CN106643192A - Medium-frequency one-way vibration sintering furnace - Google Patents

Medium-frequency one-way vibration sintering furnace Download PDF

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Publication number
CN106643192A
CN106643192A CN201610949722.0A CN201610949722A CN106643192A CN 106643192 A CN106643192 A CN 106643192A CN 201610949722 A CN201610949722 A CN 201610949722A CN 106643192 A CN106643192 A CN 106643192A
Authority
CN
China
Prior art keywords
electro
pressure
hydraulic servo
sintering furnace
frequency
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610949722.0A
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Chinese (zh)
Inventor
刘金铃
高燕
安立楠
王光
王一光
刘佃光
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Southwest Jiaotong University
Original Assignee
Southwest Jiaotong University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Southwest Jiaotong University filed Critical Southwest Jiaotong University
Priority to CN201610949722.0A priority Critical patent/CN106643192A/en
Publication of CN106643192A publication Critical patent/CN106643192A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D19/00Arrangements of controlling devices
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D19/00Arrangements of controlling devices
    • F27D2019/0006Monitoring the characteristics (composition, quantities, temperature, pressure) of at least one of the gases of the kiln atmosphere and using it as a controlling value
    • F27D2019/0009Monitoring the pressure in an enclosure or kiln zone
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D19/00Arrangements of controlling devices
    • F27D2019/0006Monitoring the characteristics (composition, quantities, temperature, pressure) of at least one of the gases of the kiln atmosphere and using it as a controlling value
    • F27D2019/0025Monitoring the temperature of a part or of an element of the furnace structure
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F27FURNACES; KILNS; OVENS; RETORTS
    • F27DDETAILS OR ACCESSORIES OF FURNACES, KILNS, OVENS, OR RETORTS, IN SO FAR AS THEY ARE OF KINDS OCCURRING IN MORE THAN ONE KIND OF FURNACE
    • F27D19/00Arrangements of controlling devices
    • F27D2019/0028Regulation

Abstract

The invention discloses a medium-frequency one-way vibration sintering furnace which comprises a hot pressing furnace body with a pressure system. A heating body of the hot pressing furnace body is an induction coil. An infrared thermometer is arranged in the induction coil, and temperature is controlled through a temperature control system; an upper pressing head is arranged at the upper portion of the pressure system, and a lower pressing head is arranged at the lower portion of the pressure system; the bottom of the lower pressing head is provided with an electro-hydraulic servo pressure application device with adjustable frequency, amplitude and pressure, and the electro-hydraulic servo pressure application device is connected to an electro-hydraulic servo system. Re-discharging of particles can be promoted in vibration sintering, volume shrinkage can be accelerated, the purpose of rapid densification is achieved, the density and mechanical property of sintered products are effectively improved, and more excellent high-performance ceramic and powder metallurgy materials can be obtained; meanwhile, the sintering time can be obviously shortened, the energy consumption is lowered, and environment pollution is reduced while the working efficiency is greatly improved.

