CN106471207A - Infiltration type rotary drilling-head completely - Google Patents
Infiltration type rotary drilling-head completely Download PDFInfo
- Publication number
- CN106471207A CN106471207A CN201580024457.9A CN201580024457A CN106471207A CN 106471207 A CN106471207 A CN 106471207A CN 201580024457 A CN201580024457 A CN 201580024457A CN 106471207 A CN106471207 A CN 106471207A
- Authority
- CN
- China
- Prior art keywords
- rotary drilling
- jointing material
- alloy
- particle matrix
- matrix composite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B10/00—Drill bits
- E21B10/46—Drill bits characterised by wear resisting parts, e.g. diamond inserts
- E21B10/54—Drill bits characterised by wear resisting parts, e.g. diamond inserts the bit being of the rotary drag type, e.g. fork-type bits
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B10/00—Drill bits
- E21B10/46—Drill bits characterised by wear resisting parts, e.g. diamond inserts
- E21B10/48—Drill bits characterised by wear resisting parts, e.g. diamond inserts the bit being of core type
-
- E—FIXED CONSTRUCTIONS
- E21—EARTH DRILLING; MINING
- E21B—EARTH DRILLING, e.g. DEEP DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
- E21B10/00—Drill bits
- E21B10/62—Drill bits characterised by parts, e.g. cutting elements, which are detachable or adjustable
Abstract
The invention discloses a kind of complete infiltration type rotary drilling-head; described drill bit has drill main body, and described drill main body includes at least one particle matrix composite with granular materialss compositionss and the jointing material with the jointing material compositionss different from described granular materialss compositionss.Described granular materialss compositionss have granular materialss melt temperature, and described jointing material compositionss have the jointing material melt temperature different from described granular materialss melt temperature.
Description
The cross reference of related application
This application claims being filed in U.S. Provisional Patent Application No.61/992 on May 13rd, 2014,654 priority,
This temporary patent application is incorporated by reference in its entirety herein.
Technical field
The present invention relates to rotary drilling-head.More particularly, it relates to complete infiltration type rotary drilling-head.
Background technology
Rotary drilling-head is widely used in boring or the drilling well of subsurface boring.There are perhaps eurypalynous rig and related side
Method is used for this kind of probing.Common probing is using the rotary drilling-head being attached to drill string one end.Rotary drilling-head generally includes and is fixed on
Multiple cutting elements in drill main body surface region.Drill string includes managing and is connected to for will be located into the drill bit of foot of hole
The equipment section of other drilling equipments in earth's surface.The brill in drill string and boring can be rotated using rotation platform or top drive
Head.In addition, the shank of drill bit can be directly coupled in the drive shaft of downhole electrical motor, downhole electrical motor subsequently can be used for rotating boring
Head.
Rotary drilling-head, particularly on the cutting end being covered with cutting element, usually plate-like or substantially cylindrical.Often
The cutting surface that individual cutting element all has generally is made up of hard ultrawear-resistant material (such as polycrystalline diamond), the end face of element
It is usually the form of circular, such element is commonly known as " polycrystalline diamond composite material " (PDC) cutter.Have many
As species, drill bit form is available;However, cutting element is generally manufactured respectively with drill main body, it is then fitted into being formed at
In the groove of drill main body outer surface.Cutting element can be fixed by any suitable means, for example, by using the material that bonds
Material, including various binding agents, or more generally, various brazing alloys.Drill main body is fixed on American Petroleum Institute (API)
(API) in threaded hardening steel handle, for drill bit is attached to drill string.During use, cutting element and its cutting surface
Contact with stratum to be drilled.During bit, cutting element is gradually pruned the surface of underlying strata, thus forming boring.
The drill main body of rotary drilling-head can be formed by steel;However, this kind of drill main body can wear and tear, the speed meeting of abrasion
There is obvious difference according to the difference of drilling environment.Wear and tear to reduce and increase the service life, drill main body also uses
Particle matrix composite makes.
