CN106493812B - A kind of timber green mould proof processing method - Google Patents
A kind of timber green mould proof processing method Download PDFInfo
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- CN106493812B CN106493812B CN201510565656.2A CN201510565656A CN106493812B CN 106493812 B CN106493812 B CN 106493812B CN 201510565656 A CN201510565656 A CN 201510565656A CN 106493812 B CN106493812 B CN 106493812B
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Abstract
A kind of timber green mould proof processing method, belongs to wood mould technical field, which carries out as follows：Using water vapour as heat medium, while logical carbon dioxide, air is excluded in process tank within 5%, is rapidly heated to 100 120 DEG C, 0.5 1MPa of pressure, keeps the temperature 2 4h；Continue water flowing steam, air compressor machine pressurization is passed through carbon dioxide, is warming up to 120 150 DEG C, 1 3MPa of pressure, keeps the temperature 4 8h；Continue to be passed through water vapour and carbon dioxide, keeps the temperature 120 150 DEG C, 1 2MPa of pressure, within drying to water content 5%；Stopping is passed through carbon dioxide, and spraying cooling adjusts humidity, Temperature fall, timber water content 4 8% within 90 DEG C.This method is handled using synchronous water vapour boiling with carbon dioxide extraction, and environmentally protective, safe and harmless, long-term anti-mold effect is good, can be used for preparing children's wooden toy, baby child's home life supplieshome life supplies etc..
Description
Technical field
The invention belongs to wood mould technical fields, are related to a kind of green of water vapour boiling and carbon dioxide extraction timber
Mildew-proof treatment method.
Background technology
It is well known that the timber such as rubber wood timber, sweetgum wood, pine due to its own there are the internal organizational structure of the easy moisture absorption or
Richness closes nutriment and volatile organism, causes it easily to go mouldy in wet environment and discoloration, it is sharp to influence following process
With.If rubber wood timber belongs to diffuse porous wood, drying shrinkage is small, easy processing, cheap, be make the high-quality timber of furniture and toy, but by
Contain the nutriments such as about 1% protein and 3% starch in it, easily goes mouldy in wet environment.
CN102265902A discloses " a kind of mould inhibitor of rubber wood timber and its application " patented technology, be first use alkylnaphthalene acid sodium solution into
Row pretreatment, then carries out mould proof processing using the mould inhibitor being made of 10% sulfuric acid, N-Ethylbutylamine, sodium tetraborate decahydrate.
CN103707375A discloses " a kind of processing method that solid wood is mould proof ", is sprayed using solid wood drying, constant temperature, dehumidifier, surface second
Four steps that varnish with lacquer carry out mould proof processing to solid wood, and the difference that the drying of patent solid wood is dried with common wood is to use steam pair
Drying shed is timed temperature adjustment and conditioning, and maximum temperature rises to 85 DEG C, bad to solid wood anti-mold effect；Constant temperature and dehumidifier
Step is primarily to control the moisture content of solid wood；Surface second spraying japanning belongs to the subsequent processing operations of solid wood, as reality
The wooden pretreatment process will influence solid wood subsequent use.It is mould proof to be applied to the early stages such as the boron phenol mixture of wood preservation in the prior art
, all there is certain toxicity, generated to human body in agent, low-toxicity industrial bactericide, the efficient organic chemical reagent mould inhibitor of low toxicity
Harm, hypotoxicity mould inhibitor can not meet the requirement safe and harmless to timber such as wooden toy industry.Solid wood drying and surface
The purposes for spraying the Combined Treatments such as japanning limitation timber, makes troubles to timber subsequent applications.
Invention content
The technical problem to be solved by the present invention is to develop a kind of to utilize the Nantural non-toxics such as saturated vapor and carbon dioxide
Medium reacts with the building stone of the easy moisture absorption in timber, removes most of nutriment and volatile organism, long-term anti-corrosion effect
The good timber green mould proof processing method of fruit.
