CN106477889B - A kind of your porcelain agate viridescent glaze and its processing method, your porcelain and its method for cooking - Google Patents

A kind of your porcelain agate viridescent glaze and its processing method, your porcelain and its method for cooking Download PDF

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CN106477889B
CN106477889B CN201610955345.1A CN201610955345A CN106477889B CN 106477889 B CN106477889 B CN 106477889B CN 201610955345 A CN201610955345 A CN 201610955345A CN 106477889 B CN106477889 B CN 106477889B
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porcelain
agate
glaze
stone
viridescent
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CN106477889A (en
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张天庆
张颖政
张颖裕
郭秀贞
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    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
    • C03C8/00Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
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    • C03CCHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
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    • C04B41/45Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
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    • C04B41/00After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
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    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
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Abstract

The present invention relates to your a kind of porcelain agate viridescent glaze and its processing method, your porcelain and its method for cooking are related to silicate ceramics technical field.Your the porcelain agate viridescent glaze contains the component of following parts by weight: you is 6~20 parts of stone, and 1~15 part of Agate, 10~70 parts of feldspar, 2~8 parts of calcite, 1~20 part of wollastonite, 0~2 part of talcum, 0~15 part of chestnut ash, 1~8 part of spot fossil, 1~20 part of black green stone.Your the enamel matter for using your porcelain agate viridescent glaze of the invention to burn out is using viridescent as keynote, can show enamel it is simple and honest be full of the sky blue, reddish black of profit, pale blue, bluish white, ovum is green, the color of emerald green blueness, bright pea green, the pale yellowish green color of revealing the exact details of enamel can also be showed.Good using your the porcelain jade sense and opal effect of your of the invention porcelain agate viridescent glaze, glaze paint is more smooth, mechanical strength is higher, water absorption rate is lower, and sintering qualified rate is high.

Description

A kind of your porcelain agate viridescent glaze and its processing method, your porcelain and its method for cooking
Technical field
The present invention relates to silicate ceramics technical fields, and in particular to a kind of your porcelain agate viridescent glaze and its processing method, Further relate to a kind of your porcelain and its method for cooking.
Background technique
Ruyao is gained the name because locating Ruzhou, be China's Song Dynasty you, brother, official, first of fixed, five big kilns of an ancient unit of weight, your produced porcelain " juice jade-like stone pool, aqueous to be dripped, glaze such as cream liposoluble is without flowing, and glaze is thick and sound such as uses up, and becomes clear without dazzling ", has " green such as day, beauty As jade, cicada's wings hacking, full glaze are bound the feet of women, support pin is burnt " typical characteristic.But due to historical reasons, Ruyao firing time only 20 Yu Nian, it is very short that burning makes the time, limits throughput, spreads seldom, and when the Southern Song Dynasty " close outstanding rare ", countries in the world and China are major at present The collection in museum only more than 60 part, becomes rare treasure.
For the prior art when firing your porcelain, it is original that the glaze of application, which is usually with feldspar, quartz, calcite and dark stone etc., Material will be ground, and be obtained after adding water to modulate.CN101747089A discloses a kind of Ru agate glaze and its processing method, agate glaze contain There is a component of following parts by weight: 6~26 parts of Agate, 40~65 parts of feldspar, 10~23 parts of calcite, 13~28 parts of black green stone, 3~8 parts of spot fossil, 2~4 parts of talcum, 5~10 parts of chestnut ash.The enamel of your porcelain burnt out using the agate glaze is with green, green For keynote, simple and honest sky blue, the reddish black and bluish white color for being full of profit of enamel can be showed, can also show that enamel is bright to reveal the exact details Pea green, pale yellowish green and pale blue color;Tire matter is fine and smooth fine and close, and porcelain degree is high, and water absorption rate is no more than 1.2%, tunks product sound Sound is clear and melodious;Thermal stability is good, without through crack, seepage defect.But use the glaze paint smoothness of your porcelain of above-mentioned Ru agate glaze And mechanical strength is all to be improved.
Summary of the invention
It can make that your ceramic glaze surface smoothness is more preferable, your higher porcelain agate of mechanical strength the object of the present invention is to provide one kind Dark green glaze, while your the porcelain viridescent glaze has effects that diseases prevention, health care, being used for a long time can be prolonged using your your porcelain of porcelain viridescent glaze Year lengthens one's life.