The drill main body of particle matrix composite is first made with the graphite jig with processing cavity.Can be by hand-held work
Tool, adds other fine-feature structures in the chamber of graphite jig.It is also possible to use and be made up of sand, clay or other materials
Insert or core are obtaining some preferable drill main body latent structures.(can be by if it is necessary, preform elements or replacing part
Any suitable material is made, including ceramic component, graphite member or the fine and close sand part with resin-coating) can be positioned on mould
Tool in and be used for limiting various features structure, including inner passage, cutting element groove, chip area and drill main body other outside
Portion's configuration or internal feature structure.The chamber of graphite jig is filled with carbide material (the such as tungsten carbide, carbonization of hard particles shape
Titanium, ramet etc.).Subsequently by preformation shaped blooms at an appropriate location with orientation positions in mould, this steel billet typically at least part
Sink in the particulate carbide material in mould.
Subsequently can swing die or by granule compress to improve the packed density of carbide powder and to form powder type.Will
Host material (such as acid bronze alloy) melts and is incorporated in carbide powder so that the host material of melting penetrates into powder shape
In formula.Mould and drill main body can be cooled down, so that host material solidifies and steel billet is connected to particle matrix composite
Upper formation bizet.Mould and all refill-units are removed from drill main body.Remove and during drill main body, typically require destruction graphite mo(u)ld
Tool.
Once drill main body removes from described mould, will be fixed on for a long time in steel handle.Can lead on the surface of steel billet
Over mechanical processing forms thread forms, threaded to provide between drill main body and steel handle.
Although steel billet can provide generally acceptable connection steel handle and the mode of drill main body, in mould during infiltration
Base can shift, lead to base cannot align with drill main body, thus resulting in drill main body cannot use, or needs to drill bit
Main body carries out extra processing or other are done over again.In addition, introduce base to need first it to be entered before infiltration as extra part
Row decontamination or cleaning, to guarantee the metallurgical binding between base and metal matrix.In addition, the material according to used by base, base and
Interaction between host material may result in the formation of both interface phases, and can thus lead to during using drill bit
The formation in crack and expansion.
Although the drill main body containing particle matrix composite compared to all steel drill main body wear-resistant and corrosion
Aspect has obvious advantage, but the low-intensity of such drill main body and soft limit their fortune in some application-specific
With.Improve hardness, intensity or other properties of these particle matrix composites, just can expand the application model of this kind of drill main body
Enclose.
Content of the invention
The present invention relates to include drill main body rotary drilling-head, this main body include at least one particle matrix composite and
A kind of jointing material.On the one hand, each of at least one particle matrix composite is respectively provided with granular materialss compositionss,
This granular materialss compositions also has granular materialss melt temperature.On the other hand, this jointing material has disunity granular materialss
The jointing material compositionss of compositionss.At this on the one hand, jointing material compositionss have gluing less than granular materialss melt temperature
Condensation material melt temperature.
It yet still another aspect, at least one in granular substrate material compositionss and jointing material compositionss can be by host material
Constitute with being dispersed in this host material multiple hard particles everywhere.
Once being formed, described jointing material penetrates into particle matrix composite and is substantially encapsulated, to form base
Uniform granule micro structure in basis.In this aspect, it is contemplated that particle matrix composite in the forming process of drill bit substantially
Will not melt.
Brief description
These and other features of the preferred embodiments of the present invention will become more to show in detailed description referring to the drawings
And be clear to, wherein:
Fig. 1 is the Some illustrative profile of an exemplary embodiment of rotary drilling-head disclosed herein.
Fig. 2 is the Some illustrative profile of second exemplary embodiment of rotary drilling-head disclosed herein.
Diagram presented herein, is not meant as the actual view of any certain material, device, system or method, and only
It is the idealization representative of disclosure herein disclosed.In addition, each in figure identical element can retain identical Digital ID.
Specific embodiment
Explanation by referring to described further below, example, drawings and claims and its above and below can more be held
Change places and understand the present invention.However, open and before describing apparatus of the present invention, system and/or method it will be appreciated that unless another
Indicate, the invention is not limited in disclosed concrete device, system and/or method, because such concrete device, system
And/or method is naturally it may happen that change.It should also be recognized that term used herein is merely to describe particular aspects,
And be not intended to be limited.