Technical solution is used by solving above-mentioned technical problem：Timber, which synchronizes, carries out saturated vapor boiling and titanium dioxide
Carbon-impregnated proposes processing, and timber is under high temperature high temperature, saturated vapor and the common atmosphere of carbon dioxide, since chemical group combines, wood
Material ingredient such as is thermally decomposed at the chemical reactions, reduces in timber the easily building stone of the moisture absorption；Saturated vapor and carbon dioxide are being located
It is flowed in reason tank, takes away the nutriments such as Partial Protein and lipid and volatile organism；Carbon dioxide is dissolved in water and generates centainly
The carbonic acid of amount plays the role of acidleach to timber and carries.
The mildew-proof treatment method carries out as follows：
One, using water vapour as heat medium, carbon dioxide gas, exclusion processing are passed through from another air inlet pipe by compressor
Air content is rapidly heated within 5% to 100-120 DEG C in tank, and processing pressure tank keeps 0.5-1MPa, soaking time 2-
4h；
Two, continue to be passed through water vapour, air compressor machine pressurization is passed through carbon dioxide, handles pressure tank 1-3MPa, be warming up to 120-
150 DEG C, soaking time 4-8h；
Three, continue to be passed through water vapour and carbon dioxide, keep the temperature 120-150 DEG C, handle pressure tank 1-2MPa, it is dry to aqueous
Within rate 5%；
Four, stop being passed through carbon dioxide, spraying cooling adjusts humidity, Temperature fall, moisture content 4- within 90 DEG C
8%.
Timber is the plank of domestic the tradition high-quality timber and fast growing wood such as maple, rubber wood timber, pine, plate thickness less than etc.
In 100mm.
The beneficial effects of the invention are as follows：This method is synchronized using timber carries out saturated vapor boiling and carbon dioxide extraction
Processing reduces the building stone of the easy moisture absorption in timber, removes the nutriments such as Partial Protein and lipid and volatile organism,
Environmentally protective, safe and harmless, long-term anti-mold effect is good；With the timber Environmental Safety of the mould proof processing of this method, can be used for preparing
Virgin wooden toy, baby child's daily necessities etc..
Specific implementation mode
The present invention is described in further detail with reference to embodiment：Following embodiment be explanation of the invention and the present invention simultaneously
It is not limited to following embodiment.
Embodiment 1
1) prepared by sample
The sample that specification is 500 × 120 × 20mm (length × width x thickness) is made in sweetgum timber.
2) water vapour boiling is handled with carbon dioxide extraction
Sweetgum wood is placed in can lead to heat medium water vapour and carbon dioxide gas, pressure resistance -0.1-4MPa timber height simultaneously
It presses in corrosion-resistant process tank, is passed through heat medium saturated vapor, carbon dioxide gas is passed through from another air inlet pipe by compressor
Body excludes air content in process tank and is rapidly heated within 5% to 100 DEG C, and processing pressure tank keeps 0.5MPa, when heat preservation
Between 2h；Continue to be passed through water vapour, air compressor machine pressurization is passed through carbon dioxide, handles pressure tank 1MPa, is warming up to 120 DEG C, when heat preservation
Between 4h；Continue to be passed through water vapour and carbon dioxide, keep the temperature 120 DEG C, pressure tank 1MPa is handled, within drying to moisture content 5%；Stop
Only it is passed through carbon dioxide, spraying cooling adjusts humidity, Temperature fall, moisture content 7.45% within 90 DEG C.
3) sample corrosion resistant performance
The mass loss rate 7.45% of sweetgum wood corrosion-proof experiment, corrosion resistant grade I.
Embodiment 2
1) prepared by sample
The sample that specification is 500 × 120 × 40mm (length × width x thickness) is made in sweetgum timber.
