CN106706687A - Distributed type X-ray diffraction measurement system - Google Patents
Distributed type X-ray diffraction measurement system Download PDFInfo
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- CN106706687A CN106706687A CN201611162677.0A CN201611162677A CN106706687A CN 106706687 A CN106706687 A CN 106706687A CN 201611162677 A CN201611162677 A CN 201611162677A CN 106706687 A CN106706687 A CN 106706687A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/20—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by using diffraction of the radiation by the materials, e.g. for investigating crystal structure; by using scattering of the radiation by the materials, e.g. for investigating non-crystalline materials; by using reflection of the radiation by the materials
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- General Health & Medical Sciences (AREA)
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- Analysing Materials By The Use Of Radiation (AREA)
Abstract
The invention discloses a distributed type X-ray diffraction measurement system which comprises at least two X-ray diffractometers and a wireless intelligent terminal, wherein the wireless intelligent terminal is loaded with analysis processing software; each X-ray diffractometer and other X-ray diffractometers are independent from each other; the X-ray diffractometers are used for acquiring X-ray diffraction diagrams in local positions; the wireless intelligent terminal is used for processing data in a remote position via the analysis processing software; the X-ray diffractometers are connected with the wireless intelligent terminal via a conversion device; the conversion device is internally provided with a WIFI (Wireless Fidelity) modules and a main controller; the wireless intelligent terminal is internally provided with a wireless network card; the WIFI module is matched with the wireless network card; the WIFI module and the wireless network card are in point-to-point connection or the WIFI module is connected with a wireless local network into which the wireless network card is accessed; after being converted by the conversion device, the X-ray diffraction diagram acquired by using the X-ray diffractometers is transmitted to the wireless intelligent terminal. By adopting the distributed type X-ray diffraction measurement system, remote monitoring on the X-ray diffractometers is achieved for a first time, the experiment efficiency is improved, the experiment cost is lowered, a system is simplified, and the operation difficulties are alleviated.
Description
Technical field
The present invention relates to measuring apparatus field, more particularly to a kind of distributed X-ray diffraction measurement system.
Background technology
X-ray diffractometer is a kind of large-scale physical testing analytical instrument, material phase analysis can be carried out, mainly by X-ray light
Several parts such as source, diffracted signal detecting system and data processing and printing chart system are constituted.
Existing X-ray diffractometer is commonly configured with microcomputer assistant experiment system, micro- meter to carry out data processing
Calculation machine assistant experiment system is typically connected by cable, and equipment cost is high and not readily portable, while staff must be in reality
Test room to be processed, it is impossible to remote operation.And, a microcomputer cannot simultaneously control many X-ray diffractometers, for needing
The sample to measure simultaneously for simultaneously, it is necessary to which many people are operated, and required experimenter is more, wastes time and energy, experiment
Inefficient, while increasing experimental facilities input, financial cost is higher.
The content of the invention
The technical problems to be solved by the invention are the drawbacks described above for overcoming prior art to exist, there is provided one kind can be simultaneously
The many controls of X-ray diffractometer of intelligent wireless terminal-pair are realized, so as to realize accurately to various samples while being analyzed inspection
The distributed X-ray diffraction measurement system of survey.
The technical solution adopted for the present invention to solve the technical problems is that a kind of distributed X-ray diffraction measurement system is wrapped
At least two X-ray diffractometers and an intelligent wireless terminal are included, the intelligent wireless terminal carries interpretation software, each
Separate between X-ray diffractometer and other X-ray diffractometers, the X-ray diffractometer obtains X-ray and spreads out in local position
Figure is penetrated, the intelligent wireless terminal is processed in remote location by interpretation software, the X-ray diffractometer is by turning
Changing device connects intelligent wireless terminal, and WIFI module and master control are provided with the conversion equipment, is set in the intelligent wireless terminal
There is wireless network card, the WIFI module is adapted with wireless network card, WIFI module and wireless network card point-to-point connection or WIFI moulds
Block is connected in the WLAN of wireless network card access, the converted device of X-ray diffractogram that the X-ray diffractometer is obtained
Transmitted after forwarding to intelligent wireless terminal, and be stored in intelligent wireless terminal, the MAC that intelligent wireless terminal passes through WIFI module
The built-in equipment Serial Number of address, master control or master control read toggle switch status devices number to recognize X-ray diffractogram source, then
Serial calculating is carried out by interpretation software, result is obtained eventually through peak-seeking algorithm.