The following description of the present invention is provided as realizing the teachings of the present invention with the most preferred embodiment of prior known.For this reason,
Those skilled in the relevant art will recognize and appreciate that, can make many changes in the various aspects of invention described herein, with
When remain to obtain beneficial effects of the present invention.It is also obvious that can be unfavorable by some features of the selection present invention
Obtain some required beneficial effects of the present invention with other features.Therefore, those skilled in the art will recognize that, to this
Many modifications that invention is made and adjustment are possible, and even desired in some cases, and constitute the present invention's
A part.Therefore, below description is provided as the exemplary illustration of principle of the present invention and not limits the present invention.
As used in text, unless the context clearly dictates otherwise, the " one " of singulative, " a kind of " and " described "
Including plural references.Thus, for example, referring to that " a kind of particle matrix composite " may include two kinds or more kinds of such granule
Groundmass composite material, unless the context indicates otherwise.
Scope herein can be expressed as starting from " about " a certain particular value and/or terminate in " about " another particular value.Work as table
When reaching such scope, on the other hand include from a particular value and/or to another particular value.Similarly, when adopting antecedent
" about " by numerical expression for during approximation it will be appreciated that this occurrence also constitutes on the other hand.It should also be understood that each model
The end value enclosing is with respect to another end value, for being still not dependent on another end value, all meaningful.
As used herein, term " optional " or " optionally " refer to the event subsequently describing or situation it may happen that or can
Can not occur, and described description inclusion wherein occurs the example of described event or situation and described event or feelings wherein do not occur
The example of condition.
As used herein, term " [metal] based alloy " (wherein [metal] be any metal) is in addition to metal alloy,
Also refer to technical pure [metal], [metal] percentage by weight wherein in alloy is higher than the weight percent of other compositions in this alloy
Than.If this kind of apoplexy due to endogenous wind lists the metal of two or more, the combination of the percentage by weight of listed metal is higher than alloy
The percentage by weight of middle other compositions.
As used herein, term " material compositions " refers to the micro structure of Chemical composition that and material.That is, having phase
With chemical constituent but the material of different micro structure is considered to have different material components.
As used herein, term " tungsten carbide " refers to comprise with any stoichiometry or non-stoichiometric ratio or percentage ratio
The arbitrary combination thing of the chemical compound of tungsten and carbon, for example, WC, W2C and WC and W2The combination of C.Tungsten carbide includes this material
Any form form of material, for example, casting mold tungsten carbide, cemented tungsten carbide, monocrystalline tungsten carbide and macrocrystalline tungsten carbide.
Fig. 1 shows a kind of drilling type rotary drilling-head 10 with drill main body 20.Drill main body 20 has and is configured to
Engage the far-end cutting zone 22 of subsurface formations and be configured to the proximal threads region 24 being optionally connected on drill string.
On the one hand, this proximal threads region defines the open inner chamber 26 extending along drill main body longitudinal axis.It is also contemplated that by structure
Cause the screw thread 28 matingly engaging and being attached to drill string can be formed at the inner wall surface of open inner chamber.As pre- in present invention institute
Phase, drill main body is complete infiltration type, and thus without needing to be fixed to for a long time on ground prop handle.
On the other hand, drill main body 20 includes at least one particle matrix composite having permeated jointing material, makes
Obtain at least one particle matrix composite to be permeated completely and substantially encapsulated by it by jointing material, substantially uniform to be formed
Granule micro structure.On the one hand, it is respectively provided with granular materialss compositionss in each particle matrix composite, this granular materials
Compositionss have granular materialss melt temperature.On the other hand, jointing material has jointing material compositionss, this jointing material group
Compound has the jointing material melt temperature less than granular materialss melt temperature.Additionally, granular materialss compositionss and jointing material
Compositionss are different material compositions.
It is contemplated that at least one in granular substrate material compositionss and jointing material compositionss by host material and is divided
It is dispersed in this host material multiple hard particles everywhere to constitute.The plurality of hard particles can substantially be dispersed randomly in whole base
In material.On the other hand, every kind of particle matrix composite is gone up by having the multiple hard particles being dispersed therein substantially
Host material constitute.