Description

A kind of intermediate frequency single vibration sintering furnace
Technical field
The present invention relates to it is used for the sintering furnace technical field that hot pressing sintering method prepares ceramics and metal material, it is specially a kind of Intermediate frequency single vibration sintering furnace.
Background technology
Material is the basis of human social development, and the progress of human society each time is all closely bound up with the development of material. And the quality of material, it is also closely related with its sintering process in addition to depending on material itself.And the realization of sintering process, It is unable to do without sintering furnace miscellaneous.Wherein, hot pressing furnace is exactly the conventional stove of a kind of sintering ceramics and metal-powder.Hot pressing is burnt Freezing of a furnace can be in vacuum or protective atmosphere, and to ceramics, compound powder is sintered between metal and some refractory metals, from And obtain the material with certain consistency and mechanical strength.The general principle of hot pressed sintering is at a high temperature of certain, to sample Product apply certain pressure, make the particle in base substrate particle under the double action of high temperature and mechanical force, realize different in green compact Contact and diffusion between powder, pore is excluded, and finally realizes the densification of material.And the hot pressing of the mechanical pressurization for adopting at present is burnt Knot pressuring method is although reliable and stable, but flexibility is inadequate.
The content of the invention
For the problems referred to above, it is an object of the invention to provide it is a kind of by providing Frequency Adjustable alternating pressure, and then improve The intermediate frequency single vibration sintering furnace of the performance of ceramics and sintered metal product.Technical scheme is as follows:
A kind of intermediate frequency single vibration sintering furnace, including the hot pressing body of heater with pressure system, the heater of the hot pressing body of heater is Induction coil, is provided with infrared radiation thermometer in induction coil, and temperature is controlled by temperature control system;Pressure system it is upper Portion is provided with seaming chuck, and bottom is provided with push-down head;Push-down head bottom is provided with the electro-hydraulic servo pressure dress of frequency, amplitude and pressure adjustable Put, electro-hydraulic servo device for exerting is connected to electrohydraulic servo system.
Further, the vibration frequency of the electro-hydraulic servo device for exerting is that 0-50Hz is adjustable.
Further, the electro-hydraulic servo device for exerting range of pressure fluctuations is that 0- pre-loaded pressure * 15%MPa are adjustable.
Further, the seaming chuck and push-down head adopt high temperature alloy, refractory metal, boron nitride, carborundum, oxidation Zirconium or aluminium oxide ceramics are made.
The invention has the beneficial effects as follows:
1) present invention realizes vibratory sintering on the basis of existing equipment, substantially reduces in the case where same sintered article is obtained Production cost;
2) present invention increased adjustable frequency, degree of amplitude modulation/big spy of pressure vibration sintering two on the basis of original high temperature sintering Point, promotes particle re-arrangement in vibratory sintering, accelerate volume contraction, reaches the purpose of fast densification, effectively improves sintered article Consistency and mechanical property, obtain more excellent high-performance ceramic and powdered metallurgical material;
3) present invention can sinter the high-performance ceramic and sintered metal product under different vibration frequencies, and research obtains high-performance pottery The frequency range of porcelain and sintered metal product optimum performance;
4) present invention can carry out the preparation of sintered metal product under different Oscillation Amplitude/pressure, and research obtains high-performance ceramic With the amplitude range of sintered metal product optimum performance;
5) present invention can carry out rapid temperature rise and drop using induction coil as heater, compare other mode of heatings and substantially contract Short sintering time, reducing energy consumption decreases environmental pollution while operating efficiency is greatly improved.
Description of the drawings
Fig. 1 is the structural representation of intermediate frequency single vibration sintering furnace of the present invention.
In figure:1- temperature control systems;2- induction coils;3- electrohydraulic servo systems;4- seaming chucks;5- push-down heads;The infrared surveys of 6- Wen Yi;7- electro-hydraulic servo device for exerting.
Specific embodiment
Below in conjunction with the accompanying drawings the present invention is described in further details with specific embodiment.As shown in figure 1, a kind of intermediate frequency list To vibratory sintering stove, including hot pressing body of heater, intermediate frequency power supply, temperature control system 1, electrohydraulic servo system 3 with pressure system;It is described The heater of hot pressing furnace interior is induction coil 2, and infrared radiation thermometer 6 is provided with induction coil 2, and by temperature control system 1 Temperature is controlled;The top of pressure system is provided with seaming chuck 4, and bottom is provided with push-down head 5;Electro-hydraulic servo actuator system is adopted Unidirectional pressuring method, the bottom of push-down head 5 is used to be provided with the electro-hydraulic servo device for exerting 7 of frequency, amplitude and pressure adjustable, electro-hydraulic servo Device for exerting 7 is connected to electrohydraulic servo system 3.
Intermediate frequency power supply adjusts induction coil 2 and heats, and by electro-hydraulic servo device for exerting 7 to on-load pressure, vibration frequency It is controlled with amplitude/pressure, a whole set of experimental provision can be controlled by parameter setting, experimental provision is by infrared survey Warm instrument 6 and pressure sensor can control and show pressure suffered in the temperature and sample of heating chamber in body of heater.
The vibration frequency of the electro-hydraulic servo device for exerting 7 of the present embodiment is 0-50Hz, and while sintering Frequency Adjustable is provided The vibration of rate.
The electro-hydraulic servo device for exerting 7 of the present embodiment can also simultaneously realize vibration on the basis of pre-loaded pressure Pressurization, range of pressure fluctuations is adjustable in 0- on-load pressures 15% MPa of *.
The seaming chuck 4 and push-down head 5 of the present embodiment adopts high temperature alloy, refractory metal, boron nitride, carborundum, zirconium oxide Or aluminium oxide ceramics is made, it is ensured that pressure head institute bearing capacity is not less than 60MPa.
Body of heater is vertical installation.Intermediate frequency power supply is the variable-frequency power sources generator for having at least two-way resonance circuit.
The operation principle of the present invention is by electro-hydraulic on the basis of original common hot-pressed sintering furnace in bottom plus one The Frequency Adjustable and amplitude/pressure apparatus of servo principle design, realizes that high-performance is made pottery by this Frequency Adjustable and amplitude/pressure apparatus The vibration hot pressed sintering of porcelain and sintered metal product, so as to improve the consistency and performance of sintered article.

