CN106634387A - Quick-drying water-based base material of color-remanding agent and preparation method thereof - Google Patents
Quick-drying water-based base material of color-remanding agent and preparation method thereof Download PDFInfo
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- CN106634387A CN106634387A CN201611200568.3A CN201611200568A CN106634387A CN 106634387 A CN106634387 A CN 106634387A CN 201611200568 A CN201611200568 A CN 201611200568A CN 106634387 A CN106634387 A CN 106634387A
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- aqueous
- fast
- agent
- drying
- dressing agent
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D151/00—Coating compositions based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers
- C09D151/08—Coating compositions based on graft polymers in which the grafted component is obtained by reactions only involving carbon-to-carbon unsaturated bonds; Coating compositions based on derivatives of such polymers grafted on to macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paints Or Removers (AREA)
Abstract
The invention provides a quick-drying water-based base material of a color-remanding agent and a preparation method thereof. The quick-drying water-based base material of the color-remanding agent is prepared from the following components in percentage by weight: 10 to 30 percent of acrylic acid modified alkyd resin, 40 to 80 percent of solvent, 1 to 2 percent of water-based wetting agent, 0.3 to 2 percent of water-based dispersing agent, 0.1 to 0.5 percent of water-based defoamer, 1 to 3 percent of adhesion promoter, 1 to 3 percent of drier and 2 to 4 percent of penetrating agent. The quick-drying water-based base material of the color-remanding agent, obtained by the invention, has the advantage of high drying speed; a sagging phenomenon is avoided, the large-scale construction by constructors is facilitated, and the construction time is saved.
Description
Technical field
The present invention relates to preparation method for coating field, specifically discloses a kind of fast-drying aqueous dressing agent base-material and its preparation side
Method.
Background technology
When Furniture Factory is to furniture spray paint, for improve production efficiency, heavy caliber high pressure spray gun, oil pump capacity, tolerance can be adopted
That what is opened is larger, walks rifle speed fast.Repaiied after color using said method, then spray paint, because dressing agent is dried insufficient, finish paint stream
When dynamic, dressing agent sagging can be made, irregular colour is even.General common dressing agent can not meet aforesaid operations requirement.At present, Furniture Factory
Because dressing agent limitation, repairing colour circle section can reduce away rifle speed, oil pump capacity, tolerance is opened little.Such mode of operation very great Cheng
Production hour is increased on degree, production cost is improve.
The content of the invention
It is an object of the invention to overcome the defect of prior art, there is provided a kind of fast-drying aqueous dressing agent base-material and its preparation
Method, the fast-drying aqueous dressing agent base-material has the advantages that rate of drying is fast, it is to avoid the phenomenon of sagging, is conducive to workmen big
Area is constructed, and saves the engineering time.
In order to realize object above and other purposes, the present invention is by realizing including technical scheme below：It is a kind of fast
Solid carbon dioxide dressing agent base-material, including following components, each weight percentages of components is：
Preferably, the molecular weight of the acrylic acid modified alkyd resin is 10000-20000, and MFT is -10
DEG C -0 DEG C, solid content is 40%-45%, and range of viscosities is 45-60s.Due to containing double bond, hydroxyl and carboxylic in alcohol acid molecular structures
Base isoreactivity group, can react with the acrylic resin containing active group, polyurethane resin, epoxy resin etc., but alcohol
The water-soluble poor of acid resin, hardness are low, and acrylic resin is of light color, outdoor weathe resistance is excellent, hardness is high, chemical-resistant is good
Advantage, the present invention adopt acrylic acid modified alkyd resin acrylic resin is grafted on alkyd resin molecule, with improve
The performances such as its rapid-drying properties, weatherability, while making it have preferable water-soluble, rate of drying and preferable mechanical hardness.
It is highly preferred that the model DSM xk-84 of the acrylic acid modified alkyd resin.The acrylic modified alkyd tree
Fat has relatively low MFT, and rate of drying is fast.
Preferably, the solvent is one or more in ethanol, isopropanol and alcohol ester 12.The hydrolysis of alcohol ester 12 is steady
It is qualitative very good, add dressing agent in when, be absorbed on acrylic acid modified alkyd resin emulsion particle, soften particle and
Cause preferably fusion when applying dressing agent, the freezing point of alcohol ester 12 is very low, reduces the freezing point of dressing agent base-material.
