CN106474173A - The method that microwave sterilization is carried out to honeysuckle - Google Patents
The method that microwave sterilization is carried out to honeysuckle Download PDFInfo
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- CN106474173A CN106474173A CN201611082232.1A CN201611082232A CN106474173A CN 106474173 A CN106474173 A CN 106474173A CN 201611082232 A CN201611082232 A CN 201611082232A CN 106474173 A CN106474173 A CN 106474173A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/185—Magnoliopsida (dicotyledons)
- A61K36/35—Caprifoliaceae (Honeysuckle family)
- A61K36/355—Lonicera (honeysuckle)
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
- A61L2/0005—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor for pharmaceuticals, biologicals or living parts
- A61L2/0011—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor for pharmaceuticals, biologicals or living parts using physical methods
- A61L2/0029—Radiation
- A61L2/0064—Microwaves
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/13—Preparation or pretreatment of starting material involving cleaning, e.g. washing or peeling
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L2202/00—Aspects relating to methods or apparatus for disinfecting or sterilising materials or objects
- A61L2202/20—Targets to be treated
- A61L2202/21—Pharmaceuticals, e.g. medicaments, artificial body parts
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Public Health (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Veterinary Medicine (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Molecular Biology (AREA)
- Biomedical Technology (AREA)
- Alternative & Traditional Medicine (AREA)
- Biotechnology (AREA)
- Botany (AREA)
- Medical Informatics (AREA)
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- Mycology (AREA)
- Pharmacology & Pharmacy (AREA)
- Medicines Containing Plant Substances (AREA)
- Apparatus For Disinfection Or Sterilisation (AREA)
Abstract
The invention discloses a kind of method for carrying out microwave sterilization to honeysuckle, comprises the following steps：(1) honeysuckle being placed in tarragon to fumigate in cage, 1.5～3h being fumigated in 50～70 DEG C, the honeysuckle after fumigating is placed in 10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=1～5:3～8) soak in, filter, dry；(2) crush, 55～80 mesh sieves are crossed, then is added water in powder, amount of water is the 45%～80% of powder weight；(3) wet powder mixture is placed in tunnel type micro wave sterilization drier and sterilizes, drying condition is：Dehumidifier 5～25Hz of frequency, 50～73 DEG C of temperature, 10～30 DEG C of cooling water temperature, 0.1～2m/s of transporting velocity, 0.5～2cm of thickness is conveyed, sterilizing Honeysuckle Flower must be done.The present invention is simple to operate, can preserve the chlorogenic acid in honeysuckle to greatest extent, lifts honeysuckle medical value.
Description
Technical field
The present invention relates to a kind of microwave sterilization method of medicinal material, and in particular to a kind of side for carrying out microwave sterilization to honeysuckle
Method.
Background technology
Perfect with national health system, to medicine hygienic requirements more and more higher, so the microorganism to medicine limits
Spend to have and clearly require, the particularly requirement of pathogenic bacteria.Social sterilization method is varied now, has going out chemically and physically
Bacterium mode.Chemical sterilization introduces high oxidation material, easily causes pharmaceutical properties to change, so adopting less, the sterilizing side of physics
Formula has the modes such as high temperature, radiation, each have their own benefit, each have their own drawback.
High-temperature sterilization includes the conventional sterilization technology such as moist hear heat test, and its shortcoming is：To material in processing procedure
Composition has a significant impact, and causes material composition loss serious, affects the use of material, such as when sterilizing to honeysuckle, make
Obtain chlorogenic acid in honeysuckle to lose in a large number, reduce the drug effect of honeysuckle；Microwave technology is in radiation sterilization techniques
Kind, he is acted on using long wave, and radiationless residual, sterilising temp are low, and action time is short, less on the impact of material nature etc. excellent
Point.But microwave technology, at this stage still in theory stage, microwave is also mainly used in drying, the microwave to different material goes out
Bacterium also needs to continue research.
Content of the invention
For above-mentioned deficiency of the prior art, the present invention provides a kind of method for carrying out microwave sterilization to honeysuckle, its
When conventional sterilization methods process honeysuckle is efficiently solved, cause the excessive problem of chlorogenic acid loss in which.
For solving above-mentioned technical problem, the technical solution used in the present invention is：
A kind of method for carrying out microwave sterilization to honeysuckle, comprises the following steps：
(1) honeysuckle is placed in tarragon to fumigate in cage, under the conditions of 50～70 DEG C, 1.5～3h is fumigated, the gold after fumigating
Honeysuckle flower is placed in 10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=1～5:3～8) in soak 30～
45min, filters, dries, and obtains pre-processing honeysuckle；
(2) step (1) gained pretreatment honeysuckle is crushed, 55～80 mesh sieves is crossed, then is added water in powder, stirring is mixed
Wet, wet powder mixture is obtained, wherein, amount of water is the 45%～80% of powder weight；
(3) 10～30min of sterilizing, tunnel in tunnel type micro wave sterilization drier are placed in the wet powder mixture in step (2)
Type micro-wave sterilization drier drying condition is：Drying machine dehumidifier 5～25Hz of frequency, 50～73 DEG C of temperature, cooling water temperature 10～
30 DEG C, wet powder mixture 0.1～2m/s of transporting velocity, wet powder mixture convey 0.5～2cm of thickness, obtain dry sterilizing honeysuckle powder
End.
