opening.
Further, heated through breather line, the gas for flowing into sample cavity by breather line end venthole is inert gas,
Beam orifice and left and right are opened from before and after sample cavity after being contacted with sample through the heating and continuous inert gas for flowing into sample cavity of breather line
Mouthful outflow, protects sample while being heated to sample, prevents sample and air contact and aoxidizes.
Further, ray entrance aperture 16 and ray perforation hole 9, ray are opened up on heating plate and the good heat-conducting block 4 of heater
Perforation hole 9 is horn opening, and 120 ° are more than towards the horn flare angle of ray exit direction.
The embodiment of the present invention is made up the open heater for synchrotron radiation X RD in-situ tests of following steps：
Take one piece of length and width, the high good heat-conducting block of good heater (such as copper billet) for being respectively 100mm, 50mm and 30mm, by itself plus
Work is into profile as shown in left in Figure 3.
(1) heating plate that 6 cross sections as shown in fig. 1 are 12mm × 1.3mm rectangles is made with line cutting technology to insert
Groove 10.
(2) as shown in Figure 4 and Figure 5,60 insertions that spaced 1mm apertures are 1mm are made with electric spark cheesing techniques
Vent cap 12.Near the vent cap length 52mm of sample cavity, end is in the good heat-conducting block middle part of heater.
(3) as shown in Figure 4, handed over metal finishing impression fabrication techniques on good former and later two end faces of heat-conducting block 4 of heater respectively
For the deep 1.5mm in UNICOM's adjacent vent holes road, the ventilation groove 13 of 0.8mm wide.
(4) as shown in Figure 4, making 6 on good former and later two end faces of heat-conducting block 4 of heater respectively is used to fasten first
Sealing end block 3, second seals the first screw hole 2 of end block 5.
(5) it is wide as shown in figure 4, making 8mm long with line cutting technology in the good leading flank central area of heat-conducting block 4 of heater
The window for being embedded in sample cavity thin sidewalls of 6mm, and continue to use metal finishing impression fabrication techniques in the edge of window by sample cavity side
For being embedded in the groove of sample cavity thin sidewalls, and it is embedded in thin sidewalls 15 before sample cavity.
(6) passage of UNICOM's sample cavity and the vent cap 12 is being made near sample cavity vent cap end.
(7) as shown in figure 1, making the second screw hole 6 for fixing sample cavity back side panel 7.
(8) the sample cavity back side panel 7 as shown in Fig. 3 right figures is made with line cutting technology.
(9) same to step (5) is made for being embedded in the groove of sample cavity thin sidewalls, and is embedded in thin after the thick sample cavities of 0.2mm
Side wall 8.
(10) the good front and rear end of heat-conducting block 4 of polishing heater.
(11) the first sealing end block 3 and second shown in Fig. 1 and Fig. 2 is made of line cutting technology and seals end block 5, set the
One screw hole 2 and air admission hole 1, and polished end faces.
(12) by the first sealing sealing of end block 3 and second end block 5 respectively with fastened by screw before and after the good heat-conducting block 4 of heater
End face, loads onto suction nozzle.
(13) sample cavity back side panel 7 is loaded onto, heating sheet type piece is inserted in heating plate slot.
(14) as shown in figure 5, in preceding thin sidewalls center, the ray entrance aperture 16 of a diameter of 1mm is processed, rear thin
Side wall center, processes the ray perforation hole 9 of inside diameter 2mm.Connection is set between vent cap 12 and sample cavity 11
Way vent hole road end and the passage 14 of sample cavity.
(15) insert thermocouple from sample cavity port and thermocouple is close to sample.By thermocouple and heating plate connection temperature control
Instrument, just can realize the control of sample temperature.
(16) heater is installed to the experiment porch at synchrotron radiation line station, sample passes through sample cavity 11, then is stretching out sample
The sample two ends in product chamber 11 apply tensile stress.Then ray is made to be injected by beam orifice entrance aperture 16, you can to carry out stress
Under sample heating process synchrotron radiation measurement.
