CN106491392B - A kind of transparent solid perfume and preparation method thereof - Google Patents

A kind of transparent solid perfume and preparation method thereof Download PDF

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Publication number
CN106491392B
CN106491392B CN201610936044.4A CN201610936044A CN106491392B CN 106491392 B CN106491392 B CN 106491392B CN 201610936044 A CN201610936044 A CN 201610936044A CN 106491392 B CN106491392 B CN 106491392B
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weight
parts
polyamide
permethyl
transparent solid
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CN201610936044.4A
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CN106491392A (en
Inventor
陶安力
于秀丽
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Chi Hua ton flavor and fragrance (Guangzhou) Co.,Ltd.
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Full Flavor & Fragrance (guangzhou) Co Ltd
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/88—Polyamides
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0216—Solid or semisolid forms
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31—Hydrocarbons
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/342—Alcohols having more than seven atoms in an unbroken chain
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37—Esters of carboxylic acids
    • A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q13/00—Formulations or additives for perfume preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin

Abstract

The invention discloses a kind of transparent solid perfume, which includes following components by weight percent, 16~60 parts by weight skin care greases, 12~30 parts by weight excipient, 20~40 parts by weight volatility greases, 5~15 parts by weight essence；The invention also discloses the preparation method of the transparent solid perfume, the volatility grease refers to the mixture of neopentyl glycol two heptanoates and Permethyl 99A.The invention belongs to perfume area, transparent solid perfume of the invention has many advantages, such as that lasting is more longlasting, skin sense is good.

