CN106675670B - A kind of environmentally friendly low-carbon high heating value boiler furnace fuel - Google Patents

A kind of environmentally friendly low-carbon high heating value boiler furnace fuel Download PDF

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Publication number
CN106675670B
CN106675670B CN201710060475.3A CN201710060475A CN106675670B CN 106675670 B CN106675670 B CN 106675670B CN 201710060475 A CN201710060475 A CN 201710060475A CN 106675670 B CN106675670 B CN 106675670B
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fuel oil
oil
green algae
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CN106675670A (en
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赵鉴明
李茂盛
李德治
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SHANGHAI QIANMAO CHEMICAL TECHNOLOGY Co Ltd
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SHANGHAI QIANMAO CHEMICAL TECHNOLOGY Co Ltd
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    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/04—Liquid carbonaceous fuels essentially based on blends of hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/16—Hydrocarbons
    • C10L1/1608—Well defined compounds, e.g. hexane, benzene
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/18—Organic compounds containing oxygen
    • C10L1/182—Organic compounds containing oxygen containing hydroxy groups; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/10—Liquid carbonaceous fuels containing additives
    • C10L1/14—Organic compounds
    • C10L1/30—Organic compounds compounds not mentioned before (complexes)
    • C10L1/305—Organic compounds compounds not mentioned before (complexes) organo-metallic compounds (containing a metal to carbon bond)
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/02—Pretreatment
    • C11B1/025—Pretreatment by enzymes or microorganisms, living or dead
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Abstract

The invention discloses a kind of environmental protection, low-carbon, high heating value boiler, furnace fuel oil, it, which is formulated composition, includes 4# fuel oil, nonstandard 0# diesel oil, biodiesel and the 180# fuel oil of 600 parts by weight when main fuel oil, the parts by weight octanol raffinate (higher alcohols) of usage amount 100 makees emulsion, the parts by weight of pure water 300, fuel oil and water are mixed through 500kHz high-frequencies, 25kw high-power ultrasonics microemulsified techniques and homogeneous cutter and clip to 50 nanometers of ＜, add the parts by weight of biphenyl 0.4, the parts by weight of ferrocene 0.4.Product of the present invention 6 months is not stratified, suitable for Industrial Stoves, boiler etc., has environmental protection, low-carbon, net heating value>9500 kilocalories/kg, it is inexpensive the advantages that.