Compared to existing technology, the present invention has the advantage that：
1. UNICOM between breather line is easy to implement, distance can be flowed through in the good heat-conducting block of heater with several times extension gas
And heated time, hence it is evident that lifting sample heating rate and maximum temperature：Skill is prepared using existing open synchrotron radiation heater
Art is difficult to realize more than the 5 unidirectional UNICOMs of vent cap, can only typically realize 3 unidirectional UNICOMs of vent cap so that gas
Body flows through the path that heat block is heated before sample cavity is flowed into and the time is extremely limited.In addition, existing open synchrotron radiation adds
Heating plate is mounted on heater lateral surface by hot device technology of preparing, and the heating quantity that on the one hand can be mounted is few, typically can only be one
Individual side mounts a piece of heating plate；On the other hand, a side of heating plate is exposed outside, and the heat of nearly half is dispersed into
In air, the heat utilization ratio that heating plate is produced is low.Above reason causes prior art to make open synchrotron radiation heater
Heating rate and the maximum temperature that can be reached are extremely limited, are difficult to realize more than 50 degrees/min of heating rate and reach 700 DEG C
Temperature above.And more than the 10 unidirectional UNICOMs of vent cap, such as the present embodiment are easily achieved using the technology of the present invention,
Realize 30 unidirectional UNICOMs of vent cap so that gas flows through path and heated time in the good heat-conducting block of heater is heated
More than 3 times of extension, meanwhile, be embedded in heating plate in the heating good heat-conducting block of heater using setting-in groove by the technology of the present invention, plus
The heat that backing is produced almost 100% is absorbed by the good heat-conducting block of heater, and using the technology of the present invention can be embedded in it is multiple plus
Backing, such as the present embodiment have been embedded in 6 heating plates.Above reason causes the liter that the present invention is easily achieved more than 100 degrees/min
Warm speed and more than 900 DEG C of temperature, the present embodiment can reach 200 degrees/min of heating rate and 1000 DEG C of the highest temperature
Degree.
2. thin sidewalls sample cavity is realized, it is to avoid ray touches heater and forms interference signal；Prior art prepares open
The sidewall thickness of synchrotron radiation heater is typically greater than 5mm, and the technology of the present invention can drop to less than sidewall thickness
0.5mm, such as the present embodiment only have 0.2mm, solve well because sidewall thickness is excessive make ray pass through beam orifice when it is easy
Touch the problem of sample cavity.
3. sample cavity side wall unloads convenient, significantly facilitates sample replacement operation, saves significantly on the time of sample replacing：It is existing
The open synchrotron radiation heater of fabrication techniques is typically employed in one piece of good heat conduction and processes, and can not be beaten when changing sample
Sample cavity is opened, and uses the open synchrotron radiation heater back side panel that the technology of the present invention makes conveniently to load and unload, significantly facilitated
Sample replacement operation.
Presently preferred embodiments of the present invention is the foregoing is only, is not intended to limit the invention, it is all in essence of the invention
Any modification, equivalent and improvement made within god and principle etc., should be included within the scope of the present invention.
Claims (9)
1. a kind of open heater preparation method for synchrotron radiation in-situ test, it is characterised in that described for synchronization
The open heater preparation method for radiating in-situ test includes：
Thin slice into thin sidewalls is embedded in heater front side wall and rear wall central area, ray entrance aperture and ray perforation hole are set
On the thin sidewalls of heater；
Multiple vent caps are set in the upper and lower part of the good heat-conducting block of heater, the vent cap is by front end face and rear end
The ventilation raceway groove between adjacent vent holes road port is arranged alternately on face, and is blocked with the termination sprue of two pieces of surfacings and is provided with logical
Two terminations of the good heat-conducting block of heater in stomata road, unidirectional UNICOM's vent cap.
2. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that thin
The good heat-conducting block of heater that piece is flush-mounted in heater constitutes heater to the inner side in two center side regions of ray and back reflection line
Sample cavity thin sidewalls, the good heat-conducting block of heater of heater is used to be embedded in the window size of thin slice more than the ray opened up on thin slice
The size in hole, it is to avoid the ray touching good heat-conducting block of heater produces interference signal.
3. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that used
It is identical with the material of the good heat-conducting block of heater in the thin slice material of setting-in.
4. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that embedding
The thickness for filling thin slice is less than 0.5 millimeter, is embedded in thin slice towards other positions of sample cavity in the surface of sample and the good heat-conducting block of heater
The flush put.
5. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that logical
The diameter in stomata road is less than 2 millimeters, and vent cap is smaller than 1 millimeter.
6. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that gas
Body enters from air admission hole, unidirectionally flows through after the vent cap that is arranged in the good heat-conducting block of the heater of heater is heated, from setting
Put the stomata in sample cavity upper side and downside center and enter sample cavity, heat is transmitted to sample by gas contact sample
Afterwards, flowed out from ray entrance aperture, ray perforation hole and sample cavity left port and right output port.
7. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that
The top of the good heat-conducting block of heater of heater, bottom set several heating plates inserting groove, and heating plate inserting groove is set
In the good heat-conducting block of heater, vent cap is around provided with.
8. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that
Sample cavity is provided with the middle of the good heat-conducting block of heater, the inside of the good heat-conducting block of heater is provided with breather line, in the good heat conduction of heater
Heating plate is fitted with block.
9. the open heater preparation method of synchrotron radiation in-situ test is used for as claimed in claim 1, it is characterised in that sample
Product chamber is the rectangular cross section sample cavity of left and right opening, and the sample for in-situ test can pass freely through sample cavity, by from
The sample termination that sample cavity is extended in left and right opening applies tensile stress.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611185802.XA CN106714341B (en) | 2016-12-21 | 2016-12-21 | Manufacturing method of open heater for synchrotron radiation in-situ test |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611185802.XA CN106714341B (en) | 2016-12-21 | 2016-12-21 | Manufacturing method of open heater for synchrotron radiation in-situ test |
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| Publication Number | Publication Date |
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| CN106714341A true CN106714341A (en) | 2017-05-24 |
| CN106714341B CN106714341B (en) | 2020-04-21 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102589964A (en) * | 2012-02-15 | 2012-07-18 | 中国科学院上海应用物理研究所 | Heating device |
| CN105021469A (en) * | 2015-07-10 | 2015-11-04 | 中山大学 | In-situ mechanical property testing device of nuclear material in high temperature irradiation simulation environment |
| CN105263198A (en) * | 2015-10-10 | 2016-01-20 | 浙江师范大学 | Open heating device for synchrotron radiation in-situ test |
| CN105445191A (en) * | 2015-11-30 | 2016-03-30 | 中国科学院长春应用化学研究所 | Multi-channel in-situ measurement atmosphere pool |
| CN205719980U (en) * | 2016-04-26 | 2016-11-23 | 东北大学 | A kind of electrochemical in-situ raman spectroscopy measurement microscopic heating stand and sample cell system |
-
2016
- 2016-12-21 CN CN201611185802.XA patent/CN106714341B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102589964A (en) * | 2012-02-15 | 2012-07-18 | 中国科学院上海应用物理研究所 | Heating device |
| CN105021469A (en) * | 2015-07-10 | 2015-11-04 | 中山大学 | In-situ mechanical property testing device of nuclear material in high temperature irradiation simulation environment |
| CN105263198A (en) * | 2015-10-10 | 2016-01-20 | 浙江师范大学 | Open heating device for synchrotron radiation in-situ test |
| CN105445191A (en) * | 2015-11-30 | 2016-03-30 | 中国科学院长春应用化学研究所 | Multi-channel in-situ measurement atmosphere pool |
| CN205719980U (en) * | 2016-04-26 | 2016-11-23 | 东北大学 | A kind of electrochemical in-situ raman spectroscopy measurement microscopic heating stand and sample cell system |
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| CN106714341B (en) | 2020-04-21 |
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