CN106617285A - Variable color fragrance bead for tobacco and preparation method of the fragrance bead - Google Patents
Variable color fragrance bead for tobacco and preparation method of the fragrance bead Download PDFInfo
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- CN106617285A CN106617285A CN201610854701.0A CN201610854701A CN106617285A CN 106617285 A CN106617285 A CN 106617285A CN 201610854701 A CN201610854701 A CN 201610854701A CN 106617285 A CN106617285 A CN 106617285A
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- red
- discoloration
- adhesive
- water
- powder
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 32
- 241000208125 Nicotiana Species 0.000 title claims abstract description 31
- 239000011324 bead Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 239000003205 fragrance Substances 0.000 title abstract description 15
- 239000000853 adhesive Substances 0.000 claims abstract description 60
- 230000001070 adhesive effect Effects 0.000 claims abstract description 60
- 239000007787 solid Substances 0.000 claims abstract description 35
- 239000000843 powder Substances 0.000 claims abstract description 34
- 239000000686 essence Substances 0.000 claims abstract description 33
- 239000011812 mixed powder Substances 0.000 claims abstract description 32
- 241000196324 Embryophyta Species 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 27
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- 238000000576 coating method Methods 0.000 claims abstract description 15
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- 229940016286 microcrystalline cellulose Drugs 0.000 claims abstract description 11
- 239000002002 slurry Substances 0.000 claims abstract description 11
- 239000008107 starch Substances 0.000 claims abstract description 11
- 235000019698 starch Nutrition 0.000 claims abstract description 11
- 238000002845 discoloration Methods 0.000 claims description 60
- 239000000243 solution Substances 0.000 claims description 42
- 235000013599 spices Nutrition 0.000 claims description 36
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- 239000002245 particle Substances 0.000 claims description 21
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- 238000005119 centrifugation Methods 0.000 claims description 10
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- WRANYHFEXGNSND-LOFNIBRQSA-N capsanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CCC(O)C2(C)C WRANYHFEXGNSND-LOFNIBRQSA-N 0.000 claims description 4
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- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 claims description 3
- 235000005767 Theobroma cacao ssp. sphaerocarpum Nutrition 0.000 claims description 3
- 240000008042 Zea mays Species 0.000 claims description 3
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 claims description 3
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- 235000001046 cacaotero Nutrition 0.000 claims description 3
- 239000006229 carbon black Substances 0.000 claims description 3
- MYSWGUAQZAJSOK-UHFFFAOYSA-N ciprofloxacin Chemical compound C12=CC(N3CCNCC3)=C(F)C=C2C(=O)C(C(=O)O)=CN1C1CC1 MYSWGUAQZAJSOK-UHFFFAOYSA-N 0.000 claims description 3
- 239000009627 gardenia yellow Substances 0.000 claims description 3
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- 235000020232 peanut Nutrition 0.000 claims description 3
- 235000007516 Chrysanthemum Nutrition 0.000 claims description 2
- 244000189548 Chrysanthemum x morifolium Species 0.000 claims description 2
- 241000723366 Coreopsis Species 0.000 claims description 2
- 241001199649 Senegalia erubescens Species 0.000 claims description 2
- 235000012730 carminic acid Nutrition 0.000 claims description 2
- 229940071676 hydroxypropylcellulose Drugs 0.000 claims 3
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims 1
- 235000018958 Gardenia augusta Nutrition 0.000 claims 1
- 235000016357 Mirtillo rosso Nutrition 0.000 claims 1
- 235000009470 Theobroma cacao Nutrition 0.000 claims 1
- 235000017606 Vaccinium vitis idaea Nutrition 0.000 claims 1
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- 229940105329 carboxymethylcellulose Drugs 0.000 claims 1
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- 235000009508 confectionery Nutrition 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 9
- 230000000391 smoking effect Effects 0.000 abstract description 6
- 238000002156 mixing Methods 0.000 abstract description 3
- 239000008187 granular material Substances 0.000 abstract 3
- 229920001661 Chitosan Polymers 0.000 abstract 1
- 235000019504 cigarettes Nutrition 0.000 description 24
- 239000000203 mixture Substances 0.000 description 10
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 6
- 239000003546 flue gas Substances 0.000 description 6
