CN106520369A - Essence for cigarette lap adhesive and use method thereof - Google Patents

Essence for cigarette lap adhesive and use method thereof Download PDF

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Publication number
CN106520369A
CN106520369A CN201611015737.6A CN201611015737A CN106520369A CN 106520369 A CN106520369 A CN 106520369A CN 201611015737 A CN201611015737 A CN 201611015737A CN 106520369 A CN106520369 A CN 106520369A
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CN
China
Prior art keywords
essence
cigarette
stabilizer
building adhesive
perfuming
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611015737.6A
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Chinese (zh)
Inventor
马舒翼
刘剑峰
董世良
熊国玺
赵国豪
赵同林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Tobacco Hunan Industrial Co Ltd
Original Assignee
China Tobacco Hunan Industrial Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by China Tobacco Hunan Industrial Co Ltd filed Critical China Tobacco Hunan Industrial Co Ltd
Priority to CN201611015737.6A priority Critical patent/CN106520369A/en
Publication of CN106520369A publication Critical patent/CN106520369A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11BPRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00Essential oils; Perfumes
    • C11B9/0007Aliphatic compounds
    • C11B9/0015Aliphatic compounds containing oxygen as the only heteroatom

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Fats And Perfumes (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The invention provides essence for a cigarette lap adhesive. The essence is prepared from 90 to 99.99wt% of a stabilizer and 0.01 to 10wt% of perfume essence through mixing. The stabilizer is prepared from 5 to 15wt% of corn starch, 1 to 3wt% of beta-cyclodextrin, 5 to 40wt% of triacetin, 15 to 30wt% of propylene glycol, 10 to 30wt% of alcohol and 5 to 64wt% of water through mixing. The perfume essence is prepared from 0.1 to 8.0wt% of menthol, 0.1 to 8.0wt% of dementholised peppermint oil, 0.1 to 10.0wt% of peppermint oil, 0.1 to 5wt% of ethyl maltol, 0.1 to 5.0wt% of fennel oil, 0.1 to 3.0wt% of anisic aldehyde, 0 .01 to 2wt% of beta-damascone with a concentration of 10%, 0.01 to 5wt% of damascone with a concentration of 10%, 15 to 40wt% of propylene glycol and 20 to 60wt% of alcohol. The essence can increase the sense of coolness when the cigarette is sucked, improve the pleasure of cigarette smoking, and is evenly released during the suction process to keep the sensory quality of the cigarette.

