CN106521935A - Ultra-soft fast soluble film and preparation method thereof - Google Patents
Ultra-soft fast soluble film and preparation method thereof Download PDFInfo
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- CN106521935A CN106521935A CN201610955222.8A CN201610955222A CN106521935A CN 106521935 A CN106521935 A CN 106521935A CN 201610955222 A CN201610955222 A CN 201610955222A CN 106521935 A CN106521935 A CN 106521935A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/188—Monocarboxylic acids; Anhydrides, halides or salts thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/248—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing sulfur
- D06M13/262—Sulfated compounds thiosulfates
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/325—Amines
- D06M13/332—Di- or polyamines
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/263—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated carboxylic acids; Salts or esters thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/53—Polyethers
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/647—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing polyether sequences
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- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Belonging to the textile industry, the invention in particular relates to an ultra-soft fast soluble film and a preparation method thereof specific to textile dyeing and finishing technology. The ultra-soft fast soluble film provided by the invention comprises the following components by weight percentage: 60-80% of stearic acid, 6-15% of diethylenetriamine, 2-5% of triethylene tetramine, 2-6% of triethanolamine, 3-6% of hydroxyethyl ethylenediamine, 2-7% of dimethyl sulfate, 0.1-1.2% of p-toluenesulfonic acid, 8-15% of fatty alcohol polyoxyethylene ether, 1.5-3.5% of a dispersing agent, 1-4% of a swelling agent, 1-3% of a leveling agent, 1-4% of a softening agent, and 2-6% of an efficient defoaming agent. The ultra-soft fast soluble film provided by the invention not only has good dye penetration and excellent dispersion properties, but also has strong acid and alkali resistance and dielectric resistance, can make the fabric fuller, smoother and more resilient, and has the advantages of no yellowing, no fading and no staining, etc.
Description
Technical field
The invention belongs to textile industry field, a kind of ultra-soft Instant film for being specific to textile dyeing and finishing technology and providing
And preparation method thereof.
Background technology
Ultra-soft Instant film is mainly used in the fabric finishing operation in textile industry, it is adaptable to cotton, fiber crops, yarn,
The clothes such as nylon fibre.The Instant film of high-quality has stronger acid and alkali-resistance, resistance to electrolyte stability, the handss with cation film
Sense characteristic, can give yarn fabric cloth excellent softness, can promote its cloth more plentiful lubrication after dyeing and finishing, be rich in bullet
Property, also increase value-added content of product.
At present, typically it is used for the dyeing and finishing of textile industry cloth on market using common instant flexible sheets, and the country is also looked forward to
Industry still using external superseded printing and dyeing assistant product, especially with some films made by high concentration solvent type, not only
Easy flavescence, staining are brought after making cloth dyeing and finishing, flexibility is not good enough, washability is poor, and its flatness is poor, wrinkle resistance and sewing
Property it is poor, the particularly more external advanced super soft instant flexible sheets consumption of film consumption increased more than 30%, cause labor intensity it is high,
Low production efficiency, production cost are high, the situation that product quality is unstable.Also it is fine that domestic high-end silk fabric, silk, cloth, chinlon are constrained simultaneously
Dimension cloth proposes shelves upgrading, foreign exchange earning.Therefore in the urgent need to by industry restructuring, improving product class, the economic effect of raising
Benefit, guarantee national industry development, solve many problems, such as energy-saving and environmental protection, benefit etc. present in existing process technology conscientiously,
Independent intellectual property right and brand names are made, material time length, production efficiency that existing conventional instant film is present thoroughly is solved
Low, energy resource consumption is big, the low realistic problem of product specification.
The content of the invention
In order to thoroughly solve defect in terms of existing some Technologies during existing conventional instant film use, this
Invention provides a kind of ultra-soft Instant film and preparation method thereof, and obtained ultra-soft Instant film not only has good
Color infiltration, dispersive property is good, can make the splendid more plentiful lubrication of fabric, high resilience, and its softness, acid-fast alkali-proof, resistance to
Electrolyte.
Technical scheme：
In order to solve above-mentioned technical problem, a kind of ultra-soft Instant film of the present invention and preparation method thereof, this is soft
Piece is made up of following percentage by weight proportioning raw materials component：
Stearic acid 60～80%, diethylenetriamine 6～15%, triethylene tetramine 2～5%, triethanolamine 2～6%, hydroxyl second
Base ethylenediamine 3～6%, dimethyl sulfate 2～7%, p-methyl benzenesulfonic acid 0.1～1.2%, aliphatic alcohol polyethenoxy base ether 8～
15%th, dispersant 1.5～3.5%, swelling agent 1～4%, levelling agent 1～3%, softening agent 1～4%, high effective antifoaming agent 2～
6%.