Further, amount of water described in step (2) is the 45%～55% of powder weight.
Further, described in step (3), tunnel type micro wave sterilization drier drying condition is：Dehumidifier frequency 7Hz, temperature
62 DEG C, 22 DEG C of cooling water temperature, wet powder mixture transporting velocity 0.5m/s, wet powder mixture convey thickness 1.2cm.
Further, in step (3), the microwave power of tunnel type micro wave sterilization drier is 22～30Kw.
Beneficial effects of the present invention are：
Stifling by tarragon, honeysuckle quick dewatering drying can be made, and also primary sterilization can be carried out to honeysuckle, meanwhile, Chinese mugwort
Hexadecylic acid and phytol in cigarette is penetrated in honeysuckle when stifling, it is possible to decrease chlorogenic acid is when stifling and in post sterilization
Loss.
When microwave power is 24Kw, dehumidifier frequency is 7Hz, and temperature of charge is 62 DEG C, and cooling water temperature is 22 DEG C, and medicinal material is defeated
Speed is sent for 0.5m/s, when medicinal material conveying thickness is 1.2cm, honeysuckle powder foot couple microwave has optimal absorption value, under the conditions of this
Chlorogenic acid loss amount in honeysuckle is minimum.
Microwave sterilization is low temperature sterilization, the thermally labile component that can be effectively retained in medicine；Its action time is short, can
More effectively retain the script proterties of medicine；While sterilization process is controlled, the green original in honeysuckle can be retained to greatest extent
Acid content.
Specific embodiment
Specific embodiment to the present invention is described below, understands this in order to those skilled in the art
Bright, it should be apparent that the invention is not restricted to the scope of specific embodiment, for those skilled in the art,
As long as in appended claim restriction and the spirit and scope of the present invention for determining, these changes are aobvious and easy to various change
See, all utilize the innovation and creation of present inventive concept all in the row of protection.
The present invention is the method for carrying out microwave sterilization to honeysuckle, and which specifically includes following process：
(1) fumigate：Honeysuckle is placed in tarragon fumigate in cage, 1.5～3h is fumigated under the conditions of 50～70 DEG C, then will be stifling
Honeysuckle afterwards is placed in 10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=1～5:3～8), in, soak
30～45min, to remove the sulfur dioxide in honeysuckle, filters, and obtains pre-processing honeysuckle.
(2) crush：Pretreatment honeysuckle powder is broken to powder diameter for 55～80 mesh, the particle diameter with 60 mesh be optimal, just
In humidification process is subsequently carried out, can also shorten sterilization time, lift sterilization effect；Wet operations are carried out after crushing, i.e.,：
Powder is added in agitator tank, purified water is added in agitator tank while stirring, is made purified water uniformly penetrating
To Honeysuckle Flower, so that Honeysuckle Flower is fully absorbed water, obtain wet powder mixture；Wherein, amount of water is the 45% of powder weight
～80%.
(3) microwave sterilization：By the wet powder mixture in step (2) be placed in tunnel type micro wave sterilization drier sterilizing 10～
30min, by the tape transport of tunnel type micro wave sterilization drier in which, its transporting velocity is 0.1～2m/ to wet powder mixture
S, with 0.5m/s as optimal transport speed；Conveying thickness is 0.5～2cm, with 1.2cm as optimal ulking thickness；While adjusting micro-
To optimal, its running power is 22～30Kw to ripple sterilization drier parameters, is optimal with 24Kw；Dehumidifier frequency be 5～
25Hz, with 7Hz as optimal dehumidifier frequency；Microwave sterilization drying machine heating-up temperature is 50～73 DEG C, with 60～70 DEG C as optimal temperature
Degree；In microwave sterilization drying machine, the temperature of cooling water is 10～30 DEG C, with 22 DEG C as optimum temperature；To ensure to fill medicinal material
Divide and effectively sterilize, rewinding is carried out in the discharge end of microwave sterilization drying machine, you can the Honeysuckle Flower dry after reaching sterilizing.