2) water vapour boiling is handled with carbon dioxide extraction
The step of timber green mould proof processing method, is as follows in the present embodiment：It is passed through heat medium saturated vapor, is passed through
Compressor is passed through carbon dioxide gas from another air inlet pipe, exclude in process tank air content within 5%, be rapidly heated to
110 DEG C, processing pressure tank keeps 0.75MPa, soaking time 3h；Continuing to be passed through water vapour, air compressor machine pressurization is passed through carbon dioxide,
Pressure tank 2MPa is handled, is warming up to 135 DEG C, soaking time 6h；Continue to be passed through water vapour and carbon dioxide, keeps the temperature 135 DEG C, processing
Pressure tank 1.5MPa, within drying to moisture content 5%；Stopping is passed through carbon dioxide, and spraying cooling is adjusted wet within 90 DEG C
Degree, Temperature fall, moisture content 9.61%.
3) sample corrosion resistant performance
The mass loss rate 6.71% of sweetgum wood corrosion-proof experiment, corrosion resistant grade I.
Embodiment 3
1) prepared by sample
The sample that specification is 500 × 120 × 60mm (length × width x thickness) is made in sweetgum timber.
2) water vapour boiling is handled with carbon dioxide extraction
The step of timber green mould proof processing method, is as follows in the present embodiment：It is passed through heat medium saturated vapor, is passed through
Compressor is passed through carbon dioxide gas from another air inlet pipe, exclude in process tank air content within 5%, be rapidly heated to
120 DEG C, processing pressure tank keeps 1.0MPa, soaking time 4h；Continuing to be passed through water vapour, air compressor machine pressurization is passed through carbon dioxide,
Pressure tank 3MPa is handled, is warming up to 150 DEG C, soaking time 8h；Continue to be passed through water vapour and carbon dioxide, keeps the temperature 150 DEG C, processing
Pressure tank 2.0MPa, within drying to moisture content 5%；Stopping is passed through carbon dioxide, and spraying cooling is adjusted wet within 90 DEG C
Degree, Temperature fall, moisture content 7.28%.
3) sample corrosion resistant performance
The mass loss rate 5.50% of sweetgum wood corrosion-proof experiment, corrosion resistant grade I.
Embodiment 4
1) prepared by sample
The sample that specification is 500 × 120 × 20mm (length × width x thickness) is made in rubber wood timber.
2) water vapour boiling is handled with carbon dioxide extraction
The step of timber green mould proof processing method, is as follows in the present embodiment：It is passed through heat medium saturated vapor, is passed through
Compressor is passed through carbon dioxide gas from another air inlet pipe, exclude in process tank air content within 5%, be rapidly heated to
105 DEG C, processing pressure tank keeps 0.6MPa, soaking time 2.5h；Continue to be passed through water vapour, air compressor machine pressurization is passed through titanium dioxide
Carbon handles pressure tank 1.25MPa, is warming up to 125 DEG C, soaking time 4.5h；Continue to be passed through water vapour and carbon dioxide, keep the temperature
125 DEG C, pressure tank 1.25MPa is handled, within drying to moisture content 5%；Stopping is passed through carbon dioxide, spraying cooling to 90 DEG C with
It is interior, adjust humidity, Temperature fall, moisture content 6.97%.
3) sample corrosion resistant performance
The mass loss rate 6.39% of rubber wood timber corrosion-resistanting test, corrosion resistant grade I.
Embodiment 5
1) prepared by sample
The sample that specification is 500 × 120 × 40mm (length × width x thickness) is made in rubber wood timber.
2) water vapour boiling is handled with carbon dioxide extraction
The step of timber green mould proof processing method, is as follows in the present embodiment：It is passed through heat medium saturated vapor, is passed through
Compressor is passed through carbon dioxide gas from another air inlet pipe, exclude in process tank air content within 5%, be rapidly heated to
115 DEG C, processing pressure tank keeps 0.8MPa, soaking time 3.5h；Continue to be passed through water vapour, air compressor machine pressurization is passed through titanium dioxide
Carbon handles pressure tank 2.25MPa, is warming up to 140 DEG C, soaking time 6.5h；Continue to be passed through water vapour and carbon dioxide, keep the temperature
140 DEG C, pressure tank 1.75MPa is handled, within drying to moisture content 5%；Stopping is passed through carbon dioxide, spraying cooling to 90 DEG C with
It is interior, adjust humidity, Temperature fall, moisture content 8.04%.
