CN106675440A - Environment-friendly wallpaper adhesive - Google Patents
Environment-friendly wallpaper adhesive Download PDFInfo
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- CN106675440A CN106675440A CN201611068027.XA CN201611068027A CN106675440A CN 106675440 A CN106675440 A CN 106675440A CN 201611068027 A CN201611068027 A CN 201611068027A CN 106675440 A CN106675440 A CN 106675440A
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- Prior art keywords
- extract
- adhesive
- environmental protection
- added
- water
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J103/00—Adhesives based on starch, amylose or amylopectin or on their derivatives or degradation products
- C09J103/02—Starch; Degradation products thereof, e.g. dextrin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Paper (AREA)
- Medicinal Preparation (AREA)
Abstract
The invention mainly relates to the technical field of chemical engineering and discloses an environment-friendly wallpaper adhesive. The environment-friendly wallpaper adhesive is prepared from the following raw materials in parts by weight: 6-8 parts of polyvinyl alcohol, 62-64 parts of corn starch, 31-33 parts of konjac starch, 6-8 parts of lactic acid bacteria, 2.6-2.8 parts of grape extracts, 1.4-1.6 parts of codonopsis lanceolata extracts and 600-700 parts of water. The environment-friendly wallpaper adhesive is safe, environmentally friendly and simple in ingredient, simple to prepare, low in cost and convenient to use; the viscosity is 3.6-3.8Pa.s; the defects of the adhesive in existing market are overcome; the economic income is improved by 12.4%; and a plurality of plant ingredients are added and the environment-friendly wallpaper adhesive is fermented through lactic acid bacteria, so that the environment-friendly wallpaper adhesive is healthy and nontoxic, the fragrance and the viscosity can be increased, the anti-microbial and insecticidal functions are achieved, mildewing is prevented and the use value is improved.
Description
Technical field
The invention mainly relates to chemical technology field, more particularly to a kind of environmental protection wall paper adhesive.
Background technology
Wallpaper, also referred to as wallpaper are a kind of using quite extensive house decorative material.Because wallpaper has color many
Various other house decorative materials such as sample, pattern are abundant, luxurious style, safety and environmental protection, easy construction, affordable to be compared
A kind of the characteristics of plan, it has also become popular home decoration products, increasingly liked by people.
Need wallpaper to be pasted on wall using adhesive in decoration process, adhesive in the market is water base class
And powdery type, but water base class contains toxic component, and powdery type is nontoxic, but easily mouldy, and use time is short, it is therefore desirable to one
Plant environmental protection wall paper adhesive.
The content of the invention
In order to make up the defect of prior art, it is an object of the invention to provide a kind of environmental protection wall paper adhesive.
A kind of environmental protection wall paper adhesive, is made up of the raw material of following weight portion：Polyvinyl alcohol 6 ~ 8, corn starch 62 ~ 64,
Konjak starch 31 ~ 33, lactic acid bacteria 6 ~ 8, Fructus Vitis viniferae extract 2.6 ~ 2.8, Radix Codonopsis lanceolatae extract 1.4 ~ 1.6, water 600 ~ 700.
Described lactic acid bacteria, is made up of the raw material of following weight portion：Bacillus acidophilus 11 ~ 13, Lactobacillus buchneri 6 ~ 8, plant
Thing lactobacilluss 5 ~ 7.
Described Fructus Vitis viniferae extract, is to clean Fructus Vitis viniferae, adds the water of 60 ~ 70 times of amounts of Fructus Vitis viniferae weight, beating, Jing after coarse filtration
0.22 μm of supermicro filtration membrane is filtered, and lyophilization to water content is 14 ~ 16%, obtains Fructus Vitis viniferae extract.
Described Radix Codonopsis lanceolatae extract, Radix Codonopsis lanceolatae root is cleaned, and is crushed, and adds the water of 80 ~ 90 times of amounts of Radix Codonopsis lanceolatae root weight,
It is original 1/10 to boil infusion to volume, and the supermicro filtration membrane of 0.22 μm of Jing is filtered after coarse filtration, and in filtrate volume fraction is added
For 80 ~ 82% alcoholic solution, 1 ~ 3 DEG C stands 12 ~ 14 hours, filters, and takes precipitation, obtains Radix Codonopsis lanceolatae extract.