It yet still another aspect, jointing material may include the second particle matrix composite.At this on the one hand, the second particle matrix
Composite is substantially gone up and is made up of the host material with the multiple hard particles being dispersed therein.It yet still another aspect, bonding material
Material may include nonmagnetic substance and/or high-abrasive material.Similarly, the host material in particle matrix composition material may include non-
Magnetic material and/or high-abrasive material.On the one hand it is contemplated that the drill bit being formed can be all by nonmagnetic substance and/or wear-resisting material
Material is formed.
The host material of bonding composite may include, and for example, cobalt-based, iron-based, Ni-based, ferrum is Ni-based, cobalt is Ni-based, ferrum cobalt
Base, aluminium base, cuprio, magnesio, molybdenio and titanium-base alloy.Alloying element may include but be not limited to one of following element or many
Kind:Magnesium (Mn), nickel (Ni), stannum (Sn), zinc (Zn), silicon (Si), molybdenum (Mo), tungsten (W), boron (B) and phosphorus (P).Bonding composite
Host material be further selected from industrial pure element, such as cobalt, aluminum, copper, magnesium, titanium, ferrum and nickel.In the way of for example and not limitation,
The host material of bonding composite may include carbon steel, steel alloy, rustless steel, tool steel, potassium steel, nickel or cobalt high temperature alloy material
The iron-based of material and low grade fever ductility or nickel-base alloy.
Hard particles may include diamond, or metal or semimetallic carbide, nitride, oxide or boride.With
Mode for example and not limitation, hard particles may include diamond or ceramic material such as carbide, nitride, oxide and boron
Compound (includes boron carbide (B4C)) and combinations thereof, such as carbonitride.More particularly, hard particles may include by
Element such as W, Ti, Mo, Nb, V, Hf, Ta, Cr, Zr, Al and Si form carbide and boride.With side for example and not limitation
Formula, the material for forming hard particles includes tungsten carbide (WC, W2C), titanium carbide (TiC), ramet (TaC), titanium diboride
(TiB2), chromium carbide, titanium nitride (TiN), vanadium carbide (VC), aluminium oxide (Al2O3), aluminium nitride (AlN), boron nitride (BN) and carbon
SiClx (SiC).Additionally, the combination of different hardness granule can be used for customizing physical property and the characteristic of particle matrix composite.
Hard particles can be formed with technology well known by persons skilled in the art.The material being best suited for hard particles is commercially available, and
And other forming method is also in the limit of power of those skilled in the art.
In one example, unrestriced mode, the substrate of particle matrix complex composition may include tungsten-bast alloy, and
And the substrate of jointing material compositionss is selected from acid bronze alloy, zinc-containing alloy and nickel-base alloy.In another example, rather than limit
The mode of system, the substrate of particle matrix complex composition may include tungsten carbide-base alloy, and the substrate of jointing material compositionss
It is selected from acid bronze alloy, zinc-containing alloy and nickel-base alloy.Use to tungsten and/or tungsten carbide is preferable, because its hardness is relatively
Height, thus less granule can be used because its fusing point is high, and is suitable for process of osmosis, because host material solidifies and cold
But before it is in time typically shorter (method making particle matrix composite compared to other, such as many powder smelting of high temperature
Gold, for example, sinter, and in these methods, the time generally at high temperature is much longer).
The jointing material melt temperature of the jointing material compositionss being had due to jointing material is less than granular materialss melting temperature
Degree, in the substantially uniform granule micro structure in the drill bit of formation, described at least one particle matrix composite is in non-
Molten condition.Once formed it is contemplated that particle matrix composite substantially on be saturated jointing material encapsulation.In addition, being
Realize required infiltration, and particle matrix complex composition does not melt, jointing material melt temperature and granular materialss melting are warm
The difference of degree is more than 500, preferably more than 1000, and is more preferably larger than 1,500.
It yet still another aspect, as shown in Figure 2 it is contemplated that described at least one particle matrix composite may include multiple
Grain groundmass composite material.At this on the one hand, every kind of particle matrix composite can be processed into and be located at and drill main body longitudinal axiss
In the layer of line located lateral.This layered approach can use jointing material of the same race, be formed at each layer can have different required
The complete infiltration type drill main body of engineering propertiess.