3) sample corrosion resistant performance
The mass loss rate 5.80% of rubber wood timber corrosion-resistanting test, corrosion resistant grade I.
Embodiment 6
1) prepared by sample
The sample that specification is 500 × 120 × 40mm (length × width x thickness) is made in pinus sylvestris var. mongolica timber.
2) water vapour boiling is handled with carbon dioxide extraction
The step of timber green mould proof processing method, is as follows in the present embodiment：It is passed through heat medium saturated vapor, is passed through
Compressor is passed through carbon dioxide gas from another air inlet pipe, exclude in process tank air content within 5%, be rapidly heated to
105 DEG C, processing pressure tank keeps 0.5MPa, soaking time 2h；Continuing to be passed through water vapour, air compressor machine pressurization is passed through carbon dioxide,
Pressure tank 1.0MPa is handled, is warming up to 125 DEG C, soaking time 4.0h；Continue to be passed through water vapour and carbon dioxide, keep the temperature 125 DEG C,
Pressure tank 1.0MPa is handled, within drying to moisture content 5%；Stopping is passed through carbon dioxide, and spraying cooling is adjusted within 90 DEG C
Humidity, Temperature fall, moisture content 10.16%.
3) sample corrosion resistant performance
The mass loss rate 8.13% of pinus sylvestris var. mongolica wood preservation experiment, corrosion resistant grade I.
Embodiment 7
1) prepared by sample
The sample that specification is 500 × 120 × 60mm (length × width x thickness) is made in pinus sylvestris var. mongolica timber.
2) water vapour boiling is handled with carbon dioxide extraction
The step of timber green mould proof processing method, is as follows in the present embodiment：It is passed through heat medium saturated vapor, is passed through
Compressor is passed through carbon dioxide gas from another air inlet pipe, exclude in process tank air content within 5%, be rapidly heated to
115 DEG C, processing pressure tank keeps 0.8MPa, soaking time 3h；Continuing to be passed through water vapour, air compressor machine pressurization is passed through carbon dioxide,
Pressure tank 2.0MPa is handled, is warming up to 140 DEG C, soaking time 6.0h；Continue to be passed through water vapour and carbon dioxide, keep the temperature 140 DEG C,
Pressure tank 1.5MPa is handled, within drying to moisture content 5%；Stopping is passed through carbon dioxide, and spraying cooling is adjusted within 90 DEG C
Humidity, Temperature fall, moisture content 8.77%.
3) sample corrosion resistant performance
The mass loss rate 8.48% of pinus sylvestris var. mongolica corrosion-resistanting test, corrosion resistant grade I.
Although the present invention is disclosed as above with embodiment, it is not limited to protection scope of the present invention, any ripe
The technical staff for knowing this technology changes and retouches made by without departing from the spirit and scope of the invention, should all belong to this
The protection domain of invention.