Description

A kind of essence for cigarette mouth building adhesive and its using method
Technical field
The present invention relates to perfuming cigarette technical field, specifically a kind of essence for cigarette mouth building adhesive and its using method.
Background technology
Essence and flavoring agent is widely used in Medicated cigarette, and essence and flavoring agent can make up cigarette tobacco leaf formulation deficiency, enrich fragrance, carry High aroma quality sense, especially in the formation of cigarette style characteristic, cigarette aesthetic quality and sucks the aspects such as the raising of pleasant feeling and plays Important function.Therefore, very popular essence is allocated, and Medicated cigarette is successfully applied to using suitable usage, be that cigarette is used The emphasis direction of essence research and development.
At present, mint aroma Medicated cigarette is received by the market, the cool feeling of oral cavity throat when its graceful Herba Menthae fragrance and suction Give the good experience of consumer to feel.But it is limited to existing perfuming technology, most mint type cigarette shows as minty note and exists Uniformly can not discharge in combustion process, with the increase of puff number, the mint flavored and cool feeling of Medicated cigarette is more and more lighter.
At present, perfuming cigarette mode mainly has tobacco perfuming, mouth bar spices line slow release perfuming, the fragrant pearl perfuming of mouth rod profit etc. several Kind, tobacco perfuming is mainly added by way of spraying in cut tobacco, and the advantage of this method is perfuming strong adaptability, general perfume (or spice) Raw material is suitable for this mode and applies, and perfuming capacity is big, and perfuming ratio highest can be 5% or so;Mouth bar spices line perfuming, by slow Release technology to process target fragrances, and be allowed to be attached on wire harness, will take shape in mouth rod, in sucking process with fragrant wire harness Middle essence slowly discharges, into oral cavity, so as to reach flavouring purpose;The fragrant pearl perfuming of profit, makes essence in soft capsule, is embedded in mouth Rod, pinches brokenly before sucking, and spice is immersed in mouth rod tow, and when sucking Medicated cigarette, fragrance component enters human body sensory organ with air-flow, So as to reach flavouring purpose.Said method obtains good application effect, but there is shortcoming, perfuming of spraying, essence loss Larger, small molecule, volatile raw material monomer easily volatilize with the air-flow in cigarette processing process, and retention rate is relatively low, also, in volume In cigarette aspiration procedure, with the rising of cigarette temperature, small molecule, the fast transfer of volatile component, Sensory Quality of Cigarette is caused Inconsequent;Cotton thread perfuming, and although the fragrant pearl perfuming of profit effectively increase that essence and flavoring agent utilization rate is high, fragrance release is more uniform Unanimously, but its complex process, manufacturing cost is higher.
By taking certain Medicated cigarette as an example, added after essence using tobacco perfuming mode, carry out sensory evaluation, met and evaluate for requiring First, two mouthfuls of flue gases are first section, and third and fourth mouthful of flue gas is stage casing, and the 4th mouthful of later flue gas is end, and score is as follows:
Change unobvious before and after flue-cured tobacco cigarette perfume, delicate fragrance, the Radix Aucklandiae, bean perfume, cream perfume, baking perfume as seen from the above table, it is believed that Its fragrance is uniform release;The release of the fragrance such as Xin Xiang, the fragrance of a flower, minty note, fragrant and sweet is uneven, with the increase of puff number, its Fragrance is more and more lighter, and aesthetic quality's score is also accordingly reduced.
Therefore, a kind of new perfuming method is developed, the fragrance of essence is uniformly discharged, so as to improve the sense organ matter of Medicated cigarette Amount, is those skilled in the art's technical problem urgently to be resolved hurrily.
The content of the invention
The purpose of the present invention is aiming at the problem that Mint Essence fragrance uniformly can not discharge, there is provided a kind of cigarette overlapping glue With essence and its using method, increase cool feeling during smoking property of cigarette, improve the pleasant feeling of cigarette smoking, and essence is made in suction During uniformly discharge, keep Sensory Quality of Cigarette.
The present invention is achieved by the following technical programs:
A kind of essence for cigarette mouth building adhesive, is mixed as following weight percent by flavoring essence and stabilizer:It is stable Agent 90-99.99%, flavoring essence 0.01-10%, wherein stabilizer are mixed by weight percentage by following raw material components: Corn starch 5-15%, beta cyclodextrin 1-3%, triacetyl glycerine 5-40%, Propylene Glycol 15-30%, ethanol 10-30%, water 5- 64%;Flavoring essence is mixed by weight percentage by following raw material components:Mentholum 0.1-8.0%, Oleum menthae 0.1- 8.0%th, mentha piperita oil 0.1-10.0%, ethylmaltol 0.1-5%, Oleum Anisi Stellati 0.1-5.0%, anisic aldehyde 0.1- 3.0%th, 10% β-damascone 0.01-2%, 10% damascone 0.01-5%, Propylene Glycol 15-40%, ethanol 20-60%.
Further, 10% β-damascone, 10% damascone solvent for use are food-grade alcohol.
Further, essence for cigarette mouth building adhesive preparation method is:After the raw material components of stabilizer are proportionally mixed, 40-50 DEG C is heated to, cools down standby after stirring, stirred after the raw material components of flavoring essence are proportionally mixed, Then stabilizer and flavoring essence are mixed according to the percentage by weight of stabilizer 90-99.99%, flavoring essence 0.01-10% Obtain the essence for cigarette mouth building adhesive.