The present invention also provides a kind of processing method of your porcelain agate viridescent glaze, your porcelain and its method for cooking.
In order to achieve the goal above, technical solution used by your porcelain agate viridescent glaze of the invention is:
Your a kind of porcelain agate viridescent glaze, the component containing following parts by weight: you is 6~20 parts of stone, 1~15 part of Agate, long 10~70 parts of stone, 2~8 parts of calcite, 1~20 part of wollastonite, 0~2 part of talcum, 0~15 part of chestnut ash, 1~8 part of spot fossil, 1~20 part of black green stone.
In your porcelain agate viridescent glaze of the invention, the effect of each component is as follows:
Agate: i.e. agate, main chemical compositions are silica, and density is 2.6~2.66g/cm3, hardness 7, With wax-like gloss, agate is added in green body and glaze, the mechanical strength of your porcelain can be improved, the microelement in agate helps In your porcelain quality, the finish and jade sense of your ceramic glaze surface are improved, skeleton function is played in glaze.
Your stone also known as Ruzhou is beautiful, Plum Blossom Jade, is Chinese name stone, gains the name because producing Ruzhou, main chemical compositions are titanium dioxide Silicon, calcium oxide, quality be fine and smooth, hardness 7, and background color has black, brown red and three kinds green, partially has plum blossom-shaped, through country mine The identification of research institute of portion physical and chemical testing, the microelement containing a variety of needed by human body such as iron, zinc, sodium, magnesium, potassium, calcium in your stone, your stone Play skeleton in glaze and reduce temperature, additionally aid quality, combines green body and glaze stronger, moreover it is possible to make glaze paint more light It is sliding.
Feldspar is cosolvent in glaze, can increase the whiteness and glossiness of glaze.
Calcite is cosolvent in glaze, can be shortened firing time, increases the light transmittance of porcelain, is improved between base and glaze Binding force.
Wollastonite, natural mineral matter, main component are calcium oxide 48.25%, silica 51.75%, white, light gray Color, light green color, grey, yellow, light red, red, brown or colourless.Dry contraction and firing of the wollastonite in green body are shunk It is all small, constriction coefficient can be reduced, and there is dissolution assistant effect, the sintering temperature of green body can be reduced, replace lime stone and stone with it When English configures glaze, glaze paint will not generate glaze bubble pin hole because of bubbing.Acicular wollastonite crystal of the wollastonite in green body Cross arrangement reticulates, and is around reinforced by anorthite and quartz, so the mechanical strength of product is higher.
Talcum mainly contains magnesia, is cosolvent in glaze, promotes the generation of middle layer between green body and glaze, improve you The thermal stability of porcelain expands firing range, increases milkiness effect.
Chestnut ash can make your ceramic glaze surface of firing generate opal effect in glaze, improve the ornamental value of your porcelain.It is using Before, it is first rinsed with water, then dry.
Black green stone and spot fossil are cosolvent and colorant in glaze, containing micro in black green stone and spot fossil Di-iron trioxide makes your porcelain being fired into that green pea green, reddish black, pale blue, ovum, emerald green blueness or light greenish blue color be presented.
Your the enamel matter for using your porcelain agate viridescent glaze of the invention to burn out is with viridescent can to show for keynote Enamel is simple and honest be full of the sky blue, reddish black of profit, pale blue, bluish white, ovum is green, the color of emerald green blueness, the bright beans revealed the exact details of enamel can also be showed Green, pale yellowish green color.It is good using your the porcelain jade sense and opal effect of your of the invention porcelain agate viridescent glaze, glaze paint is more smooth, Mechanical strength is higher, water absorption rate is lower (being no more than 1%), and sintering qualified rate is high.Containing there are many needed by human body in your stone Microelement has the effect of diseases prevention, health care, long-time service can using your porcelain using your of the invention porcelain agate viridescent glaze Promote longevity.
Technical program of the present invention also lies in: the processing method of your above-mentioned porcelain agate viridescent glaze, comprising the following steps:
1) your stone and Agate are calcined respectively at 800~900 DEG C, is then crushed, obtain your stone of graininess or powdery And Agate;
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery Building stones;
3) your stone and Agate, step 2) of chestnut ash, the resulting graininess of step 1) or powdery according to the weight ratio, are taken Then plus water for ball milling the building stones of resulting each graininess or powdery, mixing obtain glaze slip;
4) by the Concentration Modulation of glaze slip obtained by step 3) to 52~56 Baume degrees, then remove iron, it is aging to get.