Claims (1)
1. a kind of timber green mould proof processing method, it is characterized in that following these steps to carry out：
(1) selection for the treatment of of wood tank：Using it is commercially available while the logical heat medium water vapour and other gases of 1-2 kinds, pressure resistance-
The process tank of 0.1-4MPa, vacuum degree 0-0.098MPa wood vacuum high pressure corrosion resistants, and added in addition to water vapour in process tank
The uniform spraying pipeline of the other gases of 1-2 kinds；
(2) boiling of timber water vapour extracts processing step with carbon dioxide：
A) first stage is passed through carbon dioxide gas by compressor using water vapour as heat medium from another air inlet pipe, excludes
Air content is rapidly heated within 5% to 100-120 DEG C in process tank, and processing pressure tank keeps 0.5-1MPa, soaking time
2-4h；
B) second stage continues to be passed through water vapour, and air compressor machine pressurization is passed through carbon dioxide, handles pressure tank 1-3MPa, be warming up to
120-150 DEG C, soaking time 4-8h；
C) phase III continues to be passed through water vapour and carbon dioxide, keeps the temperature 120-150 DEG C, handles pressure tank 1-2MPa, drying is extremely
Within water content 5%；
D) fourth stage, stopping are passed through carbon dioxide, and spraying cooling is within 90 DEG C, adjusting humidity, Temperature fall, and timber is aqueous
Rate 4-8%；
The timber is sweetgum timber, rubber wood timber or pinus sylvestris var. mongolica timber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510565656.2A CN106493812B (en) | 2015-09-06 | 2015-09-06 | A kind of timber green mould proof processing method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510565656.2A CN106493812B (en) | 2015-09-06 | 2015-09-06 | A kind of timber green mould proof processing method |
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| CN106493812A CN106493812A (en) | 2017-03-15 |
| CN106493812B true CN106493812B (en) | 2018-09-28 |
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Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108748505A (en) * | 2018-06-26 | 2018-11-06 | 阜南县猛发工艺品有限公司 | A kind for the treatment of process improving timber stability |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB191306179A (en) * | 1913-03-12 | 1913-10-23 | Louis Dautreppe | Improved Process and Apparatus for Impregnating Wood. |
| GB596781A (en) * | 1943-07-15 | 1948-01-12 | Karl Schulhof C O Residential | Improvements in or relating to the drying and preservation of timber or the like |
| CN101890741A (en) * | 2009-05-18 | 2010-11-24 | 韦兆玖 | Method for comprehensively modifying rubber wood timber |
| CN103331793A (en) * | 2013-06-16 | 2013-10-02 | 荆州文物保护中心 | Supercritical dewatering and drying method for small water-saturated bamboo and wood articles |
| CN104942946A (en) * | 2015-07-14 | 2015-09-30 | 孙伟伦 | Environmentally-friendly antiseptic wood manufacturing method with biomass gas as heating medium |
-
2015
- 2015-09-06 CN CN201510565656.2A patent/CN106493812B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB191306179A (en) * | 1913-03-12 | 1913-10-23 | Louis Dautreppe | Improved Process and Apparatus for Impregnating Wood. |
| GB596781A (en) * | 1943-07-15 | 1948-01-12 | Karl Schulhof C O Residential | Improvements in or relating to the drying and preservation of timber or the like |
| CN101890741A (en) * | 2009-05-18 | 2010-11-24 | 韦兆玖 | Method for comprehensively modifying rubber wood timber |
| CN103331793A (en) * | 2013-06-16 | 2013-10-02 | 荆州文物保护中心 | Supercritical dewatering and drying method for small water-saturated bamboo and wood articles |
| CN104942946A (en) * | 2015-07-14 | 2015-09-30 | 孙伟伦 | Environmentally-friendly antiseptic wood manufacturing method with biomass gas as heating medium |
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| CN106493812A (en) | 2017-03-15 |
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| CB02 | Change of applicant information |
Address after: 323600 1 Green Road, Lantau Peak street, Yunhe County, Lishui, Zhejiang Applicant after: Young education equipment Limited by Share Ltd in Yunhe County Applicant after: Zhejiang Academy of Forestry Address before: 323600 No. 1, green road, lion head village, Hou Shan village, Yunhe County, Zhejiang Applicant before: Yunhe Green Forest Handicrafts Co., Ltd. Applicant before: Zhejiang Academy of Forestry |
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Effective date of registration: 20210826 Address after: 323600 1 Green Road, Lantau Peak street, Yunhe County, Lishui, Zhejiang Patentee after: Yunhe County Lulin Preschool Equipment Co.,Ltd. Address before: 323600 1 Green Road, Lantau Peak street, Yunhe County, Lishui, Zhejiang Patentee before: Yunhe County Lulin Preschool Equipment Co.,Ltd. Patentee before: Zhejiang Academy of Forestry |
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Denomination of invention: A green mould proof treatment method for wood Effective date of registration: 20220524 Granted publication date: 20180928 Pledgee: Agricultural Bank of China Limited Yunhe County sub branch Pledgor: Yunhe County Lulin Preschool Equipment Co.,Ltd. Registration number: Y2022330000778 |
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