- 230000002441 reversible effect Effects 0.000 description 5
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- 238000012216 screening Methods 0.000 description 3
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- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 description 2
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- 230000014860 sensory perception of taste Effects 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- 244000111489 Gardenia augusta Species 0.000 description 1
- VAYOSLLFUXYJDT-RDTXWAMCSA-N Lysergic acid diethylamide Chemical compound C1=CC(C=2[C@H](N(C)C[C@@H](C=2)C(=O)N(CC)CC)C2)=C3C2=CNC3=C1 VAYOSLLFUXYJDT-RDTXWAMCSA-N 0.000 description 1
- 244000061176 Nicotiana tabacum Species 0.000 description 1
- 239000002775 capsule Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
Landscapes
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention provides a variable color fragrance bead for tobacco and a preparation method of the fragrance bead. The fragrance bead is prepared by the following steps: firstly solid mixed powder material is placed in a centrifugal coating granulator, and an adhesive solution is sprinkled as a slurry material, the powder material is rotated in the centrifuge and forms mother cores, then the mother cores are still placed in the centrifugal coating granulator, a variable color fragrance adhesive solution is sprinkled as a slurry material, the solid mixed powder material is added during the process of sprinkling, enlargement and preparation of granules is continued and the granule size increases, and the granules form variable color fragrance beads for tobacco. The solid powder material is formed by evenly mixing natural plant powder, starch, chitosan and microcrystalline cellulose. The variable color fragrance adhesive solution is formed by mixing adhesives, pigments, essence, variable color printing ink and water. The method can provide tobacco with fragrance which can improve the smoking quality, and a customer can see color change of the beads directly during smoking, so that the customer can have both vision and taste experience.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to one kind is used in filter stick for cigarettes, and the cigarette that can change colour is fragrant
Material pearl and preparation method thereof.
Background technology
Add essence in cigarette, mainly there are several ways at present：1. the direct flavoring and casing in pipe tobacco；2. in filter stick
Brought into the way of fragrant line；3. parcel is added in the form of capsule in filter stick；4. added in the way of microcapsules in filter stick
Enter.The multiple cigarette brands of this several ways are being used, and consumer is difficult to find that more novel consumption experience.
Color shifting ink is a kind of by a kind of special ink by the discoloration of property material, can be used on false proof industry, toy row
Industry, gift industry, apparel industry, handicraft industry etc..Color shifting ink is largely divided into several big class：1. heat discoloration ink；2.
Ultraviolet photosensitive color-changing ink；3. Ultraluminescence color shifting ink；4. infrared excitation color shifting ink；5. water color shifting ink is met；6. light
Learn color shifting ink；7. noctilucence color shifting ink.In this several classification, since it is considered that the application in cigarette, is in cigarette
Portion, it is difficult to react with the directly contact such as ultraviolet, fluorescence, infrared ray, noctilucence, water, it is contemplated that using heat discoloration
Principle, color shifting ink is combined with carrier for essence, in being applied to cigarette, improves the novelty that essence is used.
Heat discoloration ink can must become color repeatedly with the rising of temperature, decline.(by taking 31 DEG C of redness as an example, change colour shape
Formula is 31 DEG C of presented above colourless, 31 DEG C of redness presented below).Heat discoloration ink has three big class：1. certain is shown under normal temperature
Particular color is planted, heated rear color disappears and becomes colorless, and original color is returned to after cooling immediately, because its change procedure can
It is inverse, referred to as " Reversible temperature becomes colour killing ink "；2. show colourless at normal temperatures, it is heated after be changed into another color, after cooling
Revert to again it is original colourless, because its change procedure it is reversible, referred to as " Reversible temperature becomes color development ink "；3. ink shows at normal temperatures
Color, is changed into another color after heating, be referred to as because its change procedure is reversible " Reversible temperature becomes annesl ink ".