A kind of preparation method of environmental protection wall paper adhesive, comprises the following steps：
（1）1/3 water is taken, 56 ~ 58 DEG C are heated to, polyvinyl alcohol is added, in a kettle. insulated and stirred 30 ~ 35 minutes, obtain solvent；
（2）1/2 corn starch and 1/2 konjak starch are added in 1/3 water, mix homogeneously adds lactic acid bacteria, is placed in 40 ~ 42 DEG C
Fermentation 8 ~ 10 hours, obtains fermentation material；
（3）Remaining corn starch and konjak starch are added in fermentation material, is stirred, be gradually heated to 92 ~ 94 DEG C, insulation
6 ~ 8 minutes, obtain adhesive A；
（4）Fructus Vitis viniferae extract and Radix Codonopsis lanceolatae extract are added in remaining 1/3 water, mix homogeneously obtains extract solution；
（5）By step（4）Extract solution add step（1）Solvent in, in reactor stir 30 ~ 35 minutes, obtain glue
Glutinous agent B；
（6）Adhesive A is added in adhesive B, is stirred 15 ~ 20 minutes, obtain environmental protection wall paper adhesive；
（7）Packaging, obtains finished product.
The using method of the environmental protection wall paper adhesive, opens packaging, is sprayed on two gluing surface surfaces, after spraying
Two gluing surfaces are carried out in 40 minutes gluing, be such as not run out, using sealing in time after finishing.
It is an advantage of the invention that：A kind of environmental protection wall paper adhesive that the present invention is provided, safety and environmental protection, composition is simple, prepares
Simply, cheap, viscosity is 3.6 ~ 3.8Pa.S, overcomes the shortcoming of adhesive currently on the market, easy to use, and economy is received
Enter raising 12.4%；Various plants composition is added, Jing lactic acid bacteria fermentations, health is nontoxic, can tart up and viscosity, is resistant to again
Bacterium parasite killing, prevents and treats mouldy, improves use value.
Specific embodiment
Below with the specific embodiment explanation present invention.
Embodiment 1
A kind of environmental protection wall paper adhesive, is made up of the raw material of following weight portion：Polyvinyl alcohol 6, corn starch 62, konjak starch
31st, lactic acid bacteria 6, Fructus Vitis viniferae extract 2.6, Radix Codonopsis lanceolatae extract 1.4, water 600.
Described lactic acid bacteria, is made up of the raw material of following weight portion：Bacillus acidophilus 11, Lactobacillus buchneri 6, plant breast bar
Bacterium 5.
Described Fructus Vitis viniferae extract, is to clean Fructus Vitis viniferae, adds the water of 60 times of amounts of Fructus Vitis viniferae weight, beating, Jing after coarse filtration
0.22 μm of supermicro filtration membrane is filtered, and lyophilization to water content is 14%, obtains Fructus Vitis viniferae extract.
Described Radix Codonopsis lanceolatae extract, Radix Codonopsis lanceolatae root is cleaned, and is crushed, and adds the water of 80 times of amounts of Radix Codonopsis lanceolatae root weight, is boiled
Boiling infusion to volume is original 1/10, and the supermicro filtration membrane of 0.22 μm of Jing is filtered after coarse filtration, and addition volume fraction is in filtrate
80% alcoholic solution, 1 DEG C stands 12 hours, filters, and takes precipitation, obtains Radix Codonopsis lanceolatae extract.
A kind of preparation method of environmental protection wall paper adhesive, comprises the following steps：
（1）1/3 water is taken, 58 DEG C are heated to, polyvinyl alcohol is added, in a kettle. insulated and stirred 35 minutes, obtain solvent；
（2）1/2 corn starch and 1/2 konjak starch are added in 1/3 water, mix homogeneously adds lactic acid bacteria, is placed in 40 DEG C of fermentations
10 hours, obtain fermentation material；
（3）Remaining corn starch and konjak starch are added in fermentation material, is stirred, be gradually heated to 92 DEG C, be incubated 8 points
Clock, obtains adhesive A；
（4）Fructus Vitis viniferae extract and Radix Codonopsis lanceolatae extract are added in remaining 1/3 water, mix homogeneously obtains extract solution；
（5）By step（4）Extract solution add step（1）Solvent in, in reactor stir 30 minutes, obtain adhesive
B；
（6）Adhesive A is added in adhesive B, is stirred 20 minutes, obtain environmental protection wall paper adhesive；
（7）Packaging, obtains finished product.
The using method of the environmental protection wall paper adhesive, opens packaging, is sprayed on two gluing surface surfaces, after spraying
Two gluing surfaces are carried out in 40 minutes gluing, be such as not run out, using sealing in time after finishing.
Embodiment 2
A kind of environmental protection wall paper adhesive, is made up of the raw material of following weight portion：Polyvinyl alcohol 7, corn starch 63, konjak starch
32nd, the Fructus Vitis viniferae extract 2.7 of lactic acid bacteria 7, Radix Codonopsis lanceolatae extract 1.5, water 600.
Described lactic acid bacteria, is made up of the raw material of following weight portion：Bacillus acidophilus 12, Lactobacillus buchneri 7, plant breast bar
Bacterium 6.