Further, the using method of essence for cigarette mouth building adhesive as described above, by the essence for cigarette mouth building adhesive and After overlapping glue is according to the percentage by weight mixing of overlapping glue 90-99.99%, essence for cigarette mouth building adhesive 0.01-10%, according to just Normal production technology is used for mouth rod and production of cigarettes.
Used by of the invention, the effect of each raw material is as follows:
Beta cyclodextrin and triacetyl glycerine:The effect of stabilizer and fixastive, makes fragrance slowly discharge.Corn starch with Overlapping glue has a preferable intersolubility, and maintains to add the viscosity of overlapping glue after essence, so as to the upper machine for ensureing fastener glue is suitable for Property;Beta cyclodextrin strengthens spirit solvent and corn starch dissolubility, can make the two mixing with and do not produce precipitation.
Mentholum, Oleum menthae and mentha piperita oil:Minty note note and cool feeling are provided.
Oleum Anisi Stellati and anisic aldehyde:Blender, makes minty note more harmonious with cigarette perfume, one integrated mass.
Ethylmaltol, β-damascone and damascone:Increase the fragrant and sweet and fragrant note of baking, set off Nicotiana tabacum L. this perfume by contrast.
The present invention solves the problems, such as traditional tobacco shred spraying perfuming mode Herba Menthae fragrance loss, Herba Menthae fragrance is taken out in Medicated cigarette Uniformly discharge during suction, and in different aroma strength levels, keep preferably stablizing releasing effect, so that Herba Menthae The cool feeling experience of cigarette continues, and improves Herba Menthae cigarette and sucks pleasant feeling, meanwhile, the present invention is compared with other perfuming mode production technology letters Single, cost is reduced.
Specific embodiment
With reference to embodiments the present invention is described further:
In the range of the technical program, each raw material mixes (each raw material components are unit of weight) in different proportions, respectively 3 stabilizer samples are formed, 3 flavoring essence samples form cigarette overlapping glue fragrant after both are mixed in different proportions Smart sample, essence for cigarette mouth building adhesive are mixed to get perfuming overlapping glue in different proportions with overlapping glue, make Medicated cigarette, not add The cigarette leaf group that essence overlapping glue makes is control sample, carries out sensory quality assessment to perfuming sample, according to Analyses Methods for Sensory Evaluation Results The effect of checking the technical program, the data in following each sample composition table are weight percentage, the data in sense organ evaluating meter For score value.
Stabilizer sample is constituted:
A1 A2 A3
Corn starch 15 10 5
Beta cyclodextrin 1 2 3
Triacetyl glycerine 35 20 15
Propylene Glycol 15 20 20
Ethanol 15 25 25
Water 19 23 32
It is total 100 100 100
Flavoring essence sample is constituted:
Essence for cigarette mouth building adhesive proportioning is constituted:
C1 C2
Stabilizer 98 92
Flavoring essence 2 8
It is total 100 100
Perfuming overlapping glue proportioning is constituted:
D1 D2
Overlapping glue 98 92
Essence for cigarette mouth building adhesive 2 8
It is total 100 100
Embodiment 1
Composition according to A1, B1, C1, D1 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 2 2 2
Minty note 0~10 0 2.1 2.1 2.1
Bakee fragrant 0~10 1 3 3 3
It is fragrant and sweet 0~10 1.5 1.6 1.6 1.6
Embodiment 2
Composition according to A1, B2, C1, D1 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 1.2 1.2 1.2
Minty note 0~10 0 3.2 3.2 3.1
Bakee fragrant 0~10 1 2.5 2.4 2.4
It is fragrant and sweet 0~10 1.5 2.1 2.1 2.1
Embodiment 3
Composition according to A1, B3, C1, D1 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 1 1 0.9
Minty note 0~10 0 3.8 3.9 3.6
Bakee fragrant 0~10 1 1.8 1.8 1.8
It is fragrant and sweet 0~10 1.5 1.5 1.5 1.5
Embodiment 4
Composition according to A2, B1, C2, D1 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 4 4 3.9
Minty note 0~10 0 4.3 4.3 4.3
Bakee fragrant 0~10 1 3.5 3.5 3.4
It is fragrant and sweet 0~10 1.5 1.9 1.9 1.9
Embodiment 5
Composition according to A2, B2, C1, D2 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 2.7 2.7 2.6
Minty note 0~10 0 5.3 5.3 5.3
Bakee fragrant 0~10 1 3 3 2.9
It is fragrant and sweet 0~10 1.5 2.1 2.1 2.1
Embodiment 6
Composition according to A2, B3, C2, D1 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 2.2 2.1 1.9
Minty note 0~10 0 6 6 5.8
Bakee fragrant 0~10 1 2.1 2.1 2
It is fragrant and sweet 0~10 1.5 1.7 1.7 1.7
Embodiment 7
Composition according to A3, B1, C2, D2 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 7.5 7.5 7.3
Minty note 0~10 0 6.3 6.3 6.3
Bakee fragrant 0~10 1 5 5 4.9
It is fragrant and sweet 0~10 1.5 2.2 2.2 2.1
Embodiment 8
Composition according to A3, B2, C2, D2 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 5 5 4.8
Minty note 0~10 0 8 8 7.9
Bakee fragrant 0~10 1 4 4 3.9
It is fragrant and sweet 0~10 1.5 2.5 2.5 2.5
Embodiment 9
Composition according to A3, B3, C2, D2 implements perfuming effect experiment.
Perfuming evaluation result:
Evaluation index Score value is interval Leaf group score First section score Stage casing score End score
Xin Xiang 0~10 0 4 4 3.8
Minty note 0~10 0 9 9 8.5
Bakee fragrant 0~10 1 3 3 2.9
It is fragrant and sweet 0~10 1.5 2 2 2
More than knowable to each perfuming evaluation result, with the increase of fragrance materials amount, aroma strength increase, in different aromas On intensity level, the aroma strength of each suction stage maintains to be basically unchanged, and the stable releasing effect of fragrance is obvious.
The above, the only specific embodiment of the present invention, but protection scope of the present invention is not limited thereto, any Belong to those skilled in the art the invention discloses technical scope in, the change or replacement that can be readily occurred in all are answered It is included within the scope of the present invention.Therefore, protection scope of the present invention should be defined by scope of the claims.