The content of the invention
For the above-mentioned deficiency of prior art, the technical problem to be solved in the present invention is to provide a kind of cigarette that can change colour and uses
Perfumed beads and preparation method thereof, the perfumed beads are used in heat discoloration ink in the preparation technology of perfumed beads, made by color pearl not
Only there is gay colours, suitable fragrance matter is loaded into, moreover it is possible to color changeable effect.It is added to the transparent filter stick of cigarette
In, the flue-gas temperature produced by cigarette smoking is heated to color pearl, and color pearl color of being heated changes, while flue gas is taken out of
Aroma component in bead, makes consumer experience the dual experience of vision and the sense of taste.
The technical scheme is that：A kind of discoloration tobacco aromaticss pearl, it is characterised in that the perfumed beads are by mother
Core and discoloration spices shell constitute the colour-changeable perfumed beads of a diameter of 1.0～4.0mm, wherein the particle diameter of parent nucleus be 250～
450 μm, the discoloration spices shell is wrapped in parent nucleus surface by way of coating；
The parent nucleus raw material including solid mixed powder that mass percent is 50～90% and mass percent be 10～
50% binder solution, wherein binder solution are that the water by the adhesive that mass percent is 1～20% with 80～99% is mixed
Conjunction is formulated；
The discoloration spices shell material includes the solid mixed powder that mass percent is 70～90% and quality percentage
Than for 10～30% discoloration spices adhesive solution, wherein the discoloration spices adhesive solution be by adhesive, pigment, essence,
Color shifting ink and water are according to ratio of weight and number 1～20：0.1～10：0.1～10：0.1～20：50～90 ratio is mixed；
In above-mentioned formula, the solid mixed powder be by natural plant powder, starch, shitosan, microcrystalline cellulose by
According to ratio of weight and number 1～30：1～50：1～50：1～20 ratio is mixed；
Described adhesive is the one kind in PVP, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethylcellulose calcium
Or it is various；
The pigment is water-soluble food coloring；The essence is soluble perfume；The color shifting ink is heat discoloration
Water-based ink, its discoloration cardinal temperature is 5 DEG C～60 DEG C.
The present invention preferably technical scheme：Wherein natural plant powder for mesh～80 mesh of particle diameter 30 powder, specifically by
Tobacco leaf, anise, the seed of Chinese dodder, lavender, peppermint, thyme, bay, Chinese cassia tree, Radix Glycyrrhizae, dried orange peel, cloves, Chinese ilex, Pogostemon cablin, jasmine
The powder that any one or more plant in jasmine is formed after crushing.
The present invention preferably technical scheme：Discoloration spices shell pigment include natural bata-carotene, beet red, turmeric,
Safflower yellow, lac are red, get over Exocarpium Citri Rubrum, capsanthin, chilli orange, burnt sugar coloring, red red rice, coreopsis yellow extract, red black soya bean, Kaoliang red, jade
Cream colour, radish red, cacao pigment, red yeast rice, Monascus color, the certain herbaceous plants with big flowers that falls are red, Hei Jialun is red, Gardenia Yellow, gardenia blue, and sea-buckthorn is yellow, roselle
Red, acorn cup is brown, many favour Ke palm fibre, and mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, curcumin, peanut agriculture is red, Grape Skin is red, blue ingot
Arnotto, algae are blue, plant carbon black, Mi Menghuang, Asian puccoon is red, tea uranidin, Tea Green Pigment, oranges and tangerines yellow, relation by marriage fat tree orange, it is carmine in
One or more；The essence is water-soluble flavouring essence for tobacco or water-soluble edible essence；The color of the color shifting ink includes big
Red, rhodo, it is pink, bright red, orange red, sapphire blue, dark blue, sea blue, grass green, blackish green, in green, peacock green, golden yellow, black.