Preferably, in step 1), the time of the calcining is 3.5~4h.
Preferably, in step 3), the time of the ball milling is 34~38h.The chestnut ash is rinsed with water, is made again after drying With.In order to make glaze slip reach certain fineness, after adding water for ball milling, filtered using 10000-hole sieve.
Preferably, in step 4), the measuring instrument used when modulating concentration is Baume degrees specific gravity instrument.Before except iron, first The later glaze slip sieving of concentration will be modulated.
Technical program of the present invention also lies in a kind of your porcelain, including your porcelain agate viridescent glaze and green body;Your porcelain agate Dark green glaze contains the component of following parts by weight: you is 6~20 parts of stone, and 1~15 part of Agate, 10~70 parts of feldspar, calcite 2~8 Part, 1~20 part of wollastonite, 0~2 part of talcum, 0~15 part of chestnut ash, 1~8 part of spot fossil, 1~20 part of black green stone.
Your of the invention enamel matter with green, green for keynote, can show enamel it is simple and honest be full of the sky blue, reddish black of profit, pale blue, It is bluish white, ovum is green, the color of emerald green blueness, bright pea green, the pale yellowish green color of revealing the exact details of enamel can also be showed.
Your of the invention porcelain jade sense and opal effect are good, and glaze paint is more smooth, and mechanical strength is higher, and water absorption rate is lower (no More than 1%), while tunking clear, thermal stability is good, without through crack, seepage defect.There is diseases prevention in use, protect Strong effect, long-time service can promote longevity.
Preferably, the green body contains following components in percentage by weight: wollastonite 1~5%, your stone 2~10%.Green body In other components be your the common component of porcelain billet body.Wollastonite and your stone in green body can make the tire matter more refinement of your porcelain Greasy, fine and close, porcelain degree is higher.
Technical program of the present invention also lies in: the method for cooking of your above-mentioned porcelain, comprising the following steps:
1) your the porcelain agate viridescent glaze stirred evenly is equably applied on green body, obtains glazed body;
2) glazed body obtained by step 1) is fired, is first fired with oxidizing flame in sintering procedure, temperature is risen to 950~ 1050 DEG C, then fired with reduction flame, temperature is continued to rise to 1230~1260 DEG C, 15~20min is kept the temperature, stops burning, is dropped naturally Warm to room temperature to get.
Your of the invention porcelain is in sintering procedure, and with the raising of firing temperature, wollastonite expanded by heating in green body is supported The dry of green body that disappeared is shunk, and is shortened drying time, and then shorten the production cycle, is reduced production cost, while also mentioning The high plasticity of green body;When firing temperature continues to improve, the viscosity of liquid phase is can be improved in your stone in glaze, is filled in green body Gap makes green body reach densification, not only improves the mechanical strength for improving your porcelain, and facilitate human health.In addition, green body and The agate not melted in glaze may be constructed the skeleton of porcelain body, avoids deformation and the cracking of your porcelain, improves sintering qualified rate.
In step 1), before your porcelain agate viridescent glaze is applied on green body, green body is pre-processed;The pretreatment It is that biscuiting first is carried out to the green body of forming, then the green body good to biscuiting is polished, then dedusting, finally carries out moisturizing.
In step 2), when firing using oxidizing flame, temperature is risen to 950~1050 DEG C with 5~6h.Using reduction flame When firing, temperature is continued with 6~7h to rise to 1230~1260 DEG C.
For your of the invention porcelain during firing, be divided into five stages: the first stage is the hydrofuge stage, using oxidizing fire Flame is fired, and temperature is risen to 550~600 DEG C, keeps furnace air unobstructed, the moisture in glazed body is removed;Second stage is to rise Temperature is risen to 950~1050 DEG C with oxidizing flame by thermophase, the moisture in glazed body is discharged more thorough, is also made in glazed body Organic matter and carbon full combustion remove;Phase III is fired using reduction flame, continues to rise to temperature into 1230~1260 DEG C, Ferric iron contained by spot fossil and black green stone in glaze starts to be reduced to ferrous iron as ferrous silicon salt, and glaze starts to present different The dark green of degree;Fourth stage is holding stage, by temperature in 1230~1260 DEG C of 15~20min of holding, keeps glaze sufficiently molten Melt, carry out ferric reduction reaction more thorough, guarantees that dark green purity is presented in ferrous silicon salt;5th stage was to stop burning Temperature-fall period is naturally cooling to room temperature, and glaze is made to have a good Crystallization Process, guarantees the presented cyan of ferrous silicon salt in glaze Stability, if cooling is too fast, will lead to glaze colours be in weight cyan.