Preferred feedstock weight percent composition of the present invention is：
Stearic acid 60～75%, diethylenetriamine 6～11%, triethylene tetramine 2.5～4.5%, triethanolamine 2～5%,
Hydroxyethylethylene diamine 3～5%, dimethyl sulfate 2～5%, p-methyl benzenesulfonic acid 0.1～1%, aliphatic alcohol polyethenoxy base ether 8～
13%th, dispersant 1～3%, swelling agent 1～3%, levelling agent 1～2%, softening agent 1～3%, high effective antifoaming agent 2～4%.
Described dispersant selects maleic acid-acrylic acid copolymer sodium salt dispersant
Described swelling agent selects methyl naphthalene sulfonic acid salt formaldehyde condensation products p-type swelling agent
Described levelling agent selects peregal O-25 levelling agent
Described softening agent selects RT type fatty acid softening agents
Described high effective antifoaming agent selects polyether-modified polydimethylsiloxane defoamer
A kind of ultra-soft Instant film of the present invention and preparation method thereof, specific its production craft step is：
1st, stearic acid is initially charged in a kettle., be then turned on heating valve and be slowly ramped to 110～120 DEG C；
2nd, when reaching 110～120 DEG C, diethylenetriamine, triethylene tetramine, three ethanol are sequentially added in a kettle.
Amine, hydroxyethylethylene diamine, dimethyl sulfate, p-methyl benzenesulfonic acid, dispersant, swelling agent, levelling agent, softening agent, high effective antifoaming agent,
Opening blender simultaneously carries out mix homogeneously stirring；
3rd, open steam valve slowly to be heated up, when temperature reaches 190～220 DEG C, steam off valve, static 6～
10min, opening vacuum pump carries out evacuation process, is reacted using one side, and evacuation makes material react 6 in a kettle.
～10h；
4th, after 6～10h of question response, using cooling treatment method, when material is cooled to 90～110 DEG C, add fatty alcohol
Polyoxyethylene ether is catalyzed, and uniform stirring.
5th, after reacting 8～15min, drain hole valve is opened, process is dried by drying machine, required ultra-soft is obtained
The solid product of Instant film.
6th, after will be obtained ultra-soft Instant film qualified after testing, put in storage after being packed by 25kg measurement criteria.
Beneficial effects of the present invention
The invention provides a kind of ultra-soft Instant film efficiently solve compared with the product of existing market, not only it is conventional soft
Piece material time long problem, material time, by original 90 minutes, are shortened to 10 minutes or so, improve labor productivity and section
The about consumption of the energy.But also with stronger acid and alkali-resistance, resistance to electrolyte, the more plentiful lubrication of fabric can be made, be more rich in bullet
Property, not yellowing, do not fade, not staining the features such as.Also there is dyeing and finishing simultaneously that be relatively adapted to various fabrics, have higher practicality
And use value.
Specific embodiment
In order that technical scheme and production craft step get across, below in conjunction with specific embodiment pair
The present invention is described in further detail below.
Embodiment 1
A kind of ultra-soft Instant film and preparation method thereof, is prepared by following raw material by weight percentage and is made：Hard Fat
Acid 65%, diethylenetriamine 8%, triethylene tetramine 3%, triethanolamine 2%, hydroxyethylethylene diamine 3%, dimethyl sulfate 3%,
P-methyl benzenesulfonic acid 0.5%, aliphatic alcohol polyethenoxy base ether 8%, dispersant 2%, swelling agent 1.5%, levelling agent 1%, softening agent
1%th, high effective antifoaming agent 2%.
Specifically production operation step is：
1st, it is initially charged stearic acid first in a kettle., is then turned on heating valve, starts to be slowly ramped to 110 DEG C, rise
Warm time control is in 1.5h；
2nd, when temperature reaches 110 DEG C, sequentially add in a kettle. diethylenetriamine, triethylene tetramine, triethanolamine,
Hydroxyethylethylene diamine, dimethyl sulfate, p-methyl benzenesulfonic acid, dispersant, swelling agent, levelling agent, softening agent, high effective antifoaming agent, together
Shi Kaiqi blenders carry out mix homogeneously stirring；
3rd, open steam valve slowly to be heated up, when temperature reaches 190 DEG C, steam off valve, after static 8min,
Opening vacuum pump carries out evacuation process, and the whole response time is controlled in 7h；
4th, after reacting 7h, using cooling treatment method, when material is cooled to 90 DEG C, add aliphatic alcohol polyethenoxy base ether
It is catalyzed, and is carried out uniform stirring；
5th, after question response 8min, drain hole valve is opened, process is dried by drying machine, required ultra-soft speed is obtained
The solid product of molten type film；
6th, after will be obtained ultra-soft Instant film qualified after testing, put in storage after being packed by 25kg measurement criteria.