The preparation method of a kind of discoloration tobacco aromaticss pearl that the present invention is provided, it is characterised in that comprise the following steps that：
(1) natural plants are taken as raw material, is crushed, is sieved, obtain the natural vegetable powder that particle diameter is 30 mesh～80 mesh
End, then by the natural plant powder for obtaining, starch, shitosan, microcrystalline cellulose according to ratio of weight and number 1～30：1～50：1
～50：1～20 ratio is well mixed the solid mixed powder to form parent nucleus raw material；
(2) after the adhesive that mass percent is 1～20% is mixed with the pure water that mass percent is 80～99%
It is configured to binder solution；Wherein described adhesive is PVP, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethyl
One or more in cellulose；
(3) solid mixed powder in step (1) is placed in centrifugation coating granulator, and it is viscous by what is prepared in step (2)
Mixture solution is sprayed as slurry, and powder rotates in centrifuge and forms parent nucleus；And sieved parent nucleus, particle size range
Control is at 250～450 μm；
(4) raw material of discoloration spice solution is weighed according to following parts by weight：Adhesive 1～20, pigment 0.1～10 is fragrant
Essence 0.1～10, color shifting ink 0.1～20, water 50～90；First whole adhesives, pigment, essence are dissolved into 10～30 weight portions
Water in be configured to mixed aqueous solution, then color shifting ink is dissolved into the water of 40～60 weight portions, stirring 1～2 hour it is molten
Solution is configured to completely the color shifting ink aqueous solution, then by the color shifting ink aqueous solution for preparing and adhesive, pigment, the essence aqueous solution
Stir 1～2 hour after mixing, to dissolving discoloration spices adhesive solution is formed completely；Described adhesive is PVP, hydroxypropyl fibre
One or more in dimension element, hydroxypropyl methyl cellulose, carboxymethylcellulose calcium；
(5) parent nucleus of granulation in step (3) is continued to be positioned in centrifugation coating granulator, and by step 4) in match somebody with somebody
The discoloration spices adhesive solution of system is sprayed as slurry, adds the solid prepared in step (1) to mix during sprinkling
Powder is closed, continuing amplification pill makes its particle diameter rise to 1.0～4.0mm, forms changeable colour tobacco aromaticss pearl；Wherein slurry with it is solid
The mass ratio of body mixed powder is 10～30:70～90；
The present invention preferably technical scheme：Natural plants in the step (1) are tobacco leaf, anise, the seed of Chinese dodder, smoke clothing
Any one or more in grass, peppermint, thyme, bay, Chinese cassia tree, Radix Glycyrrhizae, dried orange peel, cloves, Chinese ilex, Pogostemon cablin, jasmine.
The present invention preferably technical scheme：In step (4), the pigment is water-soluble food coloring；Including natural β recklessly
Radish element, beet red, turmeric, safflower yellow, lac are red, it is red to get over Exocarpium Citri Rubrum, capsanthin, chilli orange, burnt sugar coloring, red rice, Chrysan Yellow leaching
Cream, black soya bean are red, Kaoliang red, maize, radish red, cacao pigment, red yeast rice, Monascus color, the certain herbaceous plants with big flowers that falls is red, Hei Jialun is red, Gardenia Yellow,
Gardenia blue, sea-buckthorn is yellow, roselle is red, acorn cup is brown, many favour Ke palm fibre, and mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, curcumin, flower
Raw agriculture is red, Grape Skin is red, blue ingot arnotto, algae are blue, plant carbon black, Mi Menghuang, and Asian puccoon is red, tea uranidin, Tea Green Pigment, oranges and tangerines
One or more in yellow, relation by marriage fat tree orange, famille rose；The essence is water-soluble flavouring essence for tobacco or water-soluble edible essence；Institute
It is heat discoloration water-based ink to state color shifting ink, and its discoloration cardinal temperature is 5 DEG C～60 DEG C, and its color is including but not limited to big
Red, rhodo, it is pink, bright red, orange red, sapphire blue, dark blue, sea blue, grass green, blackish green, in green, peacock green, golden yellow, black.
Comminutor in the step (3) and step (5) is that BZJ types are centrifuged coating granulator.
Advantages of the present invention：The present invention heat discoloration ink is used in the preparation technology of perfumed beads, made by perfumed beads
Not only there is gay colours, suitable fragrance matter is loaded into, moreover it is possible to color changeable effect, impart to color grains pearl new
Version；In being added to the transparent filter stick of cigarette, the produced flue-gas temperature in aspiration procedure of cigarette is carried out to color pearl
Heating, color pearl color of being heated changes, while the aroma component that flue gas is taken out of in particle pearl, not only can carry to tobacco rolling belt
The fragrance of high suction quality, moreover it is possible to the color change of particle pearl is intuitive to see very much in suction, makes consumer experience vision
With the dual experience of the sense of taste.