Description

A kind of environmentally friendly low-carbon high heating value boiler furnace fuel
Technical field
The present invention relates to a kind of environmental protection, low-carbon, high heating value boiler, furnace fuel oil, belong to technical field of fuel oil.
Background technology
To save the energy, PM2.5 discharges are reduced, reduce fuel cost, all parts of the country implement coal and change gas engineering.Coal will be burnt Boiler, Industrial Stoves change burning natural gas, are discharged with solving sulphur, nitrogen and PM2.5.Natural gas line also without laying factory, With environmental protection, low-carbon, high heating value boiler, kiln the present invention fuel oil replacement natural gas, be an environmental protection, low-carbon, high heating value, The project benefited the nation and the people of low cost.
GB16663-1996 alcohol radical liquid fuel standard main technical requirements：
(1) alcohol content：>=70%
(2) density (20 DEG C)≤0.83~0.85
(3) mechanical admixture：% ﹤ 0.02
(4) ﹤ -30 DEG C of condensation point
(5) 200 DEG C of ignition temperature ﹥
(6) pH value：6-8
(7) 50% recovered (distilled) temperatures：80℃
(8) total sulfur content ﹤ 0.01
(9) low heat value：Not less than 21000KJ/kg
(10) stability：It is not stratified
(11) aldehyde test magenta is not in blueness
According to national standard alcohol radical liquid fuel calorific value：﹥ 21000KJ/kg (5000 kilocalories/kg), calorific value is low, less economical.
In view of this, the present inventor through researching and developing, testing for many years.Boiler, the furnace fuel oil supplied according to existing market enter Row compares, and selects several calorific value height, the boiler that price is low, environment protecting is good, furnace fuel oil to be tested.Add 30% water, Through the mixing of 500KHZ ultrasonic emulsifications technique, stirring.Add calorific value enhancer, synthesize a kind of environmental protection, low-carbon, high heating value boiler, Furnace fuel oil.All technical meets GB16663-1996 standards, and the net heating value of fuel oil is>9500 kilocalories/kg.It is comprehensive Cost declines, and the more current market sales of fuel oil of using effect is good, and completes the present invention.
The content of the invention
It is an object of the invention to provide a kind of environmental protection, low-carbon, high heating value boiler, furnace fuel oil, can solve existing skill Art calorific value is low, it is less economical the defects of.
Solve the problems, such as to be achieved through the following technical solutions required for the present invention.
The primary raw material of the present invention includes 4# fuel oil, 180# fuel oil, nonstandard 0# diesel oil, and biodiesel etc..
4# fuel oil of the present invention, SH/T0356-1996 fuel oil 4# oil quality standards, Mi Du ﹕ (20 must be met DEG C) it is more than 0.872, pour point：Less than -6 DEG C calorific values：9800 kilocalories/Kg；Flash-point；62 DEG C of ＞；Autoignition temperature；250℃.Motion is glutinous Degree：1.9-5.5mm2/s.
Heretofore described pure water；Including well water, river, running water, it must filter through activated carbon or set through soft brush treatment The soft water of standby processing.
Ferrocene (ferrocene) of the present invention is a kind of orange/yellow solid, and it is not soluble in water, is dissolved in gasoline, bavin The organo-metallic compound of oil.Chemical property is stable, has active anticancer, promotes in the present invention for energy-saving and smoke-removing, calorific value Agent, it is made into calorific value enhancer.1kg is added in 1000Kg4 fuel oil, 14% calorific value can be improved.
Heretofore described biphenyl is a kind of chip solid, can be dissolved in organic-fuel oil, is a kind of preservative and height Energy fuel, is a kind of rocket fuel propellant, the use of biphenyl in 180# fuel oil 700kg and pure water 300kg mixture Measure as 0.3~0.5kg, 10~15% energy can be lifted.The use of 0.4kg parts by weight is in actual use preferable.
The present invention relates to a kind of environmental protection, low-carbon, high heating value boiler, furnace fuel oil is characterized in that：Component is with parts by weight Calculate, including it is as follows；
Wherein described main fuel oil raw material is 4# fuel oil, 180# fuel oil, nonstandard 0# diesel oil or biodiesel.
Bio-fuel-oil refers to alcohol fuel, bio-fuel-oil and the aviation bio-fuel produced by living resources, can replace The gasoline and diesel oil that generation is produced by oil, it is the important directions of regenerative resource utilization.So-called living resources refer to profit With big gas and water, soil etc. by photosynthesis and caused various organisms, i.e. all lived organic matters that can be grown Matter.It includes plant, animal and microorganism, and different from traditional fuels such as oil, coal, nuclear energy, these emerging fuel are can Generative fuel.
Bio-fuel-oil is studied more as a kind of fuel of alternative diesel oil at present.Bio-fuel-oil is fatty acid methyl ester It is a kind of oxygen-containing clean fuel, it is concerned because it has the advantages that combustion rate is high, pollution is few, renewable.It is raw at present Thing fuel oil is mainly produced with chemical method, i.e., with the low-carbon alcohols such as animal and plant grease and methanol or ethanol in acid or base catalysis Transesterification is carried out under agent and high temperature (230~250 DEG C), generates corresponding fatty acid methyl ester or ethyl ester.
Present invention also offers a kind of preparation method of biodiesel, is extracted again by biological pre-fermentation, Ke Yiyou Effect improves oil productivity, reduces reaction temperature, meets the requirement of energy-conserving and environment-protective of new generation.
Advantages of the present invention：
The invention provides a kind of environmental protection, low-carbon, high heating value boiler, furnace fuel oil, and it is fired using nonstandard diesel oil, 4# Expect that oil, 180# fuel oil, biodiesel work as main hydrocarbon oil feedstock plus water through 500kHz ultrasonic emulsifications technique and calorific value enhancer Mixing composition in proportion.Products obtained therefrom has environmental protection, low-carbon, calorific value>9500 kilocalories/kg, burning are completely, discharge is low, price is low It is honest and clean.It is adapted to various Industrial Stoves, boiler fuel oil.
Embodiment
Embodiments of the invention are described below in detail, the embodiment is only used for explaining the present invention, and it is not intended that right The limitation of the present invention.