Embodiment 2
A kind of ultra-soft Instant film and preparation method thereof, is prepared by following raw material by weight percentage and is made：Hard Fat
Acid 60%, diethylenetriamine 10%, triethylene tetramine 4%, triethanolamine 3%, hydroxyethylethylene diamine 4%, dimethyl sulfate
2%th, p-methyl benzenesulfonic acid 0.5%, aliphatic alcohol polyethenoxy base ether 9%, dispersant 1.5%, swelling agent 1.5%, levelling agent
1.5%th, softening agent 1%, high effective antifoaming agent 2%.
Specifically production operation step is：
1st, it is initially charged stearic acid first in a kettle., is then turned on heating valve, starts to be slowly ramped to 115 DEG C, rise
Warm time control is in 1.5h；
2nd, when temperature reaches 115 DEG C, sequentially add in a kettle. diethylenetriamine, triethylene tetramine, triethanolamine,
Hydroxyethylethylene diamine, dimethyl sulfate, p-methyl benzenesulfonic acid, dispersant, swelling agent, levelling agent, softening agent, high effective antifoaming agent, together
Shi Kaiqi blenders carry out mix homogeneously stirring；
3rd, open steam valve slowly to be heated up, when temperature reaches 195 DEG C, steam off valve, after static 8min,
Opening vacuum pump carries out evacuation process, and the whole response time is controlled in 8h；
4th, after reacting 8h, using cooling treatment method, when material is cooled to 95 DEG C, add aliphatic alcohol polyethenoxy base ether
It is catalyzed, and is carried out uniform stirring；
5th, after question response 10min, drain hole valve is opened, process is dried by drying machine, required ultra-soft is obtained
The solid product of Instant film；
6th, after will be obtained ultra-soft Instant film qualified after testing, put in storage after being packed by 25kg measurement criteria.
Embodiment 3
A kind of ultra-soft Instant film and preparation method thereof, is prepared by following raw material by weight percentage and is made：Hard Fat
Acid 62%, diethylenetriamine 6%, triethylene tetramine 3.5%, triethanolamine 3%, hydroxyethylethylene diamine 3%, dimethyl sulfate
2%th, p-methyl benzenesulfonic acid 0.5%, aliphatic alcohol polyethenoxy base ether 10%, dispersant 2.5%, swelling agent 2%, levelling agent 1%, soft
Soft dose 2%, high effective antifoaming agent 2.5%.
Specifically production operation step is：
1st, it is initially charged stearic acid first in a kettle., is then turned on heating valve, starts to be slowly ramped to 115 DEG C, rise
Warm time control is in 1.5h；
2nd, when temperature reaches 115 DEG C, sequentially add in a kettle. diethylenetriamine, triethylene tetramine, triethanolamine,
Hydroxyethylethylene diamine, dimethyl sulfate, p-methyl benzenesulfonic acid, dispersant, swelling agent, levelling agent, softening agent, high effective antifoaming agent, together
Shi Kaiqi blenders carry out mix homogeneously stirring；
3rd, open steam valve slowly to be heated up, when temperature reaches 200 DEG C, steam off valve, after static 8min,
Opening vacuum pump carries out evacuation process, and the whole response time is controlled in 7h；
4th, after reacting 7h, using cooling treatment method, when material is cooled to 100 DEG C, add aliphatic alcohol polyethenoxy base
Ether is catalyzed, and carries out uniform stirring；
5th, after question response 12min, drain hole valve is opened, process is dried by drying machine, required ultra-soft is obtained
The solid product of Instant film；
6th, after will be obtained ultra-soft Instant film qualified after testing, put in storage after being packed by 25kg measurement criteria.
By 1-3 embodiments of the present invention, obtained ultra-soft Instant film testing performance index result see the table below shown.
| Sequence number | Project name | Top grade product |
| 1 | Constituent | Fatty acid imidazoline quinoline compound |
| 2 | Outward appearance | Light yellow tablet |
| 3 | PH value | 5.0-6.5 (6-9% serosity) |
| 4 | It is ionic | Cation |
| 5 | Storage time | 12 months |
| 6 | Packed weight | 25kg/ bags |
The invention provides a kind of thinking and method, implement the method and approach of the technical scheme a lot, above institute
States only be the preferred embodiment of the present invention.It should be pointed out that to those of ordinary skill in the art, without departing from this
On the premise of bright principle, some improvements and modifications can also be made, these improvements and modifications also should be regarded as the protection model of the present invention
In enclosing, in the present embodiment, clearly each ingredient not can use prior art to be realized.