Although several embodiments of the present invention above disclosed in the description, those skilled in the art should
Understand, the many modifications belonging to the present invention and other embodiment will be conceived, it has and in described above and relevant drawings is in
The beneficial effect of existing teaching.It will thus be appreciated that the invention is not restricted to specific embodiment disclosed above and many
Modification and other embodiment are intended to be included in the scope of the appended claims.In addition although there is employed herein special
Fixed term, and claims below also uses specific term, they are used only for general and descriptive meaning
Justice, rather than in order to limit the purpose of described invention, be not to limit claims below purpose.
Claims (25)
1. a kind of rotary drilling-head, including:
Drill main body, described drill main body has the far-end cutting zone being configured to engage subsurface formations and is configured to select
Selecting property it is connected to the proximal threads region on drill string;
At least one particle matrix composite, every kind of particle matrix composite is respectively provided with granular materialss compositionss, described
Grain material compositions have granular materialss melt temperature;And
A kind of jointing material, described jointing material has the jointing material compositionss different from described granular materialss compositionss, and
And there is jointing material melt temperature less than described granular materialss melt temperature,
At least one of wherein said granular substrate material compositionss and described jointing material compositionss by host material and dissipate
The multiple hard particles being distributed in described host material are constituted, and wherein said jointing material penetrates into described particle matrix material
In material, to form substantially uniform granule micro structure.
2. rotary drilling-head according to claim 1, wherein every kind of particle matrix composite is gone up wherein scattered by having substantially
The described host material being furnished with the plurality of hard particles is constituted.
3. rotary drilling-head according to claim 2, wherein said jointing material includes the second particle matrix composite.
4. rotary drilling-head according to claim 3, wherein said jointing material substantially by have wherein be scattered with multiple
The host material of hard particles is constituted.
5. rotary drilling-head according to claim 4, wherein said jointing material includes copper (Cu), nickel (Ni), cobalt (Co), ferrum
(Fe), molybdenum (Mo) simple substance or the alloy based on these metals.
6. rotary drilling-head according to claim 4, wherein said jointing material includes nonmagnetic substance.
7. rotary drilling-head according to claim 4, wherein said jointing material includes high-abrasive material.
8. rotary drilling-head according to claim 4, wherein said hard particles include diamond, or metal or semimetal
Carbide, nitride, oxide or boride.
9., according to the rotary drilling-head described in claim 5, wherein said host material includes cobalt-base alloyss, ferrous alloy, Ni-based conjunction
Gold, cobalt nickel-base alloy, iron nickel base alloy, iron cobaltio base alloy, acieral, acid bronze alloy, magnesium base alloy, tungsten-bast alloy and titanio
Alloy.
10. rotary drilling-head according to claim 2, the described host material bag in wherein said particle matrix composite
Include nonmagnetic substance.
11. rotary drilling-heads according to claim 2, the described host material bag in wherein said particle matrix composite
Include high-abrasive material.
12. rotary drilling-heads according to claim 1, wherein said jointing material includes the second particle matrix composite.
13. rotary drilling-heads according to claim 12, wherein said jointing material substantially wherein spreads by having
The described host material stating multiple hard particles is constituted.
14. rotary drilling-heads according to claim 1, wherein said at least one particle matrix composite is in the base being formed
It is in non-melt state in uniform granule micro structure in basis.
15. rotary drilling-heads according to claim 1, wherein said at least one particle matrix composite includes multiple
Grain groundmass composite material, and every kind of particle matrix composite is all processed into the longitudinal axis being located at described drill main body
It is open in the layer of positioning.
16. rotary drilling-heads according to claim 4, the described substrate of wherein said particle matrix complex composition includes tungsten
Based alloy.
17. rotary drilling-heads according to claim 16, the described substrate of wherein said jointing material compositionss is selected from cuprio
Alloy, zinc-containing alloy and nickel-base alloy.
18. rotary drilling-heads according to claim 4, the described substrate of wherein said particle matrix complex composition includes carbon
Change tungsten-bast alloy.