Embodiment 1
A kind of method for carrying out microwave sterilization to honeysuckle, comprises the following steps：
(1) honeysuckle is placed in tarragon to fumigate in cage, under the conditions of 50 DEG C, 1.5h is fumigated, the honeysuckle after fumigating is placed in
10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=1:3) 30min is soaked in, filter, dry, obtain
Pretreatment honeysuckle；
(2) by the powder that the pretreatment honeysuckle crushing of step (1) gained was 55 mesh sieves, then add water in powder, stirring
Mixed wet, wet powder mixture is obtained, wherein, amount of water is the 45% of powder weight；
(3) wet powder mixture in step (2) is placed in sterilizing 10min in tunnel type micro wave sterilization drier, tunnel declines
Ripple sterilization drier drying condition is：Drying machine microwave power 22KW, dehumidifier frequency 5Hz, 50 DEG C of baking temperature, cooling water temperature
10 DEG C, wet powder mixture transporting velocity 0.1m/s, wet powder mixture convey thickness 0.5cm, carry out rewinding in drying machine discharge end, obtain
Dry sterilizing Honeysuckle Flower.
Embodiment 2
A kind of method for carrying out microwave sterilization to honeysuckle, comprises the following steps：
(1) honeysuckle is placed in tarragon to fumigate in cage, under the conditions of 65 DEG C, 2h is fumigated, the honeysuckle after fumigating is placed in
10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=3:7) 37min is soaked in, filter, dry, obtain
Pretreatment honeysuckle；
(2) by the powder that the pretreatment honeysuckle crushing of step (1) gained was 60 mesh sieves, then add water in powder, stirring
Mixed wet, wet powder mixture is obtained, wherein, amount of water is the 55% of powder weight；
(3) wet powder mixture in step (2) is placed in sterilizing 17min in tunnel type micro wave sterilization drier, tunnel declines
Ripple sterilization drier drying condition is：Drying machine microwave power 24KW, dehumidifier frequency 7Hz, 62 DEG C of baking temperature, cooling water temperature
22 DEG C, wet powder mixture transporting velocity 0.5m/s, wet powder mixture convey thickness 1.2cm, carry out rewinding in drying machine discharge end, obtain
Dry sterilizing Honeysuckle Flower.
Embodiment 3
A kind of method for carrying out microwave sterilization to honeysuckle, comprises the following steps：
(1) honeysuckle is placed in tarragon to fumigate in cage, under the conditions of 70 DEG C, 3h is fumigated, the honeysuckle after fumigating is placed in
10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=5:8) 45min is soaked in, filter, dry, obtain
Pretreatment honeysuckle；
(2) by the powder that the pretreatment honeysuckle crushing of step (1) gained was 80 mesh sieves, then add water in powder, stirring
Mixed wet, wet powder mixture is obtained, wherein, amount of water is the 69% of powder weight；
(3) wet powder mixture in step (2) is placed in sterilizing 23min in tunnel type micro wave sterilization drier, tunnel declines
Ripple sterilization drier drying condition is：Drying machine microwave power 30KW, dehumidifier frequency 12Hz, 60 DEG C of baking temperature, coolant water temperature
12 DEG C of degree, wet powder mixture transporting velocity 0.9m/s, wet powder mixture convey thickness 1.7cm, carry out rewinding in drying machine discharge end, obtain
To dry sterilizing Honeysuckle Flower.
Embodiment 4
A kind of method for carrying out microwave sterilization to honeysuckle, comprises the following steps：
(1) honeysuckle is placed in tarragon to fumigate in cage, under the conditions of 58 DEG C, 2.6h is fumigated, the honeysuckle after fumigating is placed in
10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=2:5) 42min is soaked in, filter, dry, obtain
Pretreatment honeysuckle；
(2) by the powder that the pretreatment honeysuckle crushing of step (1) gained was 70 mesh sieves, then add water in powder, stirring
Mixed wet, wet powder mixture is obtained, wherein, amount of water is the 80% of powder weight；
(3) wet powder mixture in step (2) is placed in sterilizing 30min in tunnel type micro wave sterilization drier, tunnel declines
Ripple sterilization drier drying condition is：Drying machine microwave power 27KW, dehumidifier frequency 13Hz, 70 DEG C of baking temperature, coolant water temperature
30 DEG C of degree, wet powder mixture transporting velocity 2m/s, wet powder mixture convey thickness 2cm, carry out rewinding in drying machine discharge end, are done
Dry sterilizing Honeysuckle Flower.
Comparative example 1
Identical three groups of Honeysuckle Flowers are taken, under the same terms, is respectively adopted in moist hear heat test and the present invention
The microwave sterilization method provided by embodiment 2 carries out sterilization treatment to honeysuckle, and the content of the Chlorogenic Acid of Flos Lonicerae after process is shown in
Table 1.
Comparative example 2
Compared with Example 2, lack tarragon fumigating step, remaining step and operating condition are all same as Example 2, and
Three group Honeysuckle Flower Content of Chlorogenic Acids are determined under the same conditions, and which the results are shown in Table 2.