Described Fructus Vitis viniferae extract, is to clean Fructus Vitis viniferae, adds the water of 65 times of amounts of Fructus Vitis viniferae weight, beating, Jing after coarse filtration
0.22 μm of supermicro filtration membrane is filtered, and lyophilization to water content is 15%, obtains Fructus Vitis viniferae extract.
Described Radix Codonopsis lanceolatae extract, Radix Codonopsis lanceolatae root is cleaned, and is crushed, and adds the water of 85 times of amounts of Radix Codonopsis lanceolatae root weight, is boiled
Boiling infusion to volume is original 1/10, and the supermicro filtration membrane of 0.22 μm of Jing is filtered after coarse filtration, and addition volume fraction is in filtrate
81% alcoholic solution, 2 DEG C stand 13 hours, filter, and take precipitation, obtain Radix Codonopsis lanceolatae extract.
Preparation and application, with embodiment 1.
Embodiment 3
A kind of environmental protection wall paper adhesive, is made up of the raw material of following weight portion：Polyvinyl alcohol 8, corn starch 64, konjak starch
33rd, lactic acid bacteria 8, Fructus Vitis viniferae extract 2.8, Radix Codonopsis lanceolatae extract 1.6, water 700.
Described lactic acid bacteria, is made up of the raw material of following weight portion：Bacillus acidophilus 13, Lactobacillus buchneri 8, plant breast bar
Bacterium 7.
Described Fructus Vitis viniferae extract, is to clean Fructus Vitis viniferae, adds the water of 70 times of amounts of Fructus Vitis viniferae weight, beating, Jing after coarse filtration
0.22 μm of supermicro filtration membrane is filtered, and lyophilization to water content is 16%, obtains Fructus Vitis viniferae extract.
Described Radix Codonopsis lanceolatae extract, Radix Codonopsis lanceolatae root is cleaned, and is crushed, and adds the water of 90 times of amounts of Radix Codonopsis lanceolatae root weight, is boiled
Boiling infusion to volume is original 1/10, and the supermicro filtration membrane of 0.22 μm of Jing is filtered after coarse filtration, and addition volume fraction is in filtrate
82% alcoholic solution, 3 DEG C stand 14 hours, filter, and take precipitation, obtain Radix Codonopsis lanceolatae extract.
Preparation and application, with embodiment 1.
Comparative example 1
Remove polyvinyl alcohol, remaining preparation and application, with embodiment 1.
Comparative example 2
Remove corn starch and konjak starch, remaining preparation and application, with embodiment 1.
Comparative example 3
Remove lactic acid bacteria, remaining preparation and application, with embodiment 1.
Comparative example 4
Remove Fructus Vitis viniferae extract and Radix Codonopsis lanceolatae extract, remaining preparation and application, with embodiment 1.
Comparative example 5
All raw materials are placed directly within reactor and are stirred, remaining preparation and application, with embodiment 1.
Comparative example 6
Existing commercially available conventional wallpaper adhesive.
The using effect of embodiment and comparative example wallpaper adhesive：
The batten that tin plating flat copper wire sample is cut into 10mm width will be bonded in after glue application wallpaper in above-described embodiment,
90 degree of peel strengths are tested on peel strength testing machine, 90 degree of peel strengths of same sample are tested after placing 1 week again,
The using effect of embodiment and comparative example wallpaper adhesive is shown in Table 1.
Table 1：The using effect of embodiment and comparative example wallpaper adhesive
| Project | Peel strength 1/ (N/mm) | Peel strength 2/ (N/mm) |
| Embodiment 1 | 0.99 | 1.08 |
| Embodiment 2 | 1.00 | 1.09 |
| Embodiment 3 | 0.98 | 1.07 |
| Comparative example 1 | 0.92 | 1.02 |
| Comparative example 2 | 0.91 | 0.93 |
| Comparative example 3 | 0.92 | 1.00 |
| Comparative example 4 | 0.93 | 0.96 |
| Comparative example 5 | 0.95 | 1.01 |
| Comparative example 6 | 0.97 | 1.06 |
Note：Peel strength 1 tests immediately the result of peel strength after completing for full pattern, peel strength 2 has made for sample
The result of peel strength is tested after placing 1 week into rear room temperature.
The result of table 1 shows, the environmental protection wall paper adhesive of embodiment, and peel strength 1 and peel strength 2 are significantly greater than right
Ratio, the environmental protection wall paper adhesive for illustrating present invention offer has good using effect.
