CN106566751A - Black grain, velvet antler and flavonoids type white spirit - Google Patents

Abstract

The invention discloses a black grain, velvet antler and flavonoids type white spirit. The white spirit is prepared from the following raw materials in weight part: 180-200 of black rice, 95-105 of black buckwheat, 12-15 of green tea leaves, 8-10 of red sage root, 1-2 of liquor-making koji, 10-12 of mountain dew vegetables, 24-26 of velvet antler, 1-2 of ammonium sulfate, 35-38 of blackbark chinese pine needles, a proper amount of 50% ethanol solution, and a proper amount of water. According to the technical scheme of the invention, based on the traditional white spirit brewing process, black rice, buckwheat and other black grains are adopted as main fermentation raw materials. Therefore, the obtained white spirit is endowed with the special flavor of black grains. Meanwhile, green tea leaves, red sage roots and the like are added, so that the nutritional value of the white spirit is much higher than that of the conventional white spirit. The commodity of the white spirit is improved.

Description

A kind of black grain Cornu Cervi Pantotrichum flavone Chinese liquor

Technical field

The present invention relates to Liquor Making Technology field, more particularly to a kind of black grain Cornu Cervi Pantotrichum flavone Chinese liquor.

Background technology

In recent years, with the quickening of modern urbanization paces, inferior health problem becomes increasingly conspicuous, and the species for occurring on the market Various health food balanced cannot ensure nutrition intake, and expensive, be not suitable for long-term taking, how be reached by diet Health care effect has attracted increasing attention.China is drinks production and consumption big country, and the idea that it is not a banquet without wine is deep Enter the popular feeling, under this background functional health Chinese liquor has been a great deal of attention, and health-care spirit product in the market Matter is very different, especially in the deep processing of raw material, thoroughly other unnecessary miscellaneous tastes can not be prevented because removing to impurity Entrance, have impact on the pure of wine body local flavor, the stability of its composition is also worth discussion, therefore researches and develops the feature of high-quality and protect Strong Chinese liquor has been imperative.

Blackbark Chinese pine is Pinaceae pine genus plant, and its leaf is Folium Pini, is commonly used for medicine and food additive field, is had The effect of blood-promoting and mind-easing, anti-inflammatory anti-itch.Flavone compound in Folium Pini even more has that anticancer health care, blood sugar lowering be antibacterial, in protection Pivot nerve and cardio-cerebrovascular physiologically active, because flavone is poorly soluble in water, it is impossible to efficiently make brew agent for Use, and it makes it fabulous can mix with Chinese liquor system the characteristics of being soluble in alcohols.

Spotted deer antler is the unossified young horn of the close raw fine hair of Cervus nippon Temminck stag, and Cornu Cervi Pantotrichum is uniquely deposited as mammal circle The histoorgan that can quickly live again, wherein containing protein, aminoacid, fatty acid, phospholipid, polysaccharide etc. it is various it is organic into Point, also containing various macro- and trace-elements needed by human, due to without effective processing extraction technique, being often used to immersion In drinks, using there is inconvenience more.

Based on this, the present inventor by more than both preparation technology and with White wine brewing process be combined with each other into Go and studied and explore, brewed the new Cornu Cervi Pantotrichum flavone Chinese liquor for catering to market comsupton demand.

The content of the invention

The object of the invention is exactly to make up the defect of prior art, there is provided a kind of black grain Cornu Cervi Pantotrichum flavone Chinese liquor.

The present invention is achieved by the following technical solutions：

A kind of black grain Cornu Cervi Pantotrichum flavone Chinese liquor, is prepared by the raw materials in：Fructus zizaniae caduciflorae 180-200, black Semen Fagopyri Esculenti 95-105, green tea Leaf 12-15, Radix Salviae Miltiorrhizae 8-10, wine brewing song 1-2, Petasites tatewakianus Kitam. 10-12, Cornu Cervi Pantotrichum 24-26, ammonium sulfate 1-2, blackbark Chinese pine Folium Pini 35-38, 50% ethanol solution is appropriate, appropriate amount of water.