It is highly preferred that combination of the solvent for ethanol, isopropanol and the three of alcohol ester 12, the ethanol, the isopropyl
Alcohol, the weight ratio of the alcohol ester 12 are (5-7):(4-6):1.
Preferably, the aqueous wetting agent is type siloxane wetting agent.Aqueous dressing agent base-material surface tension is reduced, water is made
Property dressing agent base-material can be entirely spread on base material.
It is highly preferred that the one kind of the model of the aqueous wetting agent in SP-994, TEGO245 and OT-75.
Preferably, the aqueous dispersion is the EVA with pigment affinity groups.
It is highly preferred that model BYK192 of the aqueous dispersion.
Preferably, the aqueous defoamer is polyether silicone class defoamer.
It is highly preferred that the one kind of the model of the aqueous defoamer in L-61, BX-106107108 and TEGO902W.
Preferably, the adhesion promoter is silanes accelerator.Addition adhesion promoter strengthens aqueous dressing agent
Adhesive force between base material.
It is highly preferred that model silok627 of the adhesion promoter.
Preferably, model LF-1218 of the drier.Drier plays oxidation, polymerization, the drying for accelerating paint film,
The purpose of quick-drying is reached, and model LF-1218 drier is a kind of compound drier, can simultaneously promote accelerated surface to be dried
With low temperature drying.
Preferably, the bleeding agent is nonionic low-foaming penetrating agent.Addition bleeding agent improves the infiltration to deep lines base material
Effect, and foam is few, it is to avoid because causing film surface pin hole occur foam more.
It is highly preferred that model WT-100 of the bleeding agent.The bleeding agent has very low dynamic surface tension.
The present invention discloses a kind of method for preparing fast-drying aqueous dressing agent base-material as described above, comprises the following steps：
First the acrylic acid modified alkyd resin is added in mixer, stirring is opened, mixing speed is controlled in 400-450r/min；
Then the aqueous wetting agent, the solvent, the aqueous dispersion, the aqueous defoamer and the adhesive force are sequentially added
Accelerator, stirs, and adds the drier, and mixing speed is risen to into 500-800r/min, disperses 5-10min, then will stir
Mix speed and be down to 400-450r/min, add the bleeding agent, stir, obtain fast-drying aqueous dressing agent base-material.
In sum, the present invention provides a kind of fast-drying aqueous dressing agent base-material and preparation method thereof, the beneficial effect of the present invention
Really：The fast-drying aqueous dressing agent base-material that the present invention is obtained has the advantages that fast rate of drying, environmental protection, smell are little, and realizes low
Quick-drying under warm environment, thickness applies not sagging, is conducive to workmen's large-area construction, saves the engineering time；And aqueous dressing agent
Base-material and aqueous color essence compatibility is good, can arbitrarily arrange in pairs or groups, and modulates preferable color, and it is beautiful in colour to repair color back plate face, level
Sense is strong, and strong with ground adhesion, non-environmental-pollution will not be damaged to human body.
Specific embodiment
The present invention is expanded on further with reference to embodiment.It should be understood that embodiment is merely to illustrate the present invention, and it is unrestricted
The scope of the present invention.
It is the proportioning of each raw material components in embodiment 1～7 in table 1, the content of each raw material components is weight portion in table.
The weight proportion of each raw material components in the embodiment 1～5 of table 1
Wherein, solvent compares 6 by ethanol, isopropanol and alcohol ester 12 according to weight:5:1 mixes.
Embodiment 1
First the DSM XK-84 acrylic acid modified alkyd resins of 10kg are added in mixer, stirring is opened, by stirring speed
Degree control is in 400r/min；Then the TEGO245 aqueous wetting agents of 1.2kg, 80.5kg solvents, 0.8kg are sequentially added
The SILOK627 adhesion promoters of BYK192 aqueous dispersions, the TEGO902W aqueous defoamers of 0.5kg and 3kg, stirring is equal
It is even, the LF-1218 drier of 1kg is added, mixing speed is risen to into 700r/min, disperse 6min, then mixing speed is down to
400r/min, adds the WT-100 bleeding agents of 3kg, stirs, and obtains fast-drying aqueous dressing agent base-material.
