CN106515176A - Quality control method for composite optical pressed film - Google Patents
Quality control method for composite optical pressed film Download PDFInfo
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- CN106515176A CN106515176A CN201610871799.0A CN201610871799A CN106515176A CN 106515176 A CN106515176 A CN 106515176A CN 201610871799 A CN201610871799 A CN 201610871799A CN 106515176 A CN106515176 A CN 106515176A
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- Prior art keywords
- film
- roll
- control method
- quality control
- composite optical
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/06—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the heating method
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B37/00—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding
- B32B37/10—Methods or apparatus for laminating, e.g. by curing or by ultrasonic bonding characterised by the pressing technique, e.g. using action of vacuum or fluid pressure
Abstract
The invention relates to a quality control method for a composite optical pressed film. The method includes the following steps that (1) pretreatment is carried out, specifically, polymer nanoparticles of a core-shell structure are pretreated to form a continuous sheet with the thickness being 0.1-5 mm; and (2) film rolling is conducted, specifically, the continuous sheet is heated to 80-140 DEG C to be softened, the continuous sheet, an upper wrapping film and a lower wrapping film are combined at the softening temperature, and press rollers are used for extruding the sheet and the wrapping films into an optical film with the thickness being 20-200 [mu]m. The thickness uniformity of the pressed film is an important parameter of the quality of the pressed film, and the materials must be preheated before entering the press rollers so as to achieve thickness uniformity. Corresponding devices and technical solutions are provided for achieving thickness uniformity, so that continuous production and uniform thickness control of the wide optical film with the width large than 500 mm are achieved.
Description
Technical field
The invention belongs to material processing field, is related to a kind of composite optical material press mold quality control method.
Background technology
Macromolecule protein stone is a kind of NEW TYPE OF COMPOSITE optical material, and Chris Finlayson et al. are in " 3D Bulk
Ordering in Opals by Edge-Induced Rotational Shearing, Adv. Mat. 23, 1540
(2011) have studied to be clipped in the middle of two-layer PET film with core-shell structure polymer microballoon in " and be rolled into film and then by wedge
The pressure on shape metal top causes shear flow to obtain the regularly arranged preparation method to produce schemochrome of Nano microsphere;
A kind of technology of preparing for preparing macromolecule protein stone with core-shell structure polymer microballoon is disclosed in CN103534079 A, is led to
The shearing force for crossing sandwich generation makes microballoon be arranged in the structure of rule in laminar film, and then produces similar nature albumen
The optical texture color of stone;Qibin Zhao et al. are in " Large-scale ordering of nanoparticles using
viscoelastic shear processing” (Nature Communications 2016,7:11661)In to this
Preparation technology is expanded on further, and the action principle and effect of shearing force are studied in detail.In above-mentioned data
Use by then carrying out shearing the work of regular process into composite optical material film in two-layer PET film intermediate calender rolls swaging
Skill, but for rolling process is not described in detail, while in vitro mini-plant is only applicable to prepare 5-10cm
Rank sample cuttings, while prepared material thickness is uneven, are not suitable for the continuous production of big wide cut industry.
The continuous production of practical large scale technical grade macromolecule protein stone composite optical material film needs the life of matching
Can production. art, the quality technology controlling and process of rolled film determine and be smoothed out follow-up shear constitution Regularization operation, determine
The quality of product.
The content of the invention
In order to overcome the deficiencies in the prior art, the present invention to provide a kind of composite optical material press mold quality control method.
The invention provides following technical scheme:
A kind of composite optical material press mold quality control method, including following steps:
(1)Pre-treatment:Polymer core-shell structural nano microballoon forms continuous sheet by pre-treatment, and thickness is 0.1-5mm;
(2)Rolled film process:The continuous sheet is heated to 80-140 DEG C of softening, keeps softening temperature and upper and lower two-layer bag
Overlay film is combined, and is squeezed into optical thin film in the presence of pressure roller, and the thickness of the optical thin film layer is 20-200 μm.