Described black grain Cornu Cervi Pantotrichum flavone Chinese liquor preparation method is comprised the following steps that：

（1）The blackbark Chinese pine Folium Pini won is cleaned and is air-dried and is crushed after ventilating and cooling place, and according to solid-liquid ratio 1：25-30g/ ML is placed in 50% ethanol solution, is heated to 60-65 DEG C, and the supersound extraction 40-60 minute under constant power 300W, and ultrasound is complete Into rear filtration, filtrate is dried at 34-38 DEG C, obtain extract from pine needles powder standby；

（2）During steaming grain pot is put into after fructus zizaniae caduciflorae, black Semen Fagopyri Esculenti clear water are cleaned, water temperature is added water to submerge and heated to 90-95 DEG C, it is vexed to boil 40-45 minutes, the water not absorbed by material is bled off afterwards, opens gas and continue steaming and decocting 50-60 minutes, after the completion of close gas and material is vexed 15-20 minutes, 16-24 hours, wherein mixture and water are soaked with step 1 gained extract from pine needles powder after taking-up in water Mass ratio is 1：0.6-0.8, pre fermentation 6-8 days in fermentation tank are collectively disposed at after the completion of immersion by resulting material together with soak, Obtain pre fermentation material standby；

（3）Step 2 gained pre fermentation material is put into into steamer lower floor, while clean green tea, Radix Salviae Miltiorrhizae are wrapped up with double gauze After be put into steamer upper strata common steaming and decocting 40-60 minutes, after the completion of steaming and decocting take out naturally cool to room temperature, upper strata steaming and decocting material is smashed to pieces The cooking liquor of filtration gauze is collected into after mud, gauze is removed afterwards, by remaining siccative and lower floor's steaming and decocting material, wine brewing song, mountain dew Dish mixed fermentation 30-35 days, during fermentation per aerofluxuss in 4-6 days once, fermentation complete fermentation material is standby；

（4）To clean after Cornu Cervi Pantotrichum peeling, remove residual Sanguis cervi, be cut into the fritter of 3-4 millimeters, 40-50 mesh sieves were crushed after lyophilizing, Gained Pulveratum Cornu Cervi Pantotrichum is pressed into solid-liquid ratio 1：During 50-60g/mL input pH are for the sodium carbonate-bicarbonate buffer solution of 9.0-9.5, soak Bubble extracts 6-8 hours, after the completion of be added thereto to ammonium sulfate again, be cooled to 3-5 DEG C after stirring, keep 8-12 hours, it is complete Into after in 3500-4000 rev/min of lower centrifugal filtration, the lyophilized powder that Cornu Cervi Pantotrichum is obtained after gained pellet frozen is dried is standby；

（5）Step 3 gained fermentation material dress is discriminated into distillation, 220-240 DEG C of distillation 50-60 minute is controlled in still-process, then dropped Temperature is finally warming up to 200-220 DEG C of distillation 25-35 minute to 150-160 DEG C of distillation 120-130 minute, and resulting material is down to Mix with step 3 gained cooking liquor, step 4 obtained freeze-drying powder to stir evenly after room temperature and stand 1-2 days at 4-5 DEG C, after the completion of mistake Filter is obtained final product.

It is an advantage of the invention that：

The present invention is raw materials used by various cleaning digesting technoloys, reaches the mesh that raw material surface impurity and pollutant are removed completely , not only prevent the secondary pollution problem during making wine, also effectively exclude the generation of the miscellaneous taste of wine brewing, it is ensured that the perfume (or spice) of wine body Gas composition is all from sweat, while by the extraction process to blackbark Chinese pine Folium Pini and Cornu Cervi Pantotrichum high-quality, effectively will Active material ingredients in Flavonoid substances and Cornu Cervi Pantotrichum in blackbark Chinese pine Folium Pini are proposed, and cooperate with making for other fermentation raw materials With, the purpose that nutritional labeling is stably dissolved each other with Chinese liquor is realized, significantly increase the health-care effect of Chinese liquor.