Description

A kind of transparent solid perfume and preparation method thereof
Technical field
The present invention relates to perfume areas more particularly to a kind of transparent solid perfume and preparation method thereof.
Background technique
Popular perfume form is mainly liquid on the market at present, is easy to spill, and Packaging Bottle is vial, for travelling with Body is carried there are certain restrictions, due to containing more alcohol, stores improper also inflammable risk.Consumer is also desirable to There is a kind of portable perfume form of safety to come out, solid perfume has gradually attracted consumer.Glittering and translucent solid perfume Undoubtedly bigger innovation.
CN201310226279.0 discloses a kind of preparation method of novel solid perfume stick, and steps are as follows: 1) weighing down State the component of mass percent: isopropyl palmitate fat 15~18%；Microwax 10~15%；Salicylic acid benzene rouge 6~8%；Poly- second Glycol 40011~20%, remaining is water, is uniformly mixed and is heated to 80 DEG C, makes each component dissolution in uniform shape liquid mixture, 60 DEG C are cooled to, is kept the temperature spare；2) it weighs liquid mixture 50~80%, is added essence or fragrance component 10~15%, the third two Alcohol 25~45%, constant temperature, which stirs evenly, to be poured into bar molds.It is encapsulated essence aqueous solution by propylene glycol and reaches sustained release purpose, Its fragrance remaining time is short, and its skin sense is poor.
Summary of the invention
In view of the above deficiencies, the transparent solid perfume that the purpose of the present invention is to provide a kind of lastings is more longlasting, skin sense is good, The invention also discloses the preparation methods of above-mentioned transparent solid perfume.
In order to solve the above technical problem, the present invention provides previous technical solution be such that a kind of transparent solid is fragrant Water, including following weight percent composition: 16~60 parts by weight skin care greases, 12~30 parts by weight excipient, 20~40 weight Part volatility grease, 5~15 parts by weight essence, above-mentioned volatility grease refer to two heptanoate of neopentyl glycol and Permethyl 99A Mixture, wherein the weight ratio of two heptanoate of neopentyl glycol and Permethyl 99A is 63~67:33~37.
It should be noted that above-mentioned skin care grease includes following weight percent composition: 10~40 parts by weight C12-C15 Alcohol benzoic ether, 5~15 parts by weight isooctadecanols, 1~5 parts by weight isopropyl palmitate.
C12-C15 alcohol benzoic ether supplier is CRODA, trade name: Crodamol AB or supplier Evonik, commodity Name Tegosoft TN.It should be noted that above-mentioned excipient includes following weight percent composition: 10~20 parts by weight are poly- Amide -8,2~10 weight parts of polyamide -3.
Preferably, the transparent solid perfume, including following components: 30 parts by weight C12-C15 alcohol benzoic ethers；30 weights Measure two heptanoate & Permethyl 99A of part neopentyl glycol；20 weight parts of polyamide -8；2 weight parts of polyamide -3；The different tristearin of 5 parts by weight Alcohol；3 parts by weight isopropyl palmitates；10 parts by weight essence.
It should be noted that above-mentioned C12-C15 alcohol benzoic ether has salubrious skin-care effect.
The mixture of above-mentioned two heptanoate of neopentyl glycol and Permethyl 99A can promote fragrance to wave as volatility grease Hair, when use, can increase the sliding skin sense of salubrious silk.
While above-mentioned polyamide -8, Polyamide-3 form transparent solid appearance, there is skin care effect.
Above-mentioned isooctadecanol can also be improved the transparency of solid perfume system while nourishing skin.
Above-mentioned isopropyl palmitate can increase salubrious sense while skin care.
Latter technique scheme provided by the invention are as follows: the preparation method of the transparent solid perfume the following steps are included:
By C12-C15 alcohol benzoic ether, polyamide -8, Polyamide-3, isooctadecanol, isopropyl palmitate ratio by weight It is uniformly mixed and is heated to being completely dissolved, after being cooled to 50 degrees Celsius, two heptanoate & Permethyl 99A of neopentyl glycol is added, is added Essence stirs evenly, and pours into container formation.
Compared with prior art, technical solution provided by the invention has the advantage that
1. transparent solid volatilizing perfume of the invention is slightly slow, lasting is more longlasting；
2. the present invention can make this solid perfume show high transparency using the excipient of compounding, and have preferable shield Skin effect.
3. skin care grease of the invention, excipient, volatility grease play the role of skin care or improve skin sense, can make Perfume of the invention can't generate greasy feeling while with skin care sense, and when use is more salubrious, reach skin sense With the double effects of skin care, and appearance transparent, user's acceptance are higher.
4. transparent solid perfume of the invention not spirituosity, avoids skin allergy caused by alcohol；