19. rotary drilling-heads according to claim 18, the described substrate of wherein said jointing material compositionss is selected from cuprio
Alloy, zinc-containing alloy and nickel-base alloy.
20. rotary drilling-heads according to claim 1, wherein said proximal threads region defines along described drill main body
The open inner chamber that longitudinal axis extend, and wherein spiral thread is formed in the inner wall surface of described open inner chamber,
Described spiral thread is configured to matingly engage and be attached on drill string.
21. rotary drilling-heads according to claim 1, wherein said proximal threads region defines outer surface, and described
Spiral thread is defined, described spiral thread is configured to matingly engage and be attached at least a portion of outer surface
On described drill string.
22. rotary drilling-heads according to claim 1, wherein said particle matrix composite is gone up substantially by described infiltration
Jointing material encapsulates.
23. rotary drilling-heads according to claim 1, wherein said jointing material melt temperature and the melting of described granular materialss
The difference of temperature is more than 500.
24. rotary drilling-heads according to claim 1, wherein said jointing material melt temperature and the melting of described granular materialss
The difference of temperature is more than 1000.
25. rotary drilling-heads according to claim 1, wherein said jointing material melt temperature and the melting of described granular materialss
The difference of temperature is more than 1,500.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201461992654P | 2014-05-13 | 2014-05-13 | |
US61/992,654 | 2014-05-13 | ||
PCT/US2015/030535 WO2015175641A1 (en) | 2014-05-13 | 2015-05-13 | Fully infiltrated rotary drill bit |
Publications (1)
Publication Number | Publication Date |
---|---|
CN106471207A true CN106471207A (en) | 2017-03-01 |
Family
ID=54480599
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201580024457.9A Pending CN106471207A (en) | 2014-05-13 | 2015-05-13 | Infiltration type rotary drilling-head completely |
Country Status (8)
Country | Link |
---|---|
US (1) | US20150330154A1 (en) |
EP (1) | EP3143236A1 (en) |
CN (1) | CN106471207A (en) |
AU (1) | AU2015259190A1 (en) |
CA (1) | CA2948825A1 (en) |
CL (1) | CL2016002889A1 (en) |
PE (1) | PE20170018A1 (en) |
WO (1) | WO2015175641A1 (en) |
Cited By (1)
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---|---|---|---|---|
CN109159307A (en) * | 2018-08-31 | 2019-01-08 | 古治勇 | The hot-forming included chip space glass perforating drill of one kind and its production technology |
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US10378286B2 (en) * | 2015-04-30 | 2019-08-13 | Schlumberger Technology Corporation | System and methodology for drilling |
CN108015906A (en) * | 2016-10-28 | 2018-05-11 | 圣戈班磨料磨具有限公司 | Hollow drill bit and its manufacture method |
CN110291052A (en) * | 2016-12-02 | 2019-09-27 | 圣戈班磨料磨具股份有限公司 | Coring bit component |
CN110394902A (en) * | 2018-04-25 | 2019-11-01 | 圣戈班磨料磨具有限公司 | Hollow drill bit and its manufacturing method |
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- 2015-05-13 WO PCT/US2015/030535 patent/WO2015175641A1/en active Application Filing
- 2015-05-13 AU AU2015259190A patent/AU2015259190A1/en not_active Abandoned
- 2015-05-13 PE PE2016002188A patent/PE20170018A1/en not_active Application Discontinuation
- 2015-05-13 CN CN201580024457.9A patent/CN106471207A/en active Pending
- 2015-05-13 EP EP15793275.7A patent/EP3143236A1/en not_active Withdrawn
- 2015-05-13 CA CA2948825A patent/CA2948825A1/en not_active Abandoned
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2016
- 2016-11-14 CL CL2016002889A patent/CL2016002889A1/en unknown
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Also Published As
Publication number | Publication date |
---|---|
CL2016002889A1 (en) | 2017-05-05 |
AU2015259190A1 (en) | 2016-11-17 |
US20150330154A1 (en) | 2015-11-19 |
EP3143236A1 (en) | 2017-03-22 |
WO2015175641A1 (en) | 2015-11-19 |
CA2948825A1 (en) | 2015-11-19 |
PE20170018A1 (en) | 2017-03-04 |
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