The present invention, using black grains such as fructus zizaniae caduciflorae, black Semen Fagopyri Esculentis as dominant fermentation raw material, can be white on traditional liquor brewage process Wine gives black grain special local flavor, while coordinating the addition of green tea, Radix Salviae Miltiorrhizae etc., makes nutritive value content in wine liquid be far above normal Rule Chinese liquor, improves the commodity of Chinese liquor.

Specific embodiment

A kind of black grain Cornu Cervi Pantotrichum flavone Chinese liquor, by following weight portion（kg）Raw material make：Fructus zizaniae caduciflorae 180, black Semen Fagopyri Esculenti 95, green tea Leaf 12, Radix Salviae Miltiorrhizae 8, wine brewing song 1, Petasites tatewakianus Kitam. 10, Cornu Cervi Pantotrichum 24, ammonium sulfate 1, blackbark Chinese pine Folium Pini 35,50% ethanol solution are appropriate, water In right amount.

Described black grain Cornu Cervi Pantotrichum flavone Chinese liquor preparation method is comprised the following steps that：

（1）The blackbark Chinese pine Folium Pini won is cleaned and is air-dried and is crushed after ventilating and cooling place, and according to solid-liquid ratio 1：25g/mL In being placed in 50% ethanol solution, it is heated to 60 DEG C, and supersound extraction 40 minutes under constant power 300W, filtering after the completion of ultrasound, Filtrate is dried at 34 DEG C, obtains extract from pine needles powder standby；

（2）During steaming grain pot is put into after fructus zizaniae caduciflorae, black Semen Fagopyri Esculenti clear water are cleaned, water temperature is added water to submerge and heated to 90 DEG C, it is vexed to boil 45 Minute, the water not absorbed by material is bled off afterwards, open gas and continue steaming and decocting 60 minutes, after the completion of close gas and material is vexed 15 minutes, Soak in water 16 hours with step 1 gained extract from pine needles powder after taking-up, wherein mixture and the mass ratio of water are 1： 0.6, resulting material is collectively disposed at into pre fermentation 6 days in fermentation tank together with soak after the completion of immersion, obtain pre fermentation material standby；

（3）Step 2 gained pre fermentation material is put into into steamer lower floor, while clean green tea, Radix Salviae Miltiorrhizae are wrapped up with double gauze After be put into the common steaming and decocting in steamer upper strata 40 minutes, after the completion of steaming and decocting take out naturally cool to room temperature, upper strata steaming and decocting material is smashed to pieces into The cooking liquor of filtration gauze is collected after mud, gauze is removed afterwards, by remaining siccative and lower floor's steaming and decocting material, wine brewing song, Petasites tatewakianus Kitam. Mixed fermentation 30 days, during fermentation per aerofluxuss in 4 days once, fermentation complete fermentation material is standby；

（4）To clean after Cornu Cervi Pantotrichum peeling, remove residual Sanguis cervi, be cut into 3 millimeters of fritter, 40 mesh sieves were crushed after lyophilizing, by institute Obtain Pulveratum Cornu Cervi Pantotrichum and press solid-liquid ratio 1：50g/mL input pH are soak extraction 6 hours in 9.0 sodium carbonate sodium bicarbonate buffer solution, After the completion of be added thereto to ammonium sulfate again, be cooled to 3 DEG C after stirring, kept for 8 hours, after the completion of under 3500 revs/min from The heart is filtered, and the lyophilized powder that Cornu Cervi Pantotrichum is obtained after gained pellet frozen is dried is standby；

（5）Step 3 gained fermentation material dress is discriminated into distillation, 220 DEG C is controlled in still-process and is distilled 50 minutes, then be cooled to 150 DEG C distillation 120 minutes, be finally warming up to 200 DEG C distill 25 minutes, resulting material is down to after room temperature and step 3 gained steaming and decocting Liquid, the mixing of step 4 obtained freeze-drying powder are stirred evenly and stand 1 day at 4 DEG C, after the completion of filter and obtain final product.