5. transparent solid perfume of the invention can be made into the shapes such as rodlike, box-packed, it is not easy to it spills, it is easy to carry, it is convenient It uses.
Specific embodiment
With reference to embodiment, claim of the invention is described in further detail, but do not constituted pair Any restrictions of the invention, the modification of any limited times made within the scope of the invention as claimed, still in power of the invention In the claimed range of benefit.
Embodiment 1
By C12-C15 alcohol benzoic ether 30g, -8 20g of polyamide, Polyamide-3 2g, isooctadecanol 5g, palmitinic acid isopropyl Ester 3g is uniformly mixed and is heated to being completely dissolved, and after being cooled to 50 degrees Celsius, two heptanoate & Permethyl 99A of neopentyl glycol is added 30g (weight ratio of neopentyl glycol two heptanoates and Permethyl 99A are as follows: 63%:37%) is added essence 10g, stirs evenly, pour into Container formation.
Embodiment 2
By C12-C15 alcohol benzoic ether 20g, -8 10g of polyamide, Polyamide-3 10g, isooctadecanol 7.5g, palmitinic acid Isopropyl ester 5g is uniformly mixed and is heated to being completely dissolved, and after being cooled to 50 degrees Celsius, two heptanoate & different 12 of neopentyl glycol is added Alkane 40g (weight ratio of neopentyl glycol two heptanoates and Permethyl 99A are as follows: 64%:36%) is added essence 7.5g, stirs evenly, Pour into container formation.
Embodiment 3
C12-C15 alcohol benzoic ether 10g, -8 15g of polyamide, Polyamide-3 5g, isooctadecanol 15g, palmitinic acid is different Propyl ester 5g is uniformly mixed and is heated to being completely dissolved, and after being cooled to 50 degrees Celsius, two heptanoate & Permethyl 99A of neopentyl glycol is added 35g (weight ratio of neopentyl glycol two heptanoates and Permethyl 99A are as follows: 65%:35%) is added essence 15g, stirs evenly, pour into Container formation.
Embodiment 4
C12-C15 alcohol benzoic ether 40g, -8 18g of polyamide, Polyamide-3 9g, isooctadecanol 14g, palmitinic acid is different Propyl ester 4g is uniformly mixed and is heated to being completely dissolved, and after being cooled to 50 degrees Celsius, two heptanoate & Permethyl 99A of neopentyl glycol is added 20g (weight ratio of neopentyl glycol two heptanoates and Permethyl 99A are as follows: 66%:34%) is added essence 5g, stirs evenly, pour into Container formation.
Embodiment 5
C12-C15 alcohol benzoic ether 25g, -8 18g of polyamide, Polyamide-3 6g, isooctadecanol 10g, palmitinic acid is different Propyl ester 1g is uniformly mixed and is heated to being completely dissolved, and after being cooled to 50 degrees Celsius, two heptanoate & Permethyl 99A of neopentyl glycol is added 20g (weight ratio of neopentyl glycol two heptanoates and Permethyl 99A are as follows: 67%:33%) is added essence 10g, stirs evenly, pour into Container formation.
Using test
For the performance for verifying the solid perfume, we have looked for 10 volunteers to carry out measure of merit in intra-company, choose Using identical essence and by the traditional liquid perfume that is made into respectively of formula and solid perfume, when being tried out by volunteer and assessing lasting Between and skin sense preference degree, and make volunteer as shown in Table 1 to the fancy grade of traditional liquid perfume and solid perfume Application form, wherein 1 is fragrance liquid, 2 be solid perfume such as embodiment 5.
Application form of 1 volunteer of table to the fancy grade of traditional liquid perfume and solid perfume
Volunteer Age Appearance hobby Lasting persistence Skin care sense
Miss Li 30-40 2 2 about 10h, 1 about 5h 2 have moisture feeling
Miss Zhang 20-30 2 2 about 6h, 1 about 4h 2 have moisture feeling
Miss Lv 20-30 2 2 about 8h, 1 about 4h 2 have moisture feeling
Miss Chen 20-30 2 2 about 10h, 1 about 5h 2 have moisture feeling
Guo Sheng 20-30 1 2 about 4h, 1 about 1h 1 is salubrious
Wang Sheng 30-40 2 2 about 6h, 1 about 3h 1 is salubrious
Cheng Sheng 30-40 2 2 about 8h, 1 about 3h 2 have moisturizing sense
Miss Liu 30-40 2 2 about 8h, 1 about 3h 2 have moisture feeling
Liu Sheng 30-40 1 2 about 10h, 1 about 4h 2 have moisturizing sense
There are 8 people to like solid perfume appearance as can be seen from the results, all volunteers think solid perfume fragrance remaining time Relatively long, most of trier thinks that solid perfume has moisture feeling to skin, there is skin care effect；2 people prefer traditional liquid perfume The salubrious sense of water.
Be 100% with pure water light transmittance it is reference, measures transparent solid balm with 400 instrument of Lange Lico and (implement Example 5) light transmittance be 98.9%, close to the transparency of water.Specific light transmittance see the table below 2:
Table 2: the light transmittance of transparent solid perfume
Above-described is only presently preferred embodiments of the present invention, all made within the scope of the spirit and principles in the present invention What modifications, equivalent substitutions and improvements etc., should all be included in the protection scope of the present invention.