Specific embodiment
The specific embodiment of the present invention is described in further detail with reference to embodiment.Following examples are
Laboratory data.
Embodiment 1：A kind of preparation method of tobacco aromaticss pearl, comprises the following steps that：
(1) tobacco leaf, anise are taken as raw material, by 1:1 ratio is crushed, is sieved, the natural plants needed for obtaining
Powder, powder diameter is 30 mesh.Plant powder and starch, shitosan, microcrystalline cellulose are filled according to the ratio in table 1-1
Divide and be hybridly prepared into solid mixed-powder；
Table 1-1 solid mixed-powder composition of raw materials
| Species | Weight portion |
| Plant powder (tobacco leaf, anise) | 10 |
| Starch | 40 |
| Shitosan | 30 |
| Microcrystalline cellulose | 20 |
(2) take the solid mixed-powder prepared in step (1) to be placed in BZJ types centrifugation coating granulator, then prepare matter
Amount percentage is that 5% hydroxypropyl cellulose aqueous solution is sprayed as binder solution, powder rotary in centrifuge
Into parent nucleus；Wherein solid mixed-powder and the mass ratio of hydroxypropyl cellulose aqueous solution are 60:40；
(3) granulation in step (2) is formed into parent nucleus to be sieved, particle size range is controlled at 250 μm, is then continued parent nucleus
In being positioned over BZJ types centrifugation coating granulator, sprayed as slurry using discoloration spices adhesive solution, and in sprinkling process
Middle to add the solid mixed powder prepared in step (1), continuing amplification pill makes its particle diameter rise to target zone；Aimed dia
For 1.2mm, the orange flavor pearl that particle diameter is 1.2mm is obtained through screening, wherein discoloration spices adhesive solution and solid mixed powder
The mass ratio of material is 10:90；The composition of raw materials such as table 2-1 of the discoloration spices adhesive solution；
The composition of raw materials of table 2-1 discoloration spices adhesive solutions
The concrete preparation of discoloration spices adhesive solution：It is first that whole hydroxypropyl celluloses, curcumin and fragrant chrysanthemum medicinal extract is molten
Solution is configured to mixed solution in the water of 20 weight portions, and then color shifting ink is dissolved into the water of 56 weight portions, stirs 1 hour
The color shifting ink aqueous solution is prepared completely in dissolving, then adhesive, pigment and essence mixed aqueous solution and the color shifting ink aqueous solution are mixed
Close, stir dissolving in 1 hour and be configured to the spices adhesive solution that changes colour completely.
By the orange flavor pearl of a diameter of 1.2mm obtained in embodiment 1, in being applied to the transparent filter stick of cigarette.Cigarette exists
Can be appreciated that color pearl color, by orange yellowing, can experience stronger pungent fragrance during cigarette smoking during room temperature
Road, relatively coordinates with flue gas cigarette perfume.