Claims (4)

1. a kind of essence for cigarette mouth building adhesive, it is characterised in that mixed by flavoring essence and stabilizer as following weight percent and Into:Stabilizer 90-99.99%, flavoring essence 0.01-10%, wherein stabilizer are mixed by weight percentage by following raw material components Conjunction is formed:Corn starch 5-15%, beta cyclodextrin 1-3%, triacetyl glycerine 5-40%, Propylene Glycol 15-30%, ethanol 10- 30%th, water 5-64%;Flavoring essence is mixed by weight percentage by following raw material components:Mentholum 0.1-8.0%, Herba Menthae Vegetable oil 0.1-8.0%, mentha piperita oil 0.1-10.0%, ethylmaltol 0.1-5%, Oleum Anisi Stellati 0.1-5.0%, anisic aldehyde 0.1-3.0%, 10% β-damascone 0.01-2%, 10% damascone 0.01-5%, Propylene Glycol 15-40%, ethanol 20- 60%.
2. essence for cigarette mouth building adhesive as claimed in claim 1, it is characterised in that:10% β-damascone, 10% Tujue Ketone solvent for use is food-grade alcohol.
3. essence for cigarette mouth building adhesive as claimed in claim 1, it is characterised in that:Essence for cigarette mouth building adhesive preparation method For:After the raw material components of stabilizer are proportionally mixed, be heated to 40-50 DEG C, cool down after stirring it is standby, will be perfuming fragrant The raw material components of essence stir after proportionally mixing, then by stabilizer and flavoring essence according to stabilizer 90- 99.99%th, the percentage by weight of flavoring essence 0.01-10% is mixed to get the essence for cigarette mouth building adhesive.
4. as weigh claim 1-3 any one of essence for cigarette mouth building adhesive using method, it is characterised in that:Will be described Essence for cigarette mouth building adhesive and overlapping glue are according to overlapping glue 90-99.99%, the weight of essence for cigarette mouth building adhesive 0.01-10% After percentage ratio mixing, it is used for mouth rod and production of cigarettes according to normal production technology.
CN201611015737.6A 2016-11-18 2016-11-18 Essence for cigarette lap adhesive and use method thereof Pending CN106520369A (en)

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Application Number Priority Date Filing Date Title
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Publication Number Publication Date
CN106520369A true CN106520369A (en) 2017-03-22

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107674763A (en) * 2017-05-24 2018-02-09 湖北中烟工业有限责任公司 A kind of preparation method of the water-soluble cigarette controlled release cool feeling essence of aluminium-foil paper
CN107675560A (en) * 2017-05-24 2018-02-09 湖北中烟工业有限责任公司 Cigarette aluminium-foil paper preparation method with slow controlled release cool feeling essence
CN111820446A (en) * 2019-04-15 2020-10-27 湖南中烟工业有限责任公司 Mint type slow-release material with bean fragrance, tobacco stick, heating non-combustible tobacco product and preparation and application thereof
JP2021500890A (en) * 2017-11-01 2021-01-14 ニコベンチャーズ トレーディング リミテッド Fragrant vaporizable formulation

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101586057A (en) * 2009-06-25 2009-11-25 红云红河烟草(集团)有限责任公司 Essence for cigarette lap adhesive and preparation and use methods thereof
CN104161303A (en) * 2014-07-16 2014-11-26 广西中烟工业有限责任公司 Preparation method of cooling mint type cigarette filter additive and application of cooling mint type cigarette filter additive

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101586057A (en) * 2009-06-25 2009-11-25 红云红河烟草(集团)有限责任公司 Essence for cigarette lap adhesive and preparation and use methods thereof
CN104161303A (en) * 2014-07-16 2014-11-26 广西中烟工业有限责任公司 Preparation method of cooling mint type cigarette filter additive and application of cooling mint type cigarette filter additive

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107674763A (en) * 2017-05-24 2018-02-09 湖北中烟工业有限责任公司 A kind of preparation method of the water-soluble cigarette controlled release cool feeling essence of aluminium-foil paper
CN107675560A (en) * 2017-05-24 2018-02-09 湖北中烟工业有限责任公司 Cigarette aluminium-foil paper preparation method with slow controlled release cool feeling essence
JP2021500890A (en) * 2017-11-01 2021-01-14 ニコベンチャーズ トレーディング リミテッド Fragrant vaporizable formulation
JP7041261B2 (en) 2017-11-01 2022-03-23 ニコベンチャーズ トレーディング リミテッド Fragrant vaporizable formulation
CN111820446A (en) * 2019-04-15 2020-10-27 湖南中烟工业有限责任公司 Mint type slow-release material with bean fragrance, tobacco stick, heating non-combustible tobacco product and preparation and application thereof

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Application publication date: 20170322