In step 2), the gas of following weight percent: oxygen is contained in gas atmosphere when firing using reduction flame 0.8~1%, carbon monoxide 2.5~9.5%.Carbon monoxide content in atmosphere is affected to glaze colours, carbon monoxide Too high levels then make glaze colours ash green or sootiness nigrescence, and content is too low, and ferrous silicon salt is reoxidized and makes glaze paint that yellow be presented.
Specific embodiment
Below in conjunction with specific embodiment, further description of the technical solution of the present invention.
In specific embodiment, chestnut ash is first rinsed with water, is dried, and is then reused.It is dense to glaze slip in Examples 1 to 3 When degree is modulated, using Baume degrees specific gravity instrument when measuring concentration.
Embodiment 1
Your the porcelain agate viridescent glaze of the present embodiment contains the component of following parts by weight: you is 13 parts of stone, and 15 parts of Agate, feldspar 40 parts, 2 parts of calcite, 15 parts of wollastonite, 15 parts of chestnut ash, 8 parts of spot fossil, 1 part of black green stone.
The processing method of your the porcelain agate viridescent glaze of the present embodiment, comprising the following steps:
1) your stone and Agate are put into kiln in 800 DEG C of calcining 3.5h respectively, are then crushed respectively, obtain graininess or Your stone and Agate of powdery;
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery Building stones;
3) your stone and Agate, step 2) of chestnut ash, the resulting graininess of step 1) or powdery according to the weight ratio, are taken Then plus water for ball milling 36h the building stones of resulting each graininess or powdery, mixing are filtered with 10000-hole sieve, obtain glaze slip;
4) then to 52 Baume degrees, removes iron, it is aging to get.
Embodiment 2
Your the porcelain agate viridescent glaze of the present embodiment contains the component of following parts by weight: you is 6 parts of stone, and 1 part of Agate, feldspar 70 Part, 5 parts of calcite, 1 part of wollastonite, 2 parts of talcum, 1 part of spot fossil, 20 parts of black green stone.
The processing method of your the porcelain agate viridescent glaze of the present embodiment, comprising the following steps:
1) your stone respectively and Agate are put into kiln in 850 DEG C of calcining 4h, then crush respectively, obtains graininess or powder Your stone and Agate of shape;
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery Building stones;
3) according to the weight ratio, take your stone and Agate, the step 2) of the resulting graininess of step 1) or powdery resulting Then plus water for ball milling 36h the building stones of each graininess or powdery, mixing are filtered with 10000-hole sieve, obtain glaze slip;
4) then to 54 Baume degrees, removes iron, it is aging to get.
Embodiment 3
Your the porcelain agate viridescent glaze of the present embodiment contains the component of following parts by weight: you is 20 parts of stone, and 13 parts of Agate, feldspar 10 parts, 8 parts of calcite, 20 parts of wollastonite, 1 part of talcum, 8 parts of chestnut ash, 5 parts of spot fossil, 15 parts of black green stone.
The processing method of your the porcelain agate viridescent glaze of the present embodiment, comprising the following steps:
1) your stone and Agate are put into kiln in 900 DEG C of calcining 4h, are then crushed respectively, obtain graininess or powdery Your stone and Agate;
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains graininess or powdery Building stones;
3) your stone and Agate, step 2) of chestnut ash, the resulting graininess of step 1) or powdery according to the weight ratio, are taken Then plus water for ball milling 36h the building stones of resulting each graininess or powdery, mixing are filtered with 10000-hole sieve, obtain glaze slip;
4) then to 56 Baume degrees, removes iron, it is aging to get.
Embodiment 4
Your porcelain of the present embodiment, including your porcelain agate viridescent glaze and green body;Your the porcelain agate viridescent glaze is 1 institute of embodiment Your porcelain agate viridescent glaze.