From heating unit, out into this period before pressure roller, easily quickly cooling loses certain temperature to material, softens
Temperature can cause material too low into temperature during pressure roller and can not reach the bating effect of needs less than 80 degree;Heating is single
Material if first softening temperature is too high is probably due to heat resistance cannot be born and certain destruction is occurred.The limit of optical thin film layer
It is fixed, be because the too thin optical characteristics that can lead to not needs occur of film, it is too thick if be not inconsistent with the market demand.By
The preheating material of this temperature makes material keep soft state to enter roller machine so as to ensure the uniformity of press mold.
In any of the above-described scheme preferably, the polymer core-shell structural nano microballoon is powder or bulk material.
In such scheme preferably, the rolled film processes the equipment for adopting includes that raw material is continuously unreeled, transmitted
Device, sheet material heater and compound, roll-in film formation device.Compound, the roll-in film formation device includes roll-in film formation device.
In any of the above-described scheme preferably, it is described continuously unreel, conveyer includes unwinding device and transmission unit.
In any of the above-described scheme preferably, the sheet material heater includes heating unit.
In any of the above-described scheme preferably, the heating unit is arranged on the postmedian of the transmission unit.
In any of the above-described scheme preferably, the rolled film processing procedure is as follows:The continuous sheet is described
Unwinding device control is lower into the transmission unit, moves to the roll-in film formation device, sets in the transmission unit postmedian
Heating unit is put, the continuous sheet is heated to 80-140 DEG C of softening when through the heating unit, keeps softening temperature
It is compound with upper and lower two-layer coating film into the roll-in film formation device, the optical thin film is squeezed in the presence of pressure roller.
In any of the above-described scheme preferably, the thickness of the optical thin film layer is 50-140 μm.
In any of the above-described scheme preferably, the transmission unit is the transmission belt of self-powered continuous motion.
In any of the above-described scheme preferably, the transmission unit be not self-powered motion, by continuous rotary shaft
Constitute or by the less surface composition of coefficient of friction.Sheet material can be transported under the effect of less tractive force on transmission unit
It is dynamic.
In any of the above-described scheme preferably, the mode of heating of the heating unit includes electric boiling plate heating, electromagnetism
Heater plate or the heating of infrared heating unit.
In the present invention, heating unit is arranged on certain part of transmission unit, and sheet material is passed through from heating unit, heating
Direction can be to sheet material single-side heating, it is also possible to which the upper and lower surface of sheet material is heated simultaneously.
In any of the above-described scheme preferably, the device of the electric boiling plate heating is made up of electric boiling plate, heating side
Formula is heated for electrically heated rod, and the continuous sheet is passed through from the gap of two pieces of heating plates and heated.
In any of the above-described scheme preferably, the device of the Electromagnetic Heating plate heating is made up of Electromagnetic Heating plate, plus
Hot mode is inductive heating, by electromagnetic induction device to metallic plate(Electromagnetic Heating plate)Heated, then heating plate makes institute
State continuous sheet to be heated.
In any of the above-described scheme preferably, the device of the additional hot cell heating is heated by infrared heating unit,
The continuous sheet is heated by infrared radiation mode.
In any of the above-described scheme preferably, the heating unit is entered to the continuous sheet by control module control
The temperature for going out the heating unit is detected and is adjusted heating power.
In any of the above-described scheme preferably, the roll-in film formation device is pressed close in the position that the heating unit is arranged.
Ensure temperature of the material after heating as close possible to 80-150 DEG C, but be less than 150 DEG C.Preferably 140 DEG C.
If material is in the short time(10 seconds or so)Temperature 150 DEG C of energy can retention performance it is constant, but the time is slightly long
Just occur destruction, 140 DEG C be practical operation insurance numerical value.
In any of the above-described scheme preferably, the roll-in film formation device includes upper and lower volume coating film unwinding device and upper
Lower roll-in to roller pressue device.
In any of the above-described scheme preferably, the material of the coating film is polyester(PET), thermoplastic polyurethane
(TPU), polymethyl methacrylate(PMMA)Or bidirectional stretching polypropylene film(BOPP).