Claims (4)

1. a kind of intermediate frequency single vibration sintering furnace, it is characterised in that include the hot pressing body of heater with pressure system, the hot pressing furnace The heater of body is induction coil(2), induction coil(2)In be provided with infrared radiation thermometer(6), and by temperature control system(1)It is right Temperature is controlled;The top of pressure system is provided with seaming chuck(4), bottom is provided with push-down head(5);Push-down head(5)Bottom is provided with The electro-hydraulic servo device for exerting of frequency, amplitude and pressure adjustable(7), electro-hydraulic servo device for exerting(7)It is connected to electro-hydraulic servo system System(3).
2. intermediate frequency single vibration sintering furnace according to claim 1, it is characterised in that the electro-hydraulic servo device for exerting (7)Vibration frequency be 0-50Hz it is adjustable.
3. intermediate frequency single vibration sintering furnace according to claim 1, it is characterised in that the electro-hydraulic servo device for exerting (7)Range of pressure fluctuations is that 0- pre-loaded pressure * 15%MPa are adjustable.
4. intermediate frequency single vibration sintering furnace according to claim 1, it is characterised in that the seaming chuck(4)And push-down head (5)Made using high temperature alloy, refractory metal, boron nitride, carborundum, zirconium oxide or aluminium oxide ceramics.
CN201610949722.0A 2016-10-26 2016-10-26 Medium-frequency one-way vibration sintering furnace Pending CN106643192A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610949722.0A CN106643192A (en) 2016-10-26 2016-10-26 Medium-frequency one-way vibration sintering furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610949722.0A CN106643192A (en) 2016-10-26 2016-10-26 Medium-frequency one-way vibration sintering furnace

Publications (1)

Publication Number Publication Date
CN106643192A true CN106643192A (en) 2017-05-10

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CN201610949722.0A Pending CN106643192A (en) 2016-10-26 2016-10-26 Medium-frequency one-way vibration sintering furnace

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109612265A (en) * 2018-12-21 2019-04-12 景德镇陶瓷大学 A kind of unidirectional double acting high-frequency vibration hot pressing vacuum sintering furnace

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102072638A (en) * 2010-12-31 2011-05-25 邓湘凌 Bidirectional hot-pressing high-temperature oscillation sintering furnace and working method thereof
CN102102942A (en) * 2010-12-28 2011-06-22 青岛科技大学 Pressure-adjustable vibratory type hot pressed sintering furnace
CN103084574A (en) * 2013-02-21 2013-05-08 湖北长江精工材料技术有限公司 Preparation method of diamond bits and sintering device thereof
CN105066682A (en) * 2015-08-05 2015-11-18 清华大学 Rapid-densification pressure-coupling dynamic sintering furnace and sintering method
CN105135873A (en) * 2015-08-05 2015-12-09 清华大学 Dynamic pressure electric pulse double-field control sintering furnace and sintering method
CN105865205A (en) * 2016-05-19 2016-08-17 西南交通大学 Two-way hot pressing high temperature oscillation sintering furnace
CN106017098A (en) * 2016-05-19 2016-10-12 西南交通大学 One-way hot-press high-temperature oscillation sintering furnace

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102102942A (en) * 2010-12-28 2011-06-22 青岛科技大学 Pressure-adjustable vibratory type hot pressed sintering furnace
CN102072638A (en) * 2010-12-31 2011-05-25 邓湘凌 Bidirectional hot-pressing high-temperature oscillation sintering furnace and working method thereof
CN103084574A (en) * 2013-02-21 2013-05-08 湖北长江精工材料技术有限公司 Preparation method of diamond bits and sintering device thereof
CN105066682A (en) * 2015-08-05 2015-11-18 清华大学 Rapid-densification pressure-coupling dynamic sintering furnace and sintering method
CN105135873A (en) * 2015-08-05 2015-12-09 清华大学 Dynamic pressure electric pulse double-field control sintering furnace and sintering method
CN105865205A (en) * 2016-05-19 2016-08-17 西南交通大学 Two-way hot pressing high temperature oscillation sintering furnace
CN106017098A (en) * 2016-05-19 2016-10-12 西南交通大学 One-way hot-press high-temperature oscillation sintering furnace

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109612265A (en) * 2018-12-21 2019-04-12 景德镇陶瓷大学 A kind of unidirectional double acting high-frequency vibration hot pressing vacuum sintering furnace

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