The method for cooking of your porcelain of the present embodiment, comprising the following steps:
1) green body is pre-processed: biscuiting first being carried out to the green body of forming, to the good green body emery cloth of biscuiting into Row polishing, then blows away dedusting with hair dryer, then wipe clean green body with sponge and carry out moisturizing to it;
2) your the porcelain agate viridescent glaze stirred evenly is equably applied on green body, then carries out wiping bottom trimming, obtain glazed body;
3) glazed body obtained by step 2) is propped up in merging kiln with support pin and is fired, oxidizing flame is first used in sintering procedure It fires, temperature is risen to 950 DEG C with the time of 5h, then fired with reduction flame, controlling the gas atmosphere in kiln includes weight Temperature is continued to rise to 1230 DEG C, keeps the temperature 15min, stop burning by the oxygen 1% of percentage, carbon monoxide 6% with the time of 6h, from So be cooled to room temperature to get.
Embodiment 5
Your porcelain of the present embodiment, including your porcelain agate viridescent glaze and green body;Your the porcelain agate viridescent glaze is 2 institute of embodiment Your porcelain agate viridescent glaze.
The method for cooking of your porcelain of the present embodiment, comprising the following steps:
1) green body is pre-processed: biscuiting first being carried out to the green body of forming, to the good green body emery cloth of biscuiting into Row polishing, then blows away dedusting with hair dryer, then wipe clean green body with sponge and carry out moisturizing to it;
2) your the porcelain agate viridescent glaze stirred evenly is equably applied on green body, then carries out wiping bottom trimming, obtain glazed body;
3) glazed body obtained by step 2) is propped up in merging kiln with support pin and is fired, oxidizing flame is first used in sintering procedure It fires, temperature is risen to 1050 DEG C with the time of 6h, then fired with reduction flame, controlling the gas atmosphere in kiln includes weight Temperature is continued to rise to 1260 DEG C, keeps the temperature 20min, stop by the oxygen 0.8% of percentage, carbon monoxide 2.5% with the time of 7h Burn, be naturally cooling to room temperature to get.
Embodiment 6
Your porcelain of the present embodiment, including your porcelain agate viridescent glaze and green body;Your the porcelain agate viridescent glaze is 3 institute of embodiment Your porcelain agate viridescent glaze.
The method for cooking of your porcelain of the present embodiment, comprising the following steps:
1) green body is pre-processed: biscuiting first being carried out to the green body of forming, to the good green body emery cloth of biscuiting into Row polishing, then blows away dedusting with hair dryer, then wipe clean green body with sponge and carry out moisturizing to it;
2) your the porcelain agate viridescent glaze stirred evenly is equably applied on green body, then carries out wiping bottom trimming, obtain glazed body;
3) glazed body obtained by step 2) is propped up in merging kiln with support pin and is fired, oxidizing flame is first used in sintering procedure It fires, temperature is risen to 1000 DEG C with the time of 5.5h, then fired with reduction flame, controlling the gas atmosphere in kiln includes weight The oxygen 0.9% of percentage is measured, temperature is continued to rise to 1250 DEG C, keeps the temperature 18min by carbon monoxide 9.5% with the time of 6.5h, Stop burning, be naturally cooling to room temperature to get.
Embodiment 7
Your porcelain of the present embodiment, including Ru agate glaze and green body;Your the porcelain agate viridescent glaze is that embodiment 3 is resulting Your porcelain agate viridescent glaze;The green body contains following components in percentage by weight: wollastonite 1%, your stone 2%.
Embodiment 8
Your porcelain of the present embodiment, including Ru agate glaze and green body;Your the porcelain agate viridescent glaze is that embodiment 3 is resulting Your porcelain agate viridescent glaze;The green body contains following components in percentage by weight: wollastonite 5%, your stone 10%.
Embodiment 9
Your porcelain of the present embodiment, including Ru agate glaze and green body;Your the porcelain agate viridescent glaze is that embodiment 3 is resulting Your porcelain agate viridescent glaze;The green body contains following components in percentage by weight: wollastonite 3%, your stone 6%.