PET is clipped in the middle the continuous sheet optics raw material into roller, under the pressure to roller as upper lower interlayer
By sheet extrusion into film.PET can also be substituted by the thin polymer film of other materials, such as TPU, PMMA, BOPP etc., but
Need to consider the requirement of pressure and temperature and subsequent technique to carry out selecting and adjusting process parameter.
In any of the above-described scheme preferably, the coating film is PET, and thickness is 20-200 μm,
In any of the above-described scheme preferably, the thickness of the coating film is the optical thin film layer thickness after pressure roller
0.8-2 times.
The thickness of coating film here, such as PET film, its thickness in monolayer should be the rollers of two-layer PET sandwich
0.8-2 times of the thickness of optical material after pressure, this numerical value are the optimal values models of the optical characteristics for ensureing intermediate optical material
Enclose.
In any of the above-described scheme preferably, the upper and lower roll-in includes upper lower compression roller to roller pressue device, described
Upper lower compression roller is mirror roller, and the sheeting roll surface temperature is 20-200 DEG C.
The restriction of surface temperature ensure that press mold process smoothly while not destroying the chemical composition of optics raw material.
The surface of the upper lower compression roller is the smooth surface through PROCESS FOR TREATMENTs such as chrome-faceds, and pressure roller is required to control
Surface temperature.
In any of the above-described scheme preferably, the sheeting roll surface temperature is 80-130 DEG C.
In any of the above-described scheme preferably, the mode of heating of the pressure roller is oil heat or the heating of inductance surface.
In any of the above-described scheme preferably, the wide cut of the pressure roller is 20-500 centimetre.
In the case where wide cut is more than 60 centimetres, the shape design of pressure roller preferably carries out special in view of heat distortion factor
Compensation Design.
In any of the above-described scheme preferably, the gap of the upper lower compression roller is 0-5 millimeters, is accurate to 1 micron.
In any of the above-described scheme preferably, the pressure of the upper lower compression roller is 0-40 MPa.
In any of the above-described scheme preferably, the rotation linear velocity of the pressure roller is 0-5 meter per seconds.
Can guarantee that optical characteristics is not destroyed under the linear velocity.
In any of the above-described scheme preferably, the rolled film process the equipment for adopting include sheet material heater and
Compound, roll-in film formation device, the extrusion die head of the continuous sheet be close to the roll-in up and down of roll-in film formation device to roller
Interstitial site.
For not using sheet material unwinding device and heating unit, and the die head that sheet material is extruded is placed close to into pressure as far as possible
The interstitial site to roller of made membrane, amount of residual heat of such sheet material after die head extrusion can ensure that the softening shape of sheet material
State remains to the process of press mold.Now the temperature of sheet die can set 135 DEG C, in the position of the close enough pressure roller of sheet die
Put under relation, can ensure that in this softening temperature after material extrusion.
One important parameter of press mold quality is the thickness evenness of the film of compacting, wants to realize the uniform of thickness, material
Material is necessary into preheating before pressure roller.If do not preheated into before pressure roller in sheet material, the thickness of sheet material
The more difficult control of the uniformity, prepared optical thin film layer thickness uniformity are relatively inaccessible to less than 5%, are the equal of guarantee film thickness
Evenness typically should be preheated by heating unit.The present invention proposes corresponding equipment, technical solutions for this problem,
To realize being more than continuous prodution, the thickness equal control of 500mm Wide area optical films.
Description of the drawings
Fig. 1 be an a kind of preferred embodiment of composite optical material press mold quality control method of the invention pressed film equipment and
Simplified flowchart;
Fig. 2 is a kind of pressed film equipment of another preferred embodiment of composite optical material press mold quality control method of the invention and letter
Change flow chart;
Fig. 3 is without pre-heating technique and the film thickness uniformity difference through pre-heating technique and then roll-in film forming.
Specific embodiment
In order to further appreciate that the technical characteristic of the present invention, the present invention is explained in detail with reference to specific embodiment
State.Embodiment only has exemplary effect to the present invention, not with any restricted effect, those skilled in the art
The modification of any unsubstantiality made on the basis of the present invention, should all belong to protection scope of the present invention.