Claims (6)
1. a kind of environmental protection wall paper adhesive, it is characterised in that be made up of the raw material of following weight portion：Polyvinyl alcohol 6 ~ 8, Semen Maydiss forms sediment
Powder 62 ~ 64, konjak starch 31 ~ 33, lactic acid bacteria 6 ~ 8, Fructus Vitis viniferae extract 2.6 ~ 2.8, Radix Codonopsis lanceolatae extract 1.4 ~ 1.6, water 600 ~
700。
2. environmental protection wall paper adhesive according to claim 1, it is characterised in that described lactic acid bacteria, by following weight portion
Raw material is made：Bacillus acidophilus 11 ~ 13, Lactobacillus buchneri 6 ~ 8, Lactobacillus plantarum 5 ~ 7.
3. environmental protection wall paper adhesive according to claim 1, it is characterised in that described Fructus Vitis viniferae extract, is to wash Fructus Vitis viniferae
Only, the water of 60 ~ 70 times of amounts of Fructus Vitis viniferae weight are added, beating, the supermicro filtration membrane of 0.22 μm of Jing is filtered after coarse filtration, and lyophilization is to aqueous
Measure as 14 ~ 16%, obtain Fructus Vitis viniferae extract.
4. environmental protection wall paper adhesive according to claim 1, it is characterised in that described Radix Codonopsis lanceolatae extract, by Radix Codonopsis lanceolatae
Root is cleaned, and is crushed, and adds the water of 80 ~ 90 times of amounts of Radix Codonopsis lanceolatae root weight, and it is original 1/10 to boil infusion to volume, Jing after coarse filtration
0.22 μm of supermicro filtration membrane is filtered, and the alcoholic solution that volume fraction is 80 ~ 82% is added in filtrate, and 1 ~ 3 DEG C of standing 12 ~ 14 is little
When, filter, precipitation is taken, obtain Radix Codonopsis lanceolatae extract.
5. the preparation method of environmental protection wall paper adhesive described in a kind of claim 1, it is characterised in that comprise the following steps：
（1）1/3 water is taken, 56 ~ 58 DEG C are heated to, polyvinyl alcohol is added, in a kettle. insulated and stirred 30 ~ 35 minutes, obtain solvent；
（2）1/2 corn starch and 1/2 konjak starch are added in 1/3 water, mix homogeneously adds lactic acid bacteria, is placed in 40 ~ 42 DEG C
Fermentation 8 ~ 10 hours, obtains fermentation material；
（3）Remaining corn starch and konjak starch are added in fermentation material, is stirred, be gradually heated to 92 ~ 94 DEG C, insulation
6 ~ 8 minutes, obtain adhesive A；
（4）Fructus Vitis viniferae extract and Radix Codonopsis lanceolatae extract are added in remaining 1/3 water, mix homogeneously obtains extract solution；
（5）By step（4）Extract solution add step（1）Solvent in, in reactor stir 30 ~ 35 minutes, obtain glue
Glutinous agent B；
（6）Adhesive A is added in adhesive B, is stirred 15 ~ 20 minutes, obtain environmental protection wall paper adhesive；
（7）Packaging, obtains finished product.
6. the using method of environmental protection wall paper adhesive described in a kind of any one of claim 1 ~ 5, it is characterised in that open packaging,
Sprayed on two gluing surface surfaces, carried out two gluing surfaces in 40 minutes gluing after spraying, be such as not run out, using finishing
Seal in time afterwards.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611068027.XA CN106675440A (en) | 2016-11-29 | 2016-11-29 | Environment-friendly wallpaper adhesive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611068027.XA CN106675440A (en) | 2016-11-29 | 2016-11-29 | Environment-friendly wallpaper adhesive |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106675440A true CN106675440A (en) | 2017-05-17 |
Family
ID=58867319
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611068027.XA Pending CN106675440A (en) | 2016-11-29 | 2016-11-29 | Environment-friendly wallpaper adhesive |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106675440A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114479714A (en) * | 2022-03-02 | 2022-05-13 | 江西菲尓姆新材料有限公司 | Glue additive |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104231972A (en) * | 2014-09-26 | 2014-12-24 | 无锡海特信成高分子科技有限公司 | Sealant for interior decoration |
| CN105462517A (en) * | 2015-12-21 | 2016-04-06 | 青岛宏宇环保空调设备有限公司 | Environment-friendly wallpaper adhesive |
-
2016
- 2016-11-29 CN CN201611068027.XA patent/CN106675440A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104231972A (en) * | 2014-09-26 | 2014-12-24 | 无锡海特信成高分子科技有限公司 | Sealant for interior decoration |
| CN105462517A (en) * | 2015-12-21 | 2016-04-06 | 青岛宏宇环保空调设备有限公司 | Environment-friendly wallpaper adhesive |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114479714A (en) * | 2022-03-02 | 2022-05-13 | 江西菲尓姆新材料有限公司 | Glue additive |
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Application publication date: 20170517 |