Embodiment 2：A kind of preparation method of tobacco aromaticss pearl, comprises the following steps that：
(1) tobacco leaf, lavender are taken as raw material, by 2:1 ratio is crushed, is sieved, the natural plants needed for obtaining
Powder, powder diameter is 60 mesh.Plant powder and starch, shitosan, microcrystalline cellulose are filled according to the ratio in table 1-2
Divide and be hybridly prepared into solid mixed-powder；
Table 1-2 solid mixed-powder composition of raw materials
| Species | Weight portion |
| Plant powder (tobacco leaf, lavender) | 20 |
| Starch | 30 |
| Shitosan | 40 |
| Microcrystalline cellulose | 10 |
(2) the solid mixed-powder prepared in step (1) is placed in BZJ types centrifugation coating granulator, then prepares matter
Amount percentage is that the 10% hydroxypropyl methyl cellulose aqueous solution is sprayed as binder solution, and powder revolves in centrifuge
Turn to form parent nucleus, wherein solid mixed-powder and the mass ratio of the hydroxypropyl methyl cellulose aqueous solution are 70:30；
(3) granulation in step (2) is formed into parent nucleus to be sieved, particle size range is controlled at 350 μm, is then continued parent nucleus
In being positioned over BZJ types centrifugation coating granulator, sprayed as slurry using discoloration spices adhesive solution, and in sprinkling process
Middle to add the solid mixed powder prepared in step (1), continuing amplification pill makes its particle diameter rise to target zone；Aimed dia
For 1.6mm, the purple perfumed beads that particle diameter is 1.6mm are obtained through screening, wherein discoloration spices adhesive solution and solid mixed powder
The mass ratio of material is 20:80；The composition of raw materials such as table 2-2 of the discoloration spices adhesive solution；
The composition of raw materials of table 2-2 discoloration spices adhesive solutions
| Species | Weight portion |
| Adhesive (hydroxypropyl methyl cellulose) | 10 |
| Pigment (famille rose) | 0.5 |
| Color shifting ink (water color ink, the variable white of royalblue, 30 DEG C of discoloring temperature) | 10 |
| Essence (flavoring rose essence) | 5 |
| Water | 74.5 |
The concrete preparation of discoloration spices adhesive solution：First adhesive, pigment, essence are dissolved into the water of 20 weight portions and are matched somebody with somebody
Mixed solution is made, then color shifting ink is dissolved into the water of 54.5 weight portions, stirred dissolving in 2 hours and be configured to discoloration completely
The ink aqueous solution, then the mixed aqueous solution of adhesive, pigment and essence is mixed with the color shifting ink aqueous solution, stirring 2 hours is molten
Solution is configured to completely the spices adhesive solution that changes colour.
Purple perfumed beads of the diameter in 1.6mm will be obtained in embodiment 2, in being applied to the transparent filter stick of cigarette.Cigarette is being taken out
Can be appreciated that color pearl color from purple becomes red after inhaling 3 mouthfuls, stronger fragrance of a flower taste can be experienced during cigarette smoking, with flue gas
Cigarette perfume is relatively coordinated.
Embodiment 3：A kind of preparation method of tobacco aromaticss pearl, comprises the following steps that：
(1) cloves, jasmine are taken as raw material, by 4：3 ratio is crushed, is sieved, the natural vegetable powder needed for obtaining
End, powder diameter is 80 mesh.Plant powder and starch, shitosan, microcrystalline cellulose are carried out fully according to the ratio in table 1-3
It is hybridly prepared into solid mixed-powder；
Table 1-3 solid mixed-powder composition of raw materials
| Species | Weight portion |
| Plant powder (cloves, jasmine) | 30 |
| Starch | 30 |
| Shitosan | 20 |
| Microcrystalline cellulose | 20 |
(2) the solid mixed-powder prepared in step (1) is placed in BZJ types centrifugation coating granulator, then by poly- dimension
Ketone and hydroxypropyl methyl cellulose in mass ratio 1:2 ratio mixed preparing mixed adhesive, is then dissolved in mixed adhesive
In pure water, it is configured to the mixed adhesive aqueous solution that binder concn is 10% and is sprayed, powder rotates in centrifuge
Parent nucleus is formed, wherein solid mixed-powder and the mass ratio of the mixed adhesive aqueous solution are 80:20；
(3) granulation in step (2) is formed into parent nucleus to be sieved, particle size range is controlled at 450 μm, is then continued parent nucleus
In being positioned over BZJ types centrifugation coating granulator, sprayed as slurry using discoloration spices adhesive solution, and in sprinkling process
Middle to add the solid mixed powder prepared in step (1), continuing amplification pill makes its particle diameter rise to target zone；Aimed dia
For 3.0mm, the brown perfumed beads that particle diameter is 3.0mm are obtained through screening, wherein discoloration spices adhesive solution and solid mixed powder
The mass ratio of material is 30:70；The composition of raw materials such as table 2-3 of the discoloration spices adhesive solution；
The composition of raw materials of table 2-3 discoloration spices adhesive solutions
The concrete preparation of discoloration spices adhesive solution：First adhesive, pigment, essence are dissolved into the water of 30 weight portions and are matched somebody with somebody
Mixed solution is made, then color shifting ink is dissolved into the water of 35 weight portions, stirred dissolving in 2 hours and be configured to discoloration oil completely
Ink solution, then the mixed aqueous solution of adhesive, pigment and essence is mixed with the color shifting ink aqueous solution, stir 2 hours and dissolve
The spices adhesive solution that changes colour is configured to completely.