Claims (3)

1. a kind of transparent solid perfume, which is characterized in that be made of following weight percent composition: 16~60 parts by weight skin care oils Rouge, 12~30 parts by weight excipient, 20~40 parts by weight volatility greases, 5~15 parts by weight essence, the excipient include Following weight percent composition: 10~20 weight parts of polyamide -8,2~10 weight parts of polyamide -3, the volatility grease For the mixture of neopentyl glycol two heptanoates and Permethyl 99A, wherein the weight ratio of neopentyl glycol two heptanoates and Permethyl 99A Example is 63~67:33~37；The skin care grease includes following weight percent composition: 10~40 parts by weight C12-C15 alcohol Benzoic ether, 5~15 parts by weight isooctadecanols, 1~5 parts by weight isopropyl palmitate.
2. transparent solid perfume according to claim 1, which is characterized in that be made of following weight percent composition: 30 Parts by weight C12-15 alcohol benzoic ether；The mixture of 30 parts by weight neopentyl glycol two heptanoates and Permethyl 99A；20 parts by weight are poly- Amide -8；2 weight parts of polyamide -3；5 parts by weight isooctadecanols；3 parts by weight isopropyl palmitates；10 parts by weight essence.
3. a kind of preparation method of transparent solid perfume as claimed in claim 1 or 2, which comprises the following steps: C12-C15 alcohol benzoic ether, polyamide -8, Polyamide-3, isooctadecanol, isopropyl palmitate ratio by weight are uniformly mixed And be heated to being completely dissolved, after being cooled to 50 DEG C, the mixture of neopentyl glycol two heptanoates and Permethyl 99A is added, is added fragrant Essence stirs evenly, and pours into container formation.
CN201610936044.4A 2016-11-01 2016-11-01 A kind of transparent solid perfume and preparation method thereof Active CN106491392B (en)

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DE102018221937A1 (en) * 2018-12-17 2020-06-18 Henkel Ag & Co. Kgaa HAIR OILS FOR CONDITIONING KERATINE FIBERS

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1802144A (en) * 2003-04-10 2006-07-12 荷兰联合利华有限公司 Fragranced solid cosmetic compositions based on a starch delivery system
CN101801331A (en) * 2007-09-17 2010-08-11 阿利桑那化学公司 Polyamide and cosmetic composition, by the product of said composition preparation, and preparation and use the method for said composition and product
CN102847185A (en) * 2012-09-27 2013-01-02 乐美加特种纤维（连云港）有限公司 Solid transparent fragrant deodorizing agent and preparation method thereof
CN103330657A (en) * 2013-06-08 2013-10-02 吴江市利达上光制品有限公司 Preparation method of novel solid perfume stick
CN104394831A (en) * 2012-05-25 2015-03-04 化妆品武士有限公司 Composition
CN104704096A (en) * 2012-10-08 2015-06-10 帝斯曼知识产权资产管理有限公司 Flavor and fragrance formulation (ii)

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1802144A (en) * 2003-04-10 2006-07-12 荷兰联合利华有限公司 Fragranced solid cosmetic compositions based on a starch delivery system
CN101801331A (en) * 2007-09-17 2010-08-11 阿利桑那化学公司 Polyamide and cosmetic composition, by the product of said composition preparation, and preparation and use the method for said composition and product
CN104394831A (en) * 2012-05-25 2015-03-04 化妆品武士有限公司 Composition
CN102847185A (en) * 2012-09-27 2013-01-02 乐美加特种纤维（连云港）有限公司 Solid transparent fragrant deodorizing agent and preparation method thereof
CN104704096A (en) * 2012-10-08 2015-06-10 帝斯曼知识产权资产管理有限公司 Flavor and fragrance formulation (ii)
CN103330657A (en) * 2013-06-08 2013-10-02 吴江市利达上光制品有限公司 Preparation method of novel solid perfume stick

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Address after: No. 66, Hongjing Road, East District, Guangzhou Economic and Technological Development Zone, Guangdong 510000

Patentee after: Chi Hua ton flavor and fragrance (Guangzhou) Co.,Ltd.

Address before: No. 66, Hongjing Road, East District, Guangzhou Economic and Technological Development Zone, Guangdong 510000

Patentee before: DROM FRAGRANCES (GUANGZHOU) Co.,Ltd.

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