A kind of environmental protection of the present invention, low-carbon, high heating value boiler, furnace fuel oil, will be real under conditions of being heated up to 50 DEG C The mixing of recipe ingredient 1-4 in proportion described in example is applied, through 500kHz ultrasonic emulsifications, it is small to be uniformly mixed storage 24 When, got product after being filtered with the diesel refining filter of 400 sieve meshes (mesh).
The specific embodiment of the present invention is as described below.
Embodiment 1
It is ultrasonic through 500kHz by the mixing of the recipe ingredient ratio described in embodiment under conditions of being heated up to 50 DEG C Ripple emulsifies, and is uniformly mixed storage 24 hours, is produced into after being filtered with the diesel refining filter of 400 sieve meshes (mesh) Product.
Embodiment 2：
It is ultrasonic through 500kHz by the mixing of the recipe ingredient ratio described in embodiment under conditions of being heated up to 50 DEG C Ripple emulsifies, and is uniformly mixed storage 24 hours, is produced into after being filtered with the diesel refining filter of 400 sieve meshes (mesh) Product.
Embodiment 3
It is ultrasonic through 500kHz by the mixing of the recipe ingredient ratio described in embodiment under conditions of being heated up to 50 DEG C Ripple emulsifies, and is uniformly mixed storage 24 hours, is produced into after being filtered with the diesel refining filter of 400 sieve meshes (mesh) Product.
Embodiment 4
The preparation method of the biodiesel is：
Weight/blue-green algae weight × 100% of oil productivity (%)=blue-green algae extract oil of blue-green algae extract oil.
Pre fermentation blue-green algae：
0.3 times water of the blue-green algae plus dry weight is mixed into moistening, according to the inoculating strain of inoculum concentration 0.5%, 37 degrees Celsius of fermentations 5-8 hours；
The bacterial strain of the inoculation is：Mesophilic Sphingobacterium；
The mesophilic Sphingobacterium is purchased from Guangdong Culture Collection, and its numbering is JCM 21153, ATCC 43320, DSM 11723, NBRC 14963；
The ethanol that the broken rear and mass fraction of blue-green algae after fermentation is 75% presses solid-to-liquid ratio (g/ml) 1:10 mixing are placed in anti- Answer in kettle, add three hypophosphite monohydrate ammoniums and manganese sulfate catalysis, the addition of the three hypophosphite monohydrates ammonium is blue-green algae weight 0.5%, the addition of manganese sulfate is the 0.1% of blue-green algae weight；
Heated：Reaction condition is：Temperature is 200 DEG C, pressure 12MPa, reaction time 20min；Reacted Liquid；
Absolute ethyl alcohol extractive reaction liquid is added, suction filtration isolates solid residue, and liquid phase stratification is organic phase and second Alcohol solution phase；
Organic phase is evaporated under reduced pressure, vacuum distillation condition is：0.09MPa, temperature are 20 DEG C, and obtained oily liquids is indigo plant Algae extract oil, the oil productivity of blue-green algae extract oil is 30.2%, and calorific value is 6619 kilocalories/kg.
Embodiment 5
With embodiment 4, the bacterial strain of inoculation is changed into aspergillus niger；
As a result：Obtained oily liquids is blue-green algae extract oil, and the oil productivity of blue-green algae extract oil is 30.9%, calorific value 6672 Kilocalorie/kg.
Embodiment 6
With embodiment 4, the bacterial strain of inoculation is changed into aspergillus niger and mesophilic Sphingobacterium according to quantity ratio 1:1 mixing；
As a result：Obtained oily liquids is blue-green algae extract oil, and the oil productivity of blue-green algae extract oil is 45.3%, and calorific value is 10052.3 kilocalorie/kg.
Embodiment 7
Test, with embodiment 4, but without microorganism pre fermentation, extracted using ordinary temperature as a comparison；
The preparation method of the biodiesel is：
Weight/blue-green algae weight × 100% of oil productivity (%)=blue-green algae extract oil of blue-green algae extract oil.
Blue-green algae presses solid-to-liquid ratio (g/ml) 1 with the ethanol that mass fraction is 75%:10 mixing are placed in reactor, add three water Ammonium phosphate and manganese sulfate catalysis are closed, the addition of the three hypophosphite monohydrates ammonium is the 0.5% of blue-green algae weight, the addition of manganese sulfate For the 0.1% of blue-green algae weight；
Heated：Reaction condition is：Temperature is 320 DEG C, pressure 12MPa, reaction time 30min；Reacted Liquid；
Absolute ethyl alcohol extractive reaction liquid is added, suction filtration isolates solid residue, and liquid phase stratification is organic phase and second Alcohol solution phase；
Organic phase is evaporated under reduced pressure, vacuum distillation condition is：0.09MPa, temperature are 20 DEG C, and obtained oily liquids is indigo plant Algae extract oil, the oil productivity of blue-green algae extract oil is 26.82%, and calorific value is 6256.1 kilocalories/kg.
It can be seen that microbial fermentation can significantly reduce reaction temperature, oil productivity is improved, improves calorific value.
Embodiment 8
For above-described embodiment 1 into embodiment 6, test result is as follows：
Biphenyl used in above-described embodiment and ferrocene are chemical products, and biphenyl is by the scientific and technological share of energy chemistry in Jiangsu Company produces.Molecular weight：154.2, relative density：1.041 flash-point：113℃.Ferrocene is a kind of energy-saving and smoke-removing, burning promotion Agent, produced by Shanghai Pu Zhen bio tech ltd.
Product of the embodiment of the present invention is through Shanghai Chemical Research Inst's calorific value detection, net heating value：It is all higher than 9650 kilocalories/kg；It is close Degree：(20) 0.88-0.93kg/ liters.
It should be noted that the preferred specific embodiment of the present invention is the foregoing is only,
If conception under this invention changes, its caused function, the spirit still covered without departing from specification When, all should be within the scope of the invention.
In the description of this specification, reference term " one embodiment ", " some embodiments ", " example ", " specifically show The description of example " or " some examples " etc. means specific features, structure, material or the spy for combining the embodiment or example description Point is contained at least one embodiment or example of the present invention.In this manual, to the schematic representation of above-mentioned term not Necessarily refer to identical embodiment or example.Moreover, specific features, structure, material or the feature of description can be any One or more embodiments or example in combine in an appropriate manner.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that：Not In the case of departing from the principle and objective of the present invention a variety of change, modification, replacement and modification can be carried out to these embodiments, this The scope of invention is limited by claim and its equivalent.