Brown perfumed beads of the diameter in 3.0mm will be obtained in embodiment 3, in being applied to the transparent filter stick of cigarette.Cigarette is being taken out
Can be appreciated that color pearl color becomes cyan by brown after inhaling 5 mouthfuls, very strong fragrance of a flower taste can be experienced during cigarette smoking.
Claims (6)
1. a kind of discoloration tobacco aromaticss pearl, it is characterised in that the perfumed beads constitute a diameter of by parent nucleus and discoloration spices shell
The colour-changeable perfumed beads of 1.0～4.0mm, the wherein particle diameter of parent nucleus are 250～450 μm, and the discoloration spices shell passes through
The mode of coating is wrapped in parent nucleus surface；
The parent nucleus raw material is 10～50% including the solid mixed powder that mass percent is 50～90% and mass percent
Binder solution, wherein binder solution are that the water by the adhesive that mass percent is 1～20% with 80～99% mixes and matches somebody with somebody
System is formed；
It is described discoloration spices shell material be with mass percent including the solid mixed powder that mass percent is 70～90%
10～30% discoloration spices adhesive solution, wherein the discoloration spices adhesive solution is by adhesive, pigment, essence, discoloration
Ink and water are according to ratio of weight and number 1～20：0.1～10：0.1～10：0.1～20：50～90 ratio is mixed；
In above-mentioned formula, the solid mixed powder is according to weight by natural plant powder, starch, shitosan, microcrystalline cellulose
Amount portion rate 1～30：1～50：1～50：1～20 ratio is mixed；
Described adhesive is the one kind or many in PVP, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethylcellulose calcium
Kind；
The pigment is water-soluble food coloring；The essence is soluble perfume；The color shifting ink is that heat discoloration is water-soluble
Property ink, its discoloration cardinal temperature be 5 DEG C～60 DEG C.
2. a kind of discoloration tobacco aromaticss pearl according to claim 1, it is characterised in that：Wherein natural plant powder is particle diameter
The powder of 30 mesh～80 mesh, specifically by tobacco leaf, anise, the seed of Chinese dodder, lavender, peppermint, thyme, bay, Chinese cassia tree, sweet
The powder that any one or more plant in grass, dried orange peel, cloves, Chinese ilex, Pogostemon cablin, jasmine is formed after crushing.
3. a kind of discoloration tobacco aromaticss pearl according to claim 1, it is characterised in that：The pigment of discoloration spices shell includes
Natural bata-carotene, beet red, turmeric, safflower yellow, lac be red, more Exocarpium Citri Rubrum, capsanthin, chilli orange, burnt sugar coloring, red rice be red, chrysanthemum
Spend red yellow medicinal extract, black soya bean, Kaoliang red, maize, radish red, cacao pigment, red yeast rice, Monascus color, the certain herbaceous plants with big flowers that falls is red, Hei Jialun is red, Cape jasmine
Sub yellow, gardenia blue, sea-buckthorn is yellow, roselle is red, acorn cup is brown, many favour Ke palm fibre, and mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, turmeric
Element, peanut agriculture is red, Grape Skin is red, blue ingot arnotto, algae are blue, plant carbon black, Mi Menghuang, Asian puccoon is red, tea uranidin, Tea Green Pigment,
One or more in oranges and tangerines Huang, relation by marriage fat tree orange, famille rose；The essence is water-soluble flavouring essence for tobacco or water-soluble edible perfume
Essence；The color of the color shifting ink include bright red, rhodo, it is pink, bright red, orange red, sapphire blue, dark blue, sea blue, grass green, blackish green, in
Green, peacock green, golden yellow, black.