The invention provides a kind of composite optical material press mold quality control method, including following steps:
(1)Pre-treatment:Polymer core-shell structural nano microballoon forms continuous sheet by pre-treatment, and thickness is 0.1-5mm;
(2)Rolled film process:The continuous sheet is heated to 80-140 DEG C of softening, keeps softening temperature and upper and lower two-layer bag
Overlay film is combined, and is squeezed into optical thin film in the presence of pressure roller, and the thickness of the optical thin film layer is 20-200 μm.
Further, the polymer core-shell structural nano microballoon is powder or bulk material.
Further, the rolled film process the equipment for adopting include raw material continuously unreel, conveyer, sheet material adds
Thermal and compound, roll-in film formation device.Compound, the roll-in film formation device includes roll-in film formation device.
Further, it is described continuously unreel, conveyer includes unwinding device and transmission unit.
Further, the sheet material heater includes heating unit.
Further, the heating unit is arranged on the postmedian of the transmission unit.
Further, the rolled film processing procedure is as follows:The continuous sheet is under unwinding device control
Into the transmission unit, move to the roll-in film formation device, heating unit is set in the transmission unit postmedian, it is described
Continuous sheet is heated to 80-140 DEG C of softening when through the heating unit, keeps softening temperature to enter the roll-in film forming
Device is compound with upper and lower two-layer coating film, is squeezed into the optical thin film in the presence of pressure roller.
Further, the thickness of the optical thin film layer is 50-140 μm.
Further, the transmission unit is the transmission belt of self-powered continuous motion.
Further, the transmission unit is not self-powered motion, is made up of continuous rotary shaft or by rubbing
The less surface composition of coefficient.Sheet material can be moved under the effect of less tractive force on transmission unit.
Further, the mode of heating of the heating unit includes electric boiling plate heating, the heating or red of Electromagnetic Heating plate
Additional hot cell heating.
Further, the device of the electric boiling plate heating is made up of electric boiling plate, and mode of heating adds for electrically heated rod
Heat, the continuous sheet are passed through from the gap of two pieces of heating plates and are heated.
Further, the device of the Electromagnetic Heating plate heating is made up of Electromagnetic Heating plate, and mode of heating adds for inductance
Heat, by electromagnetic induction device to metallic plate(Electromagnetic Heating plate)Heated, then heating plate obtains the continuous sheet
Heating.
Further, the device of the additional hot cell heating is heated by infrared heating unit, by infrared radiation
Mode is heated to the continuous sheet.
Further, the heating unit passes in and out the heating unit by control module control to the continuous sheet
Temperature detected and adjusted heating power.
Further, the roll-in film formation device is pressed close in the position that the heating unit is arranged.
Further, the roll-in film formation device includes adding to roller for upper and lower volume coating film unwinding device and upper and lower roll-in
Pressure device.
Further, the material of the coating film is polyester(PET), thermoplastic polyurethane(TPU), polymethylacrylic acid
Methyl esters(PMMA)Or bidirectional stretching polypropylene film(BOPP).
Further, the coating film is PET, and thickness is 20-200 μm,
Further, the thickness of the coating film is 0.8-2 times of the optical thin film layer thickness after pressure roller.
Further, the upper and lower roll-in includes upper lower compression roller to roller pressue device, and the upper lower compression roller is minute surface
Roller, the sheeting roll surface temperature are 20-200 DEG C.
Further, the sheeting roll surface temperature is 80-130 DEG C.
Further, the mode of heating of the pressure roller is oil heat or the heating of inductance surface.
Further, the wide cut of the pressure roller is 20-500 centimetre.
Further, the gap of the upper lower compression roller is 0-5 millimeters, is accurate to 1 micron.
Further, the pressure of the upper lower compression roller is 0-40 MPa.
Further, the rotation linear velocity of the pressure roller is 0-5 meter per seconds.
Further, the rolled film processes the equipment for adopting includes sheet material heater and compound, roll-in film forming
Device, the extrusion die head of the continuous sheet are close to the interstitial site to roller of the roll-in up and down of roll-in film formation device.