Claims (3)
1. a kind of ultra-soft Instant film and preparation method thereof, it is characterised in that including following percentage by weight proportioning raw materials group
It is grouped into：Stearic acid 60～80%, diethylenetriamine 6～15%, triethylene tetramine 2～5%, triethanolamine 2～6%, hydroxyl second
Base ethylenediamine 3～6%, dimethyl sulfate 2～7%, p-methyl benzenesulfonic acid 0.1～1.2%, aliphatic alcohol polyethenoxy base ether 8～
15%th, dispersant 1.5～3.5%, swelling agent 1～4%, levelling agent 1～3%, softening agent 1～4%, high effective antifoaming agent 2～
6%.
2. a kind of ultra-soft Instant film according to claim 1 and preparation method thereof, it is characterised in that further preferably
Raw material weight percent composition is：Stearic acid 60～75%, diethylenetriamine 6～11%, triethylene tetramine 2.5～4.5%, three
Ethanolamine 2～5%, hydroxyethylethylene diamine 3～5%, dimethyl sulfate 2～5%, p-methyl benzenesulfonic acid 0.1～1%, poly alkyl alcohol
Oxyethylene group ether 8～13%, dispersant 1～3%, swelling agent 1～3%, levelling agent 1～2%, softening agent 1～3%, efficiently disappear
Infusion 2～4%.
Described dispersant selects maleic acid-acrylic acid copolymer sodium salt dispersant
Described swelling agent selects methyl naphthalene sulfonic acid salt formaldehyde condensation products p-type swelling agent
Described levelling agent selects peregal O-25 levelling agent
Described softening agent selects RT type fatty acid softening agents
Described high effective antifoaming agent selects polyether-modified polydimethylsiloxane defoamer.
3. a kind of ultra-soft Instant film according to claim 1 and preparation method thereof, it is characterised in that its production technology
Step is：
1st, stearic acid is initially charged in a kettle., be then turned on heating valve and be slowly ramped to 110～120 DEG C；
2nd, when reaching 110～120 DEG C, diethylenetriamine, triethylene tetramine, triethanolamine, hydroxyl are sequentially added in a kettle.
Ethylethylenediamine, dimethyl sulfate, p-methyl benzenesulfonic acid, dispersant, swelling agent, levelling agent, softening agent, high effective antifoaming agent, while
Opening blender carries out mix homogeneously stirring；
3rd, open steam valve slowly to be heated up, when temperature reaches 190～220 DEG C, steam off valve, static 6～
10min, opening vacuum pump carries out evacuation process, is reacted using one side, and evacuation makes material react 6 in a kettle.
～10h；
4th, after 6～10h of question response, using cooling treatment method, when material is cooled to 90～110 DEG C, add fatty alcohol polyoxy
Vinyl ethers are catalyzed, and uniform stirring；
5th, after reacting 8～15min, drain hole valve is opened, process is dried by drying machine, required ultra-soft is obtained instant
The solid product of type film；
6th, after will be obtained ultra-soft Instant film qualified after testing, put in storage after being packed by 25kg measurement criteria.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109322150A (en) * | 2018-08-24 | 2019-02-12 | 宁波润禾高新材料科技股份有限公司 | A kind of low viscosity environment-friendly type sheet softening agent and preparation method thereof |
| CN109440455A (en) * | 2018-10-08 | 2019-03-08 | 宁波润禾高新材料科技股份有限公司 | A kind of preparation method of the super hydrophilic sheet softening agent of cold water instant dissolving type |
| CN110820327A (en) * | 2019-11-22 | 2020-02-21 | 广州科丰达新材料科技有限公司 | Phosphorus-free soft sheet and preparation method thereof |
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| CN109322150A (en) * | 2018-08-24 | 2019-02-12 | 宁波润禾高新材料科技股份有限公司 | A kind of low viscosity environment-friendly type sheet softening agent and preparation method thereof |
| CN109440455A (en) * | 2018-10-08 | 2019-03-08 | 宁波润禾高新材料科技股份有限公司 | A kind of preparation method of the super hydrophilic sheet softening agent of cold water instant dissolving type |
| CN110820327A (en) * | 2019-11-22 | 2020-02-21 | 广州科丰达新材料科技有限公司 | Phosphorus-free soft sheet and preparation method thereof |
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Application publication date: 20170322 |