Further, the X-ray diffractometer is provided with USB port, and the conversion equipment passes through USB port and X-ray diffractometer
Master control connection, the master control connects WIFI module.
Further, the X-ray diffractometer is provided with RS232 serial ports, and the conversion equipment also includes RS232 modules and electricity
Flat modular converter, the RS232 modules connect level switch module, and the level switch module connects master control, and the master control connects
WIFI module is connect, the X-ray diffractometer is connected by RS232 serial ports with RS232 modules.
Further, the level switch module is 232 electrical level transferring chips.
Further, the intelligent wireless terminal is hand-hold wireless intelligent terminal, and hand-hold wireless intelligent terminal is smart mobile phone
Or panel computer.
Compared with prior art, the invention has the advantages that：Intelligent wireless terminal-pair X-ray diffraction is realized first
The monitoring of instrument, realizes remote operation, has liberated manpower, and original cable port is wirelessly transferred by changing realization；Meanwhile,
Realize a people and control monitoring and the multiple samples for the treatment of simultaneously, substantially reduce manpower consumption, the X-ray for conveniently transferring acquisition is spread out
Figure is penetrated, it is convenient to consult, it is easy to be analyzed the X-ray diffractogram for obtaining, conventional efficient is improved, shorten analyzing and processing
Time；System is simplified, instrument cost is reduced, operation difficulty is reduced, for the operation of staff is provided conveniently.
Brief description of the drawings
Fig. 1 is the composition figure of the embodiment of distribution X-ray diffraction measurement system one of the invention；
Fig. 2 is the connection of the distributed X-ray diffractometer and intelligent wireless terminal of the distributed X-ray diffraction measurement system of Fig. 1
Figure；
Fig. 3 is the distributed X-ray diffractometer and intelligent wireless of distribution X-ray diffraction measurement another embodiment of system of the invention
The connection figure of terminal.
Specific embodiment
To make the object, technical solutions and advantages of the present invention clearer, below in conjunction with accompanying drawing to embodiment party of the present invention
Formula is further described.
Embodiment 1
Refer to Fig. 1 and Fig. 2, an embodiment of present invention distribution X-ray diffraction measurement system, including three X-ray diffractions
Instrument 1 and an intelligent wireless terminal 2, intelligent wireless terminal 2 carry interpretation software, each X-ray diffractometer 1 and other X
Separate between x ray diffractometer x 1, X-ray diffractometer 1 obtains X-ray diffractogram, intelligent wireless terminal 2 in local position
Processed by interpretation software in remote location, the X-ray diffractometer 1 connects intelligent wireless by conversion equipment 3
It is provided with terminal 2, conversion equipment 3 in WIFI module 3-1 and master control 3-2, intelligent wireless terminal 2 and is provided with wireless network card 2-1,
WIFI module 3-1 is adapted with wireless network card 2-1, WIFI module 3-1 and wireless network card 2-1 point-to-point connections or WIFI module 3-
1 is connected in the WLAN of wireless network card 2-1 accesses, the converted device of X-ray diffractogram that X-ray diffractometer 1 is obtained
Transmitted to intelligent wireless terminal 2 after 3 conversions, and be stored in intelligent wireless terminal 2, intelligent wireless terminal 2 passes through WIFI module
The MAC Address of 3-1, master control 3-2 built-in equipment Serial Number or master control 3-2 read toggle switch status devices number and penetrate recognizing X
Ray diffraction diagram is originated, then carries out serial calculating by interpretation software, and result is obtained eventually through peak-seeking algorithm.
Port 1-1 on X-ray diffractometer 1 is USB port, the master control that conversion equipment 3 passes through USB port and X-ray diffractometer 1
3-2 is connected, the master control 3-2 connection WIFI modules 3-1；WIFI module 3-1 is TLN13UA06 chips, and master control 3-2 is
STM32F103 chips, intelligent wireless terminal 2 is smart mobile phone.