Claims (2)

1. a kind of black grain Cornu Cervi Pantotrichum flavone Chinese liquor, it is characterised in that be prepared by the raw materials in：Fructus zizaniae caduciflorae 180-200, black buckwheat Wheat 95-105, green tea 12-15, Radix Salviae Miltiorrhizae 8-10, wine brewing song 1-2, Petasites tatewakianus Kitam. 10-12, Cornu Cervi Pantotrichum 24-26, ammonium sulfate 1-2, casting skin Pinus Tabulaeformis Carr. Pine Needles 35-38,50% ethanol solution are appropriate, appropriate amount of water.

2. the black grain Cornu Cervi Pantotrichum flavone Chinese liquor according to claims 1, it is characterised in that the concrete steps of preparation method are such as Under：

（1）The blackbark Chinese pine Folium Pini won is cleaned and is air-dried and is crushed after ventilating and cooling place, and according to solid-liquid ratio 1：25- 30g/mL is placed in 50% ethanol solution, is heated to 60-65 DEG C, and the supersound extraction 40-60 minute under constant power 300W, is surpassed Filter after the completion of sound, dry filtrate at 34-38 DEG C, obtain extract from pine needles powder standby；

（2）During steaming grain pot is put into after fructus zizaniae caduciflorae, black Semen Fagopyri Esculenti clear water are cleaned, water temperature is added water to submerge and heated to 90-95 DEG C, it is vexed Boil 40-45 minutes, the water not absorbed by material bled off afterwards, open gas and continue steaming and decocting 50-60 minutes, after the completion of close gas and by material Vexed 15-20 minutes, 16-24 hours, wherein mixture and water are soaked in water with step 1 gained extract from pine needles powder after taking-up Mass ratio be 1：0.6-0.8, pre fermentation 6-8 in fermentation tank is collectively disposed at after the completion of immersion by resulting material together with soak My god, obtain pre fermentation material standby；

（3）Step 2 gained pre fermentation material is put into into steamer lower floor, while clean green tea, Radix Salviae Miltiorrhizae are wrapped up with double gauze After be put into steamer upper strata common steaming and decocting 40-60 minutes, after the completion of steaming and decocting take out naturally cool to room temperature, upper strata steaming and decocting material is smashed to pieces The cooking liquor of filtration gauze is collected into after mud, gauze is removed afterwards, by remaining siccative and lower floor's steaming and decocting material, wine brewing song, mountain dew Dish mixed fermentation 30-35 days, during fermentation per aerofluxuss in 4-6 days once, fermentation complete fermentation material is standby；

（4）To clean after Cornu Cervi Pantotrichum peeling, remove residual Sanguis cervi, be cut into the fritter of 3-4 millimeters, 40-50 mesh was crushed after lyophilizing Sieve, by gained Pulveratum Cornu Cervi Pantotrichum solid-liquid ratio 1 is pressed：During 50-60g/mL input pH are for the sodium carbonate-bicarbonate buffer solution of 9.0-9.5, Soak extraction 6-8 hours, after the completion of be added thereto to ammonium sulfate again, be cooled to 3-5 DEG C after stirring, keep 8-12 hours, After the completion of in 3500-4000 rev/min of lower centrifugal filtration, after gained pellet frozen is dried Cornu Cervi Pantotrichum lyophilized powder it is standby；

（5）Step 3 gained fermentation material dress is discriminated into distillation, 220-240 DEG C of distillation 50-60 minute is controlled in still-process, then dropped Temperature is finally warming up to 200-220 DEG C of distillation 25-35 minute to 150-160 DEG C of distillation 120-130 minute, and resulting material is down to Mix with step 3 gained cooking liquor, step 4 obtained freeze-drying powder to stir evenly after room temperature and stand 1-2 days at 4-5 DEG C, after the completion of mistake Filter is obtained final product.