Embodiment 2
First the DSM XK-84 acrylic acid modified alkyd resins of 15kg are added in mixer, stirring is opened, by stirring speed
Degree control is in 400r/min；Then TEGO245 aqueous wetting agents, 76kg solvents, the BYK192 of 0.8kg of 1.2kg are sequentially added
The SILOK627 adhesion promoters of aqueous dispersion, the TEGO902W aqueous defoamers of 0.5kg and 3kg, stir, and add
The LF-1218 drier of 1.5kg, by mixing speed 700r/min is risen to, and disperses 7min, then mixing speed is down to into 400r/
Min, adds the WT-100 bleeding agents of 2kg, stirs, and obtains fast-drying aqueous dressing agent base-material.
Embodiment 3
First the DSM XK-84 acrylic acid modified alkyd resins of 20kg are added in mixer, stirring is opened, by stirring speed
Degree control is in 430r/min；Then TEGO245 aqueous wetting agents, 70kg solvents, the BYK192 of 0.8kg of 1.2kg are sequentially added
The SILOK627 adhesion promoters of aqueous dispersion, the TEGO902W aqueous defoamers of 0.5kg and 2.5kg, stir, plus
Enter the LF-1218 drier of 2kg, mixing speed is risen to into 700r/min, disperse 7min, then mixing speed is down to into 430r/
Min, adds the WT-100 bleeding agents of 3kg, stirs, and obtains fast-drying aqueous dressing agent base-material.
Embodiment 4
First the DSM XK-84 acrylic acid modified alkyd resins of 25kg are added in mixer, stirring is opened, by stirring speed
Degree control is in 400r/min；Then TEGO245 aqueous wetting agents, 64kg solvents, the BYK192 of 0.8kg of 1.2kg are sequentially added
The SILOK627 adhesion promoters of aqueous dispersion, the TEGO902W aqueous defoamers of 0.5kg and 2kg, stir, and add
The LF-1218 drier of 2.5kg, by mixing speed 800r/min is risen to, and disperses 5min, then mixing speed is down to into 400r/
Min, adds the WT-100 bleeding agents of 4kg, stirs, and obtains fast-drying aqueous dressing agent base-material.
Embodiment 5
First the DSM XK-84 acrylic acid modified alkyd resins of 30kg are added in mixer, stirring is opened, by stirring speed
Degree control is in 400r/min；Then TEGO245 aqueous wetting agents, 60kg solvents, the BYK192 of 0.8kg of 1.2kg are sequentially added
The SILOK627 adhesion promoters of aqueous dispersion, the TEGO902W aqueous defoamers of 0.5kg and 1.5kg, stir, plus
Enter the LF-1218 drier of 3kg, mixing speed is risen to into 500-800r/min, disperse 5-10min, then mixing speed is down to
400-450r/min, adds the WT-100 bleeding agents of 3kg, stirs, and obtains fast-drying aqueous dressing agent base-material.
Test result：
The fast-drying aqueous dressing agent base-material of the acquisition of embodiment 1 to 5 is mixed colours respectively with aqueous color accurate adjustment, and acquisition is aqueous to repair color
Agent, is then sprayed aqueous dressing agent on the plank for spraying or brushing twice aqueous priming paint respectively, and high pressure is selected in spraying
Spray gun, gas output during spraying, oil mass is opened greatly, and it is fast to walk rifle speed, close with Furniture Factory construction technology, observes the face of aqueous dressing agent
Color process of osmosis, and its time needed for being dried is recorded, after unified 15min, then aqueous finish paint is sprayed, plank is erect, vertically
Place, treat its surface drying.Plank after drying varniss is carried out into performance test.
The technical performance testing result of fast-drying aqueous dressing agent base product prepared by 2 embodiment of table 1 to 5
As seen from Table 2, embodiment 1-5 obtain plank plate face color is uniform, permeability effects very well, plank is placed in into 50
DEG C, color is uniform after 7 days, plate face is not changed in, and illustrates that plate face colour stability is good.The dressing agent is applied to can brush or spray
Woodcare paint on, form of construction work is simple.It is or so about 8-15min minutes, aqueous after spraying the aqueous dressing agent at 25 DEG C of room temperature
The color of dressing agent can uniformly be adsorbed onto primed surface, illustrate that its rate of drying is fast, and the aqueous dressing agent causes workmen
Quickly constructed, it is convenient to repair, and the gapless Jing after repairing.Aqueous dressing agent is 0 with the ply adhesion of aqueous priming paint
Level, then to have sprayed that test after finish paint adhesive force be still 0 grade (former priming paint with finish paint ply adhesion be 0 grade), illustrates aqueous to repair color
Agent does not interfere with ply adhesion.