Claims (1)

1. a kind of environmental protection, low-carbon, high heating value boiler, furnace fuel oil, it is characterised in that：Component is calculated in parts by weight, including such as Under；
Wherein described main fuel oil raw material is biodiesel；
The preparation method of the biodiesel is：
(1) pre fermentation blue-green algae：
0.3 times water of the blue-green algae plus dry weight is mixed into moistening, according to the inoculating strain of inoculum concentration 0.5%, 37 degrees Celsius of fermentation 5-8 are small When；
(2) ethanol that the broken rear and mass fraction of blue-green algae after fermenting is 75% presses solid-to-liquid ratio (g/ml) 1:10 mixing are placed in reaction In kettle, three hypophosphite monohydrate ammoniums and manganese sulfate catalysis are added, the addition of the three hypophosphite monohydrates ammonium is the 0.5% of blue-green algae weight, The addition of manganese sulfate is the 0.1% of blue-green algae weight；
(3) heated：Reaction condition is：Temperature is 200 DEG C, pressure 12MPa, reaction time 20min；Reacted Liquid；
(4) absolute ethyl alcohol extractive reaction liquid is added, suction filtration isolates solid residue, and liquid phase stratification is organic phase and ethanol Water-soluble liquid phase；
(5) organic phase is evaporated under reduced pressure, vacuum distillation condition is：0.09MPa, temperature are 20 DEG C, and obtained oily liquids is indigo plant Algae extract oil；
The bacterial strain of the inoculation is：Mesophilic Sphingobacterium and aspergillus niger are 1 according to quantity ratio:1 mixing.
CN201710060475.3A 2017-01-24 2017-01-24 A kind of environmentally friendly low-carbon high heating value boiler furnace fuel Active CN106675670B (en)

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CN103484178A (en) * 2012-06-12 2014-01-01 包寅戈 Highly efficient alcohol-based fuel emulsifier
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