The course of work：The detection unit of X-ray diffractometer 1 obtains X-ray diffractogram by detecting sample, then by USB
Signal switchs to transmission of wireless signals by conversion equipment 3, and USB connection transfer devices 3 are controlled by the master control 3-2 in conversion equipment 3
The WIFI module 3-1 of system is transmitted, and is sent by the WIFI antennas on WIFI module 3-1, due to being set in intelligent wireless terminal 2
There are the wireless network card 2-1 being adapted with WIFI module 3-1, WIFI module 3-1 and wireless network card 2-1 point-to-point connections or WIFI moulds
Block 3-1 is connected in the WLAN of wireless network card 2-1 accesses, and the X-ray diffractogram that X-ray diffractometer 1 is obtained is converted
Device 3 is transmitted to intelligent wireless terminal 2 after changing, and is stored in intelligent wireless terminal 2, and intelligent wireless terminal 2 passes through WIFI
The MAC Address of module 3-1, master control 3-2 built-in equipment Serial Number or master control 3-2 read toggle switch status devices number to recognize
X-ray diffractogram is originated, then carries out serial calculating by interpretation software, and result is obtained eventually through peak-seeking algorithm.
The monitoring of intelligent wireless terminal-pair X-ray diffractometer is realized first, remote operation is realized, and has liberated manpower, will
Original cable port is wirelessly transferred by changing realization；Meanwhile, realize a people and control monitoring and the multiple samples for the treatment of simultaneously,
Manpower consumption is substantially reduced, the X-ray diffractogram of acquisition is conveniently transferred, it is convenient to consult, it is easy to the X-ray diffractogram to obtaining
It is analyzed, improves conventional efficient, shortens the analyzing and processing time；System is simplified, instrument cost is reduced, reduced
Operation difficulty, for the operation of staff is provided conveniently.
Embodiment 2
Refer to Fig. 1 and Fig. 3, an embodiment of present invention distribution X-ray diffraction measurement system, including three X-ray diffractions
Instrument 1 and an intelligent wireless terminal 2, intelligent wireless terminal 2 carry interpretation software, each X-ray diffractometer 1 and other X
Separate between x ray diffractometer x 1, X-ray diffractometer 1 obtains X-ray diffractogram, intelligent wireless terminal 2 in local position
Processed by interpretation software in remote location, the X-ray diffractometer 1 connects intelligent wireless by conversion equipment 3
It is provided with terminal 2, conversion equipment 3 in WIFI module 3-1 and master control 3-2, intelligent wireless terminal 2 and is provided with wireless network card 2-1,
WIFI module 3-1 is adapted with wireless network card 2-1, WIFI module 3-1 and wireless network card 2-1 point-to-point connections or WIFI module 3-
1 is connected in the WLAN of wireless network card 2-1 accesses, the converted device of X-ray diffractogram that X-ray diffractometer 1 is obtained
Transmitted to intelligent wireless terminal 2 after 3 forwardings, and be stored in intelligent wireless terminal 2, intelligent wireless terminal 2 passes through WIFI module
The MAC Address of 3-1, master control 3-2 built-in equipment Serial Number or master control 3-2 read toggle switch status devices number and penetrate recognizing X
Ray diffraction diagram is originated, then carries out serial calculating by interpretation software, and result is obtained eventually through peak-seeking algorithm.
Port 1-1 on X-ray diffractometer 1 is RS232 serial ports, and conversion equipment 3 also includes RS232 modules 3-4 and level
Modular converter 3-3, RS232 module 3-4 connects level switch module 3-3, level switch module 3-3 connection master control 3-2, master control
3-2 connects WIFI module 3-1, and X-ray diffractometer 1 is connected by RS232 serial ports with RS232 modules 3-4；Level switch module
3-3 is 232 electrical level transferring chips；WIFI module 3-1 is TLN13UA06 chips, and master control 3-2 is STM32F103 chips, wireless intelligence
Energy terminal 2 is panel computer.