The raw material of the composite optical material of the present invention is preferably past dry polymer core-shell structural nano microballoon powder
Or bulk material, main component be polystyrene, polyethyl acrylate, polymethyl methacrylate etc. and a small amount of crosslinking agent and
Other additives, it is consistent with the material of institute's publicity in CN103534079 A.
Embodiment 1:
As shown in figure 1, micro- with polystyrene-poly methyl methacrylate-polyethyl acrylate " core-shell " structural polymer nanometer
Ball(Diameter 250nm)Thickness prepared by powder is 0.5 millimeter of sheet material;It is equipped with using following equipment:
1. composite material sheet unreeling machine, unreels speed and is set lower than pressure roller linear velocity;
2. transmitting device, the surface contacted with sheet material are reduced using Teflon material and rub and ensure high temperature(120℃)Lower and piece
Material does not stick together, and enables sheet material to advance under less tractive force;
3. multiple rows of infrared heating fluorescent tube that the heater of pair sheet material is placed using rectangular surfaces, is placed on apart from sheet top surface 10
The top of cm height, is uniformly heated to sheet material, and heating-up temperature is 120 DEG C, and tinfoil or other measures lamp curtain are taken in periphery
Around with the excessive extra heating miscellaneous part of placement infrared ray;
4. Dong Ligao transmissive optical high temperature resistant PET films are adopted(The PET film of toray company production), 125 microns of works of thickness
For upper lower interlayer;
5. 800 millimeters of pressure roller wide cut, using cast iron quality, chrome-faced mirror process, heat-conducting oil heating mode, oil pressure pressurization,
Pressure arrange 15 MPas, adjustment gap be 300-400 microns, 0.1 meter per second of linear velocity.
Detailed process is as follows:
Pressure roller is warming up to into 120 DEG C, gap is adjusted, uniform motion starts sheet material heater and unwinding device, complex optics
Material sheet is flat on transmitting device after unreeling, and starts sheet material heating dress according to the heating power set after testing in advance
Put, it is ensured that material after heater enter nip before temperature at 80-120 DEG C.Artificial traction sheet material enters pressure roller
Gap, then rotates in pressure roller and advances under the tractive force that press mold is produced automatically, carry out continuous press mold.
Embodiment 2
As shown in Fig. 2 material and press-roller device arrange same as Example 1, but do not adopt and unreel, transmit and sheet material heating dress
Put, extruder and subsidiary sheet production line are directly docked to into roller machine, sheet die unloading position is as close possible to above pushing
To ensure material into the temperature before pressure roller, sheet die temperature facility is at 100-135 DEG C in roller gap.
Experimental example 3
As shown in figure 3, without pre-heating technique and the film thickness uniformity difference through pre-heating technique and then roll-in film forming.
A, 700 millimeters of the thin-film width after roll-in take 13 points in the width of film and measure, and are spaced 1 meter in length direction
Place takes the thickness that 13 points of same location measure film again.B, T1, T2 are not through the film of pre-heating technique roll-in film forming
Distribution of the thickness in respective point, T3, T4 are the thickness distribution after preheating the material into 80 DEG C of roll temperature in roll-in film forming.In advance
Thermal process has critical impact to the uniformity of material thickness, as seen from Figure 3, is 94 microns in default extrusion film thickness
In the case of, through thickness change of the film thickness of the technique output for preheating in length and width direction and reach positive and negative 15
Micron, and the film thickness fluctuation range for entering preheating production only has positive and negative 3 microns.
Being except not heating and softening in addition to step without pre-heating technique in embodiment 3, remaining step and process are equal
It is identical with the present invention.