4. in a kind of claims 1 to 3 described in any one discoloration tobacco aromaticss pearl preparation method, it is characterised in that tool
Body step is as follows：
(1) natural plants are taken as raw material, is crushed, is sieved, obtain the natural plant powder that particle diameter is 30 mesh～80 mesh, so
Afterwards by the natural plant powder for obtaining, starch, shitosan, microcrystalline cellulose according to ratio of weight and number 1～30：1～50：1～50：
1～20 ratio is well mixed the solid mixed powder to form parent nucleus raw material；
(2) prepare after the adhesive that mass percent is 1～20% is mixed with the pure water that mass percent is 80～99%
Composite adhesives solution；Wherein described adhesive is PVP, hydroxypropyl cellulose, hydroxypropyl methyl cellulose, carboxymethyl cellulose
One or more in element；
(3) solid mixed powder in step (1) is placed in centrifugation coating granulator, and the adhesive that will be prepared in step (2)
Solution is sprayed as slurry, and powder rotates in centrifuge and forms parent nucleus；And sieved parent nucleus, particle size range control
At 250～450 μm；
(4) raw material of discoloration spice solution is weighed according to following parts by weight：Adhesive 1～20, pigment 0.1～10, essence 0.1
～10, color shifting ink 0.1～20, water 50～90；Whole adhesives, pigment, essence are first dissolved into the water of 10～30 weight portions
In be configured to mixed aqueous solution, then color shifting ink is dissolved into the water of 40～60 weight portions, stirring dissolved within 1～2 hour
The color shifting ink aqueous solution is configured to entirely, then the color shifting ink aqueous solution for preparing is mixed with adhesive, pigment, the essence aqueous solution
Stir 1～2 hour afterwards, to dissolving discoloration spices adhesive solution is formed completely；Described adhesive is PVP, hydroxy propyl cellulose
One or more in element, hydroxypropyl methyl cellulose, carboxymethylcellulose calcium；
(5) parent nucleus of granulation in step (3) is continued to be positioned in centrifugation coating granulator, and by step 4) in prepare
Discoloration spices adhesive solution is sprayed as slurry, and the solid mixed powder prepared in step (1) is added during sprinkling
Material, continuing amplification pill makes its particle diameter rise to 1.0～4.0mm, forms changeable colour tobacco aromaticss pearl；Wherein slurry is mixed with solid
The mass ratio for closing powder is 10～30:70～90.
5. according to a kind of preparation method of the discoloration tobacco aromaticss pearl described in claim 4, it is characterised in that：The step
(1) natural plants in are tobacco leaf, anise, the seed of Chinese dodder, lavender, peppermint, thyme, bay, Chinese cassia tree, Radix Glycyrrhizae, dried orange peel, fourth
Any one or more in perfume, Chinese ilex, Pogostemon cablin, jasmine.
6. according to a kind of preparation method of the discoloration tobacco aromaticss pearl described in claim 4, it is characterised in that：In step (4)
In, the pigment is water-soluble food coloring；Including natural bata-carotene, beet red, turmeric, safflower yellow, lac be red, cowberry
Red, capsanthin, chilli orange, burnt sugar coloring, red rice are red, coreopsis yellow extract, red black soya bean, Kaoliang red, maize, radish red, cocoa shell
Color, red yeast rice, Monascus color, the certain herbaceous plants with big flowers that falls are red, Hei Jialun is red, Gardenia Yellow, gardenia blue, and sea-buckthorn is yellow, roselle is red, acorn cup is brown, many favours
Ke Zong, mulberry fruit is red, natural leaf mustard is red, the fruit of Cherokee rose is brown, curcumin, peanut agriculture is red, Grape Skin is red, blue ingot arnotto, algae are blue, plant charcoal
It is black, Mi Menghuang, Asian puccoon is red, tea uranidin, Tea Green Pigment, oranges and tangerines are yellow, relation by marriage fat tree orange, it is carmine in one or more；It is described
Essence is water-soluble flavouring essence for tobacco or water-soluble edible essence；The color shifting ink is heat discoloration water-based ink, its discoloration
Cardinal temperature be 5 DEG C～60 DEG C, its color is including but not limited to bright red, rhodo, pink, bright red, orange red, sapphire blue, dark blue, sea
It is blue, grass green, blackish green, in green, peacock green, golden yellow, black.
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