In sum, the fast-drying aqueous dressing agent base-material that the present invention is obtained has little excellent of rate of drying fast, environmental protection, smell
Point, and quick-drying under low temperature environment is realized, thickness applies not sagging, is conducive to workmen's large-area construction, saves the engineering time；And
And aqueous dressing agent base-material non-environmental-pollution, human body will not be damaged.So, the present invention is effectively overcome in prior art
Various shortcoming and have high industrial utilization.
The above, only presently preferred embodiments of the present invention, it is not any to the present invention in form and substantial restriction,
It should be pointed out that for those skilled in the art, on the premise of without departing from the inventive method, can also make
Some improvement and supplement, these are improved and supplement also should be regarded as protection scope of the present invention.All those skilled in the art,
Without departing from the spirit and scope of the present invention, when make using disclosed above technology contents it is a little more
Dynamic, modification and the equivalent variations for developing, are the Equivalent embodiments of the present invention；Meanwhile, all substantial technologicals pair according to the present invention
Change, modification and the differentiation of any equivalent variations that above-described embodiment is made, still falls within the scope of technical scheme
It is interior.
Claims (9)
1. a kind of fast-drying aqueous dressing agent base-material, it is characterised in that：Including following components, each weight percentages of components is：
2. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The acrylic acid modified alkyd resin
Molecular weight is 10000-20000, and MFT is -10 DEG C -0 DEG C.
3. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The solvent be ethanol, isopropanol and
One or more in alcohol ester 12.
4. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The aqueous wetting agent is type siloxane
Wetting agent.
5. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The aqueous dispersion is band pigment parent
With the EVA of group.
6. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The aqueous defoamer is polyethers silica
Alkanes defoamer.
7. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The adhesion promoter is silanes
Accelerator.
8. fast-drying aqueous dressing agent base-material as claimed in claim 1, it is characterised in that：The bleeding agent is that the low bubble of nonionic oozes
Agent thoroughly.
9. a kind of method of the fast-drying aqueous dressing agent base-material prepared as described in claim 1 to 8 is arbitrary, it is characterised in that：Bag
Include following steps：First the acrylic acid modified alkyd resin is added in mixer, stirring is opened, mixing speed control is existed
400-450r/min；Then the aqueous wetting agent, the solvent, the aqueous dispersion, the aqueous froth breaking are sequentially added
Agent and the adhesion promoter, stir, and add the drier, and mixing speed is risen to into 500-800r/min, disperse
5-10min, then mixing speed is down to into 400-450r/min, the bleeding agent is added, stir, acquisition is fast-drying aqueous to repair color
Agent base-material.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611200568.3A CN106634387B (en) | 2016-12-22 | 2016-12-22 | Quick-drying water-based color modifier base material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611200568.3A CN106634387B (en) | 2016-12-22 | 2016-12-22 | Quick-drying water-based color modifier base material and preparation method thereof |
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| CN106634387A true CN106634387A (en) | 2017-05-10 |
| CN106634387B CN106634387B (en) | 2020-06-23 |
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Cited By (3)
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| CN111205710A (en) * | 2020-01-18 | 2020-05-29 | 喜临门酒店家具有限公司 | Quick-drying type water-based color modifier and preparation method thereof |
| CN112251123A (en) * | 2020-09-27 | 2021-01-22 | 广东美涂士建材股份有限公司 | Ultraviolet-resistant color modifier and preparation method thereof |
| CN116535949A (en) * | 2023-05-23 | 2023-08-04 | 太仓斯迪克新材料科技有限公司 | Quick-drying antistatic coating liquid for bottom coating, antistatic film and preparation method |
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| CN112251123A (en) * | 2020-09-27 | 2021-01-22 | 广东美涂士建材股份有限公司 | Ultraviolet-resistant color modifier and preparation method thereof |
| CN112251123B (en) * | 2020-09-27 | 2021-10-26 | 广东美涂士建材股份有限公司 | Ultraviolet-resistant color modifier and preparation method thereof |
| CN116535949A (en) * | 2023-05-23 | 2023-08-04 | 太仓斯迪克新材料科技有限公司 | Quick-drying antistatic coating liquid for bottom coating, antistatic film and preparation method |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106634387B (en) | 2020-06-23 |
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