Embodiment 4:
With polystyrene-poly methyl methacrylate-polyethyl acrylate " core-shell " structural polymer Nano microsphere(Diameter
250nm)Thickness prepared by powder is 0.8 millimeter of sheet material;It is equipped with using following equipment:
1. composite material sheet unreeling machine, unreels speed and is set lower than pressure roller linear velocity;
2. transmitting device, the surface contacted with sheet material are reduced using Teflon material and rub and ensure high temperature(140℃)Lower and piece
Material does not stick together, and enables sheet material to advance under less tractive force;
3. multiple rows of infrared heating fluorescent tube that the heater of pair sheet material is placed using rectangular surfaces, is placed on apart from sheet top surface 10
The top of cm height, is uniformly heated to sheet material, and heating-up temperature is 110 DEG C, and tinfoil or other measures lamp curtain are taken in periphery
Around with the excessive extra heating miscellaneous part of placement infrared ray;
Using Dong Ligao transmissive optical high temperature resistant PET films, 120 microns of thickness is used as upper lower interlayer;
800 millimeters of pressure roller wide cut, using cast iron quality, chrome-faced mirror process, heat-conducting oil heating mode, oil pressure pressurization, pressure
Strong to arrange 15 MPas, adjustment gap is 80-100 microns, 0.1 meter per second of linear velocity.
Detailed process is as follows:
Pressure roller is warming up to into 125 DEG C, gap is adjusted, uniform motion starts sheet material heater and unwinding device, complex optics
Material sheet is flat on transmitting device after unreeling, and starts sheet material heating dress according to the heating power set after testing in advance
Put, it is ensured that material after heater enter nip before temperature at 80-120 DEG C.Artificial traction sheet material enters pressure roller
Gap, the sheet material of softening are clamped in two-layer PET for being unreeled at nip up and down, then rotate press mold in pressure roller
Automatically advance under the tractive force of generation, carry out continuous press mold.
Claims (10)
1. a kind of composite optical material press mold quality control method, including following steps:
(1)Pre-treatment:Polymer core-shell structural nano microballoon forms continuous sheet by pre-treatment, and thickness is 0.1-5mm;
(2)Rolled film process:The continuous sheet is heated to 80-140 DEG C of softening, keeps softening temperature and upper and lower two-layer bag
Overlay film is combined, and is squeezed into optical thin film in the presence of pressure roller, and the thickness of the optical thin film layer is 20-200 μm.
2. composite optical material press mold quality control method according to claim 1, it is characterised in that:The rolled film
Process the equipment for adopting include raw material continuously unreel, conveyer, sheet material heater and compound, roll-in film formation device.
3. composite optical material press mold quality control method according to claim 2, it is characterised in that:It is described continuously to put
Volume, conveyer include unwinding device and transmission unit.
4. composite optical material press mold quality control method according to claim 3, it is characterised in that:The sheet material heating
Device includes heating unit.
5. composite optical material press mold quality control method according to claim 4, it is characterised in that:The rolled film
Processing procedure is as follows:The continuous sheet enters the transmission unit under unwinding device control, to the roll-in film forming
Device is moved, and arranges heating unit, continuous sheet quilt when through the heating unit in the transmission unit postmedian
80-140 DEG C of softening is heated to, is kept softening temperature to enter the roll-in film formation device and is combined with upper and lower two-layer coating film, in pressure
The optical thin film is squeezed in the presence of roller.
6. composite optical material press mold quality control method according to claim 4, it is characterised in that:The heating unit
The roll-in film formation device is pressed close in the position of setting.
7. composite optical material press mold quality control method according to claim 1, it is characterised in that:The roll-in film forming
Device include upper and lower volume coating film unwinding device and upper and lower roll-in to roller pressue device.
8. composite optical material press mold quality control method according to claim 7, it is characterised in that:The upper and lower roll-in
Include upper lower compression roller to roller pressue device, the upper lower compression roller is mirror roller, and the sheeting roll surface temperature is 20-200 DEG C.
9. composite optical material press mold quality control method according to claim 1, it is characterised in that:The upper lower compression roller
Pressure be 0-40 MPa.
10. composite optical material press mold quality control method according to claim 1, it is characterised in that:The roll-in is thin
The equipment that film process is adopted includes sheet material heater and compound, roll-in film formation device, the extrusion die head of the continuous sheet
It is close to the interstitial site to roller of the roll-in up and down of roll-in film formation device.
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CN110418988A (en) * | 2017-03-30 | 2019-11-05 | 日本瑞翁株式会社 | Optical film, the manufacturing method of optical film, polarizing film and liquid crystal display device |
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