Comparing result is as follows：
Chlorogenic acid content in honeysuckle after the different sterilizing methods process of table 1
As shown in table 1, it is above at moist heat sterilization using the content of chlorogenic acid in the honeysuckle after the process of microwave sterilization method
Honeysuckle after reason, also, the honeysuckle that microwave sterilization method is processed, the loss late of its chlorogenic acid well below moist hear heat test at
The honeysuckle of reason, therefore, microwave sterilization method can preserve the chlorogenic acid in honeysuckle to greatest extent.
The stifling impact to honeysuckle chlorogenic acid content of 2 tarragon of table
Can be drawn by 2 data of table, only after microwave sterilization step process, its chlorogenic acid content is far below enforcement for comparative example 2
Example 2, shows through tarragon fumigating step, crushes humidification and after specific microwave sterilization condition, just cause chlorogenic acid maximum
Being stored in honeysuckle of limit.
Claims (4)
1. a kind of method that microwave sterilization is carried out to honeysuckle, it is characterised in that comprise the following steps：
(1) honeysuckle is placed in tarragon to fumigate in cage, under the conditions of 50～70 DEG C, 1.5～3h is fumigated, the honeysuckle after fumigating
It is placed in 10% sodium bicarbonate solution and 10% sodium chloride mixed solution (V:V=1～5:3～8) in, 30～45min is soaked,
Filter, dry, obtain pre-processing honeysuckle；
(2) step (1) gained pretreatment honeysuckle is crushed, 55～80 mesh sieves is crossed, then is added water in powder, stirring is mixed wet, obtains
Wet powder mixture, wherein, amount of water is the 45%～80% of powder weight；
(3) wet powder mixture in step (2) is placed in 10～30min of sterilizing in tunnel type micro wave sterilization drier, tunnel declines
Ripple sterilization drier drying condition is：Drying machine dehumidifier 5～25Hz of frequency, 50～73 DEG C of temperature, 10～30 DEG C of cooling water temperature,
Wet powder mixture 0.1～2m/s of transporting velocity, wet powder mixture convey 0.5～2cm of thickness, obtain dry sterilizing Honeysuckle Flower.
2. the method that microwave sterilization is carried out to honeysuckle according to claim 1, it is characterised in that：Described in step (2)
Amount of water is the 45%～55% of powder weight.
3. the method that microwave sterilization is carried out to honeysuckle according to claim 1, it is characterised in that：Described in step (3)
Tunnel type micro wave sterilization drier drying condition is：Dehumidifier frequency 7Hz, 62 DEG C of temperature, 22 DEG C of cooling water temperature, wet powder mixture is defeated
Speed 0.5m/s is sent, wet powder mixture conveys thickness 1.2cm.
4. the method that microwave sterilization is carried out to honeysuckle according to claim 1, it is characterised in that：Tunnel in step (3)
The microwave power of type micro-wave sterilization drier is 22～30Kw.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611082232.1A CN106474173A (en) | 2016-11-30 | 2016-11-30 | The method that microwave sterilization is carried out to honeysuckle |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201611082232.1A CN106474173A (en) | 2016-11-30 | 2016-11-30 | The method that microwave sterilization is carried out to honeysuckle |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638662A (en) * | 2019-10-11 | 2020-01-03 | 王燕丽 | A skin caring patch containing natural animal and plant extracts, and its preparation method |
| CN112111324A (en) * | 2020-09-29 | 2020-12-22 | 天宝牡丹生物科技有限公司 | Extraction method of peony flower stock solution with low cost and high extraction efficiency |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203518478U (en) * | 2013-07-29 | 2014-04-02 | 福建大忠贵祥农业科技有限公司 | Tunnel type honeysuckle microwave drier |
| CN104186723A (en) * | 2014-08-12 | 2014-12-10 | 许拾平 | Microwave processing method of honeysuckle |
-
2016
- 2016-11-30 CN CN201611082232.1A patent/CN106474173A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203518478U (en) * | 2013-07-29 | 2014-04-02 | 福建大忠贵祥农业科技有限公司 | Tunnel type honeysuckle microwave drier |
| CN104186723A (en) * | 2014-08-12 | 2014-12-10 | 许拾平 | Microwave processing method of honeysuckle |
Non-Patent Citations (2)
| Title |
|---|
| 汤宗武: "金银花药材灭菌方法的探讨", 《海峡药学》 * |
| 贾芝梅等: "中草药用于母婴同室病房空气消毒效果观察", 《山西中医》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110638662A (en) * | 2019-10-11 | 2020-01-03 | 王燕丽 | A skin caring patch containing natural animal and plant extracts, and its preparation method |
| CN112111324A (en) * | 2020-09-29 | 2020-12-22 | 天宝牡丹生物科技有限公司 | Extraction method of peony flower stock solution with low cost and high extraction efficiency |
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Application publication date: 20170308 |