Claims (7)

1. your a kind of porcelain agate viridescent glaze, it is characterised in that: the component containing following parts by weight: you is 6 ~ 20 parts of stone, Agate 1 ~ 15 parts, 10 ~ 70 parts of feldspar, 2 ~ 8 parts of calcite, 1 ~ 20 part of wollastonite, 0 ~ 2 part of talcum, 0 ~ 15 part of chestnut ash, 1 ~ 8 part of spot fossil, 1 ~ 20 part of black green stone;
Your porcelain agate viridescent glaze is by including the following steps that method is process:
1) your stone and Agate are calcined respectively at 800 ~ 900 DEG C, is then crushed, obtain your stone and agate of graininess or powdery Stone;
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains the building stones of graininess or powdery;
3) obtained by your stone and Agate, step 2 for according to the weight ratio, taking chestnut ash, the resulting graininess of step 1) or powdery Each graininess or powdery building stones, then plus water for ball milling mixing obtains glaze slip;
4) by the Concentration Modulation of glaze slip obtained by step 3) to 52 ~ 56 Baume degrees, then remove iron, it is aging to get.
2. a kind of processing method of your porcelain agate viridescent glaze as described in claim 1, it is characterised in that: the following steps are included:
1) your stone and Agate are calcined respectively at 800 ~ 900 DEG C, is then crushed, obtain your stone and agate of graininess or powdery Stone;
2) feldspar, calcite, wollastonite, talcum, black green stone, spot fossil are crushed respectively, obtains the building stones of graininess or powdery;
3) obtained by your stone and Agate, step 2 for according to the weight ratio, taking chestnut ash, the resulting graininess of step 1) or powdery Each graininess or powdery building stones, then plus water for ball milling mixing obtains glaze slip;
4) by the Concentration Modulation of glaze slip obtained by step 3) to 52 ~ 56 Baume degrees, then remove iron, it is aging to get.
3. your a kind of porcelain, it is characterised in that: including your porcelain agate viridescent glaze and green body;Your the porcelain agate viridescent glaze contains following The component of parts by weight: you is 6 ~ 20 parts of stone, 1 ~ 15 part of Agate, 10 ~ 70 parts of feldspar, 2 ~ 8 parts of calcite, 1 ~ 20 part of wollastonite, sliding 0 ~ 2 part of stone, 0 ~ 15 part of chestnut ash, 1 ~ 8 part of spot fossil, 1 ~ 20 part of black green stone.
4. your porcelain according to claim 3, it is characterised in that: the green body contains following components in percentage by weight: silicon Lime stone 1 ~ 5%, your stone 2 ~ 10%.
5. a kind of method for cooking of your porcelain as described in claim 3 or 4, it is characterised in that: the following steps are included:
1) your porcelain agate viridescent glaze is equably applied on green body, obtains glazed body;
2) glazed body obtained by step 1) is fired, is first fired with oxidizing flame in sintering procedure, temperature is risen to 950 ~ 1050 DEG C, then fired with reduction flame, temperature is continued to rise to 1230 ~ 1260 DEG C, 15 ~ 20min is kept the temperature, stops burning, be naturally cooling to room Temperature to get.
6. the method for cooking of your porcelain according to claim 5, it is characterised in that: in step 1), by your porcelain agate viridescent glaze Before applying on green body, green body is pre-processed;The pretreatment is first to carry out biscuiting to the green body of forming, then right The good green body of biscuiting is polished, then dedusting, finally carries out moisturizing.
7. the method for cooking of your porcelain according to claim 5, it is characterised in that: in step 2, fired using reduction flame When gas atmosphere in contain following weight percent gas: oxygen 0.8 ~ 1%, carbon monoxide 2.5 ~ 9.5%.
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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101747089A (en) * 2008-12-16 2010-06-23 郭秀贞 Ru agate glaze and processing method and application thereof
CN103771905A (en) * 2013-12-31 2014-05-07 广州市恒福茶业有限公司 Ruyao celeste glaze, and processing method and application thereof
CN104211447A (en) * 2014-09-10 2014-12-17 张天庆 Ru-porcelain yellow agate glaze and processing method thereof as well as Ru-porcelain and firing method thereof
CN105753323A (en) * 2016-03-23 2016-07-13 杨云超 Method for preparing jade green glaze porcelain

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101747089A (en) * 2008-12-16 2010-06-23 郭秀贞 Ru agate glaze and processing method and application thereof
CN103771905A (en) * 2013-12-31 2014-05-07 广州市恒福茶业有限公司 Ruyao celeste glaze, and processing method and application thereof
CN104211447A (en) * 2014-09-10 2014-12-17 张天庆 Ru-porcelain yellow agate glaze and processing method thereof as well as Ru-porcelain and firing method thereof
CN105753323A (en) * 2016-03-23 2016-07-13 杨云超 Method for preparing jade green glaze porcelain

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