The course of work：The detection unit of X-ray diffractometer 1 obtains X-ray diffractogram by detecting sample, then by diffraction
Figure is transferred to conversion equipment 3 by port 1-1, and diffraction pattern is switched to transmission of wireless signals by conversion equipment 3, and detailed process is as follows：
RS232 modules 3-4 receives the RS232 signal datas transmitted from the port 1-1 of X-ray diffractometer 1, by MAX232 level
Modular converter 3-3 passes through the Transistor-Transistor Logic level that the level conversion of RS232 signals is that STM32f103 master controls 3-2 can read afterwards
The WIFI module 3-1 of STM32f103 master controls 3-2 controls is transmitted, and is sent by the WIFI antennas on WIFI module 3-1, by
The wireless network card 2-1 being adapted with WIFI module 3-1 is provided with intelligent wireless terminal 2, wireless network card 2-1 receives diffraction pattern,
And set by the MAC Address of WIFI module 3-1, master control 3-2 built-in equipment Serial Number or master control 3-2 readings toggle switch state
The standby number source to recognize X-ray diffractogram, diffraction pattern is stored in intelligent wireless terminal 2, intelligent wireless terminal 2 by analysis at
Reason software carries out series of computation treatment.
The monitoring of intelligent wireless terminal-pair X-ray diffractometer is realized first, remote operation is realized, and has liberated manpower, will
Original cable port is wirelessly transferred by changing realization；Meanwhile, realize a people and control monitoring and the multiple samples for the treatment of simultaneously,
Manpower consumption is substantially reduced, the X-ray diffractogram of acquisition is conveniently transferred, it is convenient to consult, it is easy to the X-ray diffractogram to obtaining
It is analyzed, improves conventional efficient, shortens the analyzing and processing time；System is simplified, instrument cost is reduced, reduced
Operation difficulty, for the operation of staff is provided conveniently.
In the case where not conflicting, the feature in embodiment herein-above set forth and embodiment can be combined with each other.
The foregoing is only presently preferred embodiments of the present invention, be not intended to limit the invention, it is all it is of the invention spirit and
Within principle, any modification, equivalent substitution and improvements made etc. should be included within the scope of the present invention.
Claims (5)
1. a kind of distributed X-ray diffraction measurement system, it is characterised in that including at least two X-ray diffractometers and a nothing
Line intelligent terminal, the intelligent wireless terminal carries interpretation software, each X-ray diffractometer and other X-ray diffractometers
Between it is separate, the X-ray diffractometer local position obtain X-ray diffractogram, the intelligent wireless terminal is long-range
Position is processed by interpretation software, and the X-ray diffractometer connects intelligent wireless terminal by conversion equipment, described
WIFI module and master control are provided with conversion equipment, wireless network card, the WIFI module and nothing are provided with the intelligent wireless terminal
Gauze card is adapted, and WIFI module is connected to the wireless office of wireless network card access with wireless network card point-to-point connection or WIFI module
In the net of domain, transmitted to intelligent wireless terminal after the converted device forwarding of X-ray diffractogram that the X-ray diffractometer is obtained, and
Be stored in intelligent wireless terminal, intelligent wireless terminal by the built-in equipment Serial Number of the MAC Address of WIFI module, master control or
Master control reads toggle switch status devices number to recognize X-ray diffractogram source, then carries out serial meter by interpretation software
Calculate, result is obtained eventually through peak-seeking algorithm.
2. distributed X-ray diffraction measurement system according to claim 1, it is characterised in that on the X-ray diffractometer
USB port is provided with, the conversion equipment is connected by USB port with the master control of X-ray diffractometer, the master control connects WIFI module.
3. distributed X-ray diffraction measurement system according to claim 1, it is characterised in that on the X-ray diffractometer
RS232 serial ports is provided with, the conversion equipment also includes RS232 modules and level switch module, and the RS232 modules connect level
Modular converter, the level switch module connects master control, and the master control connects WIFI module, and the X-ray diffractometer passes through
RS232 serial ports is connected with RS232 modules.
4. distributed X-ray diffraction measurement system according to claim 3, it is characterised in that the level switch module
It is 232 electrical level transferring chips.
5. distributed X-ray diffraction measurement system according to claim 4, it is characterised in that the intelligent wireless terminal
It is hand-hold wireless intelligent terminal, hand-hold wireless intelligent terminal is smart mobile phone or panel computer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611162677.0A CN106706687A (en) | 2016-12-15 | 2016-12-15 | Distributed type X-ray diffraction measurement system |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611162677.0A CN106706687A (en) | 2016-12-15 | 2016-12-15 | Distributed type X-ray diffraction measurement system |
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Application publication date: 20170524 |